Crystallography Open Database

Information card for entry 1570713

Preview

Coordinates	1570713.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C10 H8 Cl4 N8 Si
Calculated formula	C10 H8 Cl4 N8 Si
Title of publication	The Hexacoordinate Si Complex SiCl4(4-Azidopyridine)2—Crystallographic Characterization of Two Conformers and Probing the Influence of SiCl4-Complexation on a Click Reaction with Phenylacetylene
Authors of publication	Riedel, Sophie; Gerwig, Maik; Gerlach, Daniela; Brendler, Erica; Gericke, Robert; Kroke, Edwin; Wagler, Jörg
Journal of publication	Inorganics
Year of publication	2023
Journal volume	11
Journal issue	12
Pages of publication	473
a	7.292 ± 0.0006 Å
b	10.7627 ± 0.0006 Å
c	10.0442 ± 0.0008 Å
α	90°
β	94.795 ± 0.006°
γ	90°
Cell volume	785.53 ± 0.1 Å³
Cell temperature	200 ± 2 K
Ambient diffraction temperature	200 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0386
Residual factor for significantly intense reflections	0.032
Weighted residual factors for significantly intense reflections	0.072
Weighted residual factors for all reflections included in the refinement	0.077
Goodness-of-fit parameter for all reflections included in the refinement	1.277
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
288922 (current)	2024-01-06	cif/ Adding structures of 1570713, 1570714, 1570715, 1570716 via cif-deposit CGI script.	1570713.cif