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Information card for entry 1571410
Preview
| Coordinates | 1571410.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C39 H29 P S |
|---|---|
| Calculated formula | C39 H29 P S |
| Title of publication | Palladium-catalyzed regio- and stereo-selective phosphination of cyclic biarylsulfonium salts to access atropoisomeric phosphines. |
| Authors of publication | Sun, Jinghui; Yan, Yifei; Chen, Xuanxuan; Huang, Zhiwei; Huang, Yinhua |
| Journal of publication | Chemical science |
| Year of publication | 2024 |
| Journal volume | 15 |
| Journal issue | 18 |
| Pages of publication | 6943 - 6948 |
| a | 11.039 ± 0.0006 Å |
| b | 15.1879 ± 0.0008 Å |
| c | 16.0708 ± 0.0007 Å |
| α | 112.211 ± 0.002° |
| β | 104.135 ± 0.002° |
| γ | 103.663 ± 0.002° |
| Cell volume | 2251.2 ± 0.2 Å3 |
| Cell temperature | 170 K |
| Ambient diffraction temperature | 170 K |
| Number of distinct elements | 4 |
| Space group number | 1 |
| Hermann-Mauguin space group symbol | P 1 |
| Hall space group symbol | P 1 |
| Residual factor for all reflections | 0.0591 |
| Residual factor for significantly intense reflections | 0.047 |
| Weighted residual factors for significantly intense reflections | 0.1012 |
| Weighted residual factors for all reflections included in the refinement | 0.1094 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.08 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 292911 (current) | 2024-07-05 | cif/ Updating files of 1571408, 1571409, 1571410 Original log message: Adding full bibliography for 1571408--1571410.cif. |
1571410.cif |
| 291145 | 2024-04-10 | cif/ Adding structures of 1571408, 1571409, 1571410 via cif-deposit CGI script. |
1571410.cif |
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Users of the data should acknowledge the original authors of the
structural data.