#------------------------------------------------------------------------------ #$Date: 2016-04-02 20:32:48 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180754 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/00/75/2007514.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2007514_Fobs loop_ _publ_author_name 'Barnes, J. C.' 'Weakley, T. J. R.' _publ_section_title ; Racemic 2-Hydroxy-2-phenylpropanamidinium Chloride and (S)-2-Hydroxy-2-phenylbutanamidinium (R)-2-Hydroxy-2-phenylethanoate ; _journal_issue 8 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 1170 _journal_page_last 1173 _journal_volume 54 _journal_year 1998 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 108.375 _cell_angle_gamma 90.000 _cell_length_a 8.8847 _cell_length_b 10.4830 _cell_length_c 11.6776 _exptl_crystal_F_000 424.00 _reflns_d_resolution_high 0.8418 _cod_data_source_file fg1392jcb33sup2.hkl _cod_data_source_block jcb33 #BEGIN Tags that were not found in dictionaries: _shelx_title ' atrolactamidinium chloride jcb33' _shelx_refln_list_code 4 _shelx_f_calc_maximum 147.57 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x+1/2, -y+1/2, z+1/2' '-x, -y, -z' '-x-1/2, y-1/2, -z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 6371.19 7167.81 47.66 o 4 0 0 66.48 79.99 2.20 o 6 0 0 783.61 771.00 7.64 o 8 0 0 13.40 11.47 1.21 o 10 0 0 21.51 20.63 1.64 o 1 1 0 229.58 197.14 1.44 o 2 1 0 228.28 225.63 2.52 o 3 1 0 375.56 382.34 3.76 o 4 1 0 193.02 232.64 3.46 o 5 1 0 416.87 383.35 4.93 o 6 1 0 28.46 19.32 1.08 o 7 1 0 7.47 7.13 1.15 o 8 1 0 82.39 82.24 3.85 o 9 1 0 6.47 9.45 1.30 o 0 2 0 117.55 122.62 1.71 o 1 2 0 21775.67 23600.04 251.60 o 2 2 0 2107.25 2104.81 7.69 o 3 2 0 1964.45 2042.96 8.73 o 4 2 0 216.74 244.00 3.66 o 5 2 0 162.90 133.77 3.30 o 6 2 0 81.15 85.46 3.23 o 7 2 0 174.50 171.47 4.47 o 8 2 0 10.60 8.87 1.22 o 9 2 0 99.76 111.89 4.56 o 1 3 0 164.61 182.60 1.84 o 2 3 0 7143.45 7771.67 62.72 o 3 3 0 108.93 87.71 2.38 o 4 3 0 68.16 72.61 2.56 o 5 3 0 18.23 5.46 0.92 o 6 3 0 1.22 -2.40 2.40 o 7 3 0 95.53 104.60 3.88 o 8 3 0 22.83 23.06 1.39 o 9 3 0 9.16 8.77 1.43 o 0 4 0 18079.09 20365.45 102.90 o 1 4 0 814.13 794.91 15.19 o 2 4 0 2003.25 2061.32 9.33 o 3 4 0 192.22 224.61 3.64 o 4 4 0 292.82 286.94 4.45 o 5 4 0 62.83 60.22 2.90 o 6 4 0 543.84 520.12 7.09 o 7 4 0 132.31 110.53 4.20 o 8 4 0 46.89 50.41 2.50 o 9 4 0 36.31 34.43 1.71 o 1 5 0 294.62 234.85 2.98 o 2 5 0 1.37 3.38 0.82 o 3 5 0 406.23 459.40 5.39 o 4 5 0 3.75 0.32 2.07 o 5 5 0 5.06 6.36 1.14 o 6 5 0 195.32 188.57 4.77 o 7 5 0 18.45 14.58 1.34 o 8 5 0 20.61 26.80 1.61 o 9 5 0 18.90 16.21 1.71 o 0 6 0 3.72 6.76 0.87 o 1 6 0 3662.27 3777.53 54.14 o 2 6 0 1344.38 1375.28 9.27 o 3 6 0 616.12 601.80 6.61 o 4 6 0 533.75 537.39 6.75 o 5 6 0 58.98 56.90 2.85 o 6 6 0 2.22 2.09 2.54 o 7 6 0 91.25 100.32 4.30 o 8 6 0 104.57 100.50 4.56 o 1 7 0 84.46 92.96 2.23 o 2 7 0 1044.39 997.30 8.68 o 3 7 0 5.24 4.61 1.20 o 4 7 0 3.06 -1.79 2.72 o 5 7 0 23.29 21.70 1.43 o 6 7 0 10.24 14.12 1.42 o 7 7 0 72.11 79.92 3.97 o 8 7 0 8.79 11.93 1.52 o 0 8 0 241.48 242.92 4.86 o 1 8 0 542.37 515.82 4.74 o 2 8 0 425.27 394.95 6.25 o 3 8 0 480.68 478.58 6.89 o 4 8 0 306.38 297.20 6.05 o 5 8 0 178.71 184.61 5.35 o 6 8 0 57.58 67.96 3.07 o 7 8 0 12.40 7.58 1.62 o 1 9 0 352.47 330.81 4.23 o 2 9 0 0.92 1.36 2.77 o 3 9 0 228.64 233.53 5.46 o 4 9 0 43.00 45.04 2.35 o 5 9 0 3.16 2.88 1.41 o 6 9 0 19.53 21.71 1.68 o 0 10 0 91.35 88.12 3.89 o 1 10 0 72.12 80.63 2.73 o 2 10 0 285.13 259.57 5.97 o 3 10 0 63.39 59.26 2.72 o 4 10 0 213.40 219.71 5.92 o 5 10 0 55.60 59.62 2.74 o 1 11 0 1.89 1.27 1.22 o 2 11 0 60.98 46.62 2.51 o 3 11 0 9.99 12.64 1.52 o 4 11 0 20.10 22.04 1.68 o 0 12 0 57.16 60.54 2.95 o 1 12 0 72.21 71.09 2.51 o 2 12 0 22.85 24.38 1.75 o -9 0 1 5.32 4.58 1.22 o -7 0 1 379.38 390.56 6.04 o -5 0 1 180.64 151.11 3.20 o -3 0 1 786.96 784.33 5.00 o -1 0 1 495.01 466.88 1.66 o 1 0 1 5235.56 5292.57 28.08 o 3 0 1 3749.26 3548.70 11.31 o 5 0 1 692.32 774.68 6.99 o 7 0 1 147.43 142.47 4.24 o 9 0 1 32.49 29.72 1.66 o -10 1 1 74.76 70.36 3.32 o -9 1 1 48.60 52.35 2.68 o -8 1 1 165.06 154.89 4.49 o -7 1 1 247.19 251.98 5.02 o -6 1 1 335.68 354.17 5.29 o -5 1 1 716.36 766.50 6.65 o -4 1 1 333.85 351.89 4.05 o -3 1 1 3648.65 3547.97 10.65 o -2 1 1 38.60 32.01 1.34 o -1 1 1 500.89 489.42 9.99 o 0 1 1 718.25 676.81 7.16 o 1 1 1 106.45 91.58 1.27 o 2 1 1 196.76 196.15 2.60 o 3 1 1 134.73 132.47 2.53 o 4 1 1 155.58 143.94 2.99 o 5 1 1 70.62 74.08 2.70 o 6 1 1 7.53 8.18 1.08 o 7 1 1 105.50 98.24 3.91 o 8 1 1 23.62 24.64 1.42 o 9 1 1 8.97 7.01 1.36 o -10 2 1 11.04 10.33 1.47 o -9 2 1 2.08 3.34 1.21 o -8 2 1 133.08 124.90 4.34 o -7 2 1 27.33 31.24 1.54 o -6 2 1 38.77 33.54 1.68 o -5 2 1 425.86 438.68 5.26 o -4 2 1 211.98 207.58 3.35 o -3 2 1 80.07 92.13 2.17 o -2 2 1 74.96 74.04 1.89 o -1 2 1 627.63 544.83 8.75 o 0 2 1 2627.90 2784.05 40.35 o 1 2 1 409.43 393.91 2.26 o 2 2 1 5713.94 5822.52 51.77 o 3 2 1 348.00 369.40 4.08 o 4 2 1 1720.68 1746.08 9.56 o 5 2 1 26.93 30.68 1.73 o 6 2 1 94.68 76.72 3.35 o 7 2 1 48.01 52.97 2.63 o 8 2 1 9.53 6.63 1.21 o 9 2 1 2.54 2.70 1.35 o -9 3 1 58.31 71.89 3.34 o -8 3 1 134.53 128.39 4.34 o -7 3 1 207.80 198.31 4.70 o -6 3 1 483.54 515.63 6.56 o -5 3 1 28.69 35.69 1.74 o -4 3 1 2831.56 2990.07 12.39 o -3 3 1 20.94 16.76 0.71 o -2 3 1 1.19 6.56 0.62 o -1 3 1 139.39 154.07 1.71 o 0 3 1 1317.14 1361.62 12.19 o 1 3 1 309.39 259.80 2.16 o 2 3 1 407.18 391.69 4.04 o 3 3 1 556.70 619.56 5.46 o 4 3 1 0.08 1.52 0.79 o 5 3 1 150.56 142.40 3.64 o 6 3 1 0.15 1.59 2.21 o 7 3 1 169.87 172.32 4.81 o 8 3 1 1.55 -0.11 2.57 o 9 3 1 11.43 10.75 1.42 o -9 4 1 4.55 2.46 2.99 o -8 4 1 16.12 14.05 1.28 o -7 4 1 44.37 41.21 1.93 o -6 4 1 24.62 29.15 1.48 o -5 4 1 68.27 80.19 2.98 o -4 4 1 28.47 18.76 1.04 o -3 4 1 0.54 -0.84 1.49 o -2 4 1 82.74 85.07 2.31 o -1 4 1 120.79 97.22 3.07 o 0 4 1 727.98 782.24 5.79 o 1 4 1 39.47 24.37 0.81 o 2 4 1 1.56 0.85 0.69 o 3 4 1 1064.94 976.87 7.28 o 4 4 1 2.25 2.39 0.95 o 5 4 1 258.56 301.91 5.22 o 6 4 1 36.23 36.25 1.56 o 7 4 1 19.42 17.51 1.41 o 8 4 1 30.40 33.83 1.77 o 9 4 1 5.95 3.67 1.49 o -9 5 1 165.66 181.14 5.85 o -8 5 1 10.08 10.46 1.32 o -7 5 1 299.33 324.74 6.21 o -6 5 1 1.81 0.00 2.52 o -5 5 1 505.60 519.81 6.61 o -4 5 1 97.44 113.14 3.35 o -3 5 1 838.51 855.95 7.11 o -2 5 1 0.08 -1.18 1.60 o -1 5 1 47.52 42.55 3.32 o 0 5 1 1261.35 1199.23 21.05 o 1 5 1 15.06 16.05 0.59 o 2 5 1 771.15 815.84 6.76 o 3 5 1 0.14 1.39 1.85 o 4 5 1 609.68 547.68 6.54 o 5 5 1 10.66 9.49 1.24 o 6 5 1 252.76 266.55 5.71 o 7 5 1 10.10 11.11 1.39 o 8 5 1 2.40 5.88 1.38 o -8 6 1 5.77 4.39 1.38 o -7 6 1 1.42 3.54 1.27 o -6 6 1 0.02 0.56 2.56 o -5 6 1 107.49 84.83 3.66 o -4 6 1 345.51 367.60 5.68 o -3 6 1 0.21 0.95 2.02 o -2 6 1 508.50 487.47 5.72 o -1 6 1 6.54 6.70 0.61 o 0 6 1 154.02 193.92 2.60 o 1 6 1 468.88 462.10 13.48 o 2 6 1 2.95 0.65 0.97 o 3 6 1 30.73 25.05 1.24 o 4 6 1 186.13 189.09 4.54 o 5 6 1 23.86 20.84 1.41 o 6 6 1 3.94 1.67 2.77 o 7 6 1 42.36 41.80 2.37 o 8 6 1 19.43 21.29 1.60 o -8 7 1 56.21 73.02 3.28 o -7 7 1 21.55 20.26 1.50 o -6 7 1 207.15 222.00 5.43 o -5 7 1 38.15 37.47 1.98 o -4 7 1 1051.14 1039.21 9.58 o -3 7 1 0.40 0.91 1.09 o -2 7 1 275.56 269.37 4.87 o -1 7 1 10.57 9.41 0.74 o 0 7 1 0.07 17.17 8.77 o 1 7 1 249.33 230.26 3.15 o 2 7 1 45.98 56.83 2.74 o 3 7 1 12.49 18.22 1.32 o 4 7 1 18.94 19.20 1.48 o 5 7 1 271.78 264.84 5.77 o 6 7 1 45.15 45.50 2.49 o 7 7 1 30.73 36.72 1.72 o 8 7 1 7.02 7.22 1.54 o -7 8 1 0.80 2.34 2.83 o -6 8 1 151.44 136.59 4.87 o -5 8 1 46.05 48.21 2.33 o -4 8 1 53.22 44.96 2.25 o -3 8 1 0.34 3.03 1.24 o -2 8 1 0.06 0.56 2.48 o -1 8 1 144.85 131.45 2.79 o 0 8 1 165.41 165.39 5.62 o 1 8 1 168.28 165.98 3.01 o 2 8 1 84.34 79.28 3.74 o 3 8 1 0.07 0.43 2.85 o 4 8 1 89.45 86.41 4.05 o 5 8 1 16.28 16.29 1.53 o 6 8 1 33.90 33.27 1.75 o 7 8 1 21.76 22.02 1.74 o -7 9 1 98.31 114.89 4.90 o -6 9 1 13.79 13.67 1.50 o -5 9 1 228.22 226.80 6.00 o -4 9 1 65.47 66.70 3.34 o -3 9 1 135.91 135.70 4.40 o -2 9 1 263.38 244.34 5.33 o -1 9 1 18.81 16.18 0.94 o 0 9 1 24.78 26.62 1.00 o 1 9 1 7.52 12.85 1.65 o 2 9 1 406.60 391.60 6.71 o 3 9 1 0.71 1.45 2.75 o 4 9 1 102.35 92.74 4.21 o 5 9 1 0.08 3.38 1.41 o 6 9 1 45.42 51.79 2.76 o -6 10 1 20.85 19.21 1.76 o -5 10 1 2.31 5.05 1.50 o -4 10 1 5.86 1.92 3.12 o -3 10 1 97.18 99.95 4.34 o -2 10 1 71.73 69.83 3.35 o -1 10 1 20.52 25.10 1.00 o 0 10 1 39.75 38.11 1.67 o 1 10 1 0.68 0.74 1.10 o 2 10 1 17.16 16.95 1.57 o 3 10 1 1.81 0.77 2.93 o 4 10 1 19.81 23.15 1.61 o 5 10 1 5.16 6.39 1.59 o -4 11 1 3.81 4.91 1.56 o -3 11 1 3.04 6.29 1.46 o -2 11 1 83.02 88.06 3.77 o -1 11 1 1.58 2.11 1.18 o 0 11 1 19.32 21.92 1.04 o 1 11 1 5.91 6.65 0.95 o 2 11 1 41.93 34.24 1.74 o 3 11 1 0.34 0.74 3.27 o 4 11 1 8.60 8.58 1.63 o -2 12 1 0.67 1.84 3.26 o -1 12 1 15.16 16.07 2.49 o 0 12 1 69.82 65.61 2.87 o 1 12 1 1.77 2.02 1.34 o 2 12 1 0.87 -3.33 3.33 o -10 0 2 9.13 9.34 1.41 o -8 0 2 259.52 271.56 5.56 o -6 0 2 304.03 355.50 5.19 o -4 0 2 1202.72 1250.26 7.28 o -2 0 2 1367.21 1273.81 5.39 o 0 0 2 2073.92 2279.87 28.95 o 2 0 2 968.76 997.63 5.64 o 4 0 2 817.17 735.96 6.37 o 6 0 2 3149.08 3062.52 15.88 o 8 0 2 574.07 612.13 8.68 o -10 1 2 31.00 35.57 1.84 o -9 1 2 122.98 133.91 4.59 o -8 1 2 405.19 374.96 6.39 o -7 1 2 35.17 36.86 1.87 o -6 1 2 412.63 379.76 5.40 o -5 1 2 569.21 501.95 5.41 o -4 1 2 28.28 14.50 0.75 o -3 1 2 403.31 395.41 3.73 o -2 1 2 462.80 504.24 3.61 o -1 1 2 62.04 41.13 1.84 o 0 1 2 513.92 595.45 3.69 o 1 1 2 1263.28 1319.56 4.00 o 2 1 2 21.00 14.85 0.73 o 3 1 2 750.54 736.49 5.72 o 4 1 2 481.72 441.84 5.11 o 5 1 2 215.16 181.07 3.95 o 6 1 2 310.00 299.22 5.42 o 7 1 2 61.08 64.35 3.02 o 8 1 2 74.43 68.66 3.23 o 9 1 2 5.97 5.73 1.40 o -10 2 2 4.15 3.65 1.33 o -9 2 2 2.98 5.72 1.20 o -8 2 2 52.85 50.23 2.34 o -7 2 2 125.42 116.80 3.77 o -6 2 2 54.78 54.69 2.38 o -5 2 2 485.95 571.86 5.90 o -4 2 2 179.60 175.86 3.08 o -3 2 2 3469.45 3448.07 11.14 o -2 2 2 571.45 558.84 4.13 o -1 2 2 30.91 24.52 0.83 o 0 2 2 244.48 223.30 1.81 o 1 2 2 161.09 171.67 1.87 o 2 2 2 2.03 1.98 0.61 o 3 2 2 439.13 467.53 4.79 o 4 2 2 721.49 720.18 6.57 o 5 2 2 1220.41 1115.40 9.02 o 6 2 2 57.91 56.74 2.69 o 7 2 2 1652.66 1656.82 13.04 o 8 2 2 0.40 1.37 1.21 o 9 2 2 93.05 97.51 4.78 o -10 3 2 2.02 0.67 2.80 o -9 3 2 59.04 56.73 2.92 o -8 3 2 161.62 163.49 4.68 o -7 3 2 191.62 177.06 4.58 o -6 3 2 200.37 203.74 4.36 o -5 3 2 226.66 209.59 3.98 o -4 3 2 20.90 46.62 2.10 o -3 3 2 14.68 9.24 0.67 o -2 3 2 232.63 243.37 3.09 o -1 3 2 3819.34 4292.99 83.46 o 0 3 2 875.12 900.78 3.80 o 1 3 2 2433.47 2566.89 14.92 o 2 3 2 222.22 229.90 3.40 o 3 3 2 0.72 1.52 1.60 o 4 3 2 525.01 504.29 5.82 o 5 3 2 254.75 235.09 4.72 o 6 3 2 63.13 66.26 2.98 o 7 3 2 125.50 125.25 4.36 o 8 3 2 15.63 19.88 1.44 o 9 3 2 5.35 0.40 2.98 o -9 4 2 5.85 5.95 1.30 o -8 4 2 47.96 46.08 2.32 o -7 4 2 37.50 30.82 1.56 o -6 4 2 98.60 115.11 3.74 o -5 4 2 16.26 15.96 1.03 o -4 4 2 370.06 386.88 4.92 o -3 4 2 54.51 57.30 2.15 o -2 4 2 220.21 217.05 3.29 o -1 4 2 301.29 314.64 6.55 o 0 4 2 709.64 759.47 10.66 o 1 4 2 49.02 38.83 1.24 o 2 4 2 39.41 43.16 1.85 o 3 4 2 231.95 211.85 3.90 o 4 4 2 448.49 442.58 5.82 o 5 4 2 121.57 117.83 3.88 o 6 4 2 1161.34 1174.58 10.80 o 7 4 2 9.21 10.26 1.36 o 8 4 2 269.10 285.31 6.66 o -9 5 2 20.66 21.83 1.61 o -8 5 2 53.60 54.76 2.54 o -7 5 2 68.31 90.73 3.84 o -6 5 2 107.47 103.80 3.85 o -5 5 2 489.79 461.53 6.24 o -4 5 2 164.57 159.52 3.77 o -3 5 2 35.18 46.89 2.32 o -2 5 2 613.99 574.68 5.61 o -1 5 2 526.56 553.64 14.06 o 0 5 2 800.88 823.76 9.88 o 1 5 2 43.20 41.59 1.38 o 2 5 2 225.74 218.66 4.00 o 3 5 2 74.42 66.15 2.91 o 4 5 2 305.01 289.87 5.08 o 5 5 2 269.50 289.71 5.51 o 6 5 2 72.93 55.84 2.85 o 7 5 2 12.76 17.31 1.49 o 8 5 2 10.13 7.05 1.52 o -9 6 2 8.55 7.29 1.53 o -8 6 2 51.96 52.95 2.57 o -7 6 2 5.90 5.34 1.27 o -6 6 2 14.82 11.98 1.29 o -5 6 2 6.00 9.53 1.21 o -4 6 2 2.06 5.51 1.07 o -3 6 2 9.22 8.00 0.99 o -2 6 2 602.87 617.23 6.36 o -1 6 2 19.15 23.62 0.75 o 0 6 2 9.50 9.00 0.64 o 1 6 2 809.77 832.38 5.61 o 2 6 2 63.27 60.59 2.86 o 3 6 2 885.88 937.22 8.60 o 4 6 2 477.85 420.68 6.42 o 5 6 2 242.22 225.50 5.33 o 6 6 2 50.92 53.09 2.56 o 7 6 2 345.41 347.36 7.19 o 8 6 2 21.48 25.12 1.79 o -8 7 2 11.08 12.26 1.54 o -7 7 2 252.99 244.12 6.05 o -6 7 2 78.82 90.91 3.96 o -5 7 2 127.28 128.87 4.39 o -4 7 2 0.06 2.06 1.17 o -3 7 2 7.50 7.26 1.14 o -2 7 2 4.04 5.47 1.03 o -1 7 2 571.56 581.10 11.54 o 0 7 2 1.84 4.18 1.38 o 1 7 2 202.59 196.03 3.02 o 2 7 2 1.79 2.36 2.54 o 3 7 2 15.46 14.90 1.40 o 4 7 2 299.82 308.89 5.97 o 5 7 2 237.36 226.30 5.68 o 6 7 2 1.55 2.79 3.05 o 7 7 2 79.20 75.01 3.90 o -8 8 2 0.65 1.90 2.95 o -7 8 2 12.17 9.32 1.51 o -6 8 2 0.75 -1.29 2.64 o -5 8 2 12.78 10.27 1.34 o -4 8 2 12.79 10.28 1.31 o -3 8 2 16.33 13.35 1.31 o -2 8 2 148.69 147.75 4.25 o -1 8 2 177.29 171.86 4.51 o 0 8 2 98.69 100.58 4.18 o 1 8 2 58.87 58.85 1.98 o 2 8 2 58.33 73.28 3.20 o 3 8 2 272.36 272.54 5.66 o 4 8 2 270.18 289.28 6.22 o 5 8 2 419.40 413.11 7.41 o 6 8 2 123.31 128.14 4.92 o 7 8 2 14.10 17.65 1.75 o -7 9 2 3.66 3.64 1.56 o -6 9 2 40.28 40.90 1.89 o -5 9 2 34.05 31.37 1.62 o -4 9 2 94.56 92.52 4.13 o -3 9 2 106.96 109.38 4.03 o -2 9 2 96.37 92.16 3.85 o -1 9 2 89.38 89.31 2.63 o 0 9 2 216.06 233.83 5.02 o 1 9 2 96.37 97.46 2.74 o 2 9 2 192.54 177.71 5.01 o 3 9 2 66.55 65.70 3.28 o 4 9 2 46.67 49.18 2.44 o 5 9 2 27.17 30.51 1.70 o 6 9 2 23.88 22.60 1.81 o -6 10 2 0.91 0.39 3.23 o -5 10 2 1.53 -1.70 2.88 o -4 10 2 55.51 48.25 2.48 o -3 10 2 1.41 1.35 1.30 o -2 10 2 9.95 8.51 1.34 o -1 10 2 11.65 12.38 0.93 o 0 10 2 26.85 30.25 1.09 o 1 10 2 89.14 91.90 2.83 o 2 10 2 223.33 237.18 5.98 o 3 10 2 53.66 68.57 3.46 o 4 10 2 71.72 69.17 3.25 o 5 10 2 8.49 10.65 1.68 o -4 11 2 1.68 2.14 3.06 o -3 11 2 143.39 127.63 5.09 o -2 11 2 0.17 -0.94 3.04 o -1 11 2 48.64 46.89 1.74 o 0 11 2 1.53 1.84 2.01 o 1 11 2 45.18 42.38 1.49 o 2 11 2 37.00 37.18 2.10 o 3 11 2 157.43 145.35 5.41 o -2 12 2 8.56 8.99 1.56 o -1 12 2 78.87 83.54 3.37 o 0 12 2 12.08 14.21 1.07 o 1 12 2 21.45 28.05 1.85 o -9 0 3 183.92 188.75 5.22 o -7 0 3 34.02 31.67 1.47 o -5 0 3 2260.90 2362.88 11.34 o -3 0 3 968.97 934.08 5.71 o -1 0 3 13510.89 14197.21 49.55 o 1 0 3 237.39 243.35 2.25 o 3 0 3 945.72 1104.50 7.39 o 5 0 3 39.16 36.46 1.74 o 7 0 3 48.72 48.24 2.59 o 9 0 3 44.99 47.23 2.32 o -10 1 3 3.66 0.51 2.67 o -9 1 3 11.02 7.11 1.26 o -8 1 3 111.53 97.45 3.76 o -7 1 3 2.80 7.39 1.05 o -6 1 3 424.41 431.09 5.68 o -5 1 3 35.30 25.65 1.38 o -4 1 3 1019.38 1021.15 6.78 o -3 1 3 2528.68 2486.93 9.37 o -2 1 3 157.05 192.80 2.56 o -1 1 3 5246.63 5827.15 62.49 o 0 1 3 5733.39 6264.83 103.94 o 1 1 3 2190.28 2290.43 7.98 o 2 1 3 818.20 828.04 5.78 o 3 1 3 2412.96 2488.44 11.08 o 4 1 3 1.42 0.99 1.64 o 5 1 3 137.58 154.35 3.85 o 6 1 3 93.66 99.99 3.84 o 7 1 3 15.43 18.79 1.35 o 8 1 3 14.63 13.63 1.32 o 9 1 3 6.62 6.70 1.35 o -10 2 3 5.60 4.40 1.36 o -9 2 3 2.71 3.07 1.20 o -8 2 3 100.98 97.68 3.85 o -7 2 3 50.71 52.36 2.53 o -6 2 3 758.61 793.80 7.70 o -5 2 3 154.84 165.69 3.41 o -4 2 3 494.23 512.50 5.06 o -3 2 3 212.93 215.52 3.10 o -2 2 3 174.35 165.96 2.56 o -1 2 3 520.66 521.22 3.03 o 0 2 3 55.73 40.40 1.12 o 1 2 3 307.02 310.81 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