#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2007741.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2007741_Fobs loop_ _publ_author_name 'Olszak, T. A.' _publ_section_title ; X-ray Structure Investigations of Potential \b-Blockers. III ; _journal_issue 10 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 1456 _journal_page_last 1459 _journal_volume 54 _journal_year 1998 _chemical_name_systematic ; 6,7-dihydroxy-1-phenyl-1,2,3,4-tetrahydroisoquinoline hydrochloride ; _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 95.171 _cell_angle_gamma 90.000 _cell_length_a 9.1180 _cell_length_b 9.1489 _cell_length_c 17.6325 _exptl_crystal_F_000 624.00 _reflns_d_resolution_high 0.8894 _[local]_cod_data_source_file na1324Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' EB20' _shelx_refln_list_code 4 _shelx_f_calc_maximum 155.38 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 65.93 60.07 4.37 o 4 0 0 43.14 60.43 9.33 o 6 0 0 41.60 58.43 16.93 o 8 0 0 322.50 314.66 26.71 o 10 0 0 216.62 229.90 21.73 o 1 1 0 154.72 151.33 4.49 o 2 1 0 68.25 72.81 3.57 o 3 1 0 87.15 86.40 5.12 o 4 1 0 83.58 91.79 6.99 o 5 1 0 1507.27 1434.06 45.31 o 6 1 0 6.06 1.22 20.95 o 7 1 0 52.84 64.83 15.41 o 8 1 0 72.46 60.88 21.67 o 9 1 0 0.85 10.76 29.76 o 10 1 0 2.58 8.73 24.25 o 0 2 0 298.54 280.15 9.60 o 1 2 0 390.21 404.20 8.49 o 2 2 0 3133.50 3030.41 26.39 o 3 2 0 309.70 349.33 12.48 o 4 2 0 2680.46 2654.10 75.45 o 5 2 0 647.95 702.70 43.15 o 6 2 0 44.73 32.35 18.23 o 7 2 0 16.44 2.86 27.42 o 8 2 0 303.77 307.42 19.18 o 9 2 0 3.19 -4.97 29.54 o 10 2 0 23.79 21.12 23.28 o 1 3 0 2306.70 2260.54 44.30 o 2 3 0 0.51 -0.84 9.17 o 3 3 0 769.82 805.68 18.26 o 4 3 0 103.77 107.62 9.15 o 5 3 0 884.08 876.47 28.39 o 6 3 0 65.00 59.03 14.17 o 7 3 0 1.59 -0.98 28.75 o 8 3 0 5.25 4.07 30.72 o 9 3 0 188.09 178.70 17.33 o 0 4 0 5.73 5.97 14.66 o 1 4 0 26.44 35.72 6.96 o 2 4 0 553.97 586.91 17.09 o 3 4 0 414.93 429.94 18.44 o 4 4 0 124.99 122.03 11.01 o 5 4 0 59.22 54.12 13.64 o 6 4 0 41.42 54.16 19.15 o 7 4 0 43.20 34.82 30.52 o 8 4 0 16.72 10.53 30.38 o 9 4 0 37.87 47.50 21.51 o 1 5 0 934.03 995.02 51.33 o 2 5 0 146.90 139.39 10.06 o 3 5 0 71.39 81.35 11.08 o 4 5 0 41.07 35.32 22.28 o 5 5 0 194.48 196.93 15.81 o 6 5 0 106.55 113.96 17.46 o 7 5 0 7.86 15.25 30.69 o 8 5 0 9.74 11.42 28.86 o 0 6 0 60.82 69.62 16.38 o 1 6 0 1336.14 1364.39 84.15 o 2 6 0 24.99 24.12 21.20 o 3 6 0 21.41 18.32 23.40 o 4 6 0 32.35 27.63 26.29 o 5 6 0 1.74 11.29 28.89 o 6 6 0 115.92 121.71 18.25 o 7 6 0 40.34 32.30 30.05 o 8 6 0 91.02 108.23 16.50 o 1 7 0 1.97 -7.32 25.43 o 2 7 0 43.56 52.15 21.28 o 3 7 0 145.47 154.40 16.79 o 4 7 0 784.30 702.43 32.41 o 5 7 0 120.09 127.19 18.16 o 6 7 0 188.11 213.43 20.90 o 7 7 0 0.06 1.29 26.12 o 0 8 0 297.52 315.21 92.37 o 1 8 0 20.40 19.21 30.05 o 2 8 0 14.48 -4.22 30.18 o 3 8 0 105.34 114.98 18.08 o 4 8 0 300.91 276.04 21.88 o 5 8 0 450.19 421.60 52.05 o 6 8 0 21.90 21.97 25.77 o 1 9 0 126.59 117.19 29.70 o 2 9 0 241.17 241.83 43.42 o 3 9 0 2.52 -3.56 28.53 o 4 9 0 44.66 38.42 21.54 o 0 10 0 20.12 17.55 37.47 o 1 10 0 74.08 53.55 18.92 o 2 10 0 8.85 -2.00 24.36 o -9 0 1 93.76 74.44 30.68 o -7 0 1 271.72 288.91 22.98 o -5 0 1 614.69 543.92 38.77 o -3 0 1 298.04 328.53 14.88 o -1 0 1 665.20 647.16 10.02 o 1 0 1 8684.53 8850.62 159.42 o 3 0 1 19.48 15.40 7.76 o 5 0 1 104.55 139.52 13.52 o 7 0 1 572.36 565.03 31.29 o 9 0 1 0.07 1.79 41.99 o -10 1 1 31.15 27.84 24.70 o -9 1 1 230.89 226.09 18.32 o -8 1 1 0.53 -5.10 29.95 o -7 1 1 9.55 11.67 26.01 o -6 1 1 85.36 83.93 12.29 o -5 1 1 495.80 561.28 30.50 o -4 1 1 251.31 255.04 10.63 o -3 1 1 20.34 26.06 4.83 o -2 1 1 13688.42 13177.96 115.30 o -1 1 1 36.91 34.39 2.20 o 1 1 1 1375.42 1370.62 12.28 o 2 1 1 2550.53 2526.89 21.59 o 3 1 1 15.95 19.44 5.28 o 4 1 1 0.18 -0.26 11.50 o 5 1 1 25.74 37.97 10.16 o 6 1 1 731.91 703.97 27.03 o 7 1 1 328.25 319.47 16.97 o 8 1 1 134.98 143.57 18.36 o 9 1 1 244.38 223.82 18.28 o 10 1 1 99.13 118.74 14.26 o -10 2 1 1.96 24.30 23.41 o -9 2 1 20.88 0.34 30.05 o -8 2 1 13.28 13.18 30.47 o -7 2 1 844.12 878.86 34.44 o -6 2 1 394.82 413.26 18.03 o -5 2 1 0.91 -3.25 16.87 o -4 2 1 6.70 1.39 12.71 o -3 2 1 4791.11 4825.39 83.88 o -2 2 1 616.44 591.83 12.21 o -1 2 1 373.49 398.46 8.62 o 0 2 1 2519.56 2363.26 49.09 o 1 2 1 3923.86 3675.31 36.37 o 2 2 1 870.70 808.65 13.27 o 3 2 1 3293.70 3315.70 31.49 o 4 2 1 405.57 413.99 16.47 o 5 2 1 1451.39 1454.06 55.48 o 6 2 1 69.04 62.40 13.27 o 7 2 1 632.26 616.88 25.00 o 8 2 1 1.54 1.67 30.82 o 9 2 1 34.45 28.95 24.19 o -9 3 1 0.41 -10.87 28.57 o -8 3 1 17.61 13.05 31.30 o -7 3 1 5.61 -2.83 28.61 o -6 3 1 118.26 120.69 14.40 o -5 3 1 542.66 500.80 34.62 o -4 3 1 23.25 24.40 12.41 o -3 3 1 25.59 20.17 9.69 o -2 3 1 428.08 425.42 12.69 o -1 3 1 68.97 67.43 4.74 o 0 3 1 97.07 101.16 4.85 o 1 3 1 1865.66 1874.69 20.95 o 2 3 1 619.70 648.75 14.69 o 3 3 1 170.93 163.83 7.66 o 4 3 1 138.00 128.61 9.31 o 5 3 1 75.33 59.81 12.62 o 6 3 1 4.63 7.37 24.42 o 7 3 1 10.08 10.91 28.91 o 8 3 1 4.23 6.76 30.73 o 9 3 1 21.88 10.55 28.29 o -9 4 1 128.38 111.79 15.73 o -8 4 1 9.35 5.99 30.52 o -7 4 1 247.79 262.55 18.72 o -6 4 1 92.03 94.71 17.31 o -5 4 1 53.10 51.18 14.39 o -4 4 1 1363.63 1339.60 32.67 o -3 4 1 1236.68 1256.58 41.90 o -2 4 1 571.87 619.47 17.45 o -1 4 1 1026.53 1036.73 27.09 o 0 4 1 26.00 24.31 6.90 o 1 4 1 6068.37 6106.89 152.38 o 2 4 1 54.80 64.69 7.49 o 3 4 1 657.75 675.42 20.53 o 4 4 1 437.89 449.97 16.76 o 5 4 1 366.82 368.03 16.33 o 6 4 1 1.77 17.59 26.79 o 7 4 1 29.65 33.06 30.55 o 8 4 1 202.69 219.48 18.48 o 9 4 1 24.85 26.03 26.17 o -8 5 1 233.27 251.38 21.99 o -7 5 1 5.92 -10.08 31.01 o -6 5 1 82.93 104.67 17.40 o -5 5 1 282.74 285.58 16.34 o -4 5 1 380.73 362.23 16.04 o -3 5 1 682.24 669.38 27.36 o -2 5 1 152.16 137.34 10.05 o -1 5 1 139.96 131.37 9.30 o 0 5 1 2708.91 2626.39 143.49 o 1 5 1 0.77 0.78 15.00 o 2 5 1 649.33 641.16 25.37 o 3 5 1 206.91 216.47 12.01 o 4 5 1 316.87 318.83 14.33 o 5 5 1 78.47 81.57 15.34 o 6 5 1 268.36 263.21 18.35 o 7 5 1 22.62 11.14 31.08 o 8 5 1 17.32 22.25 28.34 o -8 6 1 94.92 100.87 15.28 o -7 6 1 0.54 4.43 29.74 o -6 6 1 0.16 0.81 30.58 o -5 6 1 447.37 440.13 19.91 o -4 6 1 59.67 57.14 16.94 o -3 6 1 79.10 68.84 14.98 o -2 6 1 83.78 91.80 12.51 o -1 6 1 49.01 52.77 11.71 o 0 6 1 611.87 613.50 50.36 o 1 6 1 317.86 328.18 16.88 o 2 6 1 25.27 25.63 17.33 o 3 6 1 62.42 69.39 13.94 o 4 6 1 30.74 31.35 26.56 o 5 6 1 56.55 44.44 29.30 o 6 6 1 4.66 10.50 30.53 o 7 6 1 3.88 1.74 29.34 o 8 6 1 33.26 32.05 20.57 o -7 7 1 0.06 -3.09 26.22 o -6 7 1 104.60 99.09 17.74 o -5 7 1 15.91 18.09 30.67 o -4 7 1 684.27 640.67 42.35 o -3 7 1 30.18 41.08 22.48 o -2 7 1 483.58 460.01 31.06 o -1 7 1 6.26 14.99 25.51 o 0 7 1 13.60 14.33 25.16 o 1 7 1 156.68 163.77 15.60 o 2 7 1 765.74 711.45 55.94 o 3 7 1 440.38 409.61 32.15 o 4 7 1 79.34 75.00 19.38 o 5 7 1 915.00 858.30 69.65 o 6 7 1 61.13 56.37 24.33 o 7 7 1 29.74 27.54 25.78 o -6 8 1 0.39 -6.81 25.48 o -5 8 1 1.68 4.81 28.50 o -4 8 1 0.53 -11.72 30.12 o -3 8 1 34.01 56.00 21.56 o -2 8 1 254.12 243.64 29.79 o -1 8 1 2.90 -3.66 29.90 o 0 8 1 108.06 110.12 19.40 o 1 8 1 18.87 12.27 30.08 o 2 8 1 389.71 360.63 43.75 o 3 8 1 26.81 31.75 30.69 o 4 8 1 5.13 16.57 29.93 o 5 8 1 49.53 64.65 18.33 o 6 8 1 31.14 29.24 25.22 o -4 9 1 49.09 32.06 21.56 o -3 9 1 426.86 388.48 63.46 o -2 9 1 8.00 12.24 29.91 o -1 9 1 238.58 232.79 50.88 o 0 9 1 0.74 8.98 30.58 o 1 9 1 0.92 -14.14 30.56 o 2 9 1 81.57 80.95 21.44 o 3 9 1 141.37 134.71 21.79 o 4 9 1 27.48 26.02 26.18 o -2 10 1 0.10 7.79 24.04 o -1 10 1 98.86 84.94 24.43 o 0 10 1 97.44 96.56 25.93 o 1 10 1 32.82 24.57 20.96 o 2 10 1 5.30 10.91 24.14 o -10 0 2 246.29 293.39 22.39 o -8 0 2 12.79 16.95 41.89 o -6 0 2 1.16 4.91 28.40 o -4 0 2 847.81 792.43 33.43 o -2 0 2 19843.92 19327.28 251.30 o 0 0 2 7.89 11.76 1.81 o 2 0 2 748.02 746.05 15.53 o 4 0 2 2200.16 2241.74 38.99 o 6 0 2 442.43 482.09 25.49 o 8 0 2 195.93 199.78 26.46 o 10 0 2 265.48 262.50 21.20 o -10 1 2 55.73 61.09 17.80 o -9 1 2 292.24 298.79 18.70 o -8 1 2 127.19 120.79 17.90 o -7 1 2 13.70 13.39 26.01 o -6 1 2 2.23 -11.21 21.09 o -5 1 2 804.99 759.57 56.30 o -4 1 2 1.45 5.51 11.87 o -3 1 2 1.54 10.12 8.41 o -2 1 2 88.68 85.43 4.14 o 1 1 2 730.35 700.16 9.02 o 2 1 2 129.21 126.09 4.98 o 3 1 2 1445.67 1447.36 19.15 o 4 1 2 1309.60 1348.56 22.44 o 5 1 2 942.03 896.79 23.73 o 6 1 2 157.24 171.33 13.29 o 7 1 2 2.93 4.27 27.13 o 8 1 2 0.00 -19.73 30.92 o 9 1 2 72.31 69.43 17.46 o 10 1 2 155.73 134.28 14.04 o -10 2 2 33.44 48.27 15.11 o -9 2 2 1.09 15.62 29.36 o -8 2 2 9.11 22.38 30.28 o -7 2 2 133.71 141.60 16.35 o -6 2 2 21.16 25.62 22.30 o -5 2 2 223.01 229.95 18.73 o -4 2 2 91.21 96.49 8.02 o -3 2 2 283.29 294.33 12.26 o -2 2 2 1037.95 1016.59 15.52 o -1 2 2 266.16 275.88 8.38 o 0 2 2 16038.88 15852.97 175.29 o 1 2 2 16530.99 16543.52 472.71 o 2 2 2 11.55 8.50 7.46 o 3 2 2 377.57 381.02 13.15 o 4 2 2 29.62 35.63 8.64 o 5 2 2 80.54 78.50 10.57 o 6 2 2 15.94 12.76 23.05 o 7 2 2 7.92 6.09 28.07 o 8 2 2 162.22 185.05 18.70 o 9 2 2 72.66 66.71 16.89 o -9 3 2 11.64 29.19 28.53 o -8 3 2 183.31 163.01 18.57 o -7 3 2 12.56 16.74 28.75 o -6 3 2 336.37 316.25 15.59 o -5 3 2 1600.08 1520.73 83.71 o -4 3 2 762.01 768.83 57.50 o -3 3 2 74.09 82.41 7.35 o -2 3 2 188.21 196.33 8.47 o -1 3 2 3978.88 3966.75 50.92 o 0 3 2 65.31 68.41 4.89 o 1 3 2 2714.76 2699.85 28.44 o 2 3 2 1681.58 1636.86 30.63 o 3 3 2 2073.36 2105.03 27.40 o 4 3 2 94.25 101.22 9.50 o 5 3 2 362.09 374.91 16.42 o 6 3 2 29.36 30.98 25.26 o 7 3 2 3.43 11.33 29.27 o 8 3 2 52.87 60.11 19.74 o 9 3 2 140.60 173.54 16.71 o -9 4 2 45.34 42.09 22.06 o -8 4 2 338.95 326.40 19.10 o -7 4 2 25.14 26.58 30.40 o -6 4 2 95.38 97.21 15.86 o -5 4 2 3.63 -5.11 22.68 o -4 4 2 509.61 489.19 20.21 o -3 4 2 886.85 952.67 27.41 o -2 4 2 1.02 9.74 12.60 o -1 4 2 53.60 54.30 6.59 o 0 4 2 151.73 125.08 7.09 o 1 4 2 862.04 900.69 23.76 o 2 4 2 101.00 112.67 7.98 o 3 4 2 785.46 845.33 22.21 o 4 4 2 216.25 208.25 11.82 o 5 4 2 159.34 163.11 14.12 o 6 4 2 57.31 67.26 17.53 o 7 4 2 32.99 35.26 30.63 o 8 4 2 164.24 155.32 18.14 o 9 4 2 33.41 37.45 25.47 o -8 5 2 142.60 135.12 17.40 o -7 5 2 7.08 21.87 30.82 o -6 5 2 16.11 12.88 29.50 o -5 5 2 350.01 353.81 21.75 o -4 5 2 123.37 130.90 13.60 o -3 5 2 117.27 111.49 11.54 o -2 5 2 26.77 22.16 15.08 o -1 5 2 1051.16 1040.95 50.77 o 0 5 2 20.74 15.64 15.41 o 1 5 2 349.63 364.11 32.30 o 2 5 2 199.86 203.32 10.83 o 3 5 2 280.91 288.99 12.69 o 4 5 2 166.75 174.19 13.93 o 5 5 2 560.91 579.04 25.26 o 6 5 2 6.11 15.94 29.66 o 7 5 2 433.69 451.98 28.85 o 8 5 2 58.17 47.92 23.09 o -8 6 2 0.50 -5.02 25.70 o -7 6 2 12.90 26.18 29.89 o -6 6 2 135.32 148.86 18.46 o -5 6 2 164.12 158.27 17.83 o -4 6 2 2068.31 2120.85 118.38 o -3 6 2 152.42 158.05 14.57 o -2 6 2 7.93 9.89 21.16 o -1 6 2 18.83 22.90 18.22 o 0 6 2 1020.52 979.07 93.18 o 1 6 2 75.11 71.14 12.27 o 2 6 2 10.33 16.66 21.97 o 3 6 2 1.52 -15.18 24.38 o 4 6 2 599.89 585.16 28.32 o 5 6 2 16.97 24.15 29.43 o 6 6 2 0.65 6.16 30.56 o 7 6 2 28.15 28.55 23.97 o 8 6 2 25.62 37.51 20.29 o -7 7 2 10.05 5.63 26.33 o -6 7 2 2.90 -2.13 29.78 o -5 7 2 20.99 10.39 31.00 o -4 7 2 154.60 154.18 17.94 o -3 7 2 0.08 2.14 27.72 o -2 7 2 60.05 64.50 17.10 o -1 7 2 395.70 357.50 33.71 o 0 7 2 10.31 -6.05 25.98 o 1 7 2 189.29 187.16 20.42 o 2 7 2 242.14 245.21 16.85 o 3 7 2 7.47 19.01 28.59 o 4 7 2 203.48 195.01 18.21 o 5 7 2 126.83 99.73 18.01 o 6 7 2 195.83 184.20 17.82 o 7 7 2 3.83 4.82 25.35 o -6 8 2 158.56 154.86 24.24 o -5 8 2 19.76 20.03 28.76 o -4 8 2 7.61 4.42 29.97 o -3 8 2 2.39 -0.78 30.23 o -2 8 2 18.07 13.51 30.12 o -1 8 2 41.14 42.29 21.38 o 0 8 2 23.75 36.38 24.62 o 1 8 2 114.28 99.80 18.87 o 2 8 2 0.79 2.57 30.14 o 3 8 2 14.82 15.81 30.45 o 4 8 2 216.49 209.14 18.27 o 5 8 2 55.49 54.75 20.01 o 6 8 2 10.55 9.42 24.73 o -4 9 2 615.14 579.32 22.55 o -3 9 2 9.18 8.02 28.22 o -2 9 2 218.09 210.19 32.30 o -1 9 2 52.62 59.02 21.87 o 0 9 2 0.12 3.64 30.48 o 1 9 2 1.29 -2.99 30.31 o 2 9 2 18.44 21.77 29.60 o 3 9 2 70.78 62.22 20.71 o 4 9 2 7.50 4.31 25.74 o -2 10 2 0.05 1.37 23.86 o -1 10 2 9.71 8.79 25.26 o 0 10 2 20.69 23.70 26.03 o 1 10 2 18.48 8.84 25.36 o 2 10 2 19.13 15.09 23.88 o -9 0 3 0.35 -0.89 42.23 o -7 0 3 632.99 630.11 36.14 o -5 0 3 36.97 20.09 16.12 o -3 0 3 2189.64 2200.24 33.45 o -1 0 3 632.14 595.84 11.93 o 1 0 3 2913.23 2756.52 29.61 o 3 0 3 683.68 697.14 20.51 o 5 0 3 3856.55 3878.43 61.74 o 7 0 3 15.34 5.46 38.87 o 9 0 3 219.21 221.13 25.18 o -10 1 3 45.44 39.76 24.85 o -9 1 3 5.95 2.12 29.78 o -8 1 3 122.81 135.25 17.90 o -7 1 3 57.67 60.16 16.77 o -6 1 3 100.72 125.50 12.78 o -5 1 3 132.97 130.81 10.00 o -4 1 3 6599.73 6545.48 125.07 o -3 1 3 1363.29 1302.84 32.37 o -2 1 3 13304.63 13310.85 199.63 o -1 1 3 294.88 261.00 6.83 o 0 1 3 1946.87 1927.01 16.09 o 1 1 3 5304.98 5350.71 45.11 o 2 1 3 48.73 50.01 4.07 o 3 1 3 295.22 311.13 11.82 o 4 1 3 61.87 61.58 7.60 o 5 1 3 28.90 22.72 14.04 o 6 1 3 222.27 223.32 14.08 o 7 1 3 113.45 128.49 16.69 o 8 1 3 2.93 11.01 30.69 o 9 1 3 29.69 15.67 29.28 o -10 2 3 3.15 12.94 23.30 o -9 2 3 4.13 12.69 29.26 o -8 2 3 602.32 581.26 25.05 o -7 2 3 432.89 444.76 19.75 o -6 2 3 26.38 37.22 18.43 o -5 2 3 466.57 364.92 30.68 o -4 2 3 900.11 899.29 76.27 o -3 2 3 394.49 349.86 13.39 o -2 2 3 1.90 5.84 8.07 o -1 2 3 1380.23 1336.11 15.71 o 0 2 3 950.13 962.70 12.66 o 1 2 3 24143.84 25735.31 417.70 o 2 2 3 3.42 7.86 7.96 o 3 2 3 302.90 310.10 13.22 o 4 2 3 110.63 126.75 8.70 o 5 2 3 376.30 370.38 15.30 o 6 2 3 500.09 518.04 19.87 o 7 2 3 11.17 9.89 28.51 o 8 2 3 18.48 23.99 30.99 o 9 2 3 13.37 13.72 28.33 o -9 3 3 4.06 4.91 28.16 o -8 3 3 4.15 -10.79 31.03 o -7 3 3 104.03 100.80 17.10 o -6 3 3 55.07 52.66 15.72 o -5 3 3 14.62 17.31 19.78 o -4 3 3 18.08 43.46 10.22 o -3 3 3 772.99 818.74 21.28 o -2 3 3 700.46 647.01 15.83 o -1 3 3 1161.18 1152.39 27.19 o 0 3 3 710.74 718.35 13.83 o 1 3 3 2961.18 3070.22 43.66 o 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