#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2006275.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2006275_Fobs loop_ _publ_author_name 'Mague, J. T.' 'Vang, S.' 'Berge, D. G.' 'Wacholtz, W. F.' _publ_section_title ; Isomerism/Tautomerism in Hydrazones Derived from Thiophenaldehydes and 2-Hydrazinoquinoline ; _journal_issue 7 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 973 _journal_page_last 979 _journal_volume 53 _journal_year 1997 _[local]_cod_data_source_file bk13144sup5.hkl _[local]_cod_data_source_block 4 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_meas _refln_F_calc _refln_F_sigma _refln_phase_calc _refln_observed_status 0 2 0 163.13 157.51 0.60 0.10 o 0 4 0 143.23 137.33 0.87 180.15 o 0 6 0 20.87 18.63 0.34 178.91 o 0 8 0 12.19 12.91 0.25 180.98 o 0 10 0 44.35 46.27 0.44 180.84 o 0 12 0 3.68 4.43 0.38 181.39 o 0 13 1 9.14 8.75 0.23 -89.40 o 0 12 1 5.82 5.20 0.28 3.27 o 0 11 1 7.32 7.26 0.22 -89.60 o 0 10 1 9.81 10.53 0.24 179.94 o 0 9 1 4.38 4.58 0.29 91.30 o 0 8 1 54.15 54.22 0.38 180.72 o 0 7 1 20.58 21.63 0.37 90.65 o 0 6 1 55.40 53.76 0.32 180.14 o 0 5 1 12.80 12.71 0.24 91.09 o 0 4 1 21.11 20.88 0.27 179.96 o 0 3 1 32.04 31.00 0.23 269.60 o 0 2 1 9.64 9.18 0.18 -5.45 o 0 1 1 33.50 33.09 0.14 269.81 o 0 0 2 17.28 16.27 0.13 -3.03 o 0 1 2 27.63 27.69 0.15 91.11 o 0 2 2 29.41 29.65 0.20 0.18 o 0 3 2 -2.12 1.35 0.93 260.68 < 0 4 2 17.41 16.42 0.28 178.65 o 0 5 2 -1.14 1.98 1.33 91.55 < 0 6 2 55.04 55.25 0.32 180.48 o 0 7 2 8.63 9.48 0.15 -89.09 o 0 8 2 4.77 4.08 0.22 0.50 o 0 9 2 27.85 28.83 0.45 -89.28 o 0 10 2 21.01 20.53 0.35 1.25 o 0 11 2 21.12 21.29 0.36 -89.23 o 0 12 2 8.94 8.87 0.21 180.36 o 0 13 2 4.65 4.69 0.38 -88.38 o 0 13 3 8.99 8.55 0.24 90.94 o 0 12 3 14.25 15.34 0.30 180.72 o 0 11 3 3.69 4.14 0.38 268.80 o 0 10 3 0.00 1.43 2.99 183.08 < 0 9 3 15.05 15.99 0.29 -89.30 o 0 8 3 20.82 22.09 0.41 0.94 o 0 7 3 26.98 26.95 0.36 -89.11 o 0 6 3 51.83 51.13 0.33 180.45 o 0 5 3 33.40 34.55 0.30 -89.39 o 0 4 3 62.99 63.63 0.26 180.47 o 0 3 3 42.62 43.35 0.24 -89.44 o 0 2 3 107.04 104.91 0.68 0.32 o 0 1 3 14.66 13.96 0.20 -88.91 o 0 0 4 10.54 10.93 0.17 1.35 o 0 1 4 114.59 111.14 0.63 -89.76 o 0 2 4 36.97 37.00 0.22 180.86 o 0 3 4 4.13 4.37 0.16 -89.31 o 0 4 4 46.20 44.31 0.27 180.78 o 0 5 4 2.11 3.02 1.05 88.98 < 0 6 4 16.84 18.13 0.26 1.62 o 0 7 4 6.43 6.18 0.16 90.42 o 0 8 4 7.90 8.80 0.16 1.84 o 0 9 4 20.93 20.56 0.32 90.84 o 0 10 4 9.18 9.96 0.20 180.50 o 0 11 4 12.09 11.40 0.22 90.97 o 0 12 4 2.87 1.86 1.44 8.74 < 0 13 4 5.77 6.00 0.33 90.60 o 0 13 5 3.04 1.32 1.65 90.23 < 0 12 5 6.86 6.51 0.26 179.32 o 0 11 5 -1.57 0.72 1.77 -82.26 < 0 10 5 1.76 1.29 0.62 4.34 < 0 9 5 5.41 5.24 0.25 90.74 o 0 8 5 5.82 5.94 0.20 181.32 o 0 7 5 19.78 18.29 0.28 90.42 o 0 6 5 50.84 51.24 0.33 0.77 o 0 5 5 19.61 18.38 0.33 89.68 o 0 4 5 72.70 72.60 0.28 0.66 o 0 3 5 22.46 22.42 0.26 90.20 o 0 2 5 17.58 16.73 0.25 181.01 o 0 1 5 9.50 9.49 0.21 91.11 o 0 0 6 -1.35 2.00 1.22 -4.43 < 0 1 6 39.89 39.21 0.23 89.86 o 0 2 6 59.62 61.01 0.24 0.54 o 0 3 6 22.47 24.23 0.28 -89.11 o 0 4 6 43.57 44.44 0.29 0.75 o 0 5 6 10.17 10.24 0.20 90.20 o 0 6 6 26.48 27.33 0.35 181.03 o 0 7 6 15.89 16.06 0.29 90.84 o 0 8 6 12.97 12.71 0.27 181.40 o 0 9 6 7.18 6.79 0.20 269.86 o 0 10 6 2.44 2.92 0.50 179.55 < 0 11 6 4.94 5.08 0.30 91.41 o 0 12 6 25.52 25.22 0.38 180.72 o 0 13 6 13.74 13.98 0.26 90.68 o 0 13 7 13.60 13.08 0.31 -89.28 o 0 12 7 6.75 6.75 0.27 181.17 o 0 11 7 4.27 4.41 0.33 269.02 o 0 10 7 -2.30 1.12 1.63 -2.44 < 0 9 7 -3.76 1.58 1.12 92.13 < 0 8 7 9.75 10.18 0.20 1.42 o 0 7 7 9.49 9.66 0.19 91.14 o 0 6 7 39.87 38.88 0.35 180.63 o 0 5 7 39.30 40.97 0.32 90.88 o 0 4 7 50.66 51.50 0.30 180.59 o 0 3 7 41.51 41.11 0.27 90.44 o 0 2 7 36.48 36.66 0.26 0.64 o 0 1 7 16.59 17.18 0.28 89.74 o 0 0 8 70.04 72.50 0.25 0.50 o 0 1 8 5.34 4.69 0.13 266.40 o 0 2 8 2.66 2.78 0.25 182.21 o 0 3 8 36.06 36.24 0.29 90.90 o 0 4 8 28.12 28.36 0.31 180.71 o 0 5 8 -2.40 0.61 1.08 87.79 < 0 6 8 15.03 15.58 0.29 1.28 o 0 7 8 26.43 27.04 0.40 -89.23 o 0 8 8 1.56 1.45 1.69 178.52 < 0 9 8 17.41 17.39 0.35 -89.49 o 0 10 8 17.41 17.93 0.37 181.01 o 0 11 8 14.43 14.80 0.31 -89.00 o 0 12 8 2.19 2.81 1.85 1.00 < 0 13 8 9.79 10.21 0.25 -88.64 o 0 13 9 6.59 6.63 0.31 91.15 o 0 12 9 11.88 11.61 0.22 1.14 o 0 11 9 5.11 5.63 0.31 89.03 o 0 10 9 11.71 11.14 0.24 0.00 o 0 9 9 15.48 15.86 0.30 90.04 o 0 8 9 23.81 24.31 0.44 181.13 o 0 7 9 1.97 2.18 0.47 87.62 < 0 6 9 11.54 12.12 0.22 180.32 o 0 5 9 41.88 41.69 0.34 -89.21 o 0 4 9 4.78 4.96 0.18 180.15 o 0 3 9 21.14 21.76 0.33 -89.43 o 0 2 9 44.19 44.48 0.28 180.84 o 0 1 9 10.19 9.76 0.20 90.94 o 0 0 10 61.62 62.60 0.28 180.85 o 0 1 10 13.79 13.55 0.23 90.39 o 0 2 10 31.74 31.48 0.30 180.43 o 0 3 10 1.72 0.34 1.07 -4.18 < 0 4 10 15.83 15.72 0.26 0.64 o 0 5 10 17.54 17.31 0.28 90.26 o 0 6 10 2.34 3.70 0.38 183.25 < 0 7 10 2.15 3.11 1.43 94.14 < 0 8 10 8.94 8.78 0.23 179.07 o 0 9 10 18.75 19.93 0.36 -89.64 o 0 10 10 5.50 5.22 0.27 5.31 o 0 11 10 -1.34 4.02 2.35 269.68 < 0 12 10 12.88 13.11 0.27 0.64 o 0 12 11 25.22 25.72 0.42 180.57 o 0 11 11 11.46 11.02 0.24 90.85 o 0 10 11 15.33 15.35 0.32 0.18 o 0 9 11 5.89 6.16 0.27 -88.55 o 0 8 11 63.87 63.78 0.43 0.46 o 0 7 11 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0.34 90.60 o 0 0 14 15.90 14.78 0.27 -0.11 o 0 1 14 41.69 42.17 0.35 90.68 o 0 2 14 71.70 70.42 0.35 0.27 o 0 3 14 15.77 14.02 0.29 89.52 o 0 4 14 52.13 52.26 0.38 0.38 o 0 5 14 -2.63 2.71 1.23 268.42 < 0 6 14 34.89 35.62 0.43 180.39 o 0 7 14 17.53 17.16 0.37 269.82 o 0 8 14 33.73 34.18 0.48 180.39 o 0 9 14 21.98 22.05 0.38 -89.04 o 0 10 14 2.86 4.28 1.55 0.19 < 0 11 14 5.47 5.45 0.34 -88.03 o 0 11 15 11.08 10.00 0.23 91.00 o 0 10 15 11.14 11.56 0.22 180.14 o 0 9 15 19.82 19.85 0.39 -89.58 o 0 8 15 29.42 30.07 0.50 180.12 o 0 7 15 31.37 31.46 0.48 -89.57 o 0 6 15 27.32 27.77 0.46 180.91 o 0 5 15 9.97 10.08 0.20 91.04 o 0 4 15 6.02 6.78 0.22 183.52 o 0 3 15 11.29 11.26 0.25 89.36 o 0 2 15 -3.62 1.97 0.99 1.17 < 0 1 15 8.62 9.27 0.16 -88.10 o 0 0 16 26.39 26.72 0.40 180.31 o 0 1 16 2.30 0.24 1.12 -72.54 < 0 2 16 18.77 19.54 0.30 180.98 o 0 3 16 23.62 23.85 0.41 90.92 o 0 4 16 2.05 2.11 1.47 -7.32 < 0 5 16 5.37 5.41 0.28 -89.51 o 0 6 16 15.50 15.34 0.31 0.74 o 0 7 16 24.48 23.70 0.35 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4.67 5.50 0.40 76.03 o 1 11 8 7.63 7.37 0.23 -12.99 o 1 10 8 9.45 9.46 0.20 83.94 o 1 9 8 23.85 24.12 0.34 211.19 o 1 8 8 10.89 10.95 0.19 61.70 o 1 7 8 27.73 27.35 0.40 215.53 o 1 6 8 25.73 25.48 0.39 83.41 o 1 5 8 11.54 10.65 0.25 -55.51 o 1 4 8 22.36 21.83 0.34 167.52 o 1 3 8 28.25 28.75 0.31 166.06 o 1 2 8 37.28 36.80 0.29 258.63 o 1 1 8 49.38 48.93 0.28 168.41 o 1 0 8 33.08 33.04 0.28 0.12 o 1 0 7 44.85 45.79 0.27 90.82 o 1 1 7 48.23 48.41 0.27 70.56 o 1 2 7 19.04 19.06 0.30 -8.60 o 1 3 7 21.90 20.43 0.31 223.24 o 1 4 7 12.85 12.22 0.27 -36.63 o 1 5 7 53.56 52.29 0.34 261.23 o 1 6 7 17.40 18.03 0.29 99.75 o 1 7 7 11.90 12.55 0.24 95.74 o 1 8 7 11.94 12.65 0.25 247.39 o 1 9 7 26.60 27.49 0.48 113.96 o 1 10 7 20.49 20.22 0.36 264.40 o 1 11 7 14.51 14.83 0.26 233.13 o 1 12 7 7.57 7.54 0.25 53.53 o 1 13 7 8.06 8.59 0.27 235.01 o 1 13 6 0.00 1.85 3.57 203.06 < 1 12 6 12.58 12.25 0.27 258.01 o 1 11 6 13.48 13.45 0.28 207.69 o 1 10 6 18.53 19.38 0.38 39.56 o 1 9 6 8.22 7.54 0.20 249.37 o 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78.62 0.35 180.37 o 2 1 10 13.25 13.29 0.27 77.01 o 2 2 10 41.27 40.69 0.36 207.95 o 2 3 10 18.66 19.58 0.30 -58.51 o 2 4 10 19.64 20.18 0.30 -67.66 o 2 5 10 16.64 16.28 0.32 -32.64 o 2 6 10 8.33 8.64 0.19 22.12 o 2 7 10 9.22 9.09 0.19 98.87 o 2 8 10 16.25 15.59 0.30 42.35 o 2 9 10 7.16 6.89 0.24 114.36 o 2 10 10 19.28 18.86 0.41 -3.29 o 2 11 10 2.25 1.12 1.83 -66.12 < 2 11 11 3.21 5.04 1.60 110.23 < 2 10 11 7.12 6.84 0.26 -22.60 o 2 9 11 -3.82 2.90 1.35 -5.57 < 2 8 11 18.38 18.82 0.37 11.52 o 2 7 11 23.45 24.01 0.34 210.20 o 2 6 11 31.02 32.30 0.44 25.81 o 2 5 11 12.06 11.57 0.23 217.97 o 2 4 11 32.43 32.10 0.40 -28.53 o 2 3 11 27.21 27.77 0.39 17.58 o 2 2 11 27.20 27.42 0.39 -63.04 o 2 1 11 11.35 10.88 0.23 65.44 o 2 0 11 3.04 5.53 1.39 268.46 < 2 0 12 25.09 25.85 0.40 0.61 o 2 1 12 15.00 15.16 0.26 -34.39 o 2 2 12 23.09 22.81 0.41 -47.13 o 2 3 12 6.19 6.16 0.21 19.40 o 2 4 12 14.96 15.62 0.28 77.77 o 2 5 12 15.98 15.08 0.34 206.71 o 2 6 12 16.60 17.32 0.37 83.71 o 2 7 12 5.27 5.80 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2 6 15 20.07 20.43 0.36 129.91 o 2 5 15 7.99 8.47 0.21 264.98 o 2 4 15 20.57 20.44 0.34 215.44 o 2 3 15 8.52 8.83 0.19 -56.80 o 2 2 15 12.87 12.87 0.24 225.77 o 2 1 15 3.90 5.38 0.34 261.98 o 2 0 15 21.18 21.29 0.31 90.65 o 2 0 16 2.13 6.12 1.91 182.22 < 2 1 16 12.31 12.73 0.22 -21.84 o 2 2 16 7.09 7.00 0.22 138.31 o 2 3 16 7.52 7.47 0.21 8.44 o 2 4 16 6.08 6.10 0.25 124.65 o 2 5 16 5.17 5.37 0.29 172.10 o 2 6 16 5.35 6.51 0.30 -70.94 o 2 7 16 6.93 6.62 0.25 -7.98 o 2 8 16 11.89 11.56 0.23 -41.46 o 2 9 16 7.35 7.15 0.26 15.27 o 2 10 16 8.14 7.65 0.27 -2.59 o 2 9 17 -2.27 3.94 1.95 196.77 < 2 8 17 4.08 4.28 0.41 57.44 o 2 7 17 12.24 13.02 0.23 -81.19 o 2 6 17 9.81 9.63 0.20 -13.13 o 2 5 17 17.38 17.77 0.38 -82.09 o 2 4 17 12.55 12.87 0.26 68.95 o 2 3 17 9.22 9.60 0.19 80.40 o 2 2 17 10.56 10.94 0.22 263.49 o 2 1 17 17.51 17.95 0.31 69.74 o 2 0 17 44.36 45.14 0.43 -89.54 o 2 0 18 -3.05 5.90 1.89 179.95 < 2 1 18 34.62 34.30 0.46 250.29 o 2 2 18 22.75 22.33 0.34 94.97 o 2 3 18 15.24 14.86 0.32 218.54 o 2 4 18 2.22 2.98 0.56 24.20 < 2 5 18 13.21 13.65 0.30 75.41 o 2 6 18 3.17 2.64 0.44 13.75 o 2 7 18 14.97 14.52 0.27 83.65 o 2 8 18 10.65 10.03 0.22 76.68 o 2 9 18 5.44 4.78 0.34 108.32 o 2 8 19 0.00 2.74 3.47 217.10 < 2 7 19 12.23 11.90 0.21 146.59 o 2 6 19 11.37 11.97 0.20 79.36 o 2 5 19 8.99 9.34 0.21 77.22 o 2 4 19 7.85 8.58 0.22 69.26 o 2 3 19 8.65 8.89 0.22 50.86 o 2 2 19 7.67 8.36 0.24 240.41 o 2 1 19 -2.46 3.76 1.85 110.92 < 2 0 19 12.88 13.22 0.27 268.97 o 2 0 20 8.29 8.24 0.23 1.36 o 2 1 20 12.42 12.43 0.23 265.41 o 2 2 20 11.67 12.09 0.28 -64.33 o 2 3 20 12.50 12.36 0.27 140.03 o 2 4 20 12.44 12.18 0.25 96.33 o 2 5 20 10.07 9.98 0.23 176.30 o 2 6 20 5.93 6.09 0.29 109.11 o 2 7 20 11.15 10.60 0.22 -68.07 o 2 8 20 8.95 8.81 0.26 269.53 o 2 7 21 10.15 10.11 0.26 100.57 o 2 6 21 8.98 8.94 0.25 156.45 o 2 5 21 5.31 5.28 0.32 101.89 o 2 4 21 11.56 11.41 0.26 107.23 o 2 3 21 2.66 2.84 1.67 73.72 < 2 2 21 3.28 3.27 0.46 118.78 o 2 1 21 -2.90 3.01 1.52 146.46 < 2 0 21 8.67 8.81 0.23 -89.08 o 2 0 22 12.51 12.31 0.21 180.61 o 2 1 22 14.04 13.41 0.27 107.27 o 2 2 22 16.30 16.18 0.34 151.69 o 2 3 22 6.95 6.64 0.26 112.72 o 2 4 22 10.02 9.86 0.24 243.93 o 2 5 22 6.46 6.00 0.30 -20.84 o 2 6 22 13.78 14.03 0.27 -39.52 o 2 7 22 6.63 6.97 0.33 -47.30 o 2 6 23 8.39 7.95 0.27 94.23 o 2 5 23 2.88 1.24 1.60 -20.18 < 2 4 23 4.46 4.44 0.40 253.87 o 2 3 23 11.03 10.96 0.26 -40.94 o 2 2 23 8.63 8.65 0.25 254.30 o 2 1 23 8.59 9.03 0.24 -54.94 o 2 0 23 2.16 2.03 2.03 268.03 < 2 0 24 2.97 3.84 1.61 181.32 < 2 1 24 11.38 10.90 0.21 -80.89 o 2 2 24 8.18 8.00 0.26 206.61 o 2 3 24 8.22 7.93 0.26 -13.26 o 2 4 24 9.87 9.14 0.26 155.92 o 2 5 24 5.89 6.33 0.33 21.37 o 2 4 25 4.46 4.48 0.43 23.96 o 2 3 25 3.53 3.90 0.51 52.91 o 2 2 25 6.74 6.78 0.31 -0.87 o 2 1 25 4.51 5.00 0.42 12.74 o 2 0 25 6.85 6.97 0.32 -89.03 o 2 0 26 10.12 10.01 0.25 0.98 o 2 1 26 2.76 1.20 1.67 18.09 < 3 0 23 3.82 4.45 0.52 -89.01 o 3 1 23 7.78 6.91 0.28 180.86 o 3 2 23 4.69 3.81 0.40 -7.86 o 3 4 22 6.00 6.19 0.33 -86.94 o 3 3 22 4.08 3.73 0.43 190.81 o 3 2 22 5.78 5.96 0.36 243.65 o 3 1 22 5.19 4.96 0.37 225.66 o 3 0 22 13.41 12.95 0.21 180.99 o 3 0 21 10.94 10.53 0.21 91.09 o 3 1 21 -1.97 3.40 1.89 -0.15 < 3 2 21 12.28 11.51 0.23 152.71 o 3 3 21 2.52 1.89 0.63 -86.39 < 3 4 21 -1.76 1.40 2.16 168.53 < 3 5 21 -5.18 2.55 1.24 -88.91 < 3 6 20 8.59 8.25 0.26 43.60 o 3 5 20 7.06 6.77 0.28 210.90 o 3 4 20 6.46 6.70 0.30 113.09 o 3 3 20 4.82 4.47 0.34 184.47 o 3 2 20 9.28 8.63 0.23 90.02 o 3 1 20 12.11 11.15 0.23 92.26 o 3 0 20 8.78 8.65 0.23 0.97 o 3 0 19 -3.26 0.59 1.40 -77.78 < 3 1 19 9.80 9.79 0.22 12.30 o 3 2 19 7.18 6.88 0.25 -10.05 o 3 3 19 8.55 7.74 0.23 34.04 o 3 4 19 7.31 7.23 0.26 195.14 o 3 5 19 2.70 3.05 0.59 137.28 < 3 6 19 -2.28 2.29 1.87 196.05 < 3 7 18 5.62 4.87 0.35 -27.37 o 3 6 18 7.22 7.37 0.28 150.73 o 3 5 18 7.94 7.69 0.24 15.83 o 3 4 18 5.51 4.70 0.30 44.83 o 3 3 18 8.64 8.70 0.23 24.48 o 3 2 18 6.61 7.02 0.28 -57.29 o 3 1 18 4.78 4.71 0.33 -49.05 o 3 0 18 1.85 3.82 1.98 180.88 < 3 0 17 10.72 10.90 0.20 -89.59 o 3 1 17 2.87 3.63 1.49 174.90 < 3 2 17 15.05 14.95 0.28 223.70 o 3 3 17 5.53 5.93 0.31 139.91 o 3 4 17 5.79 5.49 0.30 -51.36 o 3 5 17 7.55 7.68 0.26 103.99 o 3 6 17 7.05 6.54 0.27 31.19 o 3 7 17 2.49 1.76 1.79 133.56 < 3 8 17 4.03 3.81 0.43 124.73 o 3 8 16 7.21 7.78 0.29 -47.45 o 3 7 16 11.22 11.14 0.22 134.08 o 3 6 16 16.14 16.53 0.31 -51.81 o 3 5 16 8.78 9.08 0.23 179.92 o 3 4 16 20.72 20.39 0.38 229.50 o 3 3 16 11.40 11.24 0.25 -61.86 o 3 2 16 10.08 10.19 0.21 199.44 o 3 1 16 8.32 8.52 0.22 -0.39 o 3 0 16 10.85 11.37 0.25 0.66 o 3 0 15 23.02 22.90 0.35 90.38 o 3 1 15 21.96 22.17 0.36 -8.37 o 3 2 15 15.72 15.81 0.33 118.78 o 3 3 15 7.70 8.11 0.23 265.01 o 3 4 15 10.20 11.16 0.20 196.68 o 3 5 15 13.38 14.04 0.27 212.10 o 3 6 15 10.42 10.67 0.22 -72.14 o 3 7 15 -1.38 1.53 2.27 200.70 < 3 8 15 11.58 11.13 0.24 -42.64 o 3 9 14 4.51 3.52 0.42 228.77 o 3 8 14 2.45 3.65 1.60 -14.98 < 3 7 14 13.40 13.08 0.28 214.80 o 3 6 14 9.45 9.31 0.21 149.84 o 3 5 14 9.65 9.90 0.21 158.41 o 3 4 14 2.89 2.99 0.48 182.37 < 3 3 14 8.36 8.10 0.22 64.60 o 3 2 14 13.53 13.52 0.29 267.60 o 3 1 14 14.16 14.67 0.27 -67.93 o 3 0 14 -3.97 5.72 1.45 182.88 < 3 0 13 25.97 25.99 0.47 90.23 o 3 1 13 59.24 59.54 0.44 -15.16 o 3 2 13 48.66 49.04 0.44 168.56 o 3 3 13 13.68 13.89 0.28 -89.83 o 3 4 13 11.78 12.27 0.24 205.30 o 3 5 13 17.20 18.56 0.38 161.81 o 3 6 13 3.41 3.05 0.41 -35.27 o 3 7 13 9.83 10.19 0.22 183.52 o 3 8 13 11.10 10.33 0.20 188.44 o 3 9 13 12.61 12.01 0.24 212.53 o 3 10 12 5.21 5.09 0.39 218.76 o 3 9 12 9.15 8.87 0.25 -44.49 o 3 8 12 9.45 9.57 0.22 129.45 o 3 7 12 17.31 18.01 0.33 14.24 o 3 6 12 11.06 11.45 0.23 72.61 o 3 5 12 22.03 21.16 0.36 15.63 o 3 4 12 8.20 8.22 0.21 5.28 o 3 3 12 2.38 2.19 1.62 126.44 < 3 2 12 9.03 9.47 0.23 -33.87 o 3 1 12 12.69 13.17 0.30 135.44 o 3 0 12 5.35 4.73 0.31 4.12 o 3 0 11 7.30 7.78 0.21 -87.69 o 3 1 11 10.51 10.47 0.21 120.53 o 3 2 11 11.71 12.45 0.19 10.23 o 3 3 11 5.28 4.90 0.28 130.15 o 3 4 11 4.31 4.33 0.33 168.22 o 3 5 11 7.39 7.19 0.23 204.51 o 3 6 11 4.74 5.05 0.32 -76.19 o 3 7 11 13.93 14.44 0.27 101.46 o 3 8 11 9.26 8.80 0.26 37.64 o 3 9 11 11.23 11.55 0.22 87.75 o 3 10 11 10.47 10.41 0.25 120.46 o 3 10 10 6.38 6.70 0.33 8.34 o 3 9 10 8.85 8.49 0.23 74.43 o 3 8 10 7.31 7.69 0.25 240.60 o 3 7 10 6.19 6.26 0.27 -49.67 o 3 6 10 13.68 14.02 0.26 216.94 o 3 5 10 8.25 8.39 0.21 -4.61 o 3 4 10 14.75 14.73 0.30 -36.57 o 3 3 10 1.62 3.02 1.95 71.77 < 3 2 10 16.73 15.87 0.34 -48.00 o 3 1 10 17.57 18.04 0.34 257.16 o 3 0 10 11.61 12.10 0.22 180.88 o 3 0 9 21.56 21.31 0.31 90.73 o 3 1 9 29.83 29.83 0.44 229.95 o 3 2 9 7.39 7.25 0.21 65.60 o 3 3 9 18.87 18.84 0.33 258.69 o 3 4 9 10.41 10.76 0.19 -13.93 o 3 5 9 5.52 5.52 0.28 61.69 o 3 6 9 6.75 6.96 0.25 2.79 o 3 7 9 8.63 8.24 0.22 268.13 o 3 8 9 8.26 8.25 0.22 -82.68 o 3 9 9 11.54 11.69 0.20 -83.62 o 3 10 9 10.94 11.12 0.24 -71.05 o 3 10 8 3.35 3.38 1.54 -18.91 < 3 9 8 8.71 9.00 0.23 242.28 o 3 8 8 7.40 7.63 0.24 14.59 o 3 7 8 14.32 14.42 0.29 159.72 o 3 6 8 12.37 12.66 0.23 23.47 o 3 5 8 22.90 22.33 0.45 178.47 o 3 4 8 13.26 13.58 0.25 165.77 o 3 3 8 17.11 17.38 0.35 205.51 o 3 2 8 24.64 25.17 0.44 173.57 o 3 1 8 12.93 13.76 0.27 102.47 o 3 0 8 13.96 14.06 0.28 180.06 o 3 0 7 2.69 3.14 1.31 269.23 < 3 1 7 24.45 24.74 0.41 38.09 o 3 2 7 11.39 11.08 0.21 95.49 o 3 3 7 10.95 10.70 0.23 23.57 o 3 4 7 17.89 18.71 0.35 156.93 o 3 5 7 15.31 14.31 0.31 -81.46 o 3 6 7 18.01 17.55 0.35 206.61 o 3 7 7 4.58 5.22 0.34 114.22 o 3 8 7 7.11 7.35 0.25 192.13 o 3 9 7 8.04 8.12 0.24 161.56 o 3 10 7 6.44 6.34 0.29 182.05 o 3 11 7 13.79 13.60 0.28 225.03 o 3 11 6 3.43 3.30 0.54 213.76 < 3 10 6 3.00 3.41 0.52 92.93 < 3 9 6 3.23 2.75 0.44 246.32 o 3 8 6 9.34 9.24 0.20 133.97 o 3 7 6 17.52 17.68 0.36 -70.22 o 3 6 6 15.62 15.95 0.28 111.92 o 3 5 6 11.40 11.08 0.22 3.73 o 3 4 6 26.58 26.11 0.44 55.09 o 3 3 6 24.83 25.34 0.44 77.59 o 3 2 6 21.64 21.48 0.43 35.25 o 3 1 6 1.05 1.66 2.06 157.90 < 3 0 6 6.00 6.12 0.22 -0.24 o 3 0 5 10.75 10.61 0.23 -88.91 o 3 1 5 16.13 16.59 0.33 -81.89 o 3 2 5 17.29 17.20 0.32 245.53 o 3 3 5 5.51 5.36 0.25 4.98 o 3 4 5 10.59 10.58 0.19 -62.03 o 3 5 5 27.58 27.74 0.44 84.69 o 3 6 5 6.39 6.30 0.26 92.14 o 3 7 5 9.86 9.83 0.20 140.90 o 3 8 5 7.57 7.70 0.23 105.87 o 3 9 5 11.57 11.83 0.23 191.74 o 3 10 5 14.44 14.39 0.29 44.82 o 3 11 5 6.32 6.32 0.32 121.81 o 3 11 4 4.93 5.50 0.40 158.75 o 3 10 4 2.42 1.42 1.77 72.62 < 3 9 4 7.79 7.90 0.24 165.75 o 3 8 4 8.59 8.37 0.22 196.91 o 3 7 4 18.98 19.57 0.36 79.04 o 3 6 4 14.54 15.22 0.32 253.47 o 3 5 4 14.99 14.93 0.26 7.62 o 3 4 4 18.35 19.26 0.33 263.55 o 3 3 4 29.64 28.38 0.40 -62.12 o 3 2 4 2.73 2.14 0.41 -25.68 o 3 1 4 4.94 5.17 0.25 -17.29 o 3 0 4 6.12 6.20 0.21 1.96 o 3 0 3 5.69 5.23 0.22 -89.74 o 3 1 3 27.10 27.24 0.39 155.65 o 3 2 3 14.19 14.20 0.27 0.31 o 3 3 3 6.23 6.57 0.22 203.72 o 3 4 3 8.98 8.50 0.22 -32.08 o 3 5 3 21.99 22.34 0.33 -68.96 o 3 6 3 11.78 11.75 0.22 241.33 o 3 7 3 4.09 4.03 0.39 101.63 o 3 8 3 2.38 2.26 1.67 195.67 < 3 9 3 11.60 11.38 0.20 141.62 o 3 10 3 7.81 7.36 0.25 22.31 o 3 11 3 7.90 7.79 0.27 -71.54 o 3 11 2 8.53 8.21 0.26 76.32 o 3 10 2 19.82 19.24 0.40 4.95 o 3 9 2 31.27 30.41 0.50 157.22 o 3 8 2 16.11 16.48 0.32 267.68 o 3 7 2 37.48 37.40 0.47 206.75 o 3 6 2 26.34 26.11 0.45 214.32 o 3 5 2 9.78 9.86 0.19 244.75 o 3 4 2 2.02 3.45 1.67 164.48 < 3 3 2 23.53 23.58 0.42 77.78 o 3 2 2 4.52 3.92 0.28 -16.63 o 3 1 2 3.86 3.96 0.32 209.04 o 3 0 2 17.99 18.28 0.30 180.76 o 3 0 1 21.50 21.55 0.41 90.94 o 3 1 1 40.20 39.75 0.38 -32.62 o 3 2 1 19.39 18.33 0.30 48.26 o 3 3 1 44.47 41.94 0.39 -24.40 o 3 4 1 23.01 22.60 0.43 185.14 o 3 5 1 8.06 7.79 0.19 100.15 o 3 6 1 25.45 26.73 0.48 205.92 o 3 7 1 28.02 28.79 0.48 185.64 o 3 8 1 15.02 14.60 0.33 -84.38 o 3 9 1 13.76 14.12 0.29 179.70 o 3 10 1 9.00 9.22 0.23 -35.06 o 3 11 1 9.99 9.43 0.24 88.14 o 3 11 0 6.20 6.03 0.33 -88.26 o 3 10 0 -1.68 1.35 2.16 -88.97 < 3 9 0 12.28 11.87 0.24 -88.69 o 3 8 0 7.18 7.49 0.25 91.68 o 3 7 0 8.84 9.15 0.22 91.16 o 3 6 0 2.70 0.90 0.50 254.61 < 3 5 0 9.33 9.62 0.19 269.86 o 3 4 0 1.61 0.63 0.66 106.15 < 3 3 0 32.21 30.81 0.40 -89.52 o 3 2 0 25.85 25.90 0.39 90.58 o 3 1 0 23.03 23.61 0.42 91.02 o 4 0 0 8.65 8.68 0.21 0.03 o 4 1 0 6.86 6.52 0.26 0.78 o 4 2 0 18.21 18.33 0.38 0.76 o 4 3 0 2.74 3.20 1.75 181.42 < 4 4 0 10.03 9.74 0.21 1.12 o 4 5 0 17.72 16.59 0.33 181.10 o 4 6 0 11.80 11.68 0.20 180.90 o 4 7 0 4.63 4.82 0.38 181.15 o 4 8 0 3.30 4.23 1.68 181.24 < 4 9 0 -5.97 0.52 1.10 175.73 < 4 9 1 5.04 5.46 0.39 -29.28 o 4 8 1 13.51 13.85 0.28 243.97 o 4 7 1 8.81 8.53 0.23 -28.15 o 4 6 1 15.85 16.17 0.31 202.04 o 4 5 1 7.05 6.84 0.27 127.30 o 4 4 1 14.53 15.15 0.21 155.25 o 4 3 1 16.25 16.29 0.31 154.77 o 4 2 1 8.58 8.59 0.23 76.06 o 4 1 1 6.99 6.76 0.25 173.36 o 4 0 1 4.83 4.52 0.33 91.16 o 4 0 2 -2.78 1.89 1.64 3.49 < 4 1 2 14.84 14.58 0.28 125.00 o 4 2 2 19.62 19.57 0.37 217.26 o 4 3 2 5.45 5.50 0.32 136.56 o 4 4 2 16.31 16.45 0.29 239.02 o 4 5 2 10.95 10.86 0.23 21.55 o 4 6 2 18.05 18.07 0.40 -9.29 o 4 7 2 6.64 6.86 0.29 49.72 o 4 8 2 8.08 8.13 0.26 28.99 o 4 9 2 3.09 1.66 1.62 242.29 < 4 9 3 11.45 11.21 0.23 -57.56 o 4 8 3 4.52 4.75 0.42 181.84 o 4 7 3 23.78 23.69 0.41 238.80 o 4 6 3 6.52 6.72 0.29 207.66 o 4 5 3 19.18 19.86 0.40 244.13 o 4 4 3 2.18 1.73 1.74 244.44 < 4 3 3 7.33 7.07 0.25 -31.00 o 4 2 3 6.65 6.80 0.27 209.08 o 4 1 3 3.00 3.29 0.52 136.08 < 4 0 3 4.66 5.05 0.35 -88.50 o 4 0 4 19.03 19.30 0.37 180.98 o 4 1 4 22.18 22.63 0.36 -73.41 o 4 2 4 2.63 3.07 0.58 196.06 < 4 3 4 25.13 25.10 0.49 -61.45 o 4 4 4 12.03 11.75 0.23 44.55 o 4 5 4 9.79 9.62 0.22 17.45 o 4 6 4 9.24 9.25 0.23 67.49 o 4 7 4 17.00 17.59 0.32 57.61 o 4 8 4 7.99 8.14 0.29 12.81 o 4 9 4 5.69 6.13 0.37 43.72 o 4 9 5 11.68 11.93 0.23 115.24 o 4 8 5 10.52 10.21 0.24 -50.39 o 4 7 5 5.09 5.18 0.37 46.89 o 4 6 5 8.61 8.32 0.23 241.40 o 4 5 5 7.47 7.44 0.25 250.76 o 4 4 5 9.26 9.37 0.21 97.14 o 4 3 5 5.07 4.73 0.33 148.43 o 4 2 5 22.09 22.39 0.37 23.54 o 4 1 5 19.74 20.06 0.38 25.13 o 4 0 5 -1.48 0.97 2.10 -86.57 < 4 0 6 8.56 8.27 0.22 2.32 o 4 1 6 12.94 12.66 0.26 233.01 o 4 2 6 8.16 8.05 0.23 112.86 o 4 3 6 4.93 5.26 0.33 142.70 o 4 4 6 13.00 13.68 0.24 117.13 o 4 5 6 7.37 7.42 0.25 -54.74 o 4 6 6 9.02 8.73 0.23 63.71 o 4 7 6 6.48 6.87 0.30 222.74 o 4 8 6 2.86 3.69 1.85 249.52 < 4 9 6 11.74 11.23 0.23 127.99 o 4 8 7 16.53 17.01 0.33 212.49 o 4 7 7 10.36 10.99 0.23 78.71 o 4 6 7 11.21 11.79 0.21 161.35 o 4 5 7 2.80 3.71 1.65 65.42 < 4 4 7 7.31 7.29 0.25 48.45 o 4 3 7 -2.95 3.53 1.45 225.21 < 4 2 7 7.39 7.11 0.25 72.13 o 4 1 7 7.27 7.20 0.26 193.72 o 4 0 7 10.69 11.48 0.20 91.23 o 4 0 8 13.55 13.90 0.28 180.65 o 4 1 8 24.66 24.17 0.36 54.19 o 4 2 8 21.45 21.36 0.38 251.80 o 4 3 8 14.31 14.14 0.27 7.63 o 4 4 8 5.79 6.14 0.30 246.75 o 4 5 8 10.39 9.49 0.20 243.96 o 4 6 8 5.82 5.57 0.31 166.76 o 4 7 8 6.98 6.68 0.29 256.70 o 4 8 8 7.19 7.35 0.31 -78.92 o 4 8 9 -2.06 3.47 2.10 -0.55 < 4 7 9 12.05 11.37 0.27 -19.29 o 4 6 9 12.33 12.75 0.21 211.59 o 4 5 9 4.28 4.04 0.40 -20.02 o 4 4 9 5.37 5.60 0.33 251.79 o 4 3 9 15.51 15.40 0.29 232.41 o 4 2 9 26.07 26.47 0.51 10.26 o 4 1 9 16.40 16.59 0.33 230.04 o 4 0 9 10.34 9.39 0.29 88.90 o 4 0 10 11.23 11.05 0.21 180.15 o 4 1 10 15.84 15.94 0.35 67.62 o 4 2 10 8.94 8.88 0.25 156.83 o 4 3 10 13.24 13.21 0.28 5.03 o 4 4 10 -3.10 2.61 1.31 -57.86 < 4 5 10 14.61 14.91 0.24 -28.67 o 4 6 10 8.18 8.41 0.26 4.31 o 4 7 10 7.15 6.70 0.30 -6.52 o 4 8 10 6.47 6.25 0.33 27.22 o 4 7 11 6.83 6.32 0.30 202.02 o 4 6 11 8.07 7.67 0.27 20.68 o 4 5 11 9.44 9.80 0.23 -56.36 o 4 4 11 15.71 15.75 0.27 -39.48 o 4 3 11 13.18 13.03 0.20 -10.04 o 4 2 11 0.96 2.57 1.09 -68.24 < 4 1 11 1.59 3.26 2.01 83.11 < 4 0 11 11.59 11.18 0.26 90.19 o 4 0 12 -1.30 5.00 2.55 180.32 < 4 1 12 5.77 5.66 0.30 -83.95 o 4 2 12 4.41 3.91 0.38 -16.99 o 4 3 12 10.49 10.56 0.22 259.10 o 4 4 12 7.43 7.22 0.27 47.06 o 4 5 12 2.41 5.25 1.98 179.43 < 4 6 12 6.88 6.40 0.31 139.74 o 4 7 12 5.34 5.00 0.38 93.69 o 4 7 13 3.39 3.45 0.56 79.13 < 4 6 13 5.07 5.89 0.40 262.00 o 4 5 13 7.47 7.27 0.29 94.16 o 4 4 13 6.19 5.91 0.30 105.21 o 4 3 13 0.96 2.82 2.67 67.60 < 4 2 13 10.78 10.77 0.23 50.36 o 4 1 13 5.03 4.71 0.33 -21.25 o 4 0 13 3.75 3.39 0.41 90.57 o 4 0 14 9.75 10.29 0.22 0.98 o 4 1 14 8.24 8.37 0.25 133.03 o 4 2 14 2.56 3.55 1.60 6.45 < 4 3 14 9.38 9.38 0.23 148.85 o 4 4 14 7.52 7.20 0.26 260.85 o 4 5 14 1.01 4.17 2.71 222.66 < 4 6 14 4.90 4.90 0.40 -62.34 o 4 6 15 7.40 7.32 0.29 151.17 o 4 5 15 8.71 8.61 0.26 -74.32 o 4 4 15 4.89 5.38 0.38 238.88 o 4 3 15 4.06 4.96 0.42 179.69 o 4 2 15 2.60 4.22 1.84 222.80 < 4 1 15 15.16 15.45 0.37 154.25 o 4 0 15 2.57 4.23 1.98 91.24 < 4 0 16 17.39 16.34 0.36 180.78 o 4 1 16 -2.41 2.99 1.82 -50.00 < 4 2 16 9.12 9.10 0.25 245.02 o 4 3 16 6.41 6.06 0.33 51.43 o 4 4 16 3.23 4.33 1.58 1.02 < 4 5 16 5.70 7.05 0.37 63.69 o 4 4 17 6.15 6.67 0.35 -57.43 o 4 3 17 11.92 12.13 0.22 -88.88 o 4 2 17 -2.66 1.96 1.98 39.48 < 4 1 17 10.20 10.86 0.26 -84.72 o 4 0 17 4.02 3.81 0.51 87.16 o 4 0 18 14.64 13.90 0.31 0.45 o 4 1 18 19.92 20.58 0.44 -79.70 o 4 2 18 14.90 15.64 0.26 71.79 o 4 3 18 6.65 6.12 0.32 -30.57 o 4 2 19 3.63 5.71 1.79 120.64 < 4 1 19 3.65 4.60 0.57 267.39 < 4 0 19 14.76 15.26 0.26 90.64 o 5 1 12 3.15 4.43 1.78 -29.11 < 5 0 12 7.95 7.83 0.31 1.02 o 5 0 11 8.47 7.76 0.28 -88.67 o 5 1 11 0.00 1.55 3.90 113.22 < 5 2 11 4.51 3.74 0.44 -34.14 o 5 3 10 2.56 2.48 1.99 246.45 < 5 2 10 6.78 6.34 0.33 -65.92 o 5 1 10 11.43 11.71 0.25 260.77 o 5 0 10 2.03 0.59 0.83 -1.71 < 5 0 9 13.51 13.65 0.25 90.71 o 5 1 9 7.61 7.50 0.30 169.33 o 5 2 9 3.56 3.26 1.50 95.52 < 5 3 9 10.40 10.59 0.25 208.80 o 5 4 9 8.47 8.75 0.29 -36.42 o 5 4 8 2.98 3.23 0.63 66.39 < 5 3 8 3.08 1.88 1.61 28.04 < 5 2 8 2.88 2.57 1.79 22.79 < 5 1 8 2.68 5.13 1.97 -39.09 < 5 0 8 2.47 0.89 1.87 -6.19 < 5 0 7 5.34 5.32 0.38 -89.24 o 5 1 7 3.33 1.54 1.56 104.20 < 5 2 7 9.01 9.35 0.27 119.13 o 5 3 7 -1.43 1.77 2.54 1.49 < 5 4 7 8.25 8.27 0.30 124.66 o 5 5 6 9.76 10.11 0.27 70.91 o 5 4 6 9.74 9.65 0.26 67.81 o 5 3 6 6.51 6.87 0.35 68.74 o 5 2 6 -2.64 2.86 1.93 116.12 < 5 1 6 -1.40 2.33 2.73 227.18 < 5 0 6 7.00 7.37 0.30 179.71 o 5 0 5 10.78 11.02 0.23 269.89 o 5 1 5 14.27 14.44 0.23 129.37 o 5 2 5 10.27 10.49 0.26 262.08 o 5 3 5 16.89 16.74 0.30 94.94 o 5 4 5 -2.49 1.52 1.96 233.44 < 5 5 5 8.49 8.18 0.29 53.84 o 5 5 4 -4.12 1.61 1.56 226.29 < 5 4 4 6.18 6.13 0.34 4.30 o 5 3 4 9.40 9.05 0.28 -57.22 o 5 2 4 22.35 22.05 0.42 83.02 o 5 1 4 9.52 9.48 0.25 -57.37 o 5 0 4 -4.26 1.62 1.36 176.71 < 5 0 3 5.04 4.52 0.38 -88.43 o 5 1 3 12.07 11.52 0.24 137.36 o 5 2 3 10.03 9.67 0.24 -6.57 o 5 3 3 11.27 11.02 0.26 102.00 o 5 4 3 5.79 5.91 0.37 2.41 o 5 5 3 -1.45 2.33 2.60 -19.71 < 5 5 2 7.25 6.86 0.30 194.69 o 5 4 2 7.10 6.99 0.31 127.24 o 5 3 2 10.64 11.13 0.24 242.85 o 5 2 2 8.45 8.31 0.26 194.39 o 5 1 2 8.04 7.76 0.27 250.16 o 5 0 2 5.29 5.73 0.37 181.47 o 5 0 1 10.09 9.98 0.23 91.36 o 5 1 1 7.54 6.92 0.28 -16.64 o 5 2 1 9.51 9.19 0.24 192.48 o 5 3 1 5.71 5.18 0.37 -38.76 o 5 4 1 7.35 7.77 0.32 234.88 o 5 5 1 4.91 4.38 0.40 -76.20 o 5 5 0 2.06 0.30 2.08 -87.14 < 5 4 0 3.50 3.19 1.62 90.06 < 5 3 0 2.23 5.85 2.09 90.74 < 5 2 0 10.52 10.03 0.23 91.13 o 5 1 0 11.95 12.16 0.22 90.77 o