#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/00/73/2007359.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2007359_Fobs loop_ _publ_author_name 'Arai, Y.' 'Hashizume, D.' 'Kogo, H.' 'Ohashi, Y.' 'Ohgo, Y.' _publ_section_title ; Bis(dimethylglyoximato-N,N')[methyl (R)-ethanoato-C^2^][tris(2-cyanoethyl)phosphine-P]cobalt(III) ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 739 _journal_page_last 741 _journal_volume 54 _journal_year 1998 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _exptl_crystal_F_000 596.00 _[local]_cod_data_source_file na1314sup2.hkl _[local]_cod_data_source_block cobaloxime #BEGIN Tags that were not found in dictionaries: _shelx_title ' R-1-mce' _shelx_refln_list_code 4 _shelx_f_calc_maximum 144.23 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1774.13 1956.52 61.68 o 2 0 0 53.56 83.35 3.49 o 3 0 0 20801.67 21493.22 677.25 o 4 0 0 3498.27 3977.17 131.38 o 5 0 0 174.76 197.44 7.86 o 6 0 0 1224.26 1170.09 41.24 o 7 0 0 162.44 126.50 6.88 o 8 0 0 431.88 436.59 15.89 o 9 0 0 47.98 45.53 4.60 o 10 0 0 3.68 10.30 3.55 o 11 0 0 236.91 237.92 12.17 o 12 0 0 35.01 32.89 4.48 o 13 0 0 4.69 0.98 5.23 o 14 0 0 9.47 17.90 4.57 o 1 1 0 8201.78 8297.31 266.03 o 2 1 0 3658.94 3959.63 125.98 o 3 1 0 17145.79 18337.38 585.49 o 4 1 0 5793.00 5954.16 191.35 o 5 1 0 5627.95 5823.25 190.55 o 6 1 0 532.74 502.36 17.05 o 7 1 0 1685.57 1753.50 60.09 o 8 1 0 144.91 140.99 7.64 o 9 1 0 135.76 135.93 8.29 o 10 1 0 185.10 166.29 9.86 o 11 1 0 56.90 56.28 5.46 o 12 1 0 21.22 32.61 4.19 o 13 1 0 9.67 -7.14 7.86 < 14 1 0 13.73 1.97 8.81 o 0 2 0 223.65 251.05 8.48 o 1 2 0 326.88 330.08 10.80 o 2 2 0 567.50 586.36 21.05 o 3 2 0 3728.25 4113.09 135.36 o 4 2 0 3588.55 3701.96 125.53 o 5 2 0 283.54 369.48 13.00 o 6 2 0 2129.87 2093.60 69.54 o 7 2 0 226.97 230.64 10.05 o 8 2 0 641.76 646.24 22.33 o 9 2 0 300.66 304.56 12.90 o 10 2 0 406.20 381.03 15.59 o 11 2 0 47.32 46.50 4.50 o 12 2 0 88.65 110.99 9.23 o 13 2 0 23.32 31.32 4.80 o 14 2 0 18.52 21.72 5.04 o 1 3 0 650.40 699.95 25.03 o 2 3 0 2516.82 2661.65 92.61 o 3 3 0 784.28 776.23 24.67 o 4 3 0 251.10 198.22 8.06 o 5 3 0 370.25 350.14 12.61 o 6 3 0 66.76 78.26 5.67 o 7 3 0 262.30 239.69 10.49 o 8 3 0 247.68 235.60 10.86 o 9 3 0 203.52 188.66 10.19 o 10 3 0 222.14 212.61 11.67 o 11 3 0 69.59 57.77 5.01 o 12 3 0 48.22 49.29 5.11 o 13 3 0 127.71 127.55 11.08 o 0 4 0 946.94 938.42 33.83 o 1 4 0 343.99 313.61 11.24 o 2 4 0 34.95 31.70 2.80 o 3 4 0 1564.53 1475.27 50.25 o 4 4 0 357.94 352.80 12.76 o 5 4 0 380.53 384.09 14.05 o 6 4 0 26.77 21.94 3.04 o 7 4 0 507.07 505.94 18.33 o 8 4 0 530.03 559.08 20.43 o 9 4 0 401.72 388.77 15.77 o 10 4 0 9.29 4.99 6.99 o 11 4 0 52.56 59.41 6.01 o 12 4 0 204.60 219.02 12.89 o 13 4 0 22.60 26.05 5.42 o 1 5 0 3.61 7.17 2.31 o 2 5 0 571.92 516.05 17.66 o 3 5 0 73.95 77.90 5.75 o 4 5 0 1327.48 1381.42 49.44 o 5 5 0 317.13 303.08 12.20 o 6 5 0 71.36 61.96 6.43 o 7 5 0 696.84 685.60 24.08 o 8 5 0 879.04 906.14 30.87 o 9 5 0 60.01 61.80 5.88 o 10 5 0 44.66 50.38 4.65 o 11 5 0 15.14 15.66 4.48 o 12 5 0 20.20 21.39 5.01 o 0 6 0 386.45 373.56 14.18 o 1 6 0 490.64 515.79 18.19 o 2 6 0 109.32 129.55 7.67 o 3 6 0 1752.19 1754.29 55.20 o 4 6 0 549.04 557.94 19.81 o 5 6 0 84.24 83.55 7.03 o 6 6 0 197.15 193.81 10.27 o 7 6 0 192.70 193.21 10.62 o 8 6 0 142.80 118.37 9.55 o 9 6 0 121.52 128.41 9.65 o 10 6 0 22.18 25.13 4.53 o 11 6 0 3.18 -2.82 5.87 < 1 7 0 528.42 548.90 19.96 o 2 7 0 597.51 565.60 20.54 o 3 7 0 172.40 165.36 9.31 o 4 7 0 201.53 195.56 10.32 o 5 7 0 330.68 303.40 13.47 o 6 7 0 97.99 117.18 8.78 o 7 7 0 99.18 87.01 8.95 o 8 7 0 125.79 137.67 9.97 o 9 7 0 77.67 69.80 6.65 o 10 7 0 118.21 139.27 11.11 o 0 8 0 930.06 886.29 30.63 o 1 8 0 127.33 117.99 8.65 o 2 8 0 76.04 78.59 7.90 o 3 8 0 93.06 89.74 8.38 o 4 8 0 271.92 269.88 13.09 o 5 8 0 118.55 109.19 9.13 o 6 8 0 179.96 183.43 11.31 o 7 8 0 8.33 0.36 7.53 o 8 8 0 8.12 3.43 8.20 o 9 8 0 51.05 43.49 5.30 o 1 9 0 216.69 219.00 12.34 o 2 9 0 13.35 7.26 7.29 o 3 9 0 4.18 2.09 7.45 o 4 9 0 64.60 70.05 6.24 o 5 9 0 173.97 152.00 11.13 o 6 9 0 27.99 29.63 4.90 o 7 9 0 32.23 38.71 5.14 o 0 10 0 245.49 249.21 14.11 o 1 10 0 21.62 25.97 4.99 o 2 10 0 29.17 36.82 5.02 o 3 10 0 10.09 7.38 8.21 o -14 0 1 25.39 37.90 5.12 o -13 0 1 2.89 -3.29 7.38 < -12 0 1 33.21 29.05 4.44 o -11 0 1 102.78 104.18 8.74 o -10 0 1 306.00 311.04 13.47 o -9 0 1 5.70 15.85 3.25 o -8 0 1 198.34 178.79 8.61 o -7 0 1 15.11 16.08 2.63 o -6 0 1 1401.63 1397.72 48.04 o -5 0 1 2738.01 2721.31 86.48 o -4 0 1 1749.48 1972.50 63.10 o -3 0 1 462.03 459.52 14.74 o -2 0 1 1956.10 2257.87 73.76 o -1 0 1 18761.62 18118.10 555.43 o 1 0 1 14669.67 15418.95 475.81 o 2 0 1 216.87 248.06 8.17 o 3 0 1 187.67 185.15 6.97 o 4 0 1 2633.95 2947.85 100.98 o 5 0 1 182.15 149.35 6.59 o 6 0 1 12.85 -1.32 3.99 < 7 0 1 356.34 358.68 13.25 o 8 0 1 5.50 6.35 2.83 o 9 0 1 177.24 172.18 9.21 o 10 0 1 540.17 516.69 19.35 o 11 0 1 166.60 178.63 10.41 o 12 0 1 32.62 39.31 4.59 o 13 0 1 2.65 -7.31 7.52 < 14 0 1 31.40 38.17 5.30 o -14 1 1 7.73 4.72 7.72 o -13 1 1 11.49 5.23 5.36 o -12 1 1 43.35 46.51 4.68 o -11 1 1 122.29 109.44 9.19 o -10 1 1 45.52 38.17 3.86 o -9 1 1 186.76 174.93 9.36 o -8 1 1 190.44 211.91 9.63 o -7 1 1 200.02 193.44 8.79 o -6 1 1 3318.14 3236.13 103.13 o -5 1 1 1777.50 2008.57 65.23 o -4 1 1 11069.48 11749.06 396.48 o -3 1 1 14063.28 14729.05 476.12 o -2 1 1 1249.88 1496.59 51.93 o -1 1 1 1953.56 2082.03 67.43 o 0 1 1 14174.77 14780.76 459.05 o 1 1 1 4859.03 5100.76 171.79 o 2 1 1 320.65 379.83 12.22 o 3 1 1 1240.07 1322.16 43.15 o 4 1 1 3999.08 4408.67 145.46 o 5 1 1 736.95 763.52 24.46 o 6 1 1 662.32 588.03 19.61 o 7 1 1 208.04 216.35 9.34 o 8 1 1 25.53 21.45 3.23 o 9 1 1 66.85 66.91 6.73 o 10 1 1 94.25 88.76 7.76 o 11 1 1 151.17 150.50 10.08 o 12 1 1 59.02 62.58 5.93 o 13 1 1 14.96 17.58 4.37 o 14 1 1 30.05 28.62 5.15 o -14 2 1 7.27 -5.51 8.58 < -13 2 1 65.14 76.32 6.43 o -12 2 1 4.19 6.49 4.20 o -11 2 1 104.32 104.46 8.69 o -10 2 1 318.05 322.21 14.11 o -9 2 1 544.76 526.12 19.33 o -8 2 1 1144.91 1100.62 35.79 o -7 2 1 2668.05 2867.94 93.94 o -6 2 1 552.87 662.44 21.94 o -5 2 1 3025.58 3080.66 97.99 o -4 2 1 2684.89 2837.67 89.67 o -3 2 1 499.20 551.88 17.74 o -2 2 1 1707.07 1758.48 55.83 o -1 2 1 267.61 280.65 9.36 o 0 2 1 590.96 601.83 21.05 o 1 2 1 370.09 365.92 11.86 o 2 2 1 33.12 37.55 3.48 o 3 2 1 77.94 95.22 4.85 o 4 2 1 3244.31 3061.17 96.72 o 5 2 1 660.24 559.76 18.60 o 6 2 1 113.62 133.73 6.79 o 7 2 1 655.92 653.62 22.20 o 8 2 1 144.52 133.49 7.81 o 9 2 1 119.53 120.33 8.11 o 10 2 1 59.71 65.17 5.30 o 11 2 1 17.77 3.77 6.93 o 12 2 1 53.60 46.52 4.91 o 13 2 1 59.05 63.28 5.46 o 14 2 1 5.44 11.18 4.82 o -13 3 1 24.69 6.33 9.48 o -12 3 1 413.98 417.68 18.29 o -11 3 1 155.62 126.47 10.29 o -10 3 1 212.10 199.12 11.17 o -9 3 1 453.28 444.74 17.23 o -8 3 1 723.87 696.99 24.09 o -7 3 1 47.15 48.35 4.27 o -6 3 1 452.31 480.43 16.78 o -5 3 1 25.57 21.30 2.47 o -4 3 1 47.68 53.33 4.26 o -3 3 1 2327.95 2400.90 76.60 o -2 3 1 1532.12 1787.49 57.79 o -1 3 1 708.19 682.81 26.61 o 0 3 1 2778.01 3096.98 105.79 o 1 3 1 2364.09 2428.02 77.08 o 2 3 1 157.98 172.85 7.02 o 3 3 1 350.95 368.25 12.73 o 4 3 1 752.35 809.59 25.99 o 5 3 1 12.79 18.61 2.48 o 6 3 1 15.75 18.75 2.74 o 7 3 1 4.45 10.53 2.85 o 8 3 1 258.98 265.23 11.79 o 9 3 1 218.39 223.70 11.01 o 10 3 1 8.38 -2.31 6.73 < 11 3 1 61.53 67.73 6.07 o 12 3 1 194.89 200.22 12.39 o 13 3 1 34.52 34.42 5.27 o -13 4 1 180.44 180.85 12.91 o -12 4 1 21.07 30.94 5.20 o -11 4 1 156.94 160.26 10.66 o -10 4 1 81.12 81.03 8.26 o -9 4 1 69.73 61.92 5.68 o -8 4 1 476.37 464.07 17.43 o -7 4 1 249.51 223.60 10.48 o -6 4 1 107.39 103.15 6.70 o -5 4 1 51.25 42.77 3.69 o -4 4 1 606.70 598.12 19.97 o -3 4 1 43.50 55.94 4.50 o -2 4 1 446.21 429.70 14.58 o -1 4 1 150.79 149.77 6.55 o 0 4 1 507.09 571.77 18.74 o 1 4 1 300.18 268.31 9.92 o 2 4 1 841.46 812.31 26.00 o 3 4 1 505.18 558.43 18.69 o 4 4 1 980.94 962.68 30.91 o 5 4 1 202.80 188.09 8.81 o 6 4 1 422.18 396.52 14.90 o 7 4 1 752.84 701.77 24.25 o 8 4 1 452.84 418.86 16.68 o 9 4 1 44.38 57.08 5.34 o 10 4 1 35.97 37.65 4.30 o 11 4 1 131.92 129.33 10.19 o 12 4 1 41.46 45.33 5.29 o 13 4 1 40.02 47.41 5.53 o -12 5 1 75.56 69.40 7.04 o -11 5 1 2.99 4.37 4.28 o -10 5 1 41.38 42.14 4.53 o -9 5 1 194.69 197.69 10.93 o -8 5 1 461.95 445.86 17.38 o -7 5 1 88.11 92.34 7.73 o -6 5 1 272.45 261.45 11.32 o -5 5 1 130.21 136.83 7.60 o -4 5 1 180.62 201.39 8.91 o -3 5 1 944.26 912.86 29.54 o -2 5 1 622.09 651.01 21.60 o -1 5 1 356.68 406.23 14.36 o 0 5 1 22.47 33.33 3.24 o 1 5 1 257.98 258.98 10.19 o 2 5 1 161.03 172.88 7.89 o 3 5 1 1501.47 1528.01 53.35 o 4 5 1 414.14 430.22 15.73 o 5 5 1 113.61 127.56 7.75 o 6 5 1 313.05 320.01 13.33 o 7 5 1 233.96 230.60 11.08 o 8 5 1 507.72 507.16 19.54 o 9 5 1 265.71 261.82 13.11 o 10 5 1 1.14 6.74 6.91 o 11 5 1 4.51 0.01 7.60 o 12 5 1 36.50 36.53 5.20 o -11 6 1 25.07 31.15 5.22 o -10 6 1 44.75 45.07 4.95 o -9 6 1 72.97 73.24 6.10 o -8 6 1 203.94 203.79 11.00 o -7 6 1 249.44 263.20 12.13 o -6 6 1 5.12 -6.48 5.94 < -5 6 1 99.24 101.14 7.23 o -4 6 1 315.54 334.48 13.31 o -3 6 1 375.75 342.53 13.40 o -2 6 1 445.13 384.76 14.51 o -1 6 1 283.85 296.15 11.99 o 0 6 1 23.90 28.46 3.21 o 1 6 1 580.99 577.30 20.14 o 2 6 1 1588.14 1615.00 51.08 o 3 6 1 268.91 265.26 11.39 o 4 6 1 1096.73 1049.70 34.51 o 5 6 1 336.47 327.12 13.47 o 6 6 1 50.88 50.49 4.22 o 7 6 1 279.25 256.03 12.53 o 8 6 1 283.25 299.83 14.11 o 9 6 1 12.70 -2.13 7.44 < 10 6 1 52.61 54.98 5.13 o 11 6 1 15.57 26.00 4.91 o -10 7 1 40.03 29.46 5.22 o -9 7 1 78.55 80.69 6.65 o -8 7 1 38.50 35.23 4.44 o -7 7 1 15.12 21.21 4.04 o -6 7 1 144.37 147.36 9.30 o -5 7 1 72.10 75.55 7.37 o -4 7 1 163.02 162.06 9.06 o -3 7 1 552.90 509.94 18.99 o -2 7 1 202.55 211.44 10.60 o -1 7 1 424.84 408.53 15.90 o 0 7 1 1237.98 1234.44 40.20 o 1 7 1 399.02 415.16 16.12 o 2 7 1 87.75 89.34 7.63 o 3 7 1 275.51 288.05 12.69 o 4 7 1 263.72 262.15 11.75 o 5 7 1 127.88 113.97 8.44 o 6 7 1 200.72 206.32 11.44 o 7 7 1 135.88 123.51 9.78 o 8 7 1 6.83 1.53 7.58 o 9 7 1 205.47 205.72 12.79 o 10 7 1 25.71 24.72 5.23 o -9 8 1 1.54 -2.31 8.42 < -8 8 1 67.56 74.63 6.60 o -7 8 1 71.29 67.43 6.29 o -6 8 1 73.59 75.60 6.14 o -5 8 1 236.56 208.43 11.72 o -4 8 1 297.01 290.06 13.33 o -3 8 1 1.50 5.76 3.75 o -2 8 1 27.90 31.71 3.91 o -1 8 1 295.92 262.29 12.80 o 0 8 1 2.64 3.83 6.76 o 1 8 1 103.45 93.77 8.43 o 2 8 1 7.19 2.84 6.47 o 3 8 1 26.03 27.45 4.03 o 4 8 1 34.16 39.86 4.14 o 5 8 1 248.18 249.29 12.60 o 6 8 1 49.66 60.25 5.86 o 7 8 1 55.01 51.68 5.06 o 8 8 1 82.84 87.36 7.18 o 9 8 1 6.73 9.37 4.93 o -7 9 1 8.24 10.86 4.96 o -6 9 1 128.58 140.49 10.99 o -5 9 1 54.49 55.41 5.19 o -4 9 1 90.66 91.06 9.10 o -3 9 1 80.53 73.25 6.30 o -2 9 1 36.30 33.99 4.46 o -1 9 1 8.61 13.98 4.14 o 0 9 1 326.02 322.89 14.77 o 1 9 1 41.13 49.64 4.69 o 2 9 1 23.84 21.87 4.32 o 3 9 1 58.10 58.85 6.03 o 4 9 1 66.75 70.54 6.29 o 5 9 1 18.38 17.49 4.44 o 6 9 1 47.06 51.28 5.15 o 7 9 1 0.16 -11.39 8.34 < -3 10 1 1.90 3.04 8.13 o -2 10 1 24.53 25.76 4.75 o -1 10 1 154.58 181.52 11.81 o 0 10 1 0.43 -0.64 7.97 < 1 10 1 100.88 113.48 10.24 o 2 10 1 33.30 31.61 5.15 o 3 10 1 7.03 4.98 4.76 o -14 0 2 0.60 -7.74 8.21 < -13 0 2 2.06 6.10 7.17 o -12 0 2 50.68 55.30 5.65 o -11 0 2 297.61 282.54 13.45 o -10 0 2 1.96 5.17 3.60 o -9 0 2 127.18 126.99 7.91 o -8 0 2 296.72 263.81 10.98 o -7 0 2 0.50 0.08 4.19 o -6 0 2 421.60 436.66 15.00 o -5 0 2 1512.67 1580.46 52.40 o -4 0 2 3247.65 3835.57 127.17 o -3 0 2 76.20 93.99 4.38 o -2 0 2 725.50 782.75 25.76 o -1 0 2 272.51 329.79 11.57 o 0 0 2 19808.16 20326.41 624.13 o 1 0 2 1535.91 1685.22 55.71 o 2 0 2 33.71 24.29 1.90 o 3 0 2 696.66 822.71 28.19 o 4 0 2 599.78 715.73 22.73 o 5 0 2 142.02 189.37 7.69 o 6 0 2 931.05 896.90 28.75 o 7 0 2 7.03 8.92 2.61 o 8 0 2 1.78 6.93 2.88 o 9 0 2 130.56 131.70 8.24 o 10 0 2 334.85 332.52 13.97 o 11 0 2 380.25 369.12 15.95 o 12 0 2 120.21 112.76 9.39 o 13 0 2 30.82 35.87 4.77 o 14 0 2 1.33 3.18 8.32 o -14 1 2 15.41 4.63 8.66 o -13 1 2 18.64 17.84 4.51 o -12 1 2 23.45 26.85 4.18 o -11 1 2 76.92 79.43 5.96 o -10 1 2 484.95 505.66 18.77 o -9 1 2 14.86 23.23 3.31 o -8 1 2 163.19 156.97 8.29 o -7 1 2 1707.53 1867.20 63.40 o -6 1 2 736.57 680.66 22.28 o -5 1 2 1082.89 987.63 34.98 o -4 1 2 3808.93 4123.59 136.24 o -3 1 2 2000.14 1995.80 63.10 o -2 1 2 2043.27 2169.86 72.64 o -1 1 2 546.04 547.44 18.53 o 0 1 2 174.99 155.49 5.36 o 1 1 2 1802.71 1835.44 61.36 o 2 1 2 3934.21 4285.97 136.97 o 3 1 2 479.10 445.00 14.54 o 4 1 2 413.26 382.38 12.97 o 5 1 2 2300.77 2262.10 73.30 o 6 1 2 404.63 450.50 15.65 o 7 1 2 739.29 714.44 23.79 o 8 1 2 290.99 291.84 11.95 o 9 1 2 69.45 69.65 6.66 o 10 1 2 174.07 167.44 9.60 o 11 1 2 188.63 191.10 10.94 o 12 1 2 45.41 48.33 4.70 o 13 1 2 16.38 20.42 4.53 o 14 1 2 24.38 25.60 5.19 o -14 2 2 13.01 10.40 5.02 o -13 2 2 23.31 26.26 4.81 o -12 2 2 108.48 121.19 9.80 o -11 2 2 217.68 207.66 11.32 o -10 2 2 271.22 267.35 12.62 o -9 2 2 468.25 470.30 17.68 o -8 2 2 593.83 563.07 19.93 o -7 2 2 46.55 46.33 4.11 o -6 2 2 2855.79 2816.21 91.10 o -5 2 2 318.34 302.91 11.05 o -4 2 2 2628.84 2692.88 85.26 o -3 2 2 1465.55 1478.74 48.21 o -2 2 2 3466.41 3479.19 114.49 o -1 2 2 1389.81 1613.25 51.33 o 0 2 2 391.66 381.37 12.40 o 1 2 2 1550.96 1581.87 50.47 o 2 2 2 2668.84 2969.31 99.73 o 3 2 2 772.80 856.09 30.18 o 4 2 2 1047.33 952.23 33.84 o 5 2 2 112.94 112.37 6.04 o 6 2 2 264.85 241.61 9.81 o 7 2 2 267.76 291.05 11.68 o 8 2 2 111.85 128.99 7.79 o 9 2 2 90.56 85.68 7.37 o 10 2 2 117.83 114.00 8.57 o 11 2 2 47.61 52.26 4.51 o 12 2 2 59.99 63.88 6.29 o 13 2 2 59.53 54.71 5.65 o 14 2 2 24.83 33.85 5.28 o -13 3 2 214.27 194.79 13.11 o -12 3 2 26.89 15.50 4.91 o -11 3 2 235.07 211.66 11.90 o -10 3 2 362.47 352.47 15.14 o -9 3 2 230.54 198.59 10.40 o -8 3 2 524.37 451.94 16.93 o -7 3 2 720.09 725.21 24.44 o -6 3 2 621.17 617.52 20.79 o -5 3 2 249.62 240.23 9.41 o -4 3 2 485.78 493.03 16.45 o -3 3 2 1284.04 1399.22 46.79 o -2 3 2 2379.81 2589.81 82.00 o -1 3 2 218.62 258.18 9.18 o 0 3 2 120.17 134.63 5.83 o 1 3 2 2773.53 2844.30 97.86 o 2 3 2 1150.17 1212.05 40.77 o 3 3 2 79.89 75.75 4.75 o 4 3 2 1295.95 1320.12 45.65 o 5 3 2 90.36 90.94 5.74 o 6 3 2 272.34 247.14 10.39 o 7 3 2 81.56 91.05 6.52 o 8 3 2 223.07 206.75 10.18 o 9 3 2 18.51 21.13 3.69 o 10 3 2 81.51 84.40 8.13 o 11 3 2 20.58 19.29 4.17 o 12 3 2 110.10 109.89 9.90 o 13 3 2 79.57 102.71 10.18 o -13 4 2 16.75 11.55 5.38 o -12 4 2 248.84 230.03 13.34 o -11 4 2 6.29 6.92 4.27 o -10 4 2 28.13 25.40 4.03 o -9 4 2 373.49 366.74 15.17 o -8 4 2 530.69 519.87 19.10 o -7 4 2 561.52 529.60 18.99 o -6 4 2 64.62 63.06 5.93 o -5 4 2 847.76 799.44 26.21 o -4 4 2 33.28 31.90 2.69 o -3 4 2 2401.67 2458.37 79.60 o -2 4 2 1752.61 1876.11 61.80 o -1 4 2 871.55 978.54 34.83 o 0 4 2 93.63 107.02 5.56 o 1 4 2 1536.19 1532.01 51.65 o 2 4 2 0.60 1.01 2.38 o 3 4 2 460.68 428.00 14.82 o 4 4 2 452.62 476.03 16.61 o 5 4 2 63.24 80.78 5.81 o 6 4 2 138.51 146.73 8.18 o 7 4 2 410.44 401.29 15.38 o 8 4 2 438.60 442.87 17.07 o 9 4 2 384.89 385.72 16.22 o 10 4 2 16.22 9.27 4.07 o 11 4 2 61.45 65.10 6.20 o 12 4 2 92.20 103.34 10.18 o 13 4 2 43.92 44.21 5.56 o -12 5 2 2.64 7.79 4.72 o -11 5 2 18.83 18.56 4.36 o -10 5 2 14.93 15.82 4.17 o -9 5 2 83.39 86.07 8.07 o -8 5 2 218.29 225.20 11.34 o -7 5 2 446.07 408.88 15.93 o -6 5 2 23.43 21.87 3.22 o -5 5 2 69.71 86.53 6.27 o -4 5 2 750.98 748.97 24.87 o -3 5 2 204.79 193.92 8.69 o -2 5 2 1000.93 1001.53 32.06 o -1 5 2 281.79 298.15 11.19 o 0 5 2 398.49 422.91 15.04 o 1 5 2 488.44 466.44 16.39 o 2 5 2 1635.86 1630.82 56.68 o 3 5 2 68.71 58.51 5.49 o 4 5 2 2311.25 2311.40 71.81 o 5 5 2 378.78 386.15 14.86 o 6 5 2 184.83 187.33 9.56 o 7 5 2 336.02 343.02 14.34 o 8 5 2 918.03 903.70 31.16 o 9 5 2 30.16 28.09 4.47 o 10 5 2 25.27 24.52 4.37 o 11 5 2 4.98 7.47 7.58 o 12 5 2 18.92 21.74 5.05 o -11 6 2 4.46 -8.83 8.38 < -10 6 2 52.22 61.78 5.06 o -9 6 2 67.95 65.25 5.80 o -8 6 2 133.65 115.82 9.23 o -7 6 2 59.64 59.76 5.22 o -6 6 2 29.20 28.70 3.60 o -5 6 2 87.08 85.22 6.75 o -4 6 2 254.85 280.27 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