#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/00/39/2003931.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2003931_Fobs loop_ _publ_author_name 'Brayshaw, P. A.' 'Harrowfield, J. M.' 'Sobolev, A. N.' _publ_section_title ; A Strongly Luminescent Organic-Solvent-Soluble Salt of the Tris(dipicolinato)europium(III) Trianion ; _journal_issue 9 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 1799 _journal_page_last 1802 _journal_volume 51 _journal_year 1995 _space_group_IT_number 13 _symmetry_space_group_name_Hall '-P 2yc' _symmetry_space_group_name_H-M 'P 1 2/c 1' _exptl_crystal_F_000 2320.00 _[local]_cod_data_source_file na1151sup2.hkl _[local]_cod_data_source_block EUDIPIC #BEGIN Tags that were not found in dictionaries: _shelx_title ' Eu(dipic)3 * 3NEt4 * 4H(2)O' _shelx_refln_list_code 4 _shelx_f_calc_maximum 381.78 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 972.43 607.47 43.64 o 4 0 0 49371.08 46107.69 262.53 o 5 0 0 29901.98 29525.05 237.48 o 6 0 0 3524.04 4593.83 111.38 o 7 0 0 3328.49 3435.90 107.28 o 8 0 0 17271.05 15263.26 216.37 o 9 0 0 262.53 128.21 60.64 o 10 0 0 19981.04 19356.42 279.99 o 11 0 0 1925.96 1740.92 119.07 o 12 0 0 63746.50 68184.84 584.83 o 13 0 0 152.56 -9.89 98.45 o 14 0 0 36731.15 37899.86 473.02 o 15 0 0 425.31 83.37 112.32 o 16 0 0 20442.37 21791.71 398.67 o 17 0 0 42.77 -47.70 98.55 o 18 0 0 12868.88 13245.32 338.79 o 19 0 0 93.14 -15.39 114.04 o 20 0 0 15113.60 15317.33 386.05 o 21 0 0 38.11 -161.54 126.17 o 22 0 0 5533.25 5962.51 264.26 o 23 0 0 .16 -109.66 107.01 o 24 0 0 1786.94 1910.40 171.75 o 25 0 0 47.94 89.48 117.41 o 26 0 0 3704.48 3791.01 249.64 o 27 0 0 53.92 -174.28 138.71 o 28 0 0 3115.32 3108.31 243.52 o 0 1 0 17680.81 19794.98 126.45 o 1 1 0 30422.57 29463.11 159.40 o 2 1 0 7584.41 7958.81 96.22 o 3 1 0 17313.77 21281.55 174.41 o 4 1 0 57824.88 58840.75 316.91 o 5 1 0 6629.80 7150.38 129.84 o 6 1 0 4267.39 4124.48 111.08 o 7 1 0 771.95 532.07 63.71 o 8 1 0 12273.24 11326.50 191.67 o 9 1 0 6744.74 7275.02 172.00 o 10 1 0 1146.94 1174.65 90.72 o 11 1 0 10100.53 10743.77 229.59 o 12 1 0 1866.32 2124.25 124.57 o 13 1 0 9674.73 9500.12 245.45 o 14 1 0 7297.80 7133.93 225.70 o 15 1 0 9838.09 10369.50 278.88 o 16 1 0 3977.84 4186.66 195.44 o 17 1 0 5042.01 5113.41 216.05 o 18 1 0 1873.38 2210.25 163.39 o 19 1 0 1867.71 1821.58 152.08 o 20 1 0 248.65 -75.83 127.91 o 21 1 0 3509.00 3468.27 223.35 o 22 1 0 828.60 996.48 139.53 o 23 1 0 679.80 581.76 133.72 o 24 1 0 785.65 859.39 143.50 o 25 1 0 33.51 11.21 110.37 o 26 1 0 1068.11 925.45 174.49 o 27 1 0 246.77 225.13 129.94 o 28 1 0 626.52 526.72 166.64 o 0 2 0 5592.02 6048.78 106.68 o 1 2 0 58543.27 56401.81 299.58 o 2 2 0 11388.47 12034.23 148.23 o 3 2 0 8910.80 9794.15 147.28 o 4 2 0 1201.22 1095.37 72.18 o 5 2 0 52902.69 55458.05 375.24 o 6 2 0 2913.51 2675.64 101.36 o 7 2 0 22285.66 22569.55 270.32 o 8 2 0 12701.50 12754.62 215.74 o 9 2 0 1445.94 1446.87 94.49 o 10 2 0 45.27 24.56 59.42 o 11 2 0 6439.80 6505.09 188.88 o 12 2 0 583.27 511.65 81.03 o 13 2 0 20930.50 21191.35 351.92 o 14 2 0 8906.32 9062.70 243.57 o 15 2 0 7268.55 7874.66 241.08 o 16 2 0 500.23 762.97 106.20 o 17 2 0 4562.87 4137.60 194.52 o 18 2 0 500.85 635.67 115.78 o 19 2 0 1871.60 1962.34 168.69 o 20 2 0 1622.64 1671.49 158.39 o 21 2 0 1014.93 932.49 150.23 o 22 2 0 1195.27 1192.09 159.41 o 23 2 0 1216.31 1338.25 159.92 o 24 2 0 1348.95 1252.13 170.01 o 25 2 0 1927.06 1811.54 204.16 o 26 2 0 138.98 -36.18 151.86 o 27 2 0 1495.95 1420.81 198.14 o 0 3 0 43192.41 41135.69 317.29 o 1 3 0 637.46 774.86 67.78 o 2 3 0 381.27 531.02 63.70 o 3 3 0 1036.47 993.86 77.98 o 4 3 0 44.01 -69.61 60.84 o 5 3 0 440.69 418.90 62.68 o 6 3 0 346.45 453.14 60.74 o 7 3 0 10646.35 11013.06 209.03 o 8 3 0 6540.94 6256.21 166.26 o 9 3 0 1968.78 1811.97 109.58 o 10 3 0 4109.58 4789.46 163.75 o 11 3 0 4271.70 4090.36 163.34 o 12 3 0 108.09 42.50 78.58 o 13 3 0 127.51 34.04 85.41 o 14 3 0 442.81 532.73 84.80 o 15 3 0 195.82 337.14 92.34 o 16 3 0 135.22 98.55 86.83 o 17 3 0 535.88 453.54 104.98 o 18 3 0 88.73 -23.75 105.18 o 19 3 0 857.98 818.43 135.15 o 20 3 0 989.33 992.31 134.13 o 21 3 0 1193.52 1106.89 156.25 o 22 3 0 280.30 262.33 105.79 o 23 3 0 1800.61 1610.54 173.99 o 24 3 0 246.95 122.10 114.76 o 25 3 0 722.10 807.30 152.98 o 26 3 0 103.70 259.38 137.08 o 27 3 0 122.39 -77.97 149.21 o 0 4 0 5898.58 5491.54 143.83 o 1 4 0 60852.55 60411.41 448.34 o 2 4 0 7.05 21.81 31.29 o 3 4 0 23821.64 23379.34 294.30 o 4 4 0 610.22 708.68 76.24 o 5 4 0 13385.61 14374.29 244.61 o 6 4 0 1058.75 1075.55 91.12 o 7 4 0 32898.97 32007.59 381.21 o 8 4 0 1.56 8.66 64.51 o 9 4 0 23701.53 24836.17 363.01 o 10 4 0 845.04 1107.81 98.56 o 11 4 0 15681.53 16088.88 318.55 o 12 4 0 140.75 181.51 86.12 o 13 4 0 14768.56 14026.76 321.24 o 14 4 0 13.11 163.68 78.88 o 15 4 0 8894.63 9428.32 286.48 o 16 4 0 3.89 90.30 90.30 o 17 4 0 6859.80 6713.92 258.69 o 18 4 0 314.85 567.58 112.62 o 19 4 0 8626.26 8484.50 305.61 o 20 4 0 1.75 46.88 97.02 o 21 4 0 5842.68 5824.93 273.23 o 22 4 0 55.97 -42.09 110.17 o 23 4 0 3038.05 2898.98 206.11 o 24 4 0 52.61 -34.55 127.60 o 25 4 0 2722.84 2493.32 214.46 o 26 4 0 376.28 395.24 133.10 o 0 5 0 1273.02 991.79 87.86 o 1 5 0 12760.63 12467.60 233.54 o 2 5 0 6711.15 6666.77 177.98 o 3 5 0 667.96 685.13 80.11 o 4 5 0 10699.35 10395.17 228.87 o 5 5 0 2049.86 2175.57 119.57 o 6 5 0 19992.37 20278.21 325.29 o 7 5 0 1735.22 1497.91 108.86 o 8 5 0 15006.48 15217.72 296.40 o 9 5 0 27.55 59.72 70.12 o 10 5 0 12960.03 13486.62 301.82 o 11 5 0 21.32 154.40 82.96 o 12 5 0 8677.71 9087.50 265.78 o 13 5 0 1689.78 1877.33 145.76 o 14 5 0 6126.50 5941.70 231.97 o 15 5 0 1578.35 1686.59 144.53 o 16 5 0 8605.44 8602.50 291.25 o 17 5 0 2233.57 2402.92 181.13 o 18 5 0 6130.10 6064.16 265.70 o 19 5 0 484.71 554.03 121.79 o 20 5 0 5649.88 5978.80 273.13 o 21 5 0 165.34 333.37 99.98 o 22 5 0 3088.68 3456.97 234.55 o 23 5 0 76.83 -81.13 116.49 o 24 5 0 1723.92 1286.70 181.12 o 25 5 0 15.82 -138.81 127.90 o 26 5 0 1686.73 1338.78 204.87 o 0 6 0 3353.24 2872.23 134.47 o 1 6 0 514.04 564.34 75.22 o 2 6 0 11156.46 10567.18 243.85 o 3 6 0 76.36 9.99 76.23 o 4 6 0 18123.71 17481.96 320.16 o 5 6 0 470.10 609.89 98.25 o 6 6 0 16260.13 17930.56 328.86 o 7 6 0 2.06 77.86 71.24 o 8 6 0 12091.56 11722.17 285.87 o 9 6 0 1025.81 1133.30 119.86 o 10 6 0 12090.33 12727.78 318.90 o 11 6 0 151.70 291.28 104.77 o 12 6 0 14514.98 14382.46 351.49 o 13 6 0 113.49 -36.79 98.76 o 14 6 0 6539.24 7306.75 264.59 o 15 6 0 135.36 .00 102.63 o 16 6 0 4877.53 4794.03 228.36 o 17 6 0 979.98 925.14 144.63 o 18 6 0 6809.84 6329.29 284.57 o 19 6 0 344.73 326.34 117.41 o 20 6 0 2061.82 1860.39 202.73 o 21 6 0 .89 154.91 87.14 o 22 6 0 3199.14 3087.57 229.15 o 23 6 0 125.15 354.97 115.47 o 24 6 0 2467.74 2746.26 246.36 o 0 7 0 564.09 428.68 92.24 o 1 7 0 6503.92 6246.65 212.10 o 2 7 0 336.61 401.46 95.91 o 3 7 0 10321.13 10224.48 270.72 o 4 7 0 1023.96 909.37 113.54 o 5 7 0 8824.22 8360.01 253.55 o 6 7 0 1366.39 1434.52 136.48 o 7 7 0 3700.41 3643.33 180.34 o 8 7 0 885.93 980.70 120.17 o 9 7 0 6345.04 6987.02 252.57 o 10 7 0 67.60 25.89 74.70 o 11 7 0 5703.14 5412.71 237.56 o 12 7 0 205.41 55.34 109.76 o 13 7 0 4049.38 3945.52 208.17 o 14 7 0 60.56 -95.29 92.85 o 15 7 0 2392.51 2219.86 183.58 o 16 7 0 49.11 -46.78 100.39 o 17 7 0 3732.26 3474.58 225.90 o 18 7 0 25.09 102.12 105.08 o 19 7 0 1773.65 1725.40 162.98 o 20 7 0 .37 -192.82 121.59 o 21 7 0 2076.42 2012.04 219.55 o 22 7 0 90.45 -74.70 139.83 o 23 7 0 1516.04 1455.98 184.79 o 0 8 0 1120.96 1083.15 133.11 o 1 8 0 1020.66 1127.48 119.25 o 2 8 0 1283.10 1331.76 144.02 o 3 8 0 69.86 41.48 108.44 o 4 8 0 30.72 62.68 91.32 o 5 8 0 9.01 305.95 89.18 o 6 8 0 411.33 403.19 106.40 o 7 8 0 1091.56 997.63 138.82 o 8 8 0 1018.29 879.08 124.45 o 9 8 0 1514.68 1385.99 151.05 o 10 8 0 4828.03 4806.98 228.26 o 11 8 0 579.15 551.28 138.10 o 12 8 0 5.89 44.13 101.00 o 13 8 0 522.76 787.63 120.47 o 14 8 0 9.49 .00 99.47 o 15 8 0 334.17 516.21 118.22 o 16 8 0 46.30 30.68 110.88 o 17 8 0 1780.03 2043.51 180.61 o 18 8 0 52.09 288.32 106.40 o 19 8 0 879.81 829.63 143.81 o 20 8 0 439.34 146.76 161.23 o 21 8 0 555.55 470.35 143.30 o 22 8 0 248.77 26.70 154.40 o 0 9 0 1530.06 1614.41 154.62 o 1 9 0 8362.76 8508.20 280.63 o 2 9 0 52.49 54.02 105.48 o 3 9 0 7181.03 7015.72 268.58 o 4 9 0 1293.45 1361.10 141.88 o 5 9 0 2304.66 2393.45 174.91 o 6 9 0 445.12 550.26 112.31 o 7 9 0 2058.62 2059.07 175.93 o 8 9 0 215.08 173.05 102.43 o 9 9 0 1919.74 1970.98 175.42 o 10 9 0 121.59 308.60 93.05 o 11 9 0 4586.90 4285.12 246.70 o 12 9 0 294.28 137.79 130.66 o 13 9 0 3074.57 3027.23 219.16 o 14 9 0 243.51 296.68 115.06 o 15 9 0 1750.37 1377.83 177.76 o 16 9 0 182.07 157.46 121.18 o 17 9 0 2017.47 1616.96 178.27 o 18 9 0 10.53 301.87 94.37 o 19 9 0 2327.87 2413.14 219.04 o 0 10 0 666.71 927.88 127.09 o 1 10 0 3327.85 3431.39 200.82 o 2 10 0 2148.84 2062.23 184.49 o 3 10 0 5306.47 5058.71 240.40 o 4 10 0 397.27 282.52 143.19 o 5 10 0 4441.45 4448.60 236.61 o 6 10 0 467.30 651.26 122.10 o 7 10 0 4186.77 4135.75 228.65 o 8 10 0 6.95 -175.40 114.45 o 9 10 0 2375.21 2393.10 189.18 o 10 10 0 740.78 467.91 141.06 o 11 10 0 1499.33 1571.47 192.84 o 12 10 0 42.70 32.61 101.41 o 13 10 0 968.57 881.21 166.54 o 14 10 0 19.10 -128.82 137.99 o 15 10 0 1639.40 1819.35 198.34 o 16 10 0 552.24 580.43 153.69 o 17 10 0 1228.65 1145.40 179.08 o 0 11 0 3693.16 3502.66 228.24 o 1 11 0 22.06 138.30 100.79 o 2 11 0 4388.70 4278.78 254.85 o 3 11 0 15.56 60.44 123.32 o 4 11 0 3960.26 4063.47 250.97 o 5 11 0 8.76 31.39 97.33 o 6 11 0 5372.83 5137.68 278.72 o 7 11 0 40.41 137.59 104.36 o 8 11 0 5537.13 5568.33 293.30 o 9 11 0 24.72 -245.41 131.98 o 10 11 0 3794.94 3987.75 253.52 o 11 11 0 38.30 157.87 115.78 o 12 11 0 3378.63 3352.09 247.70 o 13 11 0 11.11 .00 109.15 o 14 11 0 2290.22 2186.14 219.86 o 0 12 0 1101.94 1154.87 159.30 o 1 12 0 92.11 78.07 113.23 o 2 12 0 677.33 845.11 154.92 o 3 12 0 494.55 567.17 131.27 o 4 12 0 973.27 1055.49 153.39 o 5 12 0 1228.19 1325.19 167.05 o 6 12 0 715.95 467.30 166.13 o 7 12 0 1030.31 1185.54 165.93 o 8 12 0 446.01 415.42 139.32 o 9 12 0 324.25 559.73 141.26 o -28 1 1 1490.38 1293.10 206.09 o -27 1 1 19.57 49.63 127.60 o -26 1 1 1789.04 1858.61 180.71 o -25 1 1 48.92 122.30 111.70 o -24 1 1 3771.62 3429.20 220.59 o -23 1 1 54.14 -69.51 111.09 o -22 1 1 6288.60 6058.84 268.65 o -21 1 1 115.17 205.67 99.98 o -20 1 1 7224.99 7277.54 272.96 o -19 1 1 622.04 514.19 119.14 o -18 1 1 6887.59 6742.99 244.52 o -17 1 1 1437.85 1248.00 128.94 o -16 1 1 13207.79 13461.33 323.64 o -15 1 1 514.13 709.36 97.74 o -14 1 1 19991.69 20845.54 356.37 o -13 1 1 33.53 49.84 67.47 o -12 1 1 16157.03 17173.12 296.49 o -11 1 1 5125.04 5707.31 170.00 o -10 1 1 35167.62 35596.87 381.79 o -9 1 1 6186.11 6334.41 160.05 o -8 1 1 8864.63 8762.46 169.22 o -7 1 1 18686.69 18958.14 227.63 o -6 1 1 10599.68 10873.34 167.92 o -5 1 1 1943.57 1949.03 79.02 o -4 1 1 4825.99 5034.88 99.91 o -3 1 1 448.15 392.64 46.79 o -2 1 1 22015.63 23369.57 159.43 o -1 1 1 6367.07 6051.10 79.34 o 0 1 1 73982.05 78678.12 1001.22 o 1 1 1 3234.91 3723.57 66.86 o 2 1 1 43715.84 43111.30 226.51 o 3 1 1 4238.74 4492.81 90.52 o 4 1 1 45360.76 49559.68 300.50 o 5 1 1 352.09 314.43 61.26 o 6 1 1 17398.39 17945.03 216.81 o 7 1 1 879.82 833.08 62.79 o 8 1 1 11743.35 10452.80 190.42 o 9 1 1 311.41 427.15 60.85 o 10 1 1 14962.11 15279.82 259.46 o 11 1 1 1909.76 1903.49 114.17 o 12 1 1 16490.61 16617.93 300.47 o 13 1 1 6465.70 6603.81 199.37 o 14 1 1 12181.04 12725.28 287.32 o 15 1 1 3054.84 3542.41 172.18 o 16 1 1 9167.18 9509.62 278.75 o 17 1 1 3053.80 3720.50 187.67 o 18 1 1 6276.44 6964.09 258.17 o 19 1 1 103.29 173.05 95.70 o 20 1 1 3358.13 3383.14 201.33 o 21 1 1 26.69 -9.17 97.33 o 22 1 1 3711.14 4215.18 222.33 o 23 1 1 64.67 -30.37 107.01 o 24 1 1 2731.19 2396.21 199.07 o 25 1 1 193.01 124.85 103.45 o 26 1 1 2210.15 2281.14 217.41 o 27 1 1 23.61 25.28 117.41 o 28 1 1 1717.22 1345.00 208.44 o -27 2 1 714.53 717.21 132.50 o -26 2 1 993.70 848.08 159.81 o -25 2 1 1701.30 1773.80 175.31 o -24 2 1 1190.04 1134.40 156.55 o -23 2 1 6072.74 5277.38 261.30 o -22 2 1 1330.89 1007.21 150.64 o -21 2 1 4581.66 4766.07 241.71 o -20 2 1 1834.98 1553.79 165.02 o -19 2 1 1956.56 1771.03 151.26 o -18 2 1 1277.12 1492.08 138.92 o -17 2 1 3697.18 3521.38 193.70 o -16 2 1 6058.16 5743.46 221.67 o -15 2 1 1311.84 1094.90 124.45 o -14 2 1 12577.51 13558.89 296.31 o -13 2 1 6512.84 6452.74 201.82 o -12 2 1 4317.23 4551.17 169.56 o -11 2 1 3443.98 3968.31 148.14 o -10 2 1 1118.29 1214.49 90.31 o -9 2 1 20555.01 21396.28 293.50 o -8 2 1 3253.40 3498.28 118.89 o -7 2 1 7386.85 6648.20 151.63 o -6 2 1 307.38 205.47 59.83 o -5 2 1 24997.07 25886.93 255.95 o -4 2 1 771.40 683.87 65.14 o -3 2 1 5326.68 5404.25 112.86 o -2 2 1 1206.94 1111.13 61.47 o -1 2 1 23916.19 24217.28 200.38 o 0 2 1 2497.03 2783.26 82.10 o 1 2 1 11241.77 10731.56 139.65 o 2 2 1 3509.86 3675.55 92.32 o 3 2 1 2635.19 2799.93 89.84 o 4 2 1 22.87 60.23 56.26 o 5 2 1 18205.36 19139.46 228.88 o 6 2 1 18303.45 19525.80 242.40 o 7 2 1 77682.55 81917.70 516.84 o 8 2 1 106.25 140.03 58.81 o 9 2 1 17027.07 17948.61 274.04 o 10 2 1 359.40 579.52 74.91 o 11 2 1 23162.02 23618.30 350.26 o 12 2 1 8228.77 9029.00 232.26 o 13 2 1 1450.59 1565.84 118.95 o 14 2 1 964.69 990.60 111.30 o 15 2 1 1271.36 1239.83 118.03 o 16 2 1 330.75 551.28 103.45 o 17 2 1 956.13 958.79 121.29 o 18 2 1 2825.53 2843.21 180.12 o 19 2 1 3309.64 3579.39 204.18 o 20 2 1 592.53 532.94 121.39 o 21 2 1 4491.49 4614.84 229.27 o 22 2 1 11.51 46.27 93.05 o 23 2 1 4521.06 4696.82 249.15 o 24 2 1 708.62 808.63 145.03 o 25 2 1 1450.31 1233.68 169.09 o 26 2 1 1199.64 1352.51 185.19 o 27 2 1 1168.23 1154.57 188.56 o -27 3 1 3980.78 3686.85 267.28 o -26 3 1 .42 98.04 105.38 o -25 3 1 3599.16 3575.09 241.79 o -24 3 1 27.26 88.06 115.57 o -23 3 1 5151.21 4949.30 263.23 o -22 3 1 790.85 670.33 145.34 o -21 3 1 11186.98 11254.78 360.53 o -20 3 1 20.92 -124.03 105.69 o -19 3 1 11352.74 10178.00 317.51 o -18 3 1 507.49 352.44 123.53 o -17 3 1 8545.01 8704.09 278.61 o -16 3 1 464.70 426.12 116.29 o -15 3 1 6717.25 6884.57 235.05 o -14 3 1 1239.19 1386.71 117.22 o -13 3 1 9783.99 9422.18 249.41 o -12 3 1 554.14 602.05 87.65 o -11 3 1 20675.34 21672.20 346.55 o -10 3 1 5724.01 6086.32 182.65 o -9 3 1 45296.30 44316.60 447.27 o -8 3 1 2250.81 2951.82 118.87 o -7 3 1 18509.55 18200.36 261.67 o -6 3 1 193.44 267.94 60.85 o -5 3 1 10207.66 10351.21 184.97 o -4 3 1 1646.35 2110.55 93.28 o -3 3 1 22250.21 22578.36 252.12 o -2 3 1 1406.81 1391.41 77.68 o -1 3 1 34123.19 33389.64 287.75 o 0 3 1 1948.91 2341.48 97.06 o 1 3 1 21536.25 23267.73 247.55 o 2 3 1 124.70 14.88 55.85 o 3 3 1 18016.25 19445.02 239.14 o 4 3 1 4179.22 3587.67 119.12 o 5 3 1 13714.18 12952.04 212.44 o 6 3 1 6.48 72.97 50.45 o 7 3 1 35425.64 34983.67 366.29 o 8 3 1 4599.62 4464.84 146.84 o 9 3 1 22105.47 23017.92 327.99 o 10 3 1 12739.72 15165.84 281.17 o 11 3 1 13633.06 13655.15 280.35 o 12 3 1 640.32 699.79 80.31 o 13 3 1 13378.17 13751.77 304.49 o 14 3 1 .13 86.22 71.24 o 15 3 1 9646.31 9889.61 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