#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2006097.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2006097_Fobs loop_ _publ_author_name 'Elerman, Y.' 'Geselle, M.' _publ_section_title ; Bis[N-(4-bromophenyl)salicylaldimine]copper(II) ; _journal_issue 5 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 549 _journal_page_last 551 _journal_volume 53 _journal_year 1997 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _exptl_crystal_F_000 606.00 _[local]_cod_data_source_file cf1096sup2.hkl _[local]_cod_data_source_block CF1096 #BEGIN Tags that were not found in dictionaries: _shelx_title ' ' _shelx_refln_list_code 4 _shelx_f_calc_maximum 200.80 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 2397.58 2555.75 99.13 o 2 0 0 15135.84 16528.33 68.96 o 3 0 0 3685.78 4766.71 47.41 o 4 0 0 11779.46 13308.86 77.58 o 5 0 0 672.92 879.21 25.86 o 6 0 0 2128.07 2241.13 38.79 o 7 0 0 3914.31 5361.47 56.03 o 8 0 0 2483.07 2810.03 43.10 o 9 0 0 936.05 918.00 25.86 o 10 0 0 417.67 435.30 12.93 o 11 0 0 624.25 568.90 17.24 o 12 0 0 41.50 77.58 12.93 o 13 0 0 783.95 784.40 25.86 o 14 0 0 149.74 146.54 12.93 o 15 0 0 566.82 642.17 21.55 o 1 1 0 59.02 73.27 43.10 o 2 1 0 243.24 275.83 8.62 o 3 1 0 1494.90 1439.49 21.55 o 4 1 0 3617.93 3465.13 34.48 o 5 1 0 3852.48 3792.68 38.79 o 6 1 0 3672.02 3460.82 43.10 o 7 1 0 4488.06 4590.00 51.72 o 8 1 0 985.12 900.76 25.86 o 9 1 0 2816.93 2766.93 43.10 o 10 1 0 1428.29 1491.21 38.79 o 11 1 0 1125.56 1124.87 30.17 o 12 1 0 826.27 866.28 25.86 o 13 1 0 248.23 267.21 12.93 o 14 1 0 234.28 228.42 12.93 o 0 2 0 9603.82 11903.84 34.48 o 1 2 0 12615.12 12382.24 241.35 o 2 2 0 299.74 418.06 12.93 o 3 2 0 2742.89 2460.93 21.55 o 4 2 0 87.13 120.68 4.31 o 5 2 0 1383.69 1077.47 21.55 o 6 2 0 56.03 51.72 8.62 o 7 2 0 557.40 448.23 12.93 o 8 2 0 1042.26 1030.06 25.86 o 9 2 0 1753.56 1581.72 38.79 o 10 2 0 1135.28 1163.66 30.17 o 11 2 0 876.45 900.76 30.17 o 12 2 0 151.94 142.23 12.93 o 13 2 0 7.54 25.86 30.17 o 14 2 0 103.57 103.44 12.93 o 1 3 0 564.90 624.93 8.62 o 2 3 0 1558.25 1754.11 21.55 o 3 3 0 1736.03 1810.14 21.55 o 4 3 0 957.44 982.65 17.24 o 5 3 0 840.69 1008.51 21.55 o 6 3 0 277.90 323.24 8.62 o 7 3 0 754.63 844.73 25.86 o 8 3 0 489.75 568.90 17.24 o 9 3 0 1443.63 1530.00 34.48 o 10 3 0 126.99 68.96 12.93 o 11 3 0 155.73 172.39 12.93 o 12 3 0 194.02 249.97 12.93 o 13 3 0 31.07 47.41 12.93 o 14 3 0 43.32 21.55 34.48 o 0 4 0 161.40 202.56 4.31 o 1 4 0 6213.13 6391.53 47.41 o 2 4 0 1836.31 2034.26 43.10 o 3 4 0 6857.77 7081.11 43.10 o 4 4 0 145.46 168.08 4.31 o 5 4 0 1758.01 1598.96 25.86 o 6 4 0 162.43 155.16 8.62 o 7 4 0 1910.98 1995.47 30.17 o 8 4 0 923.58 956.79 25.86 o 9 4 0 2221.58 2193.72 38.79 o 10 4 0 394.01 340.48 12.93 o 11 4 0 293.31 228.42 12.93 o 12 4 0 809.78 711.13 21.55 o 13 4 0 6.56 12.93 12.93 o 14 4 0 310.07 310.31 17.24 o 1 5 0 265.28 262.90 4.31 o 2 5 0 11.44 12.93 4.31 o 3 5 0 1105.08 1142.11 21.55 o 4 5 0 18.80 -17.24 17.24 < 5 5 0 568.12 555.97 17.24 o 6 5 0 869.42 849.04 21.55 o 7 5 0 851.90 857.66 21.55 o 8 5 0 1024.43 986.96 30.17 o 9 5 0 245.16 224.11 8.62 o 10 5 0 746.97 719.75 21.55 o 11 5 0 62.80 68.96 12.93 o 12 5 0 151.05 124.99 12.93 o 13 5 0 221.21 193.94 12.93 o 0 6 0 2431.76 2542.82 30.17 o 1 6 0 64.06 51.72 4.31 o 2 6 0 1724.40 1771.35 17.24 o 3 6 0 140.05 146.54 8.62 o 4 6 0 1166.39 1155.04 25.86 o 5 6 0 49.85 0.00 17.24 x 6 6 0 1031.88 969.72 25.86 o 7 6 0 413.64 413.75 12.93 o 8 6 0 1002.41 948.17 25.86 o 9 6 0 145.32 142.23 8.62 o 10 6 0 44.21 43.10 8.62 o 11 6 0 150.93 163.77 12.93 o 12 6 0 156.40 120.68 12.93 o 1 7 0 133.28 137.92 4.31 o 2 7 0 111.63 107.75 4.31 o 3 7 0 37.82 64.65 8.62 o 4 7 0 29.01 47.41 8.62 o 5 7 0 43.70 34.48 8.62 o 6 7 0 15.31 17.24 8.62 o 7 7 0 55.89 56.03 8.62 o 8 7 0 12.74 17.24 21.55 o 9 7 0 17.10 12.93 21.55 o 10 7 0 10.07 17.24 8.62 o 11 7 0 3.32 -12.93 25.86 < 12 7 0 6.91 21.55 30.17 o 0 8 0 634.51 534.42 17.24 o 1 8 0 61.68 81.89 4.31 o 2 8 0 583.44 487.01 8.62 o 3 8 0 731.97 892.14 25.86 o 4 8 0 831.85 771.47 21.55 o 5 8 0 393.79 405.13 12.93 o 6 8 0 379.13 297.38 12.93 o 7 8 0 169.01 206.87 12.93 o 8 8 0 215.73 206.87 12.93 o 9 8 0 87.22 112.06 12.93 o 10 8 0 16.73 21.55 12.93 o 1 9 0 55.45 56.03 8.62 o 2 9 0 5.54 -25.86 17.24 < 3 9 0 30.34 21.55 21.55 o 4 9 0 60.76 64.65 8.62 o 5 9 0 28.29 21.55 21.55 o 6 9 0 0.11 8.62 21.55 o 7 9 0 5.96 -4.31 8.62 < 8 9 0 48.37 47.41 12.93 o 9 9 0 4.65 -8.62 12.93 < 0 10 0 424.40 383.58 12.93 o 1 10 0 256.84 288.76 12.93 o 2 10 0 37.97 21.55 12.93 o 3 10 0 312.54 288.76 12.93 o 4 10 0 314.78 301.69 12.93 o 5 10 0 284.99 297.38 12.93 o 6 10 0 58.14 56.03 12.93 o 7 10 0 34.84 56.03 12.93 o 1 11 0 0.11 -8.62 17.24 < 2 11 0 6.07 17.24 12.93 o 3 11 0 0.75 -25.86 25.86 < 4 11 0 0.18 12.93 12.93 o 5 11 0 3.68 -43.10 25.86 < -15 1 1 6.72 -64.65 30.17 < -14 1 1 278.49 297.38 12.93 o -13 1 1 5.80 -17.24 30.17 < -12 1 1 1339.62 1452.42 38.79 o -11 1 1 44.41 56.03 12.93 o -10 1 1 2145.24 2245.44 43.10 o -9 1 1 5.14 21.55 21.55 o -8 1 1 7056.64 6710.46 60.34 o -7 1 1 202.10 224.11 8.62 o -6 1 1 10170.55 10804.83 64.65 o -5 1 1 857.25 1107.63 21.55 o -4 1 1 5852.86 5473.53 34.48 o -3 1 1 18.53 21.55 4.31 o -2 1 1 2099.29 2090.28 17.24 o -1 1 1 586.58 719.75 21.55 o 0 1 1 6583.33 7175.92 17.24 o 1 1 1 61.71 47.41 43.10 o 2 1 1 7643.65 8274.94 56.03 o 3 1 1 4228.04 4727.92 51.72 o 4 1 1 4.85 25.86 8.62 o 5 1 1 2930.19 3516.85 47.41 o 6 1 1 364.76 590.45 17.24 o 7 1 1 3249.96 3762.51 51.72 o 8 1 1 41.97 38.79 8.62 o 9 1 1 3441.16 4128.85 56.03 o 10 1 1 243.13 245.66 12.93 o 11 1 1 4028.41 4602.93 60.34 o 12 1 1 19.39 -17.24 30.17 < 13 1 1 495.03 577.52 17.24 o 14 1 1 35.73 30.17 12.93 o -14 2 1 726.68 724.06 17.24 o -13 2 1 387.19 405.13 12.93 o -12 2 1 570.70 521.49 12.93 o -11 2 1 272.21 237.04 12.93 o -10 2 1 150.70 107.75 12.93 o -9 2 1 122.71 94.82 8.62 o -8 2 1 60.77 43.10 8.62 o -7 2 1 959.44 1245.55 25.86 o -6 2 1 143.65 155.16 8.62 o -5 2 1 735.74 974.03 21.55 o -4 2 1 2198.17 2361.81 25.86 o -3 2 1 4651.64 5128.74 30.17 o -2 2 1 1967.08 2193.72 21.55 o -1 2 1 10857.41 12071.93 150.85 o 0 2 1 40320.14 42913.31 181.01 o 1 2 1 138.85 185.32 17.24 o 2 2 1 16081.82 17170.50 51.72 o 3 2 1 5237.55 5305.44 34.48 o 4 2 1 5516.93 5788.15 43.10 o 5 2 1 2092.96 1995.47 34.48 o 6 2 1 2413.38 2404.90 38.79 o 7 2 1 4098.90 4357.27 56.03 o 8 2 1 468.27 443.92 12.93 o 9 2 1 597.95 646.48 17.24 o 10 2 1 170.54 193.94 12.93 o 11 2 1 81.98 86.20 12.93 o 12 2 1 67.87 94.82 12.93 o 13 2 1 8.94 12.93 30.17 o 14 2 1 55.03 86.20 12.93 o -14 3 1 1.35 4.31 30.17 o -13 3 1 719.45 728.37 21.55 o -12 3 1 6.15 -21.55 25.86 < -11 3 1 1174.61 986.96 30.17 o -10 3 1 584.34 538.73 21.55 o -9 3 1 4646.98 4249.53 47.41 o -8 3 1 163.49 137.92 8.62 o -7 3 1 6712.48 6098.46 47.41 o -6 3 1 705.54 719.75 21.55 o -5 3 1 6495.81 6223.44 43.10 o -4 3 1 376.75 336.17 8.62 o -3 3 1 6144.19 6137.25 34.48 o -2 3 1 979.50 909.38 17.24 o -1 3 1 9978.86 10356.60 99.13 o 0 3 1 7859.21 8942.97 288.76 o 1 3 1 17639.12 18795.31 47.41 o 2 3 1 5270.27 5439.05 34.48 o 3 3 1 2856.94 2926.40 25.86 o 4 3 1 1461.69 1236.93 21.55 o 5 3 1 0.09 4.31 17.24 o 6 3 1 2193.12 1930.82 30.17 o 7 3 1 329.18 310.31 8.62 o 8 3 1 2044.32 1525.69 34.48 o 9 3 1 332.23 262.90 12.93 o 10 3 1 1645.67 1521.38 43.10 o 11 3 1 3.22 0.00 25.86 x 12 3 1 1356.50 1452.42 38.79 o 13 3 1 34.44 34.48 12.93 o 14 3 1 543.98 624.93 21.55 o -14 4 1 53.50 38.79 12.93 o -13 4 1 138.75 116.37 12.93 o -12 4 1 40.33 38.79 12.93 o -11 4 1 68.08 17.24 25.86 o -10 4 1 173.06 155.16 12.93 o -9 4 1 2.00 0.00 21.55 x -8 4 1 71.58 77.58 8.62 o -7 4 1 19.34 4.31 17.24 o -6 4 1 0.44 -30.17 17.24 < -5 4 1 47.84 51.72 4.31 o -4 4 1 562.95 551.66 17.24 o -3 4 1 2.77 0.00 12.93 x -2 4 1 79.37 60.34 4.31 o -1 4 1 2209.77 2098.90 30.17 o 0 4 1 10.09 30.17 4.31 o 1 4 1 2662.93 2697.97 21.55 o 2 4 1 439.40 366.34 8.62 o 3 4 1 24.27 0.00 12.93 x 4 4 1 1179.87 1142.11 21.55 o 5 4 1 803.78 805.94 21.55 o 6 4 1 423.27 336.17 12.93 o 7 4 1 6.47 8.62 17.24 o 8 4 1 1093.16 930.93 25.86 o 9 4 1 8.37 -38.79 21.55 < 10 4 1 6.47 0.00 12.93 x 11 4 1 259.97 224.11 12.93 o 12 4 1 39.22 25.86 30.17 o 13 4 1 1.35 -8.62 34.48 < -13 5 1 114.30 112.06 12.93 o -12 5 1 22.68 -38.79 30.17 < -11 5 1 2.33 0.00 25.86 x -10 5 1 342.28 314.62 12.93 o -9 5 1 2490.20 2439.38 38.79 o -8 5 1 563.78 525.80 17.24 o -7 5 1 747.58 741.30 21.55 o -6 5 1 228.23 193.94 8.62 o -5 5 1 1228.37 1146.42 25.86 o -4 5 1 1947.55 2142.00 30.17 o -3 5 1 326.02 318.93 8.62 o -2 5 1 6.87 0.00 8.62 x -1 5 1 1320.31 1301.58 17.24 o 0 5 1 2438.74 2413.52 47.41 o 1 5 1 648.47 599.07 12.93 o 2 5 1 3472.79 3529.78 99.13 o 3 5 1 4186.57 4344.34 38.79 o 4 5 1 2184.62 2047.19 30.17 o 5 5 1 158.70 133.61 8.62 o 6 5 1 558.01 530.11 12.93 o 7 5 1 34.72 0.00 21.55 x 8 5 1 991.85 1008.51 25.86 o 9 5 1 0.56 0.00 21.55 x 10 5 1 19.52 8.62 8.62 o 11 5 1 271.19 215.49 12.93 o 12 5 1 245.37 206.87 12.93 o 13 5 1 9.56 0.00 30.17 x -13 6 1 27.54 25.86 12.93 o -12 6 1 29.09 8.62 12.93 o -11 6 1 0.68 -38.79 25.86 < -10 6 1 112.64 107.75 12.93 o -9 6 1 319.98 310.31 12.93 o -8 6 1 111.23 124.99 8.62 o -7 6 1 12.07 -21.55 21.55 < -6 6 1 20.12 25.86 8.62 o -5 6 1 72.58 51.72 8.62 o -4 6 1 338.17 331.86 8.62 o -3 6 1 65.33 77.58 8.62 o -2 6 1 2320.77 2288.54 21.55 o -1 6 1 54.67 34.48 4.31 o 0 6 1 500.48 435.30 8.62 o 1 6 1 261.40 241.35 4.31 o 2 6 1 604.76 586.14 12.93 o 3 6 1 432.05 374.96 12.93 o 4 6 1 102.97 112.06 8.62 o 5 6 1 32.28 12.93 17.24 o 6 6 1 133.36 120.68 8.62 o 7 6 1 14.98 8.62 8.62 o 8 6 1 33.66 34.48 8.62 o 9 6 1 105.24 86.20 8.62 o 10 6 1 15.54 0.00 25.86 x 11 6 1 11.38 -8.62 25.86 < 12 6 1 11.13 -38.79 30.17 < -12 7 1 134.19 129.30 12.93 o -11 7 1 5.36 4.31 25.86 o -10 7 1 263.02 267.21 12.93 o -9 7 1 128.48 124.99 8.62 o -8 7 1 1375.32 1288.65 34.48 o -7 7 1 56.34 73.27 8.62 o -6 7 1 1021.58 1055.92 30.17 o -5 7 1 54.64 56.03 8.62 o -4 7 1 1081.33 1172.28 25.86 o -3 7 1 160.32 150.85 8.62 o -2 7 1 420.65 392.20 12.93 o -1 7 1 24.35 4.31 12.93 o 0 7 1 882.74 892.14 17.24 o 1 7 1 570.66 538.73 8.62 o 2 7 1 953.50 926.62 21.55 o 3 7 1 833.51 840.42 25.86 o 4 7 1 373.55 357.72 8.62 o 5 7 1 683.99 698.20 21.55 o 6 7 1 118.48 116.37 8.62 o 7 7 1 661.36 650.79 21.55 o 8 7 1 22.06 8.62 8.62 o 9 7 1 258.12 280.14 12.93 o 10 7 1 10.26 -8.62 25.86 < 11 7 1 268.48 293.07 12.93 o -11 8 1 16.91 12.93 25.86 o -10 8 1 33.09 17.24 25.86 o -9 8 1 28.58 30.17 8.62 o -8 8 1 16.65 8.62 25.86 o -7 8 1 58.71 51.72 8.62 o -6 8 1 75.79 73.27 8.62 o -5 8 1 14.98 17.24 21.55 o -4 8 1 8.73 21.55 8.62 o -3 8 1 267.86 306.00 8.62 o -2 8 1 0.74 8.62 17.24 o -1 8 1 170.03 181.01 4.31 o 0 8 1 111.91 77.58 8.62 o 1 8 1 204.21 237.04 8.62 o 2 8 1 135.28 176.70 8.62 o 3 8 1 12.26 17.24 21.55 o 4 8 1 23.40 25.86 8.62 o 5 8 1 78.61 81.89 8.62 o 6 8 1 35.40 34.48 8.62 o 7 8 1 0.68 -12.93 8.62 < 8 8 1 31.74 17.24 25.86 o 9 8 1 33.48 43.10 12.93 o 10 8 1 0.43 17.24 25.86 o -9 9 1 87.84 120.68 12.93 o -8 9 1 31.70 30.17 12.93 o -7 9 1 160.52 189.63 12.93 o -6 9 1 264.07 202.56 12.93 o -5 9 1 161.00 224.11 12.93 o -4 9 1 71.58 43.10 8.62 o -3 9 1 115.85 150.85 8.62 o -2 9 1 63.46 51.72 8.62 o -1 9 1 601.59 663.72 12.93 o 0 9 1 255.58 241.35 12.93 o 1 9 1 45.26 38.79 8.62 o 2 9 1 147.82 163.77 17.24 o 3 9 1 220.29 219.80 8.62 o 4 9 1 72.44 90.51 8.62 o 5 9 1 190.45 172.39 8.62 o 6 9 1 129.05 150.85 12.93 o 7 9 1 186.77 168.08 12.93 o 8 9 1 207.42 245.66 12.93 o 9 9 1 53.72 51.72 12.93 o -7 10 1 5.03 8.62 25.86 o -6 10 1 20.38 8.62 12.93 o -5 10 1 20.88 12.93 25.86 o -4 10 1 11.47 17.24 25.86 o -3 10 1 30.89 47.41 8.62 o -2 10 1 31.69 4.31 17.24 o -1 10 1 0.80 8.62 12.93 o 0 10 1 11.76 12.93 12.93 o 1 10 1 17.32 -4.31 25.86 < 2 10 1 14.33 17.24 8.62 o 3 10 1 0.17 17.24 21.55 o 4 10 1 0.40 -38.79 25.86 < 5 10 1 3.97 0.00 25.86 x 6 10 1 7.45 21.55 25.86 o 7 10 1 9.66 -25.86 25.86 < -5 11 1 91.44 73.27 12.93 o -4 11 1 54.64 47.41 12.93 o -3 11 1 90.24 94.82 12.93 o -2 11 1 144.80 172.39 8.62 o -1 11 1 148.12 133.61 8.62 o 0 11 1 33.75 25.86 12.93 o 1 11 1 0.74 8.62 17.24 o 2 11 1 2.23 -12.93 17.24 < 3 11 1 73.60 60.34 12.93 o 4 11 1 150.13 176.70 12.93 o -15 0 2 284.67 318.93 12.93 o -14 0 2 1767.91 1745.49 43.10 o -13 0 2 92.58 107.75 12.93 o -12 0 2 2376.27 2335.95 47.41 o -11 0 2 286.28 262.90 12.93 o -10 0 2 2725.63 2551.44 47.41 o -9 0 2 181.01 159.46 8.62 o -8 0 2 1693.27 1176.59 34.48 o -7 0 2 1675.67 2012.71 38.79 o -6 0 2 9969.38 9516.18 60.34 o -5 0 2 3026.40 3547.02 34.48 o -4 0 2 688.59 517.18 12.93 o -3 0 2 1091.48 1284.34 17.24 o -2 0 2 47.98 77.58 4.31 o -1 0 2 32442.77 33591.08 374.96 o 0 0 2 14634.53 16433.51 198.25 o 1 0 2 4456.57 4943.41 176.70 o 2 0 2 519.55 521.49 12.93 o 3 0 2 23573.76 22493.18 68.96 o 4 0 2 77.79 77.58 4.31 o 5 0 2 8573.10 7917.22 51.72 o 6 0 2 2151.11 2055.80 34.48 o 7 0 2 10521.14 9369.64 68.96 o 8 0 2 153.35 107.75 8.62 o 9 0 2 1013.42 749.92 21.55 o 10 0 2 337.23 331.86 12.93 o 11 0 2 733.12 724.06 21.55 o 12 0 2 33.54 73.27 12.93 o 13 0 2 413.33 383.58 17.24 o 14 0 2 234.90 288.76 12.93 o -15 1 2 2.79 21.55 30.17 o -14 1 2 22.65 34.48 12.93 o -13 1 2 4.65 25.86 30.17 o -12 1 2 85.51 112.06 12.93 o -11 1 2 526.74 555.97 17.24 o -10 1 2 839.08 818.87 21.55 o -9 1 2 1254.17 1215.38 34.48 o -8 1 2 1585.36 1590.34 34.48 o -7 1 2 1597.49 1512.76 30.17 o -6 1 2 8122.19 8124.09 51.72 o -5 1 2 2802.01 2758.31 30.17 o -4 1 2 3309.52 3197.92 30.17 o -3 1 2 4958.13 5003.75 30.17 o -2 1 2 4435.72 4387.44 25.86 o -1 1 2 187.60 137.92 43.10 o 0 1 2 2193.37 2012.71 21.55 o 1 1 2 16971.34 17110.16 185.32 o 2 1 2 25.64 8.62 12.93 o 3 1 2 1295.91 1258.48 25.86 o 4 1 2 237.40 249.97 8.62 o 5 1 2 0.60 0.00 21.55 x 6 1 2 257.00 310.31 8.62 o 7 1 2 282.64 357.72 12.93 o 8 1 2 61.70 73.27 12.93 o 9 1 2 382.28 495.63 12.93 o 10 1 2 149.62 185.32 12.93 o 11 1 2 936.93 1077.47 30.17 o 12 1 2 53.98 60.34 12.93 o 13 1 2 203.26 241.35 12.93 o 14 1 2 225.83 245.66 12.93 o -14 2 2 0.60 -51.72 34.48 < -13 2 2 392.30 340.48 12.93 o -12 2 2 117.93 116.37 12.93 o -11 2 2 224.08 189.63 12.93 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