#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/00/68/2006846.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2006846_Fobs loop_ _publ_author_name 'Lassaba, E.' 'Benharref, A.' 'Giorgi, M.' 'Pierrot, M.' _publ_section_title ; Cyclopropanation of a \b-Himachalene Monoepoxide Derivative ; _journal_issue 12 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 1943 _journal_page_last 1945 _journal_volume 53 _journal_year 1997 _[local]_cod_data_source_file ln1007sup2.hkl _[local]_cod_data_source_block ecl1 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_meas _refln_F_calc _refln_F_sigma _refln_phase_calc _refln_observed_status 0 -2 0 409.17 421.70 1.41 -0.05 o 0 -4 0 444.54 467.45 2.00 180.73 o 0 -6 0 228.92 227.13 0.62 0.50 o 0 -8 0 283.32 280.16 0.73 1.08 o 0 -10 0 244.29 248.85 0.85 180.57 o 0 -12 0 220.70 222.55 0.95 180.94 o 0 -14 0 179.69 184.80 1.07 0.78 o 0 -16 0 77.08 80.82 1.12 1.55 o 0 -18 0 20.48 17.67 1.66 186.01 o -1 -19 0 36.29 38.06 1.28 -88.95 o -1 -18 0 25.00 24.36 1.39 92.60 o -1 -17 0 -14.21 5.67 3.61 -88.66 < -1 -16 0 65.83 62.92 0.96 91.48 o -1 -15 0 5.40 8.87 6.01 96.87 < -1 -14 0 157.52 159.75 1.08 -89.22 o -1 -13 0 -9.33 9.45 4.19 -88.99 < -1 -12 0 30.42 32.04 0.83 -86.78 o -1 -11 0 58.39 56.34 0.93 -88.34 o -1 -10 0 192.66 197.16 0.85 90.94 o -1 -9 0 154.94 158.54 0.80 269.86 o -1 -8 0 63.98 68.39 0.83 91.35 o -1 -7 0 125.52 117.15 0.70 90.94 o -1 -6 0 406.96 424.14 2.53 -89.43 o -1 -5 0 -4.85 13.90 2.90 -85.02 < -1 -4 0 265.84 262.30 0.50 89.82 o -1 -3 0 146.06 151.95 0.44 -89.22 o -1 -2 0 14.23 11.64 0.34 114.68 o -1 -1 0 88.27 85.85 0.31 268.95 o -2 0 0 463.23 490.79 1.52 0.13 o -2 -1 0 296.11 304.55 1.59 180.24 o -2 -2 0 98.49 107.11 0.44 -0.06 o -2 -3 0 367.11 377.54 1.95 180.15 o -2 -4 0 137.81 130.24 0.54 -0.48 o -2 -5 0 388.80 385.46 2.38 179.84 o -2 -6 0 13.07 7.61 0.87 177.62 o -2 -7 0 73.76 69.11 0.75 0.38 o -2 -8 0 209.95 198.81 0.76 179.77 o -2 -9 0 69.13 79.85 0.90 180.89 o -2 -10 0 169.20 174.36 0.88 180.21 o -2 -11 0 78.61 75.66 1.00 180.12 o -2 -12 0 38.55 39.19 0.72 181.12 o -2 -13 0 140.51 136.69 1.05 0.40 o -2 -14 0 42.26 42.14 0.81 0.73 o -2 -15 0 19.19 23.54 1.34 180.46 o -2 -16 0 19.08 15.58 1.42 178.41 o -2 -17 0 -8.04 0.72 4.94 -46.16 < -2 -18 0 12.38 16.01 2.45 -1.62 o -2 -19 0 35.95 32.52 1.16 0.38 o -3 -19 0 13.60 12.89 2.30 93.18 o -3 -18 0 7.38 1.23 5.37 263.72 o -3 -17 0 4.49 6.40 6.78 -88.49 < -3 -16 0 8.37 13.49 4.79 90.08 o -3 -15 0 64.68 61.67 0.90 -88.99 o -3 -14 0 27.33 23.18 1.01 89.97 o -3 -13 0 68.51 69.48 1.03 90.40 o -3 -12 0 88.25 87.64 1.06 90.14 o -3 -11 0 208.93 216.56 0.93 90.40 o -3 -10 0 78.71 65.69 0.95 90.01 o -3 -9 0 73.97 75.06 0.90 -89.39 o -3 -8 0 20.41 23.94 0.76 -89.66 o -3 -7 0 187.03 162.71 0.73 89.50 o -3 -6 0 -5.98 6.03 3.25 267.95 < -3 -5 0 50.48 42.63 0.74 91.52 o -3 -4 0 32.75 33.15 0.49 90.24 o -3 -3 0 128.30 131.74 0.54 269.33 o -3 -2 0 93.62 100.84 0.51 89.84 o -3 -1 0 160.90 159.26 0.47 89.52 o -4 0 0 100.73 103.54 0.56 179.15 o -4 -1 0 416.36 421.41 2.19 0.49 o -4 -2 0 44.96 40.65 0.60 180.21 o -4 -3 0 274.39 288.09 0.59 0.59 o -4 -4 0 294.56 293.79 0.63 180.32 o -4 -5 0 526.15 537.98 2.69 180.42 o -4 -6 0 58.43 56.16 0.84 179.78 o -4 -7 0 82.53 66.31 0.79 181.63 o -4 -8 0 96.61 112.71 0.85 0.70 o -4 -9 0 296.89 295.50 0.84 0.72 o -4 -10 0 66.65 68.81 0.91 180.40 o -4 -11 0 55.74 56.14 0.80 0.98 o -4 -12 0 86.04 85.05 1.11 180.75 o -4 -13 0 38.32 43.26 0.80 183.68 o -4 -14 0 33.28 37.17 0.94 0.74 o -4 -15 0 26.23 28.09 1.13 -0.30 o -4 -16 0 40.68 38.18 0.99 1.09 o -4 -17 0 122.30 120.69 1.31 0.98 o -4 -18 0 37.35 38.15 1.13 180.73 o -4 -19 0 -16.41 3.11 3.80 -2.15 < -5 -18 0 48.38 45.34 0.97 91.31 o -5 -17 0 9.21 7.86 5.03 268.60 o -5 -16 0 -11.31 4.17 4.38 107.63 < -5 -15 0 93.44 86.38 1.28 -88.60 o -5 -14 0 112.79 119.32 1.21 -89.07 o -5 -13 0 112.20 110.05 1.14 90.20 o -5 -12 0 71.01 70.55 1.05 -88.78 o -5 -11 0 292.35 296.95 0.97 90.60 o -5 -10 0 185.35 184.23 0.95 90.89 o -5 -9 0 4.98 6.10 5.21 -81.14 < -5 -8 0 163.57 168.52 0.85 90.47 o -5 -7 0 73.97 79.85 0.87 -87.61 o -5 -6 0 86.67 96.12 0.81 -87.78 o -5 -5 0 204.89 211.69 0.72 90.57 o -5 -4 0 197.34 196.43 0.69 -89.75 o -5 -3 0 269.82 270.75 0.65 90.74 o -5 -2 0 333.98 350.03 0.63 90.69 o -5 -1 0 143.57 139.82 0.63 -88.85 o -6 0 0 241.80 237.91 0.68 1.06 o -6 -1 0 57.09 54.16 0.77 1.12 o -6 -2 0 35.30 33.86 0.51 -0.71 o -6 -3 0 74.94 73.45 0.76 0.60 o -6 -4 0 245.76 254.27 0.74 180.91 o -6 -5 0 85.17 79.28 0.82 180.86 o -6 -6 0 55.79 55.99 0.82 1.39 o -6 -7 0 37.74 37.93 0.62 -0.55 o -6 -8 0 271.10 277.04 0.88 0.69 o -6 -9 0 119.58 121.45 0.96 0.56 o -6 -10 0 51.17 50.47 0.87 181.88 o -6 -11 0 -5.27 3.91 5.56 178.85 < -6 -12 0 96.02 93.43 1.16 181.31 o -6 -13 0 73.97 73.83 1.07 180.75 o -6 -14 0 116.09 123.06 1.19 0.82 o -6 -15 0 -4.86 5.58 7.09 179.04 < -6 -16 0 63.25 61.22 0.94 1.16 o -6 -17 0 18.65 23.62 1.82 1.56 o -6 -18 0 65.47 65.14 0.89 181.17 o -7 -17 0 7.14 9.29 5.86 -89.25 < -7 -16 0 12.66 4.92 2.10 98.57 o -7 -15 0 0.00 10.18 10.49 89.98 < -7 -14 0 17.09 12.03 1.56 -88.30 o -7 -13 0 22.95 21.15 1.15 269.89 o -7 -12 0 23.99 19.17 1.10 -87.34 o -7 -11 0 89.51 91.69 1.12 -89.85 o -7 -10 0 67.44 65.54 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