Crystallography Open Database

Information card for entry 1570315

Preview

Coordinates	1570315.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C41 H52 F4 Ge O4 P2 S
Calculated formula	C41 H52 F4 Ge O4 P2 S
Title of publication	Intramolecular donor-stabilized tetra-coordinated germanium(iv) di-cations and their Lewis acidic properties.
Authors of publication	Peddi, Balakrishna; Khan, Souvik; Gonnade, Rajesh G.; Yildiz, Cem B.; Majumdar, Moumita
Journal of publication	Chemical science
Year of publication	2023
Journal volume	14
Journal issue	47
Pages of publication	13755 - 13764
a	17.3764 ± 0.0016 Å
b	9.2749 ± 0.0009 Å
c	25.485 ± 0.002 Å
α	90°
β	103.688 ± 0.003°
γ	90°
Cell volume	3990.6 ± 0.6 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	7
Space group number	13
Hermann-Mauguin space group symbol	P 1 2/c 1
Hall space group symbol	-P 2yc
Residual factor for all reflections	0.0437
Residual factor for significantly intense reflections	0.0307
Weighted residual factors for significantly intense reflections	0.0767
Weighted residual factors for all reflections included in the refinement	0.0789
Goodness-of-fit parameter for all reflections included in the refinement	1.05
Diffraction radiation wavelength	1.54178 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
288746 (current)	2024-01-06	cif/ Updating files of 1570312, 1570313, 1570314, 1570315, 1570316, 1570317, 1570318, 1570319, 1570320, 1570321, 1570322, 1570323, 1570324, 1570325, 1570326, 1570327 Original log message: Adding full bibliography for 1570312--1570327.cif.	1570315.cif
287656	2023-11-17	cif/ Adding structures of 1570312, 1570313, 1570314, 1570315, 1570316, 1570317, 1570318, 1570319, 1570320, 1570321, 1570322, 1570323, 1570324, 1570325, 1570326, 1570327 via cif-deposit CGI script.	1570315.cif