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Information card for entry 1571565
Preview
| Coordinates | 1571565.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C41 H35 F N2 O5 |
|---|---|
| Calculated formula | C41 H35 F N2 O5 |
| Title of publication | Organocatalytic diastereo- and atropo-selective construction of eight-membered bridged (hetero)biaryls <i>via</i> asymmetric intramolecular [3 + 2] cycloaddition. |
| Authors of publication | Wang, Yue; Huang, Yue; Bao, Xiaoze; Wei, Xingfu; Wei, Shiqiang; Qu, Jingping; Wang, Baomin |
| Journal of publication | Chemical science |
| Year of publication | 2024 |
| Journal volume | 15 |
| Journal issue | 23 |
| Pages of publication | 8880 - 8887 |
| a | 9.0844 ± 0.0003 Å |
| b | 10.3859 ± 0.0004 Å |
| c | 18.7463 ± 0.0006 Å |
| α | 75.426 ± 0.002° |
| β | 89.765 ± 0.002° |
| γ | 88.695 ± 0.002° |
| Cell volume | 1711.35 ± 0.1 Å3 |
| Cell temperature | 302 K |
| Ambient diffraction temperature | 302 K |
| Number of distinct elements | 5 |
| Space group number | 1 |
| Hermann-Mauguin space group symbol | P 1 |
| Hall space group symbol | P 1 |
| Residual factor for all reflections | 0.08 |
| Residual factor for significantly intense reflections | 0.0635 |
| Weighted residual factors for significantly intense reflections | 0.151 |
| Weighted residual factors for all reflections included in the refinement | 0.1708 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.094 |
| Diffraction radiation wavelength | 1.54178 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 292918 (current) | 2024-07-05 | cif/ Updating files of 1571565, 1571566 Original log message: Adding full bibliography for 1571565--1571566.cif. |
1571565.cif |
| 291756 | 2024-05-08 | cif/ Adding structures of 1571565, 1571566 via cif-deposit CGI script. |
1571565.cif |
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Users of the data should acknowledge the original authors of the
structural data.