#------------------------------------------------------------------------------
#$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $
#$Revision: 26848 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/00/62/2006286.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2006286_Fobs
loop_
_publ_author_name
'Zavalij, P. Y.'
'Chirayil, T.'
'Whittingham, M. S.'
_publ_section_title
;
 Layered Tetramethylammonium Vanadium Oxide [N(CH~3~)~4~]V~3~O~7~ by
 X-ray Rietveld Refinement
;
_journal_issue                   7
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              879
_journal_page_last               881
_journal_volume                  53
_journal_year                    1997
_space_group_IT_number           14
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_[local]_cod_data_source_file    br1166sup2.hkl
_[local]_cod_data_source_block   tmav3o7
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_intensity_meas
_refln_intensity_calc
1 0 -1 1661 1751
1 0 1 317 269
1 1 0 1418 1498
2 1 0 822 1127
0 1 1 0 2
3 0 -1 1886 1787
1 1 -1 44 35
1 1 1 555 395
3 0 1 142 106
4 0 0 9716 10000
2 1 -1 217 197
2 1 1 205 216
3 1 0 6293 6600
0 0 2 0 9
3 1 -1 3619 3698
3 1 1 5698 5838
2 0 -2 909 884
2 0 2 2094 1970
4 1 0 4947 5069
0 1 2 757 787
1 1 -2 163 200
1 1 2 111 119
4 1 -1 889 937
4 1 1 331 370
5 0 -1 55 61
5 0 1 268 278
2 1 -2 6635 7089
2 1 2 633 660
0 2 0 3463 3951
1 2 0 677 718
5 1 0 4196 4297
4 0 -2 770 632
3 1 -2 25 25
2 2 0 891 904
4 0 2 57 58
6 0 0 1173 1201
0 2 1 3889 4094
3 1 2 46 48
5 1 -1 4 4
1 2 -1 343 362
1 2 1 583 575
5 1 1 698 624
2 2 -1 1109 1080
2 2 1 2088 2166
3 2 0 17 18
4 1 -2 3529 3413
4 1 2 651 660
6 1 0 704 706
1 0 -3 2233 2231
1 0 3 5476 5316
3 2 -1 1 1
3 2 1 4 6
4 2 0 199 258
6 1 -1 533 602
6 1 1 51 52
0 2 2 359 439
0 1 3 25 30
5 1 -2 0 0
3 0 -3 8 9
1 2 -2 850 975
1 1 -3 362 416
1 2 2 894 1024
4 2 -1 478 546
1 1 3 5 6
4 2 1 335 385
3 0 3 482 560
5 1 2 115 133
7 0 -1 18 21
6 0 -2 2 2
7 0 1 426 455
2 2 -2 26 28
2 1 -3 348 372
2 2 2 190 206
2 1 3 164 152
6 0 2 445 382
5 2 0 2 2
7 1 0 1439 1391
3 1 -3 167 149
3 2 -2 17 15
3 2 2 235 258
3 1 3 13 14
7 1 -1 12 13
5 2 -1 223 237
5 2 1 416 442
6 1 -2 688 742
7 1 1 181 201
8 0 0 194 228
6 1 2 236 288
4 1 -3 557 552
4 2 -2 28 27
5 0 -3 63 66
4 2 2 89 89
6 2 0 19 19
4 1 3 680 663
5 0 3 195 215
8 1 0 466 462
6 2 -1 225 223
1 3 0 222 208
6 2 1 228 202
5 1 -3 187 205
7 1 -2 0 0
0 2 3 21 23
5 2 -2 181 198
2 3 0 84 91
1 2 -3 407 431
8 1 -1 453 476
1 2 3 1030 1063
0 3 1 1 1
5 2 2 51 50
0 0 4 1779 1732
1 3 -1 45 45
7 1 2 2 2
8 1 1 32 32
1 3 1 0 1
5 1 3 228 235
2 2 -3 8 9
2 2 3 11 11
2 3 -1 5 5
2 0 -4 590 582
2 3 1 35 36
3 3 0 1652 1677
7 2 0 0 0
2 0 4 823 792
8 0 -2 117 112
3 2 -3 57 67
8 0 2 29 28
3 2 3 78 77
0 1 4 88 87
7 2 -1 25 25
9 0 -1 35 34
3 3 -1 59 59
1 1 -4 93 92
3 3 1 5 5
6 1 -3 141 138
6 2 -2 92 91
1 1 4 2 2
7 2 1 9 9
9 0 1 49 52
4 3 0 823 892
6 2 2 7 8
2 1 -4 32 34
6 1 3 361 374
9 1 0 1250 1281
2 1 4 56 53
8 1 -2 291 270
4 2 -3 62 57
7 0 -3 3 2
0 3 2 5 5
4 0 -4 331 350
1 3 -2 280 297
1 3 2 49 53
4 3 -1 4 5
4 2 3 4 5
8 1 2 203 205
4 3 1 6 6
3 1 -4 288 287
9 1 -1 18 18
7 0 3 146 148
4 0 4 885 882
2 3 -2 143 142
9 1 1 822 805
3 1 4 106 105
2 3 2 41 41
8 2 0 5 6
5 3 0 855 1020
7 1 -3 29 33
5 2 -3 78 89
7 2 -2 208 239
3 3 -2 196 225
4 1 -4 141 160
8 2 -1 12 13
10 0 0 97 105
3 3 2 5 5
5 3 -1 141 145
7 2 2 20 21
8 2 1 0 0
5 2 3 11 12
5 3 1 61 62
7 1 3 50 50
4 1 4 157 160
4 3 -2 1 1
9 1 -2 26 34
4 3 2 27 33
6 3 0 223 269
10 1 0 173 199
5 1 -4 339 387
0 2 4 0 0
1 2 -4 57 66
6 2 -3 4 4
9 1 2 22 24
1 2 4 129 143
6 0 -4 1 1
5 1 4 191 214
6 3 -1 139 151
10 1 -1 152 165
2 2 -4 3 3
6 2 3 16 15
9 2 0 10 10
6 3 1 1 1
8 1 -3 148 140
2 2 4 18 17
10 1 1 9 8
8 2 -2 168 159
0 3 3 76 70
6 0 4 16 15
5 3 -2 236 217
1 3 -3 14 12
1 3 3 6 6
8 2 2 19 18
5 3 2 1 1
3 2 -4 47 46
9 2 -1 24 24
8 1 3 414 408
10 0 -2 108 105
2 3 -3 451 419
9 2 1 1 1
3 2 4 15 14
6 1 -4 80 75
2 3 3 86 82
7 3 0 678 665
1 0 -5 0 0
10 0 2 31 30
1 0 5 3 3
9 0 -3 120 114
7 2 -3 88 86
6 1 4 1 1
3 3 -3 234 239
4 2 -4 44 45
3 3 3 51 51
7 3 -1 292 295
11 0 -1 176 179
10 1 -2 531 565
6 3 -2 26 28
7 2 3 173 188
7 3 1 204 223
4 2 4 9 10
9 0 3 1 1
11 0 1 6 6
0 4 0 46 50
6 3 2 3 4
3 0 -5 176 194
0 1 5 106 115
1 4 0 1563 1695
1 1 -5 741 763
10 1 2 143 144
11 1 0 183 184
1 1 5 270 267
4 3 -3 253 250
9 1 -3 2 2
3 0 5 118 123
9 2 -2 412 426
2 4 0 346 374
2 1 -5 44 48
7 1 -4 214 234
10 2 0 38 42
4 3 3 218 240
5 2 -4 83 91
0 4 1 53 58
11 1 -1 1 1
1 4 -1 90 93
2 1 5 76 78
1 4 1 53 54
9 2 2 67 66
9 1 3 260 252
11 1 1 662 642
5 2 4 5 5
8 3 0 377 372
10 2 -1 63 63
3 1 -5 1008 1014
2 4 -1 35 35
2 4 1 14 14
7 1 4 123 127
3 4 0 508 523
8 2 -3 8 8
10 2 1 53 52
8 0 -4 8 7
3 1 5 26 24
5 3 -3 124 113
7 3 -2 39 35
8 3 -1 42 37
3 4 -1 31 28
7 3 2 1 1
8 3 1 35 32
5 3 3 121 114
8 2 3 16 15
3 4 1 11 10
4 1 -5 1 1
6 2 -4 25 25
5 0 -5 161 163
4 4 0 355 361
8 0 4 6 6
12 0 0 342 342
4 1 5 77 84
8 1 -4 27 30
11 1 -2 2 2
0 4 2 56 65
6 2 4 31 37
5 0 5 115 142
1 4 -2 182 222
1 4 2 195 238
4 4 -1 8 10
4 4 1 3 4
0 3 4 1 1
10 1 -3 28 33
1 3 -4 93 109
6 3 -3 97 113
10 2 -2 252 294
1 3 4 10 11
11 1 2 3 3
2 4 -2 57 66
2 4 2 70 79
5 1 -5 168 187
8 1 4 3 3
2 3 -4 17 18
12 1 0 24 26
0 2 5 497 535
5 4 0 303 325
6 3 3 193 207
1 2 -5 74 79
9 3 0 546 582
10 2 2 33 35
11 2 0 9 10
2 3 4 4 5
1 2 5 152 158
8 3 -2 44 46
10 1 3 283 290
9 2 -3 3 3
3 4 -2 12 12
2 2 -5 143 141
5 1 5 2 2
7 2 -4 40 39
12 1 -1 47 46
3 4 2 136 134
8 3 2 40 40
3 3 -4 204 204
5 4 -1 15 15
9 3 -1 100 100
11 2 -1 17 17
2 2 5 496 505
5 4 1 18 19
12 1 1 11 12
9 3 1 0 0
9 2 3 6 6
3 3 4 23 24
11 2 1 88 94
3 2 -5 4 4
7 2 4 10 8
12 0 -2 21 18
11 0 -3 165 151
6 1 -5 4 3
4 4 -2 38 36
7 3 -3 63 63
3 2 5 140 143
9 1 -4 156 168
4 3 -4 122 134
4 4 2 9 10
6 4 0 38 42
12 0 2 37 37
7 3 3 124 121
4 3 4 59 57
7 0 -5 107 102
4 2 -5 0 0
6 1 5 32 31
11 0 3 123 115
6 4 -1 11 11
6 4 1 11 11
9 1 4 104 108
12 1 -2 0 1
11 1 -3 4 4
4 2 5 364 387
8 2 -4 28 30
11 2 -2 474 510
9 3 -2 14 15
0 4 3 217 234
5 4 -2 37 40
1 4 -3 31 33
10 3 0 90 95
1 4 3 9 9
5 3 -4 208 218
7 0 5 157 161
5 4 2 35 36
10 2 -3 3 3
13 0 -1 218 216
0 0 6 199 194
12 1 2 12 11
9 3 2 10 10
10 0 -4 110 105
11 2 2 85 81
2 4 -3 63 60
7 1 -5 56 53
5 2 -5 6 6
13 0 1 2 2
2 4 3 237 239
11 1 3 150 151
5 3 4 16 17
8 2 4 6 6
10 3 -1 69 72
12 2 0 137 146
2 0 -6 1 1
7 4 0 13 14
8 3 -3 40 46
13 1 0 51 60
10 3 1 44 51
10 2 3 6 7
2 0 6 24 28
3 4 -3 78 91
5 2 5 174 200
12 2 -1 0 0
7 1 5 87 99
3 4 3 64 72
10 0 4 0 0
7 4 -1 7 8
13 1 -1 27 30
8 3 3 208 234
0 1 6 0 0
6 4 -2 13 15
10 1 -4 2 3
1 1 -6 5 6
7 4 1 3 3
12 2 1 254 284
6 3 -4 79 87
1 1 6 0 0
13 1 1 11 11
6 4 2 1 1