Crystallography Open Database

Information card for entry 1573554

Preview

Coordinates	1573554.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C10.09 H14.96 Cl0.17 Dy0.17 N0.7
Calculated formula	C10.087 H14.9565 Cl0.173913 Dy0.173913 N0.695652
Title of publication	Rare earth benzene tetraanion-bridged amidinate complexes.
Authors of publication	Jin, Peng-Bo; Luo, Qian-Cheng; Gransbury, Gemma K.; Winpenny, Richard E. P.; Mills, David P.; Zheng, Yan-Zhen
Journal of publication	Chemical science
Year of publication	2025
Journal volume	16
Journal issue	4
Pages of publication	1907 - 1924
a	23.9612 ± 0.0013 Å
b	10.5893 ± 0.0004 Å
c	22.5423 ± 0.0013 Å
α	90°
β	112.235 ± 0.006°
γ	90°
Cell volume	5294.4 ± 0.5 Å³
Cell temperature	100.01 ± 0.1 K
Ambient diffraction temperature	100.01 ± 0.1 K
Number of distinct elements	5
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0604
Residual factor for significantly intense reflections	0.0498
Weighted residual factors for significantly intense reflections	0.1084
Weighted residual factors for all reflections included in the refinement	0.1165
Goodness-of-fit parameter for all reflections included in the refinement	1.015
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
298113 (current)	2025-03-04	cif/ Updating files of 1573553, 1573554, 1573555, 1573556, 1573557, 1573558, 1573559, 1573560, 1573561 Original log message: Adding full bibliography for 1573553--1573561.cif.	1573554.cif
297004	2025-01-01	cif/ Adding structures of 1573553, 1573554, 1573555, 1573556, 1573557, 1573558, 1573559, 1573560, 1573561 via cif-deposit CGI script.	1573554.cif