Crystallography Open Database

Information card for entry 1570322

Preview

Coordinates	1570322.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C58.01 H44 F6.03 Ge O8.03 P2 S2.01
Calculated formula	C58.012 H44 F6.036 Ge O8.036 P2 S2.012
Title of publication	Intramolecular donor-stabilized tetra-coordinated germanium(iv) di-cations and their Lewis acidic properties.
Authors of publication	Peddi, Balakrishna; Khan, Souvik; Gonnade, Rajesh G.; Yildiz, Cem B.; Majumdar, Moumita
Journal of publication	Chemical science
Year of publication	2023
Journal volume	14
Journal issue	47
Pages of publication	13755 - 13764
a	9.896 ± 0.005 Å
b	15.315 ± 0.008 Å
c	17.58 ± 0.008 Å
α	105.27 ± 0.013°
β	93.87 ± 0.014°
γ	100.521 ± 0.014°
Cell volume	2508 ± 2 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1962
Residual factor for significantly intense reflections	0.1035
Weighted residual factors for significantly intense reflections	0.2554
Weighted residual factors for all reflections included in the refinement	0.3296
Goodness-of-fit parameter for all reflections included in the refinement	1.041
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
288746 (current)	2024-01-06	cif/ Updating files of 1570312, 1570313, 1570314, 1570315, 1570316, 1570317, 1570318, 1570319, 1570320, 1570321, 1570322, 1570323, 1570324, 1570325, 1570326, 1570327 Original log message: Adding full bibliography for 1570312--1570327.cif.	1570322.cif
287656	2023-11-17	cif/ Adding structures of 1570312, 1570313, 1570314, 1570315, 1570316, 1570317, 1570318, 1570319, 1570320, 1570321, 1570322, 1570323, 1570324, 1570325, 1570326, 1570327 via cif-deposit CGI script.	1570322.cif