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Information card for entry 1570715
Preview
| Coordinates | 1570715.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C13 H10 N4 |
|---|---|
| Calculated formula | C13 H10 N4 |
| Title of publication | The Hexacoordinate Si Complex SiCl4(4-Azidopyridine)2—Crystallographic Characterization of Two Conformers and Probing the Influence of SiCl4-Complexation on a Click Reaction with Phenylacetylene |
| Authors of publication | Riedel, Sophie; Gerwig, Maik; Gerlach, Daniela; Brendler, Erica; Gericke, Robert; Kroke, Edwin; Wagler, Jörg |
| Journal of publication | Inorganics |
| Year of publication | 2023 |
| Journal volume | 11 |
| Journal issue | 12 |
| Pages of publication | 473 |
| a | 9.1259 ± 0.0003 Å |
| b | 11.9037 ± 0.0003 Å |
| c | 9.7351 ± 0.0004 Å |
| α | 90° |
| β | 99.034 ± 0.003° |
| γ | 90° |
| Cell volume | 1044.42 ± 0.06 Å3 |
| Cell temperature | 180 ± 2 K |
| Ambient diffraction temperature | 180 ± 2 K |
| Number of distinct elements | 3 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/n 1 |
| Hall space group symbol | -P 2yn |
| Residual factor for all reflections | 0.0421 |
| Residual factor for significantly intense reflections | 0.0374 |
| Weighted residual factors for significantly intense reflections | 0.0897 |
| Weighted residual factors for all reflections included in the refinement | 0.0922 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.075 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 288922 (current) | 2024-01-06 | cif/ Adding structures of 1570713, 1570714, 1570715, 1570716 via cif-deposit CGI script. |
1570715.cif |
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Users of the data should acknowledge the original authors of the
structural data.