Crystallography Open Database

Information card for entry 1570721

Preview

Coordinates	1570721.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C35 H38.5 B10 N11.5 O8.12 Pb2
Calculated formula	C35 H38.5 B10 N11.5 O8.125 Pb2
Title of publication	Synthesis and Structures of Lead(II) Complexes with Substituted Derivatives of the <i>Closo</i>-Decaborate Anion with a Pendant N<sub>3</sub> Group.
Authors of publication	Matveev, Evgenii Yu; Dontsova, Olga S.; Avdeeva, Varvara V.; Kubasov, Alexey S.; Zhdanov, Andrey P.; Nikiforova, Svetlana E.; Goeva, Lyudmila V.; Zhizhin, Konstantin Yu; Malinina, Elena A.; Kuznetsov, Nikolay T.
Journal of publication	Molecules (Basel, Switzerland)
Year of publication	2023
Journal volume	28
Journal issue	24
Pages of publication	8073
a	16.8622 ± 0.0008 Å
b	17.0582 ± 0.0008 Å
c	18.224 ± 0.0009 Å
α	90°
β	109.153 ± 0.002°
γ	90°
Cell volume	4951.8 ± 0.4 Å³
Cell temperature	150 K
Ambient diffraction temperature	150 K
Number of distinct elements	6
Space group number	13
Hermann-Mauguin space group symbol	P 1 2/n 1
Hall space group symbol	-P 2yac
Residual factor for all reflections	0.1173
Residual factor for significantly intense reflections	0.0706
Weighted residual factors for significantly intense reflections	0.1628
Weighted residual factors for all reflections included in the refinement	0.1868
Goodness-of-fit parameter for all reflections included in the refinement	1.014
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
288932 (current)	2024-01-07	cif/ Adding structures of 1570721 via cif-deposit CGI script.	1570721.cif