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Information card for entry 1570930
Preview
| Coordinates | 1570930.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C23 H30 B N O3 |
|---|---|
| Calculated formula | C23 H30 B N O3 |
| Title of publication | Copper-catalyzed carbonylative multi-component borylamidation of alkenes for synthesizing γ-boryl amides with CO as both methylene and carbonyl sources. |
| Authors of publication | Geng, Hui-Qing; Zhao, Yan-Hua; Yang, Peng; Wu, Xiao-Feng |
| Journal of publication | Chemical science |
| Year of publication | 2024 |
| Journal volume | 15 |
| Journal issue | 11 |
| Pages of publication | 3996 - 4004 |
| a | 13.6717 ± 0.0012 Å |
| b | 16.5727 ± 0.0014 Å |
| c | 19.6345 ± 0.0017 Å |
| α | 85.336 ± 0.002° |
| β | 85.8 ± 0.002° |
| γ | 78.852 ± 0.002° |
| Cell volume | 4342.8 ± 0.6 Å3 |
| Cell temperature | 110 ± 2 K |
| Ambient diffraction temperature | 110 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0746 |
| Residual factor for significantly intense reflections | 0.0561 |
| Weighted residual factors for significantly intense reflections | 0.1413 |
| Weighted residual factors for all reflections included in the refinement | 0.1572 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.025 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 290861 (current) | 2024-04-05 | cif/ Updating files of 1570930 Original log message: Adding full bibliography for 1570930.cif. |
1570930.cif |
| 289712 | 2024-02-06 | cif/ Adding structures of 1570930 via cif-deposit CGI script. |
1570930.cif |
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Users of the data should acknowledge the original authors of the
structural data.