Crystallography Open Database

Information card for entry 1571350

Preview

Coordinates	1571350.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C102 H108 Ce O10 Si4
Calculated formula	C94 H92 Ce O8 Si4
Title of publication	Siloxide tripodal ligands as a scaffold for stabilizing lanthanides in the +4 oxidation state.
Authors of publication	Tricoire, Maxime; Hsueh, Fang-Che; Keener, Megan; Rajeshkumar, Thayalan; Scopelliti, Rosario; Zivkovic, Ivica; Maron, Laurent; Mazzanti, Marinella
Journal of publication	Chemical science
Year of publication	2024
Journal volume	15
Journal issue	18
Pages of publication	6874 - 6883
a	15.94855 ± 0.00011 Å
b	22.45159 ± 0.00016 Å
c	25.0337 ± 0.00019 Å
α	90°
β	90°
γ	90°
Cell volume	8963.82 ± 0.11 Å³
Cell temperature	139.99 ± 0.1 K
Ambient diffraction temperature	139.99 ± 0.1 K
Number of distinct elements	5
Space group number	19
Hermann-Mauguin space group symbol	P 21 21 21
Hall space group symbol	P 2ac 2ab
Residual factor for all reflections	0.0431
Residual factor for significantly intense reflections	0.0409
Weighted residual factors for significantly intense reflections	0.1073
Weighted residual factors for all reflections included in the refinement	0.1097
Goodness-of-fit parameter for all reflections included in the refinement	1.03
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
292913 (current)	2024-07-05	cif/ Updating files of 1571342, 1571343, 1571344, 1571345, 1571346, 1571347, 1571348, 1571349, 1571350, 1571351, 1571352, 1571353, 1571354 Original log message: Adding full bibliography for 1571342--1571354.cif.	1571350.cif
290738	2024-04-03	cif/ Adding structures of 1571342, 1571343, 1571344, 1571345, 1571346, 1571347, 1571348, 1571349, 1571350, 1571351, 1571352, 1571353, 1571354 via cif-deposit CGI script.	1571350.cif