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Information card for entry 1571248
Preview
| Coordinates | 1571248.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C18 H22 N2 O3 |
|---|---|
| Calculated formula | C18 H22 N2 O3 |
| Title of publication | Aza-Achmatowicz rearrangement coupled with intermolecular aza-Friedel-Crafts enables total syntheses of uleine and aspidosperma alkaloids. |
| Authors of publication | Ma, Foqing; Li, Yunlong; Akkarasereenon, Kornkamon; Qiu, Huiying; Cheung, Yuen Tsz; Guo, Zhihong; Tong, Rongbiao |
| Journal of publication | Chemical science |
| Year of publication | 2024 |
| Journal volume | 15 |
| Journal issue | 15 |
| Pages of publication | 5730 - 5737 |
| a | 8.9869 ± 0.0006 Å |
| b | 9.3453 ± 0.0005 Å |
| c | 11.174 ± 0.0006 Å |
| α | 83.313 ± 0.005° |
| β | 81.185 ± 0.005° |
| γ | 61.479 ± 0.006° |
| Cell volume | 813.81 ± 0.09 Å3 |
| Cell temperature | 100 ± 2 K |
| Ambient diffraction temperature | 100 ± 2 K |
| Number of distinct elements | 4 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0393 |
| Residual factor for significantly intense reflections | 0.0346 |
| Weighted residual factors for significantly intense reflections | 0.0866 |
| Weighted residual factors for all reflections included in the refinement | 0.0907 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.035 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 1.54184 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 291578 (current) | 2024-05-05 | cif/ Updating files of 1571247, 1571248 Original log message: Adding full bibliography for 1571247--1571248.cif. |
1571248.cif |
| 290502 | 2024-03-15 | cif/ Adding structures of 1571247, 1571248 via cif-deposit CGI script. |
1571248.cif |
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Users of the data should acknowledge the original authors of the
structural data.