#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/00/54/2005410.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2005410_Fobs loop_ _publ_author_name 'Nicol\`o, F.' 'Bruno, G.' 'Tresoldi, G.' _publ_section_title ; Bis[bis(2-pyridyl-N) sulfide]palladium(II) Bis(tetrafluoroborate) ; _journal_issue 9 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 2188 _journal_page_last 2191 _journal_volume 52 _journal_year 1996 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _exptl_crystal_F_000 648.00 _[local]_cod_data_source_file na1236sup2.hkl _[local]_cod_data_source_block tres1 #BEGIN Tags that were not found in dictionaries: _shelx_title 'tres1 in P2(1)/n' _shelx_refln_list_code 7 _shelx_f_multiplier 1.46007 #END Tags that were not found in dictionaries loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_meas _refln_F_sigma _refln_F_calc 2 0 0 100.17 0.23 100.99 4 0 0 43.80 0.27 43.00 6 0 0 26.23 0.36 25.21 8 0 0 10.46 0.84 9.76 1 1 0 114.32 1.30 111.20 2 1 0 160.53 0.85 160.01 3 1 0 87.04 0.21 87.73 4 1 0 21.26 0.31 20.92 5 1 0 37.29 0.25 37.28 7 1 0 6.82 0.83 6.58 9 1 0 20.22 0.55 20.41 0 2 0 45.30 0.19 44.71 2 2 0 22.34 0.22 22.45 3 2 0 35.16 0.23 34.15 4 2 0 83.48 0.35 84.06 5 2 0 29.67 0.31 29.33 6 2 0 49.34 0.33 49.37 7 2 0 17.92 0.51 18.54 8 2 0 26.36 0.45 25.47 1 3 0 10.29 0.24 11.01 2 3 0 9.85 0.36 8.57 3 3 0 20.33 0.27 21.15 5 3 0 83.27 0.37 81.90 6 3 0 12.59 0.58 12.81 7 3 0 36.50 0.38 36.69 8 3 0 8.29 1.09 8.25 9 3 0 18.77 0.61 19.23 0 4 0 11.00 0.31 9.83 1 4 0 5.16 0.46 6.12 2 4 0 39.75 0.24 40.49 3 4 0 31.37 0.25 30.96 4 4 0 48.35 0.29 47.97 5 4 0 18.20 0.40 17.44 6 4 0 31.38 0.35 30.67 8 4 0 30.41 0.43 30.72 1 5 0 88.91 1.10 87.64 2 5 0 57.59 0.28 57.35 3 5 0 48.37 0.28 47.32 4 5 0 10.54 0.51 11.29 5 5 0 42.28 0.31 42.48 7 5 0 15.91 0.51 15.30 9 5 0 17.04 0.64 15.96 0 6 0 100.40 0.32 100.20 1 6 0 8.37 0.34 6.38 2 6 0 60.30 0.28 62.89 4 6 0 23.81 0.33 24.35 5 6 0 10.89 0.59 10.75 6 6 0 19.13 0.44 19.16 8 6 0 13.58 0.66 12.91 1 7 0 63.15 0.22 64.99 3 7 0 54.44 0.30 54.77 4 7 0 11.56 0.53 12.06 5 7 0 27.47 0.36 26.64 7 7 0 13.63 0.61 13.66 0 8 0 65.92 0.31 66.67 1 8 0 6.92 0.49 7.84 2 8 0 40.42 0.29 40.47 3 8 0 14.05 0.45 13.40 4 8 0 29.39 0.33 29.53 5 8 0 6.63 1.04 8.08 6 8 0 21.82 0.43 21.82 8 8 0 11.62 0.82 12.09 1 9 0 28.20 0.22 27.74 2 9 0 16.20 0.40 17.02 3 9 0 38.61 0.32 38.44 4 9 0 16.93 0.43 17.10 5 9 0 19.77 0.45 19.52 7 9 0 21.77 0.52 23.23 2 10 0 20.83 0.37 19.40 3 10 0 9.08 0.69 9.19 4 10 0 27.50 0.38 26.71 6 10 0 25.54 0.45 25.40 1 11 0 13.87 0.57 12.40 2 11 0 15.97 0.46 16.06 3 11 0 28.81 0.38 28.74 5 11 0 24.03 0.46 23.10 0 12 0 26.99 0.39 26.90 1 12 0 12.54 0.42 11.74 2 12 0 26.08 0.41 26.73 3 12 0 8.66 0.81 9.86 4 12 0 14.48 0.57 14.14 1 13 0 29.47 0.30 30.66 3 13 0 19.26 0.50 19.50 5 13 0 9.08 0.97 10.14 0 14 0 21.27 0.49 20.27 2 14 0 28.29 0.45 29.60 1 15 0 15.76 0.48 14.95 -9 0 1 17.41 0.63 19.08 -5 0 1 9.41 0.61 9.05 -3 0 1 8.04 0.55 5.73 -1 0 1 101.89 1.08 106.69 1 0 1 118.35 1.05 119.90 3 0 1 72.08 0.30 71.49 5 0 1 55.13 0.32 55.47 7 0 1 23.75 0.43 22.35 9 0 1 17.58 0.63 17.78 -9 1 1 7.64 1.19 6.99 -8 1 1 22.60 0.58 22.61 -7 1 1 11.41 0.76 12.43 -6 1 1 16.41 0.34 15.46 -4 1 1 60.88 0.40 58.92 -3 1 1 66.54 0.22 64.74 -2 1 1 95.25 0.70 95.55 -1 1 1 16.02 0.15 17.26 1 1 1 30.12 0.15 30.39 2 1 1 86.66 0.18 85.81 3 1 1 24.36 0.19 23.21 4 1 1 74.52 0.25 74.09 5 1 1 7.28 0.66 6.35 6 1 1 40.06 0.34 38.76 8 1 1 9.52 0.66 8.59 -9 2 1 17.20 0.63 17.22 -7 2 1 25.73 0.41 25.94 -6 2 1 9.52 0.74 8.86 -5 2 1 74.43 0.35 72.42 -4 2 1 23.52 0.29 23.96 -3 2 1 58.46 0.26 56.54 -1 2 1 6.01 0.38 3.99 0 2 1 43.66 0.14 43.94 1 2 1 83.92 0.20 84.30 2 2 1 8.40 0.44 8.04 3 2 1 43.19 0.25 43.82 4 2 1 59.20 0.30 57.76 5 2 1 56.84 0.32 56.78 6 2 1 22.93 0.41 24.19 7 2 1 23.17 0.43 22.92 9 2 1 19.85 0.59 19.50 -8 3 1 33.10 0.42 32.99 -6 3 1 51.69 0.33 52.29 -4 3 1 70.05 0.31 69.60 -2 3 1 32.59 0.22 33.64 -1 3 1 10.44 0.28 10.57 0 3 1 96.50 0.40 94.84 1 3 1 46.11 0.16 43.12 3 3 1 25.93 0.25 24.67 4 3 1 17.45 0.34 16.65 6 3 1 43.46 0.33 44.75 7 3 1 7.99 0.97 6.70 8 3 1 24.37 0.49 25.27 -9 4 1 18.90 0.58 18.95 -8 4 1 7.71 1.08 8.25 -7 4 1 31.70 0.39 32.18 -6 4 1 10.20 0.69 9.78 -5 4 1 60.75 0.33 60.53 -4 4 1 27.18 0.29 26.49 -3 4 1 84.49 0.33 85.25 -2 4 1 31.11 0.23 28.42 -1 4 1 63.58 0.79 64.20 0 4 1 18.97 0.16 19.32 1 4 1 86.14 1.26 87.83 3 4 1 14.80 0.33 16.38 4 4 1 12.99 0.41 12.18 5 4 1 23.92 0.34 23.11 7 4 1 11.84 0.66 11.18 9 4 1 20.63 0.58 21.15 -8 5 1 18.66 0.56 19.00 -6 5 1 16.32 0.46 16.07 -4 5 1 44.82 0.30 44.86 -3 5 1 9.13 0.48 8.07 -2 5 1 50.02 0.27 50.54 -1 5 1 39.58 0.42 36.76 0 5 1 95.61 0.37 95.96 1 5 1 26.35 0.23 26.68 2 5 1 51.76 0.27 52.44 4 5 1 33.38 0.28 33.42 6 5 1 23.72 0.40 23.49 7 5 1 13.06 0.63 13.51 8 5 1 16.34 0.62 16.54 -9 6 1 12.25 0.87 13.27 -7 6 1 19.81 0.46 19.05 -6 6 1 7.60 0.89 8.61 -5 6 1 30.21 0.33 29.91 -3 6 1 39.08 0.28 39.59 -2 6 1 15.93 0.32 15.44 -1 6 1 50.50 0.82 48.78 1 6 1 94.46 1.06 91.47 2 6 1 30.68 0.26 30.94 3 6 1 54.52 0.30 54.92 5 6 1 47.58 0.33 47.17 6 6 1 13.84 0.54 12.29 7 6 1 19.84 0.49 20.90 8 6 1 9.52 0.89 8.48 -8 7 1 12.78 0.72 11.55 -6 7 1 15.84 0.48 15.30 -4 7 1 37.05 0.31 36.83 -3 7 1 10.94 0.47 9.65 -2 7 1 48.39 0.28 47.79 -1 7 1 4.81 0.66 2.62 0 7 1 41.64 0.22 40.77 1 7 1 11.17 0.30 10.38 2 7 1 56.66 0.29 57.70 4 7 1 60.51 0.34 60.42 6 7 1 32.30 0.38 32.38 8 7 1 9.74 0.91 10.36 -7 8 1 17.89 0.52 18.02 -5 8 1 25.39 0.38 25.03 -4 8 1 18.62 0.41 18.29 -3 8 1 33.21 0.30 31.85 -2 8 1 10.15 0.47 9.16 -1 8 1 36.87 0.50 36.55 0 8 1 16.53 0.27 16.72 1 8 1 40.36 0.60 40.69 2 8 1 22.40 0.32 22.21 3 8 1 48.27 0.32 49.08 4 8 1 6.82 0.93 7.44 5 8 1 28.60 0.38 28.42 6 8 1 12.81 0.64 12.64 7 8 1 19.23 0.53 19.15 -7 9 1 8.95 1.02 9.43 -6 9 1 26.47 0.44 26.67 -4 9 1 20.32 0.39 19.55 -3 9 1 10.11 0.62 9.65 -2 9 1 31.32 0.31 31.21 0 9 1 48.57 0.21 48.37 1 9 1 12.36 0.49 12.43 2 9 1 29.99 0.31 31.23 4 9 1 12.86 0.53 13.78 5 9 1 6.45 1.02 4.74 6 9 1 22.87 0.46 21.95 -7 10 1 19.71 0.56 20.07 -5 10 1 33.61 0.39 33.03 -3 10 1 33.37 0.35 34.32 -2 10 1 8.52 0.68 8.31 -1 10 1 32.19 0.25 32.40 0 10 1 10.39 0.50 11.04 1 10 1 25.59 0.27 24.53 2 10 1 6.00 0.97 7.82 3 10 1 23.94 0.37 23.80 5 10 1 12.90 0.62 13.33 7 10 1 13.44 0.78 15.42 -6 11 1 22.94 0.50 22.19 -4 11 1 26.22 0.42 26.89 -3 11 1 9.66 0.67 7.21 -2 11 1 35.05 0.35 36.64 -1 11 1 9.40 0.47 8.70 0 11 1 14.82 0.34 14.25 2 11 1 20.10 0.41 20.26 4 11 1 19.97 0.45 20.78 6 11 1 13.38 0.73 14.75 -5 12 1 17.87 0.55 17.81 -3 12 1 20.13 0.45 20.18 -2 12 1 10.70 0.67 10.66 -1 12 1 33.78 0.27 34.73 0 12 1 7.27 0.65 6.08 1 12 1 22.65 0.30 22.65 3 12 1 22.00 0.43 22.81 5 12 1 14.30 0.63 13.36 -4 13 1 11.95 0.71 11.96 -2 13 1 27.12 0.42 26.98 0 13 1 21.57 0.34 21.99 1 13 1 9.45 0.79 8.53 2 13 1 30.47 0.41 29.46 4 13 1 19.39 0.54 19.19 -3 14 1 13.35 0.64 12.42 -1 14 1 18.02 0.39 17.61 1 14 1 17.08 0.40 16.85 3 14 1 24.99 0.50 25.12 0 15 1 15.04 0.45 14.68 -8 0 2 28.50 0.44 27.85 -6 0 2 39.53 0.33 40.42 -4 0 2 38.03 0.27 39.06 0 0 2 100.51 0.17 100.86 2 0 2 69.28 0.26 68.87 4 0 2 27.12 0.28 28.27 6 0 2 45.22 0.34 45.60 -9 1 2 21.51 0.74 21.77 -7 1 2 27.73 0.29 26.78 -6 1 2 11.31 0.45 10.09 -5 1 2 25.78 0.46 26.28 -4 1 2 7.42 0.49 8.20 -3 1 2 60.15 0.39 60.25 -2 1 2 46.98 0.17 45.16 -1 1 2 35.56 0.20 35.29 0 1 2 73.35 0.17 70.36 1 1 2 154.59 1.39 154.50 2 1 2 47.75 0.26 45.79 3 1 2 63.85 0.25 63.77 5 1 2 47.56 0.22 46.78 6 1 2 9.57 0.55 8.29 7 1 2 30.24 0.44 30.03 9 1 2 19.95 0.42 20.13 -8 2 2 24.71 0.47 25.74 -7 2 2 11.66 0.68 10.49 -6 2 2 30.22 0.34 29.88 -4 2 2 77.70 0.32 76.98 -3 2 2 36.23 0.24 33.05 -2 2 2 75.49 0.26 75.31 -1 2 2 42.09 0.26 40.96 0 2 2 50.77 0.68 50.50 1 2 2 155.11 2.26 154.57 2 2 2 36.83 0.23 37.71 4 2 2 51.23 0.29 50.84 5 2 2 9.15 0.68 7.74 6 2 2 42.18 0.34 41.83 8 2 2 11.37 0.82 11.17 -9 3 2 15.33 0.67 14.73 -8 3 2 7.14 1.14 6.23 -7 3 2 29.48 0.39 30.05 -6 3 2 13.17 0.55 13.13 -5 3 2 60.32 0.32 59.11 -4 3 2 17.61 0.35 17.54 -3 3 2 85.11 0.31 86.23 -2 3 2 5.14 0.72 4.34 -1 3 2 117.19 0.18 115.27 1 3 2 96.63 0.90 96.82 2 3 2 8.18 0.44 8.12 3 3 2 13.34 0.34 14.02 4 3 2 17.86 0.34 16.99 5 3 2 37.25 0.31 37.21 6 3 2 10.60 0.67 9.61 7 3 2 23.12 0.44 23.41 9 3 2 13.58 0.76 11.76 -9 4 2 7.47 1.21 6.07 -8 4 2 19.49 0.53 20.02 -6 4 2 7.82 0.85 6.62 -5 4 2 10.10 0.60 9.75 -4 4 2 84.51 0.34 82.59 -3 4 2 6.09 0.69 3.80 -2 4 2 89.32 0.30 90.33 -1 4 2 46.04 0.17 44.59 0 4 2 52.22 0.27 53.38 1 4 2 24.87 0.29 25.51 2 4 2 67.39 0.28 66.13 3 4 2 10.96 0.41 10.37 4 4 2 31.69 0.30 32.07 5 4 2 13.45 0.48 12.92 6 4 2 22.49 0.41 21.21 8 4 2 18.17 0.59 19.41 -9 5 2 14.90 0.67 14.48 -7 5 2 26.66 0.42 26.15 -5 5 2 46.45 0.32 45.10 -4 5 2 24.08 0.31 23.87 -3 5 2 40.21 0.27 40.02 -2 5 2 37.19 0.25 36.21 -1 5 2 90.67 0.22 91.91 0 5 2 21.51 0.17 22.00 1 5 2 80.56 0.77 78.10 2 5 2 5.87 0.68 3.25 3 5 2 22.43 0.29 23.37 4 5 2 10.56 0.53 10.21 5 5 2 31.50 0.33 30.24 6 5 2 14.80 0.52 15.83 7 5 2 13.26 0.63 12.93 -8 6 2 20.08 0.53 19.62 -7 6 2 8.68 0.88 7.13 -6 6 2 27.64 0.38 27.18 -5 6 2 10.28 0.61 10.99 -4 6 2 42.58 0.30 40.49 -3 6 2 25.69 0.29 24.54 -2 6 2 33.73 0.25 33.89 -1 6 2 16.61 0.23 16.86 0 6 2 74.26 0.39 75.22 1 6 2 40.72 0.43 41.58 2 6 2 55.83 0.29 56.74 3 6 2 9.72 0.53 9.61 4 6 2 50.00 0.32 49.57 6 6 2 34.02 0.37 34.21 8 6 2 14.78 0.67 14.70 -7 7 2 23.79 0.45 24.10 -5 7 2 31.02 0.34 30.79 -4 7 2 8.64 0.64 7.44 -3 7 2 13.17 0.43 13.19 -1 7 2 6.32 0.50 7.49 0 7 2 9.29 0.32 8.42 1 7 2 53.27 0.54 52.58 3 7 2 57.77 0.32 58.86 4 7 2 12.55 0.52 13.02 5 7 2 40.95 0.34 42.26 7 7 2 24.48 0.47 23.85 -8 8 2 16.61 0.65 16.61 -6 8 2 29.33 0.39 29.14 -5 8 2 11.78 0.58 11.67 -4 8 2 24.16 0.36 24.20 -3 8 2 7.19 0.76 7.55 -2 8 2 30.02 0.29 30.71 -1 8 2 9.28 0.38 9.83 0 8 2 42.39 0.25 42.16 1 8 2 27.11 0.56 27.20 2 8 2 33.27 0.29 33.24 3 8 2 13.10 0.49 13.30 4 8 2 39.20 0.33 39.70 6 8 2 27.86 0.42 28.34 -7 9 2 19.13 0.53 18.89 -6 9 2 10.50 0.72 9.86 -5 9 2 20.28 0.44 20.98 -4 9 2 8.05 0.79 7.15 -3 9 2 36.85 0.32 36.85 -1 9 2 44.36 0.25 44.63 0 9 2 18.83 0.37 19.12 1 9 2 32.86 0.24 32.54 2 9 2 13.65 0.44 13.48 3 9 2 22.85 0.36 22.61 5 9 2 13.19 0.56 11.87 7 9 2 18.19 0.56 18.45 -6 10 2 22.21 0.48 23.13 -4 10 2 27.48 0.38 28.51 -2 10 2 48.95 0.33 48.29 -1 10 2 5.45 0.79 3.74 0 10 2 38.96 0.31 39.29 1 10 2 6.84 1.07 6.52 2 10 2 19.40 0.40 18.76 4 10 2 21.02 0.43 21.92 6 10 2 13.33 0.66 13.84 -5 11 2 24.79 0.46 25.45 -3 11 2 38.99 0.36 39.12 -1 11 2 39.19 0.39 40.35 0 11 2 9.10 0.54 10.21 1 11 2 24.88 0.27 25.76 3 11 2 26.18 0.40 26.61 5 11 2 12.34 0.64 11.48 -6 12 2 14.86 0.68 14.68 -4 12 2 19.27 0.49 18.59 -2 12 2 27.79 0.39 27.86 -1 12 2 17.75 0.39 18.41 0 12 2 25.20 0.30 25.16 2 12 2 24.57 0.41 26.14 3 12 2 7.95 0.87 7.32 4 12 2 17.58 0.53 17.54 -5 13 2 14.31 0.68 14.02 -3 13 2 7.16 1.10 7.83 -1 13 2 22.65 0.32 22.54 1 13 2 19.39 0.35 19.30 2 13 2 6.78 1.10 7.81 3 13 2 22.71 0.49 23.70 -2 14 2 13.53 0.62 13.57 0 14 2 9.86 0.60 8.95 2 14 2 19.74 0.52 20.19 -1 15 2 13.99 0.73 14.05 1 15 2 8.70 0.72 9.88 -9 0 3 22.19 0.53 21.58 -7 0 3 37.72 0.36 37.56 -5 0 3 48.64 0.31 48.74 -3 0 3 109.16 0.30 112.16 -1 0 3 113.08 0.63 111.62 1 0 3 140.85 1.42 136.97 3 0 3 23.16 0.27 22.25 5 0 3 45.65 0.31 45.56 7 0 3 39.12 0.38 38.84 9 0 3 15.56 0.70 15.10 -8 1 3 29.06 0.34 29.35 -6 1 3 38.82 0.27 38.82 -4 1 3 87.56 0.25 85.35 -3 1 3 4.62 0.75 3.93 -2 1 3 62.43 0.41 64.39 -1 1 3 23.45 0.22 21.66 0 1 3 50.13 0.13 47.70 1 1 3 4.39 0.45 3.48 2 1 3 53.11 0.22 51.09 3 1 3 24.26 0.19 24.28 4 1 3 29.99 0.39 30.76 5 1 3 13.69 0.36 13.39 6 1 3 31.65 0.29 31.90 7 1 3 6.86 0.90 4.83 8 1 3 15.31 0.45 14.31 -9 2 3 21.50 0.54 21.47 -7 2 3 32.66 0.38 32.04 -6 2 3 18.64 0.44 19.55 -5 2 3 38.02 0.30 39.08 -4 2 3 12.52 0.42 11.89 -3 2 3 74.03 0.32 74.24 -2 2 3 33.05 0.23 32.55 -1 2 3 60.43 0.43 62.23 0 2 3 46.79 0.68 47.62 1 2 3 111.58 1.44 109.96 2 2 3 12.46 0.33 12.29 3 2 3 51.15 0.28 53.44 4 2 3 20.79 0.33 22.62 5 2 3 46.21 0.31 46.73 6 2 3 12.40 0.64 12.49 7 2 3 30.03 0.40 29.34 9 2 3 10.19 1.03 11.01 -8 3 3 16.49 0.57 15.95 -6 3 3 19.27 0.44 19.25 -4 3 3 48.18 0.28 48.41 -3 3 3 12.96 0.36 12.71 -2 3 3 35.52 0.24 35.14 -1 3 3 14.68 0.59 16.17 0 3 3 58.83 0.20 60.09 1 3 3 15.86 0.41 14.74 2 3 3 125.95 0.29 125.53 3 3 3 14.80 0.34 15.97 4 3 3 44.75 0.28 45.60 6 3 3 40.04 0.35 39.89 8 3 3 12.73 0.75 12.81 -9 4 3 16.19 0.68 16.84 -7 4 3 27.21 0.40 26.34 -5 4 3 37.18 0.31 36.99 -3 4 3 43.74 0.26 42.59 -2 4 3 9.61 0.42 8.84 -1 4 3 84.03 0.21 82.59 0 4 3 15.64 0.20 13.93 1 4 3 110.84 1.36 109.58 3 4 3 44.66 0.27 46.46 5 4 3 32.00 0.33 32.06 7 4 3 16.42 0.55 16.54 -8 5 3 15.66 0.63 16.51 -7 5 3 9.00 0.88 10.60 -6 5 3 26.36 0.38 26.66 -4 5 3 49.37 0.30 49.23 -3 5 3 13.86 0.37 13.63 -2 5 3 71.49 0.31 71.59 -1 5 3 16.96 0.32 17.77 0 5 3 58.37 0.19 58.32 2 5 3 78.60 0.33 80.92 3 5 3 28.88 0.28 27.97 4 5 3 37.33 0.30 37.09 5 5 3 16.87 0.44 16.46 6 5 3 26.62 0.40 27.87 8 5 3 12.88 0.76 13.03 -9 6 3 15.62 0.70 16.21 -7 6 3 23.60 0.45 23.98 -5 6 3 25.37 0.35 24.76 -4 6 3 13.94 0.45 13.89 -3 6 3 49.62 0.29 49.06 -2 6 3 21.81 0.29 21.39 -1 6 3 45.90 0.22 45.95 0 6 3 12.25 0.30 12.44 1 6 3 21.01 0.56 22.37 3 6 3 26.56 0.29 26.38 4 6 3 16.80 0.42 16.19 5 6 3 24.10 0.39 25.26 7 6 3 23.44 0.46 22.34 -8 7 3 22.40 0.49 22.02 -6 7 3 37.72 0.36 36.65 -5 7 3 8.65 0.73 6.84 -4 7 3 44.20 0.31 43.62 -3 7 3 16.65 0.37 16.88 -2 7 3 49.80 0.29 49.83 -1 7 3 24.03 0.34 22.69 0 7 3 30.11 0.19 30.50 1 7 3 11.65 0.54 11.53 2 7 3 17.92 0.34 17.75 3 7 3 6.46 0.83 6.61 4 7 3 25.76 0.35 26.03 5 7 3 6.69 0.99 5.29 6 7 3 24.75 0.43 24.63 8 7 3 16.42 0.65 15.43 -7 8 3 21.67 0.49 21.24 -6 8 3 7.93 0.98 7.74 -5 8 3 27.80 0.38 28.03 -3 8 3 31.55 0.31 30.62 -1 8 3 28.58 0.43 27.71 0 8 3 22.15 0.69 22.37 1 8 3 25.69 0.86 25.01 3 8 3 23.70 0.35 23.87 4 8 3 6.25 0.98 4.98 5 8 3 27.32 0.38 27.04 7 8 3 21.86 0.52 21.77 -6 9 3 24.24 0.44 24.39 -5 9 3 9.50 0.75 9.31 -4 9 3 34.25 0.34 33.45 -2 9 3 32.53 0.31 32.12 -1 9 3 20.75 0.38 20.46 0 9 3 33.06 0.29 32.81 1 9 3 8.39 0.49 8.62 2 9 3 33.96 0.31 33.62 3 9 3 11.82 0.55 12.21 4 9 3 32.76 0.35 33.04 5 9 3 7.93 0.94 7.22 6 9 3 17.18 0.56 17.37 -7 10 3 13.54 0.71 13.79 -6 10 3 8.18 0.93 6.54 -5 10 3 23.00 0.45 22.62 -3 10 3 25.93 0.36 25.56 -2 10 3 7.66 0.74 7.53 -1 10 3 38.35 0.46 38.48 0 10 3 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