#------------------------------------------------------------------------------ #$Date: 2016-04-02 20:32:48 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180754 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/00/75/2007561.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2007561_Fobs loop_ _publ_author_name 'Charfi, M.' 'Jouini, A.' 'Pierrot, M.' _publ_section_title ; Piperazine-1,4-diium Dihydrogendiphosphate ; _journal_issue 8 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first IUC9800042 _journal_volume 54 _journal_year 1998 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _exptl_crystal_F_000 552.00 _cod_data_source_file qb0052sup2.hkl _cod_data_source_block pip2 #BEGIN Tags that were not found in dictionaries: _shelx_title ' [C4H12N2 H2P2O7]' _shelx_refln_list_code 4 _shelx_f_calc_maximum 100.99 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 1.28 2.33 0.38 o 5 0 0 15.26 13.66 0.73 o 6 0 0 5636.32 6150.20 223.51 o 7 0 0 6.78 7.13 0.81 o 8 0 0 743.37 776.89 23.87 o 9 0 0 233.79 253.30 8.29 o 10 0 0 1953.83 1937.29 63.80 o 11 0 0 328.18 334.87 10.11 o 12 0 0 1006.99 1063.14 33.64 o 13 0 0 194.78 187.19 5.52 o 1 1 0 3777.44 3695.90 104.97 o 2 1 0 173.76 161.01 3.78 o 3 1 0 1852.70 1738.95 51.19 o 4 1 0 1825.67 1877.20 53.77 o 5 1 0 33.08 45.37 1.32 o 6 1 0 882.98 960.51 27.55 o 7 1 0 0.03 0.71 0.62 o 8 1 0 333.53 376.37 9.07 o 9 1 0 528.69 525.81 14.02 o 10 1 0 0.87 4.34 0.89 o 11 1 0 548.94 572.60 12.59 o 12 1 0 1.90 4.15 1.91 o 13 1 0 333.30 345.60 12.64 o 14 1 0 23.76 26.83 1.84 o 0 2 0 7135.33 7172.26 225.34 o 1 2 0 71.26 62.26 1.51 o 2 2 0 3156.64 2500.05 88.03 o 3 2 0 616.44 629.00 18.69 o 4 2 0 0.22 4.45 0.71 o 5 2 0 2773.97 2943.28 72.32 o 6 2 0 1959.18 2004.24 49.70 o 7 2 0 863.83 908.28 22.45 o 8 2 0 265.85 298.21 7.52 o 9 2 0 154.86 169.54 4.08 o 10 2 0 230.19 235.42 7.66 o 11 2 0 228.04 241.31 7.59 o 12 2 0 11.20 11.07 3.11 o 13 2 0 1.27 2.23 1.12 o 14 2 0 54.15 57.42 3.06 o 1 3 0 104.86 86.16 2.27 o 2 3 0 3.70 9.37 0.85 o 3 3 0 498.22 534.85 10.58 o 4 3 0 33.16 25.29 1.07 o 5 3 0 57.29 52.01 1.34 o 6 3 0 81.82 76.27 1.95 o 7 3 0 437.14 448.54 11.37 o 8 3 0 69.41 75.80 2.22 o 9 3 0 49.62 59.82 1.77 o 10 3 0 1.49 3.23 1.25 o 11 3 0 1427.43 1408.55 34.75 o 12 3 0 9.96 10.25 2.91 o 13 3 0 91.01 90.56 4.65 o 14 3 0 2.19 4.65 3.11 o 0 4 0 39.37 43.50 2.28 o 1 4 0 24.52 24.15 1.46 o 2 4 0 43.97 57.02 2.00 o 3 4 0 396.18 388.48 8.38 o 4 4 0 43.02 43.78 1.72 o 5 4 0 2879.50 2889.27 63.18 o 6 4 0 0.78 1.88 1.38 o 7 4 0 1350.07 1412.84 30.61 o 8 4 0 0.42 2.17 1.42 o 9 4 0 381.87 417.99 12.27 o 10 4 0 86.50 88.85 2.40 o 11 4 0 420.26 475.09 13.32 o 12 4 0 13.04 11.89 1.04 o 13 4 0 122.32 103.10 8.03 o 1 5 0 11.76 10.30 1.48 o 2 5 0 23.65 25.63 1.94 o 3 5 0 3.41 3.50 1.36 o 4 5 0 646.66 688.63 15.07 o 5 5 0 3.17 3.42 1.65 o 6 5 0 1125.65 1171.06 28.77 o 7 5 0 2.76 3.90 1.68 o 8 5 0 274.43 294.76 7.30 o 9 5 0 74.76 80.44 2.52 o 10 5 0 297.17 315.82 10.10 o 11 5 0 0.10 1.45 2.08 o 12 5 0 160.96 149.40 6.36 o 0 6 0 36.13 33.93 3.09 o 1 6 0 0.82 0.05 47.47 o 2 6 0 837.99 865.06 22.21 o 3 6 0 107.77 104.35 3.36 o 4 6 0 218.93 223.49 6.03 o 5 6 0 400.41 392.66 11.69 o 6 6 0 3.01 3.35 1.92 o 7 6 0 311.13 305.08 9.00 o 8 6 0 5.41 5.81 2.23 o 9 6 0 191.37 191.27 6.83 o 10 6 0 12.88 11.14 2.41 o 11 6 0 109.49 93.26 5.23 o 1 7 0 0.33 0.30 9.36 o 2 7 0 14.68 14.84 2.66 o 3 7 0 21.50 21.00 2.63 o 4 7 0 436.65 441.35 19.20 o 5 7 0 17.53 12.77 2.56 o 6 7 0 956.96 977.62 32.58 o 7 7 0 46.65 48.54 3.55 o 8 7 0 327.05 327.16 12.97 o 9 7 0 40.75 31.95 3.42 o 0 8 0 56.12 55.58 5.27 o 1 8 0 5.54 7.45 3.99 o 2 8 0 523.65 501.86 19.64 o 3 8 0 0.10 3.03 3.25 o 4 8 0 86.94 82.94 4.93 o 5 8 0 54.87 56.58 4.35 o -14 1 1 199.03 228.16 6.90 o -13 1 1 29.87 28.08 1.60 o -12 1 1 307.66 349.56 11.42 o -11 1 1 10.70 12.58 1.39 o -10 1 1 1088.96 1194.44 36.77 o -9 1 1 58.56 44.63 1.63 o -8 1 1 1770.29 1677.77 54.80 o -7 1 1 53.94 85.04 2.74 o -6 1 1 165.33 247.33 9.36 o -5 1 1 102.12 137.17 5.47 o -4 1 1 5.44 0.40 0.61 o -3 1 1 1392.05 1345.64 36.48 o -2 1 1 1993.80 1770.55 54.30 o -1 1 1 59.46 77.25 1.87 o 0 1 1 173.27 125.32 5.48 o 1 1 1 2492.92 2558.69 65.18 o 3 1 1 4112.27 4190.35 129.70 o 4 1 1 482.80 381.40 9.35 o 5 1 1 106.93 95.10 2.69 o 6 1 1 776.84 692.74 15.69 o 7 1 1 1137.04 1158.43 29.18 o 8 1 1 1991.24 2018.10 49.83 o 9 1 1 665.24 708.26 19.38 o 10 1 1 497.19 466.48 12.40 o 11 1 1 111.86 125.80 2.80 o 12 1 1 13.85 13.11 1.04 o 13 1 1 27.38 19.97 1.07 o 14 1 1 13.37 12.56 2.16 o -14 2 1 89.03 84.40 4.00 o -13 2 1 43.79 56.10 2.74 o -12 2 1 21.91 18.43 2.21 o -11 2 1 400.26 402.29 14.17 o -10 2 1 165.15 169.53 5.74 o -9 2 1 2071.10 2090.52 65.57 o -8 2 1 150.95 148.07 5.69 o -7 2 1 4.23 0.13 1.22 o -6 2 1 105.81 98.85 2.43 o -5 2 1 369.64 490.02 15.65 o -4 2 1 3216.51 3221.13 77.06 o -3 2 1 416.92 412.84 11.13 o -2 2 1 616.13 617.66 17.20 o -1 2 1 1312.82 1264.30 31.73 o 0 2 1 781.79 686.83 14.11 o 1 2 1 8470.24 8869.30 206.21 o 2 2 1 4.33 4.97 0.59 o 3 2 1 1230.69 1108.66 28.60 o 4 2 1 3118.01 3494.17 88.79 o 5 2 1 310.55 282.93 6.53 o 6 2 1 93.73 81.42 1.96 o 7 2 1 1784.77 1766.90 44.37 o 8 2 1 8.81 6.70 0.89 o 9 2 1 320.94 339.59 7.64 o 10 2 1 1.41 2.28 0.95 o 11 2 1 1.22 0.22 2.05 o 12 2 1 6.97 9.81 1.36 o 13 2 1 16.92 15.42 1.08 o 14 2 1 5.65 7.48 2.67 o -14 3 1 98.60 75.99 5.46 o -13 3 1 166.50 172.15 7.25 o -12 3 1 5.64 4.47 2.23 o -11 3 1 11.98 8.41 3.83 o -10 3 1 13.55 6.58 2.07 o -9 3 1 17.81 23.58 1.42 o -8 3 1 6.95 6.99 1.00 o -7 3 1 12.87 15.67 1.09 o -6 3 1 86.94 95.28 2.13 o -5 3 1 844.28 891.23 24.46 o -4 3 1 0.61 0.93 1.12 o -3 3 1 1120.87 1019.22 26.53 o -2 3 1 900.76 914.53 21.42 o -1 3 1 0.53 21.59 1.09 o 0 3 1 389.57 444.30 10.98 o 1 3 1 397.71 308.41 8.31 o 2 3 1 364.85 361.98 7.99 o 3 3 1 606.95 555.79 12.67 o 4 3 1 155.68 183.34 3.74 o 5 3 1 82.54 79.04 1.84 o 6 3 1 0.16 0.66 0.91 o 7 3 1 30.70 35.88 1.43 o 8 3 1 203.41 207.83 5.05 o 9 3 1 1.17 1.21 1.20 o 10 3 1 25.95 27.02 1.41 o 11 3 1 20.22 24.39 1.36 o 12 3 1 12.27 18.02 1.17 o 13 3 1 333.15 334.71 13.22 o 14 3 1 132.37 141.00 6.87 o -13 4 1 21.34 17.24 3.17 o -12 4 1 2.29 0.82 7.53 o -11 4 1 15.10 13.06 1.36 o -10 4 1 21.04 22.43 1.53 o -9 4 1 3109.31 3107.94 113.06 o -8 4 1 39.19 36.93 2.10 o -7 4 1 91.17 85.19 2.89 o -6 4 1 92.91 92.55 2.25 o -5 4 1 2199.74 2307.82 52.54 o -4 4 1 17.16 19.28 1.40 o -3 4 1 3202.72 3304.05 70.12 o -2 4 1 4.61 4.17 1.02 o -1 4 1 555.48 541.93 11.64 o 0 4 1 0.04 0.20 3.34 o 1 4 1 174.81 184.43 4.83 o 2 4 1 622.98 616.39 14.13 o 3 4 1 110.25 112.94 2.65 o 4 4 1 20.25 17.11 1.60 o 5 4 1 5.11 8.89 1.47 o 6 4 1 276.16 269.57 6.37 o 7 4 1 2341.05 2250.83 65.78 o 8 4 1 205.57 193.22 4.58 o 9 4 1 7.38 12.51 1.52 o 10 4 1 20.60 17.82 1.68 o 11 4 1 124.43 121.72 3.52 o 12 4 1 9.63 10.94 1.48 o 13 4 1 0.11 1.69 1.75 o -12 5 1 41.34 35.97 2.36 o -11 5 1 50.76 48.83 1.89 o -10 5 1 36.22 28.03 2.45 o -9 5 1 0.03 3.73 2.41 o -8 5 1 349.98 336.72 10.53 o -7 5 1 5.32 3.62 1.61 o -6 5 1 406.74 411.68 10.46 o -5 5 1 1140.54 1146.34 27.38 o -4 5 1 66.45 69.64 2.22 o -3 5 1 1318.90 1337.53 30.18 o -2 5 1 244.83 253.57 5.41 o -1 5 1 1039.49 1053.51 22.80 o 0 5 1 0.75 1.06 1.60 o 1 5 1 383.88 410.02 9.15 o 2 5 1 321.47 297.91 6.60 o 3 5 1 232.37 216.45 5.00 o 4 5 1 393.85 384.67 8.65 o 5 5 1 1.40 6.04 1.88 o 6 5 1 4.91 11.17 2.08 o 7 5 1 1044.92 1040.04 30.19 o 8 5 1 5.89 4.44 2.15 o 9 5 1 284.20 283.55 8.32 o 10 5 1 0.24 1.15 1.53 o 11 5 1 494.01 485.52 16.98 o 12 5 1 319.90 315.82 13.31 o -11 6 1 94.23 84.11 4.04 o -10 6 1 36.44 34.90 3.20 o -9 6 1 10.86 11.00 2.34 o -8 6 1 0.62 0.57 3.91 o -7 6 1 65.61 58.11 2.87 o -6 6 1 321.54 306.40 9.49 o -5 6 1 3.59 2.31 2.44 o -4 6 1 2469.56 2546.11 78.56 o -3 6 1 788.42 782.18 17.99 o -2 6 1 1736.19 1773.31 46.88 o -1 6 1 145.80 137.71 3.55 o 0 6 1 1428.64 1510.17 35.58 o 1 6 1 282.26 266.68 6.16 o 2 6 1 1888.76 1930.84 49.39 o 3 6 1 867.35 826.43 22.78 o 4 6 1 260.22 255.32 7.30 o 5 6 1 0.91 1.64 2.36 o 6 6 1 84.86 92.49 3.22 o 7 6 1 0.47 3.06 2.27 o 8 6 1 326.30 342.05 12.28 o 9 6 1 208.88 213.18 7.13 o 10 6 1 272.06 243.21 9.86 o 11 6 1 33.06 34.24 3.26 o -9 7 1 7.07 5.36 3.63 o -8 7 1 189.89 174.33 6.52 o -7 7 1 0.20 4.48 3.11 o -6 7 1 318.42 338.51 11.92 o -5 7 1 0.07 0.47 9.07 o -4 7 1 42.72 48.42 2.96 o -3 7 1 68.35 69.55 3.14 o -2 7 1 240.23 247.37 8.27 o -1 7 1 4.78 6.23 3.71 o 0 7 1 311.43 294.33 7.93 o 1 7 1 0.32 0.20 20.54 o 2 7 1 4.28 5.51 2.67 o 3 7 1 0.23 1.06 2.93 o 4 7 1 281.86 258.97 9.66 o 5 7 1 118.59 127.47 4.68 o 6 7 1 108.67 93.88 3.96 o 7 7 1 111.10 115.02 5.35 o 8 7 1 34.44 35.43 3.41 o -5 8 1 281.03 259.12 11.71 o -4 8 1 409.57 402.96 12.80 o -3 8 1 147.25 142.21 6.97 o -2 8 1 111.26 105.92 4.70 o -1 8 1 41.23 47.98 3.64 o 0 8 1 170.42 172.22 6.20 o 1 8 1 1.78 0.32 22.59 o 2 8 1 193.41 186.60 6.75 o 3 8 1 23.23 23.71 3.98 o 4 8 1 158.54 155.50 7.55 o 5 8 1 64.13 60.64 4.76 o -8 0 2 247.46 261.18 7.73 o -7 0 2 656.70 630.18 21.63 o -6 0 2 755.08 685.58 24.24 o -5 0 2 34.75 70.04 2.76 o -4 0 2 254.17 204.96 7.91 o 0 0 2 721.73 773.38 36.87 o 1 0 2 1487.31 1421.13 50.24 o 3 0 2 2765.61 2545.02 82.81 o 4 0 2 161.24 169.58 5.88 o 5 0 2 93.87 118.67 3.76 o 6 0 2 182.98 223.64 6.67 o 7 0 2 110.14 90.99 2.99 o 8 0 2 579.32 509.70 16.20 o 9 0 2 3000.73 2964.52 112.55 o 10 0 2 711.75 735.92 25.82 o 11 0 2 1277.87 1279.96 49.50 o 12 0 2 121.20 130.31 4.18 o 13 0 2 940.03 969.81 33.94 o 14 0 2 106.58 111.17 3.98 o -13 1 2 0.12 0.47 1.11 o -12 1 2 162.13 177.57 5.66 o -11 1 2 202.30 171.63 5.01 o -9 1 2 89.91 102.83 3.12 o -8 1 2 219.00 227.93 10.67 o -7 1 2 59.11 63.41 2.16 o -6 1 2 370.62 434.57 15.73 o -5 1 2 741.14 721.02 27.73 o -4 1 2 1637.63 1760.61 55.37 o -3 1 2 363.65 403.97 12.72 o -2 1 2 2564.82 2349.73 64.99 o -1 1 2 1660.93 1479.23 46.03 o 0 1 2 558.90 533.97 12.56 o 1 1 2 1.21 3.32 0.51 o 2 1 2 3607.27 3323.45 83.92 o 3 1 2 5952.22 6423.50 206.93 o 4 1 2 227.07 224.50 5.10 o 5 1 2 847.33 866.19 22.41 o 6 1 2 2179.62 2406.74 55.82 o 7 1 2 1972.69 2094.36 48.59 o 8 1 2 62.19 50.56 1.40 o 9 1 2 814.33 860.87 19.50 o 10 1 2 284.15 283.78 6.62 o 11 1 2 789.43 765.67 19.42 o 12 1 2 44.00 46.96 1.67 o 13 1 2 3.92 5.70 1.28 o 14 1 2 193.56 198.09 6.28 o -14 2 2 30.57 35.84 2.83 o -13 2 2 1.72 10.34 2.07 o -12 2 2 327.00 318.03 19.99 o -11 2 2 133.82 129.47 4.65 o -10 2 2 41.52 33.13 1.96 o -9 2 2 550.70 608.65 22.55 o -8 2 2 211.40 202.59 6.80 o -7 2 2 2011.79 2075.13 79.21 o -6 2 2 1.28 3.77 0.62 o -5 2 2 292.21 269.64 7.42 o -4 2 2 1816.77 1777.30 47.73 o -3 2 2 899.59 867.23 19.14 o -2 2 2 1543.30 1548.19 45.20 o -1 2 2 0.89 4.33 0.70 o 0 2 2 5467.01 5155.73 126.13 o 1 2 2 1675.89 1665.98 42.79 o 2 2 2 260.93 203.38 4.62 o 3 2 2 4117.90 4192.46 98.02 o 4 2 2 7395.62 7773.15 229.86 o 5 2 2 4360.36 4578.99 108.74 o 6 2 2 740.03 819.38 19.64 o 7 2 2 1320.10 1314.93 30.51 o 8 2 2 194.56 216.03 5.15 o 9 2 2 1983.72 2049.51 56.22 o 10 2 2 7.62 5.60 1.17 o 11 2 2 319.26 324.90 9.86 o 12 2 2 63.41 75.38 2.17 o 13 2 2 175.28 187.10 5.88 o 14 2 2 79.59 86.36 4.15 o -14 3 2 82.90 90.96 18.54 o -13 3 2 1.38 2.75 2.64 o -12 3 2 30.28 27.55 2.73 o -11 3 2 103.55 114.39 4.71 o -10 3 2 39.67 39.53 2.70 o -9 3 2 118.00 127.06 4.31 o -8 3 2 85.44 81.89 2.60 o -7 3 2 2956.68 3041.89 81.62 o -6 3 2 1002.50 1033.03 23.43 o -5 3 2 99.80 90.78 2.23 o -4 3 2 182.93 219.51 4.25 o -3 3 2 169.50 132.70 3.18 o -2 3 2 3185.67 3224.29 73.07 o -1 3 2 1483.69 1466.16 34.12 o 0 3 2 585.98 546.43 12.81 o 1 3 2 18.03 18.18 1.00 o 2 3 2 17.39 10.96 1.02 o 3 3 2 922.88 940.19 27.75 o 4 3 2 487.60 542.39 12.38 o 5 3 2 458.17 446.46 9.88 o 6 3 2 539.11 579.30 12.16 o 7 3 2 4.71 3.73 1.27 o 8 3 2 442.59 442.63 10.51 o 9 3 2 1274.56 1258.61 30.40 o 10 3 2 712.26 695.92 18.51 o 11 3 2 125.04 123.79 3.19 o 12 3 2 2.52 4.58 1.58 o 13 3 2 21.49 20.97 2.16 o 14 3 2 81.68 96.35 5.11 o -13 4 2 651.30 604.38 27.83 o -12 4 2 136.13 140.82 5.67 o -11 4 2 218.23 222.76 10.31 o -10 4 2 251.17 268.96 6.71 o -9 4 2 437.42 472.18 13.28 o -8 4 2 701.55 730.93 17.97 o -7 4 2 248.33 254.23 6.44 o -6 4 2 493.21 504.37 13.25 o -5 4 2 176.00 190.87 4.70 o -4 4 2 3.41 1.13 1.12 o -3 4 2 1255.07 1292.57 28.15 o -2 4 2 409.16 405.14 9.41 o -1 4 2 1126.49 1117.70 23.32 o 0 4 2 109.11 113.00 3.05 o 1 4 2 1014.43 997.17 24.88 o 2 4 2 1556.23 1546.01 33.74 o 3 4 2 3553.37 3559.06 77.61 o 4 4 2 2032.19 2120.52 59.93 o 5 4 2 1920.68 1988.01 38.98 o 6 4 2 959.69 976.80 20.95 o 7 4 2 917.85 950.83 22.14 o 8 4 2 105.94 103.91 2.82 o 9 4 2 43.29 46.85 2.11 o 10 4 2 40.24 38.30 1.84 o 11 4 2 127.52 121.73 3.57 o 12 4 2 0.05 2.17 0.75 o 13 4 2 42.95 47.21 3.17 o -12 5 2 502.24 467.76 27.58 o -11 5 2 58.03 65.36 2.23 o -10 5 2 225.42 232.46 6.15 o -9 5 2 25.12 25.31 1.79 o -8 5 2 751.80 775.98 21.62 o -7 5 2 1.48 2.05 1.76 o -6 5 2 1243.37 1294.02 34.65 o -5 5 2 19.19 22.26 1.65 o -4 5 2 40.17 38.14 1.84 o -3 5 2 49.74 49.99 2.25 o -2 5 2 32.18 29.71 1.91 o -1 5 2 710.92 742.70 15.51 o 0 5 2 47.85 45.20 1.86 o 1 5 2 132.23 139.71 3.08 o 2 5 2 82.40 86.81 2.42 o 3 5 2 368.77 412.33 11.22 o 4 5 2 593.93 484.08 12.63 o 5 5 2 718.04 704.00 15.94 o 6 5 2 0.74 0.70 2.05 o 7 5 2 187.11 191.80 5.08 o 8 5 2 8.41 6.12 2.06 o 9 5 2 1.47 3.61 1.78 o 10 5 2 54.35 47.03 2.29 o 11 5 2 1.43 0.81 2.96 o 12 5 2 37.47 40.60 3.05 o -11 6 2 16.20 11.99 4.60 o -10 6 2 100.43 101.16 4.38 o -9 6 2 85.32 83.13 2.81 o -8 6 2 74.78 66.01 3.15 o -7 6 2 67.09 75.80 3.01 o -6 6 2 0.74 2.14 1.20 o -5 6 2 318.80 324.72 8.23 o -4 6 2 37.10 40.91 2.28 o -3 6 2 7.88 7.43 1.77 o -2 6 2 91.53 88.20 2.89 o -1 6 2 44.78 40.30 2.33 o 0 6 2 308.41 329.15 7.42 o 1 6 2 43.01 41.39 2.49 o 2 6 2 322.82 342.01 8.06 o 3 6 2 104.93 114.40 3.46 o 4 6 2 208.99 200.07 5.71 o 5 6 2 24.82 29.39 2.27 o 6 6 2 199.53 193.28 7.09 o 7 6 2 170.82 164.04 5.10 o 8 6 2 11.66 7.43 2.10 o 9 6 2 5.64 7.59 2.74 o 10 6 2 0.08 2.33 1.65 o -8 7 2 298.79 316.93 11.54 o -7 7 2 267.07 256.13 9.01 o -6 7 2 170.00 165.19 5.80 o -5 7 2 7.74 9.58 2.51 o -4 7 2 22.93 22.74 3.11 o -3 7 2 28.17 24.60 2.53 o -2 7 2 144.75 143.30 5.09 o -1 7 2 172.39 174.82 5.06 o 0 7 2 0.21 0.02 124.85 o 1 7 2 60.91 60.27 2.89 o 2 7 2 78.98 88.30 3.14 o 3 7 2 271.52 280.15 10.58 o 4 7 2 191.39 187.92 6.84 o 5 7 2 485.76 478.66 16.51 o 6 7 2 72.06 78.03 3.99 o 7 7 2 1.42 4.07 3.84 o 8 7 2 2.95 2.61 2.56 o -5 8 2 241.45 222.76 8.96 o -4 8 2 219.46 203.29 10.45 o -3 8 2 359.65 363.61 13.68 o -2 8 2 12.84 24.15 3.65 o -1 8 2 394.07 397.33 15.78 o 0 8 2 288.38 302.26 10.71 o 1 8 2 235.59 217.56 8.70 o 2 8 2 1.40 1.73 4.08 o 3 8 2 43.55 40.98 4.15 o 4 8 2 8.56 4.52 3.93 o 5 8 2 12.07 10.18 4.98 o -12 1 3 369.63 400.74 10.95 o -11 1 3 2004.41 1998.95 64.79 o -10 1 3 990.38 1007.54 31.57 o -9 1 3 1208.52 1189.60 42.95 o -8 1 3 94.43 96.22 3.70 o -7 1 3 14.50 14.68 1.14 o -6 1 3 52.31 59.25 2.25 o -5 1 3 57.44 67.98 1.97 o -4 1 3 117.71 119.39 3.08 o -3 1 3 2438.64 2590.95 68.78 o -2 1 3 932.65 787.62 18.11 o -1 1 3 4818.47 4698.14 100.67 o 0 1 3 2966.81 2757.01 67.69 o 2 1 3 1396.79 1264.44 27.17 o 3 1 3 722.31 825.15 18.97 o 4 1 3 0.24 1.29 0.87 o 5 1 3 943.38 895.15 21.83 o 6 1 3 780.87 781.29 18.29 o 7 1 3 1207.89 1180.07 34.21 o 8 1 3 35.74 49.13 2.23 o 9 1 3 0.11 0.36 1.52 o 10 1 3 0.53 2.56 1.28 o 11 1 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