Crystallography Open Database

Information card for entry 1574207

Preview

Coordinates	1574207.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	KT-75
Formula	C36 H64 Cr O2 Si5
Calculated formula	C36 H64 Cr O2 Si5
Title of publication	Metal–silicon triple bonds: reactivity of the silylidyne complexes [Cp*(CO)2M≡Si–Tbb] (M = Cr – W)
Authors of publication	Tomer, Kanishk; Schnakenburg, Gregor; Das, Ujjal; Filippou, Alexander C.
Journal of publication	Chemical Science
Year of publication	2025
Journal volume	16
Journal issue	18
Pages of publication	7773 - 7793
a	12.061 ± 0.003 Å
b	15.143 ± 0.004 Å
c	12.602 ± 0.003 Å
α	90°
β	97.363 ± 0.006°
γ	90°
Cell volume	2282.6 ± 1 Å³
Cell temperature	100 K
Ambient diffraction temperature	100 K
Number of distinct elements	5
Space group number	11
Hermann-Mauguin space group symbol	P 1 21/m 1
Hall space group symbol	-P 2yb
Residual factor for all reflections	0.1195
Residual factor for significantly intense reflections	0.083
Weighted residual factors for significantly intense reflections	0.23
Weighted residual factors for all reflections included in the refinement	0.2701
Goodness-of-fit parameter for all reflections included in the refinement	1.025
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
300652 (current)	2025-07-06	cif/ Updating files of 1574207, 1574208, 1574209, 1574210, 1574211, 1574212, 1574213, 1574214 Original log message: Adding full bibliography for 1574207--1574214.cif.	1574207.cif
298566	2025-03-25	cif/ Adding structures of 1574207, 1574208, 1574209, 1574210, 1574211, 1574212, 1574213, 1574214 via cif-deposit CGI script.	1574207.cif