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Information card for entry 1571632
Preview
| Coordinates | 1571632.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C20 H22 Cl N O3 S2 |
|---|---|
| Calculated formula | C20 H22 Cl N O3 S2 |
| Title of publication | Palladium-catalyzed selective C-C bond cleavage of keto-vinylidenecyclopropanes: construction of structurally rich dihydrofurans and tetrahydrofurans. |
| Authors of publication | Ning, Chao; Yu, Ziqi; Shi, Min; Wei, Yin |
| Journal of publication | Chemical science |
| Year of publication | 2024 |
| Journal volume | 15 |
| Journal issue | 24 |
| Pages of publication | 9192 - 9200 |
| a | 19.7752 ± 0.0008 Å |
| b | 9.1254 ± 0.0003 Å |
| c | 11.5285 ± 0.0004 Å |
| α | 90° |
| β | 96.477 ± 0.001° |
| γ | 90° |
| Cell volume | 2067.12 ± 0.13 Å3 |
| Cell temperature | 293 ± 2 K |
| Ambient diffraction temperature | 293 ± 2 K |
| Number of distinct elements | 6 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/c 1 |
| Hall space group symbol | -P 2ybc |
| Residual factor for all reflections | 0.0522 |
| Residual factor for significantly intense reflections | 0.0429 |
| Weighted residual factors for significantly intense reflections | 0.1105 |
| Weighted residual factors for all reflections included in the refinement | 0.1191 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.066 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 292859 (current) | 2024-07-05 | cif/ Updating files of 1571631, 1571632 Original log message: Adding full bibliography for 1571631--1571632.cif. |
1571632.cif |
| 291846 | 2024-05-15 | cif/ Adding structures of 1571631, 1571632 via cif-deposit CGI script. |
1571632.cif |
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Users of the data should acknowledge the original authors of the
structural data.