#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2006731.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2006731_Fobs loop_ _publ_author_name 'Hensen, K.' 'Pickel, P.' 'Lemke, A.' 'Bolte, M.' _publ_section_title ; 4-Methylpyridinium Pentachloro(4-methylpyridine-N)titanate(IV) Acetonitrile Solvate at 143K ; _journal_issue 11 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 1583 _journal_page_last 1585 _journal_volume 53 _journal_year 1997 _space_group_IT_number 31 _symmetry_space_group_name_Hall 'P 2ac -2' _symmetry_space_group_name_H-M 'P m n 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 7.1807 _cell_length_b 10.8165 _cell_length_c 12.6864 _exptl_crystal_F_000 460.00 _reflns_d_resolution_high 0.7971 _[local]_cod_data_source_file sk1120sup2.hkl _[local]_cod_data_source_block he15 #BEGIN Tags that were not found in dictionaries: _shelx_title ' he15 in Pmn2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 174.90 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y, z+1/2' '-x, y, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 -15 22.99 -30.43 30.43 o 0 1 -15 74.78 78.19 47.87 o 1 1 -15 17.42 11.94 43.41 o 2 1 -15 136.09 175.76 37.63 o 0 2 -15 855.51 832.13 69.53 o 1 2 -15 25.69 -15.45 35.61 o 2 2 -15 226.56 176.45 35.82 o 0 3 -15 198.12 211.02 52.62 o 1 3 -15 75.19 97.23 33.47 o 2 3 -15 1.30 -38.04 38.04 o 0 4 -15 168.10 182.17 52.20 o 1 4 -15 50.19 -11.31 45.54 o 0 0 -14 21.87 26.63 32.44 o 2 0 -14 103.22 64.77 40.36 o 0 1 -14 561.54 571.33 57.91 o 1 1 -14 29.11 -26.53 28.72 o 2 1 -14 491.51 443.55 48.50 o 3 1 -14 19.93 31.99 29.88 o 0 2 -14 262.24 335.49 50.83 o 1 2 -14 48.31 51.36 26.95 o 2 2 -14 70.08 81.22 25.11 o 3 2 -14 47.82 35.07 30.58 o 0 3 -14 94.44 142.97 47.66 o 1 3 -14 6.81 -3.97 26.95 o 2 3 -14 31.77 -2.77 30.23 o 3 3 -14 2.62 0.15 25.21 o 0 4 -14 74.20 34.34 47.44 o 1 4 -14 3.03 -13.84 51.78 o 2 4 -14 228.72 228.94 63.19 o 3 4 -14 40.55 -2.37 29.79 o 0 5 -14 338.98 375.54 55.79 o 1 5 -14 3.48 -25.74 25.74 o 2 5 -14 101.97 107.25 53.15 o 1 0 -13 200.41 233.42 30.80 o 3 0 -13 173.18 141.70 46.49 o 0 1 -13 167.08 233.61 29.91 o 1 1 -13 1.75 -13.55 16.43 o 2 1 -13 28.16 44.34 28.55 o 3 1 -13 165.02 143.15 31.63 o 4 1 -13 96.81 101.51 32.22 o 0 2 -13 921.45 874.92 65.30 o 1 2 -13 191.56 194.49 24.93 o 2 2 -13 745.78 770.57 35.53 o 3 2 -13 46.47 32.77 27.51 o 4 2 -13 410.43 351.55 40.48 o 0 3 -13 161.96 181.85 49.45 o 1 3 -13 55.32 42.84 25.79 o 2 3 -13 8.18 24.01 20.98 o 3 3 -13 86.62 63.78 25.91 o 4 3 -13 86.75 108.61 39.57 o 0 4 -13 324.54 383.68 51.14 o 1 4 -13 26.25 26.85 25.32 o 2 4 -13 98.59 69.05 23.90 o 3 4 -13 91.70 77.09 27.79 o 4 4 -13 148.77 153.13 31.97 o 0 5 -13 548.51 486.17 57.80 o 1 5 -13 105.55 51.79 41.32 o 2 5 -13 797.74 837.94 67.94 o 3 5 -13 1.23 -4.85 23.83 o 0 6 -13 235.83 263.85 54.74 o 1 6 -13 200.83 206.56 38.94 o 2 6 -13 17.74 -24.85 24.85 o 3 6 -13 188.63 257.40 43.85 o 0 7 -13 200.34 203.41 53.26 o 1 7 -13 75.51 130.65 34.07 o 0 0 -12 890.55 876.40 58.22 o 2 0 -12 721.11 750.13 56.32 o 4 0 -12 507.55 489.34 53.78 o 0 1 -12 827.53 819.45 40.64 o 1 1 -12 774.03 705.97 27.03 o 2 1 -12 919.76 928.48 37.53 o 3 1 -12 502.60 460.04 36.13 o 4 1 -12 328.88 321.75 36.83 o 5 1 -12 450.71 417.96 42.01 o 0 2 -12 1101.04 1020.00 45.28 o 1 2 -12 67.52 81.16 21.34 o 2 2 -12 76.01 94.64 20.54 o 3 2 -12 502.36 434.41 31.10 o 4 2 -12 539.51 548.86 42.47 o 5 2 -12 55.55 16.22 42.48 o 0 3 -12 123.99 70.69 34.76 o 1 3 -12 291.58 278.13 24.92 o 2 3 -12 636.68 623.09 32.94 o 3 3 -12 197.50 226.67 27.34 o 4 3 -12 91.34 107.05 27.25 o 5 3 -12 171.24 125.53 36.09 o 0 4 -12 51.33 38.99 36.03 o 1 4 -12 341.58 308.98 33.76 o 2 4 -12 502.90 517.98 36.29 o 3 4 -12 52.80 53.24 24.27 o 4 4 -12 15.50 -21.27 21.27 o 5 4 -12 327.87 405.27 46.14 o 0 5 -12 1088.78 1179.56 78.30 o 1 5 -12 94.96 55.40 26.06 o 2 5 -12 43.55 8.10 25.04 o 3 5 -12 147.02 118.18 24.41 o 4 5 -12 549.41 522.26 35.16 o 0 6 -12 554.02 629.25 63.19 o 1 6 -12 189.70 198.90 34.37 o 2 6 -12 110.61 86.34 32.49 o 3 6 -12 103.54 73.12 44.91 o 4 6 -12 266.41 259.73 33.36 o 0 7 -12 92.40 133.56 48.29 o 1 7 -12 12.42 8.40 27.37 o 2 7 -12 89.26 87.32 31.98 o 3 7 -12 16.93 4.77 27.19 o 0 8 -12 389.15 477.19 64.35 o 1 8 -12 17.67 -0.73 40.42 o 2 8 -12 843.75 808.99 72.80 o 1 0 -11 370.93 384.80 30.76 o 3 0 -11 243.47 221.16 40.58 o 5 0 -11 227.77 270.08 49.66 o 0 1 -11 1340.55 1253.53 94.73 o 1 1 -11 66.66 72.89 15.57 o 2 1 -11 315.83 372.15 33.52 o 3 1 -11 285.76 248.09 33.64 o 4 1 -11 690.69 663.33 40.81 o 5 1 -11 185.78 162.27 34.09 o 6 1 -11 123.35 90.90 36.04 o 0 2 -11 185.49 169.52 25.13 o 1 2 -11 532.92 568.97 29.09 o 2 2 -11 3084.34 2685.73 81.88 o 3 2 -11 230.06 238.73 25.48 o 4 2 -11 73.61 63.93 65.41 o 5 2 -11 405.15 402.15 39.23 o 6 2 -11 702.36 673.37 49.50 o 0 3 -11 355.86 424.15 47.66 o 1 3 -11 542.29 536.50 28.27 o 2 3 -11 380.85 397.06 26.99 o 3 3 -11 532.24 570.96 32.79 o 4 3 -11 188.40 186.38 27.45 o 5 3 -11 157.37 213.64 36.12 o 6 3 -11 132.70 158.08 55.58 o 0 4 -11 1620.22 1639.42 87.07 o 1 4 -11 375.61 352.34 29.98 o 2 4 -11 243.70 265.81 26.08 o 3 4 -11 558.50 537.14 36.33 o 4 4 -11 769.73 717.48 36.14 o 5 4 -11 84.79 72.47 36.31 o 0 5 -11 735.71 619.95 58.86 o 1 5 -11 550.74 572.66 39.58 o 2 5 -11 929.67 953.78 38.15 o 3 5 -11 210.48 197.41 26.94 o 4 5 -11 307.73 313.41 31.09 o 5 5 -11 456.99 475.91 36.67 o 0 6 -11 575.70 622.91 58.75 o 1 6 -11 12.35 10.99 32.23 o 2 6 -11 57.79 53.60 46.60 o 3 6 -11 46.59 66.65 23.93 o 4 6 -11 326.51 356.07 33.77 o 5 6 -11 48.95 48.26 27.60 o 0 7 -11 85.29 44.80 37.30 o 1 7 -11 241.76 238.39 35.08 o 2 7 -11 119.00 182.09 33.16 o 3 7 -11 174.41 229.94 35.66 o 4 7 -11 21.08 -12.83 23.46 o 0 8 -11 154.19 230.78 49.66 o 1 8 -11 62.39 36.65 29.13 o 2 8 -11 54.94 42.00 29.76 o 3 8 -11 283.17 258.32 41.07 o 0 9 -11 339.25 311.51 57.48 o 1 9 -11 70.94 30.42 34.19 o 2 9 -11 464.17 437.67 62.45 o 0 0 -10 2050.56 1930.85 87.91 o 2 0 -10 100.85 90.07 22.93 o 4 0 -10 1040.13 1104.54 68.47 o 6 0 -10 70.34 73.54 49.98 o 0 1 -10 1502.54 1657.90 57.57 o 1 1 -10 585.17 601.10 22.92 o 2 1 -10 890.49 906.97 34.28 o 3 1 -10 245.74 265.37 23.82 o 4 1 -10 629.84 620.14 52.20 o 5 1 -10 333.44 348.30 36.84 o 6 1 -10 118.89 114.34 34.18 o 0 2 -10 1014.59 1028.52 41.76 o 1 2 -10 42.78 54.85 16.26 o 2 2 -10 909.91 1019.90 37.37 o 3 2 -10 248.82 242.48 23.42 o 4 2 -10 540.55 561.04 38.72 o 5 2 -10 281.58 272.55 34.20 o 6 2 -10 260.92 282.84 53.73 o 0 3 -10 486.93 456.88 31.30 o 1 3 -10 365.19 381.78 25.37 o 2 3 -10 167.94 187.53 29.59 o 3 3 -10 175.82 194.20 23.72 o 4 3 -10 274.20 303.75 27.65 o 5 3 -10 254.13 216.08 33.05 o 6 3 -10 39.17 19.49 31.26 o 0 4 -10 84.47 164.21 36.56 o 1 4 -10 61.23 69.46 19.00 o 2 4 -10 1074.38 1096.84 41.80 o 3 4 -10 170.88 184.69 23.54 o 4 4 -10 27.30 44.21 20.84 o 5 4 -10 96.33 138.46 27.23 o 6 4 -10 254.52 243.78 42.95 o 0 5 -10 759.48 777.92 55.26 o 1 5 -10 504.87 453.33 35.43 o 2 5 -10 795.76 858.67 35.61 o 3 5 -10 1207.14 1141.48 41.57 o 4 5 -10 376.70 398.42 31.57 o 5 5 -10 13.17 36.29 25.11 o 6 5 -10 213.93 254.10 55.90 o 0 6 -10 121.69 149.41 40.58 o 1 6 -10 142.00 178.47 30.51 o 2 6 -10 789.14 858.02 50.56 o 3 6 -10 36.54 74.20 23.34 o 4 6 -10 39.22 21.04 23.74 o 5 6 -10 134.01 163.63 31.02 o 0 7 -10 653.21 645.52 61.60 o 1 7 -10 273.30 203.92 33.21 o 2 7 -10 93.29 95.13 29.38 o 3 7 -10 63.41 26.12 26.66 o 4 7 -10 397.04 393.56 41.66 o 5 7 -10 242.36 229.10 39.49 o 0 8 -10 1184.85 1218.55 80.41 o 1 8 -10 201.45 193.75 33.36 o 2 8 -10 619.77 698.98 47.54 o 3 8 -10 134.51 160.84 46.23 o 4 8 -10 544.35 500.80 36.71 o 0 9 -10 442.07 433.02 58.33 o 1 9 -10 44.49 7.89 32.97 o 2 9 -10 129.09 122.00 34.97 o 3 9 -10 41.42 50.68 64.72 o 0 10 -10 30.36 -39.52 39.52 o 1 10 -10 108.39 75.39 35.07 o 2 10 -10 97.25 164.95 51.99 o 1 0 -9 156.63 209.81 50.67 o 3 0 -9 21.08 32.27 19.92 o 5 0 -9 287.16 258.36 45.23 o 7 0 -9 36.40 78.51 55.37 o 0 1 -9 598.66 608.54 30.80 o 1 1 -9 96.15 87.38 13.88 o 2 1 -9 101.63 84.59 22.10 o 3 1 -9 94.22 87.88 19.23 o 4 1 -9 253.34 196.54 36.24 o 5 1 -9 438.09 412.45 38.19 o 6 1 -9 24.63 4.16 29.66 o 7 1 -9 159.21 188.04 39.98 o 0 2 -9 4050.34 4056.63 111.35 o 1 2 -9 64.62 36.63 22.49 o 2 2 -9 633.72 630.74 31.33 o 3 2 -9 210.28 183.53 21.04 o 4 2 -9 1571.44 1637.28 63.07 o 5 2 -9 37.22 48.02 26.75 o 6 2 -9 101.84 106.50 31.08 o 7 2 -9 107.65 106.96 37.97 o 0 3 -9 702.29 681.63 33.34 o 1 3 -9 66.02 34.06 16.19 o 2 3 -9 269.11 238.87 21.89 o 3 3 -9 36.46 45.25 18.16 o 4 3 -9 274.89 259.52 24.84 o 5 3 -9 97.13 128.78 25.35 o 6 3 -9 65.82 76.36 46.70 o 7 3 -9 20.81 -30.12 47.44 o 0 4 -9 156.83 177.73 37.09 o 1 4 -9 36.43 46.46 16.83 o 2 4 -9 1410.18 1440.16 46.85 o 3 4 -9 31.51 28.71 18.43 o 4 4 -9 65.41 87.47 22.80 o 5 4 -9 146.23 147.71 25.64 o 6 4 -9 315.87 345.37 33.21 o 0 5 -9 297.05 310.77 42.80 o 1 5 -9 275.52 271.99 22.95 o 2 5 -9 2138.94 2109.83 65.72 o 3 5 -9 341.70 315.98 24.70 o 4 5 -9 68.26 63.30 22.41 o 5 5 -9 155.99 117.89 27.12 o 6 5 -9 491.39 492.27 36.12 o 0 6 -9 1126.06 1320.41 80.41 o 1 6 -9 53.03 63.10 30.64 o 2 6 -9 42.17 23.36 18.76 o 3 6 -9 239.12 254.46 48.10 o 4 6 -9 542.07 519.49 34.93 o 5 6 -9 11.31 -8.45 26.15 o 6 6 -9 9.59 15.44 32.59 o 0 7 -9 855.04 849.56 64.77 o 1 7 -9 261.80 312.23 33.96 o 2 7 -9 41.63 10.01 69.05 o 3 7 -9 89.19 92.56 23.72 o 4 7 -9 438.50 408.48 31.94 o 5 7 -9 286.47 234.64 37.57 o 0 8 -9 481.37 420.45 53.36 o 1 8 -9 404.50 404.86 37.34 o 2 8 -9 207.36 217.83 33.53 o 3 8 -9 4.88 -30.26 30.43 o 4 8 -9 250.78 282.75 35.74 o 5 8 -9 609.87 478.88 67.31 o 0 9 -9 850.10 899.33 72.17 o 1 9 -9 166.14 168.98 54.42 o 2 9 -9 217.86 231.18 35.68 o 3 9 -9 189.77 233.84 59.17 o 4 9 -9 415.97 456.27 57.54 o 0 10 -9 173.46 164.21 49.87 o 1 10 -9 25.95 37.06 28.77 o 2 10 -9 496.00 506.04 45.28 o 0 11 -9 313.06 324.82 61.71 o 1 11 -9 105.63 83.98 34.64 o 0 0 -8 2112.49 2234.96 93.73 o 2 0 -8 664.81 678.47 32.76 o 4 0 -8 880.08 915.92 59.07 o 6 0 -8 124.03 123.31 45.97 o 0 1 -8 1075.19 1003.20 37.81 o 1 1 -8 226.86 227.02 15.15 o 2 1 -8 1741.22 1758.22 40.04 o 3 1 -8 84.31 94.72 18.09 o 4 1 -8 395.41 391.52 26.12 o 5 1 -8 188.45 229.23 30.61 o 6 1 -8 239.52 247.65 35.11 o 7 1 -8 37.82 87.50 34.11 o 0 2 -8 412.20 420.12 38.83 o 1 2 -8 51.43 50.65 12.66 o 2 2 -8 395.67 383.83 22.95 o 3 2 -8 202.38 177.25 20.05 o 4 2 -8 187.62 182.36 21.87 o 5 2 -8 327.99 298.80 25.94 o 6 2 -8 51.68 -17.80 47.39 o 7 2 -8 260.50 253.71 40.95 o 0 3 -8 688.91 377.01 229.35 o 1 3 -8 395.61 399.49 21.96 o 2 3 -8 610.17 622.16 27.03 o 3 3 -8 802.40 769.10 31.25 o 4 3 -8 225.37 219.43 22.82 o 5 3 -8 36.69 44.20 20.79 o 6 3 -8 122.22 102.38 40.21 o 7 3 -8 367.05 349.32 41.95 o 0 4 -8 265.98 240.89 25.20 o 1 4 -8 189.35 182.48 19.52 o 2 4 -8 1002.59 1019.42 34.64 o 3 4 -8 12.12 29.28 14.93 o 4 4 -8 113.82 133.35 34.62 o 5 4 -8 330.77 331.29 28.53 o 6 4 -8 204.10 201.51 28.10 o 7 4 -8 47.07 0.00 48.92 o 0 5 -8 700.68 752.24 53.26 o 1 5 -8 1031.98 1052.32 41.97 o 2 5 -8 577.48 591.64 29.99 o 3 5 -8 427.05 403.58 22.12 o 4 5 -8 324.95 303.58 20.97 o 5 5 -8 809.27 837.26 37.64 o 6 5 -8 88.76 69.17 34.67 o 7 5 -8 172.07 169.38 57.80 o 0 6 -8 463.95 507.52 50.93 o 1 6 -8 443.85 444.02 33.69 o 2 6 -8 522.40 542.12 28.84 o 3 6 -8 276.75 293.39 24.63 o 4 6 -8 245.98 211.52 20.34 o 5 6 -8 315.19 276.82 29.07 o 6 6 -8 93.72 113.24 33.80 o 0 7 -8 681.98 654.71 56.00 o 1 7 -8 223.37 253.82 42.48 o 2 7 -8 301.07 284.24 31.29 o 3 7 -8 252.08 267.23 25.79 o 4 7 -8 299.78 294.44 23.12 o 5 7 -8 98.07 93.92 25.10 o 6 7 -8 56.38 55.77 35.02 o 0 8 -8 1631.23 1572.22 87.60 o 1 8 -8 180.63 157.29 30.27 o 2 8 -8 456.55 495.60 38.42 o 3 8 -8 117.82 136.96 27.37 o 4 8 -8 714.91 725.68 35.09 o 5 8 -8 97.04 74.90 25.36 o 0 9 -8 82.40 89.08 41.10 o 1 9 -8 3.89 44.05 27.45 o 2 9 -8 811.90 886.84 48.82 o 3 9 -8 88.20 91.72 45.54 o 4 9 -8 73.02 114.60 26.39 o 0 10 -8 66.50 10.36 43.22 o 1 10 -8 175.94 178.97 34.95 o 2 10 -8 13.54 68.79 48.61 o 3 10 -8 359.26 419.39 63.08 o 4 10 -8 29.23 62.98 43.32 o 0 11 -8 177.68 209.54 56.00 o 1 11 -8 10.56 -1.27 48.61 o 2 11 -8 896.80 941.91 85.06 o 1 0 -7 394.33 394.18 27.58 o 3 0 -7 106.29 29.81 46.49 o 5 0 -7 564.78 606.32 58.65 o 7 0 -7 166.67 210.17 50.61 o 0 1 -7 2174.06 2228.28 64.67 o 1 1 -7 97.95 127.08 12.26 o 2 1 -7 1092.19 1143.36 29.16 o 3 1 -7 763.23 750.52 27.97 o 4 1 -7 935.07 922.44 48.97 o 5 1 -7 87.93 113.45 26.75 o 6 1 -7 197.12 217.87 30.57 o 7 1 -7 399.78 391.13 39.14 o 8 1 -7 136.71 131.16 39.34 o 0 2 -7 827.78 837.36 32.68 o 1 2 -7 434.48 457.89 17.54 o 2 2 -7 2854.09 2768.85 60.47 o 3 2 -7 196.86 182.64 15.21 o 4 2 -7 220.51 218.75 23.22 o 5 2 -7 364.19 389.05 27.24 o 6 2 -7 517.20 519.41 43.64 o 7 2 -7 84.81 90.03 32.75 o 0 3 -7 602.69 430.08 280.76 o 1 3 -7 356.85 322.76 15.69 o 2 3 -7 2609.80 2626.84 63.29 o 3 3 -7 555.68 627.43 22.82 o 4 3 -7 257.51 221.31 18.35 o 5 3 -7 65.64 35.95 19.58 o 6 3 -7 459.33 449.41 30.96 o 7 3 -7 262.23 288.05 65.83 o 0 4 -7 1417.15 1273.77 92.19 o 1 4 -7 252.11 264.56 19.45 o 2 4 -7 710.94 723.42 28.33 o 3 4 -7 746.30 758.76 37.34 o 4 4 -7 639.51 686.87 37.76 o 5 4 -7 10.55 24.54 16.50 o 6 4 -7 129.06 134.61 24.77 o 7 4 -7 425.76 508.79 67.52 o 0 5 -7 2756.63 2852.79 119.83 o 1 5 -7 276.80 250.29 20.53 o 2 5 -7 1207.62 1167.32 37.48 o 3 5 -7 19.32 39.34 14.84 o 4 5 -7 1020.28 1022.99 31.27 o 5 5 -7 343.94 352.35 26.62 o 6 5 -7 228.45 239.74 37.56 o 7 5 -7 15.08 12.98 36.57 o 0 6 -7 2227.07 2141.23 97.11 o 1 6 -7 292.39 232.35 48.42 o 2 6 -7 18.25 20.79 16.47 o 3 6 -7 178.03 142.45 20.34 o 4 6 -7 992.37 1003.60 31.85 o 5 6 -7 344.96 340.04 37.73 o 6 6 -7 1.50 25.61 24.37 o 7 6 -7 83.13 97.11 48.40 o 0 7 -7 718.14 737.13 58.12 o 1 7 -7 308.94 295.74 31.52 o 2 7 -7 844.12 862.59 34.39 o 3 7 -7 18.46 22.97 18.89 o 4 7 -7 349.47 337.02 27.52 o 5 7 -7 385.90 371.26 35.11 o 6 7 -7 186.14 160.56 29.12 o 0 8 -7 589.97 557.39 55.90 o 1 8 -7 159.59 158.64 29.38 o 2 8 -7 76.40 49.26 25.03 o 3 8 -7 555.99 520.13 30.35 o 4 8 -7 386.76 367.00 28.21 o 5 8 -7 85.12 80.76 26.10 o 6 8 -7 39.19 2.54 37.41 o 0 9 -7 193.95 254.66 48.61 o 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11 187.86 146.98 34.57 o 6 1 11 120.91 124.90 43.53 o 0 2 11 187.30 240.50 38.67 o 1 2 11 519.35 565.43 28.87 o 2 2 11 3044.10 2949.81 66.05 o 3 2 11 229.33 263.14 30.82 o 4 2 11 72.64 51.25 32.81 o 5 2 11 393.05 446.26 32.09 o 6 2 11 689.33 659.78 62.34 o 0 3 11 344.18 464.09 47.97 o 1 3 11 558.42 516.61 28.28 o 2 3 11 393.45 389.65 32.88 o 3 3 11 544.34 494.46 29.72 o 4 3 11 181.91 227.75 37.62 o 5 3 11 162.70 144.20 26.30 o 6 3 11 137.66 196.22 48.40 o 0 4 11 1571.69 1671.86 81.47 o 1 4 11 382.00 362.03 32.07 o 2 4 11 233.69 266.80 26.01 o 3 4 11 564.44 513.77 25.03 o 4 4 11 742.94 721.14 33.05 o 5 4 11 86.94 100.68 32.59 o 0 5 11 753.36 776.23 58.12 o 1 5 11 550.38 598.37 39.52 o 2 5 11 913.20 917.72 34.83 o 3 5 11 215.90 169.23 20.87 o 4 5 11 317.59 328.69 24.40 o 5 5 11 451.62 420.87 55.05 o 0 6 11 587.02 574.62 56.11 o 1 6 11 13.77 2.99 18.50 o 2 6 11 65.90 66.93 21.78 o 3 6 11 45.98 61.79 26.94 o 4 6 11 332.36 341.34 67.15 o 5 6 11 50.44 69.08 33.18 o 0 7 11 85.10 107.81 29.10 o 1 7 11 244.81 300.86 27.81 o 2 7 11 118.31 154.84 25.01 o 3 7 11 174.12 182.09 27.78 o 4 7 11 20.90 87.28 41.95 o 0 8 11 167.14 213.12 34.56 o 1 8 11 59.93 64.69 20.02 o 2 8 11 61.14 104.93 41.10 o 3 8 11 284.72 358.84 51.46 o 0 9 11 343.69 368.35 52.94 o 1 9 11 68.48 52.45 45.60 o 2 9 11 459.91 489.66 61.39 o 0 0 12 871.44 815.22 56.43 o 2 0 12 698.79 626.60 55.48 o 4 0 12 495.84 483.11 56.11 o 0 1 12 825.28 824.17 39.78 o 1 1 12 775.16 739.92 31.98 o 2 1 12 927.03 990.44 46.83 o 3 1 12 501.65 520.18 39.38 o 4 1 12 327.89 257.40 34.17 o 0 2 12 1075.10 1079.92 66.57 o 1 2 12 64.19 40.94 20.05 o 2 2 12 77.99 82.21 22.58 o 3 2 12 493.85 481.62 82.42 o 4 2 12 523.71 552.51 42.95 o 0 3 12 129.75 153.32 44.70 o 1 3 12 303.94 366.00 35.68 o 2 3 12 646.01 640.19 32.17 o 3 3 12 209.24 230.92 30.32 o 4 3 12 94.81 146.28 34.95 o 0 4 12 58.04 46.18 41.00 o 1 4 12 331.15 333.36 34.22 o 2 4 12 493.90 491.65 38.53 o 3 4 12 50.68 30.39 22.58 o 4 4 12 18.73 -28.85 39.94 o 5 4 12 320.27 369.20 54.74 o 0 5 12 1072.62 1121.34 71.43 o 1 5 12 103.23 98.07 30.07 o 2 5 12 50.63 78.69 27.79 o 3 5 12 150.79 185.89 35.00 o 4 5 12 539.00 503.00 33.20 o 0 6 12 568.52 650.38 62.55 o 1 6 12 180.29 193.75 32.20 o 2 6 12 108.24 111.16 31.92 o 3 6 12 97.51 85.62 49.40 o 4 6 12 274.67 300.09 50.30 o 0 7 12 96.71 91.40 47.76 o 1 7 12 11.08 -18.46 28.65 o 2 7 12 82.95 116.23 42.37 o 3 7 12 18.12 29.48 39.94 o 1 8 12 16.45 27.47 40.79 o 2 8 12 847.00 764.61 66.46 o 1 0 13 205.05 280.02 48.29 o 3 0 13 176.92 132.40 46.18 o 0 1 13 147.04 183.65 45.65 o 1 1 13 1.64 30.21 22.17 o 2 1 13 20.17 23.89 27.05 o 3 1 13 165.86 155.96 34.09 o 4 1 13 85.86 23.04 44.70 o 0 2 13 929.82 888.87 65.09 o 1 2 13 196.46 171.99 32.90 o 2 2 13 730.12 729.65 44.04 o 3 2 13 51.24 114.15 36.01 o 4 2 13 415.34 464.62 61.92 o 0 3 13 155.42 211.86 46.81 o 1 3 13 51.02 46.31 52.94 o 2 3 13 11.30 -17.25 25.95 o 3 3 13 82.04 117.34 34.06 o 4 3 13 82.85 61.08 63.08 o 0 4 13 311.65 321.86 50.61 o 1 4 13 29.65 46.73 29.44 o 2 4 13 99.55 48.22 43.80 o 3 4 13 90.86 107.76 33.85 o 0 5 13 561.18 582.22 61.39 o 1 5 13 102.75 114.66 42.21 o 2 5 13 797.30 831.14 53.31 o 3 5 13 1.55 6.23 40.68 o 0 6 13 218.66 239.02 59.38 o 1 6 13 210.87 292.70 57.27 o 2 0 14 115.74 207.74 51.99 o 0 1 14 566.08 573.77 60.02 o 1 1 14 25.99 75.02 46.18 o 2 1 14 487.42 544.38 44.61 o 3 1 14 21.68 -6.87 43.32 o 0 2 14 265.43 296.40 51.88 o 1 2 14 49.55 42.59 31.65 o 2 2 14 77.06 126.37 35.64 o 3 2 14 45.51 6.45 42.69 o 0 3 14 99.23 51.99 42.80 o 1 3 14 6.03 -10.40 27.69 o 2 3 14 27.85 90.13 49.87 o 3 3 14 1.95 21.34 44.49 o 0 4 14 83.10 102.50 47.66 o 1 4 14 1.78 9.24 37.51 o 2 4 14 225.38 246.73 58.33 o 1 0 15 26.74 45.01 46.60 o 1 1 15 18.61 41.63 46.39 o 2 1 15 147.08 184.07 54.84 o 0 2 15 866.42 949.52 75.13 o 1 2 15 23.98 -27.79 42.48 o 0 3 15 199.48 197.39 55.69 o 1 3 15 79.16 114.01 55.48 o