#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/00/80/2008043.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2008043_Fobs loop_ _publ_author_name 'Jeong, J. H.' 'Kim, D. Y.' 'Lee, D. J.' 'Lee, B. W.' 'Doh, M. K.' _publ_section_title ; Oxonium \L-{N,N'-bis[2(S)-pyrrolidinylmethyl]ethane-1,2-diamine}-cis-\a-dichlorocobalt(III) dichloride dihydrate ; _journal_issue 1 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 56 _journal_page_last 58 _journal_volume 55 _journal_year 1999 _space_group_IT_number 96 _symmetry_space_group_name_Hall 'P 4nw 2abw' _symmetry_space_group_name_H-M 'P 43 21 2' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 12.8517 _cell_length_b 12.8517 _cell_length_c 13.0371 _exptl_crystal_F_000 996.00 _reflns_d_resolution_high 0.8024 _[local]_cod_data_source_file bk1391sup2.hkl _[local]_cod_data_source_block BK1391 #BEGIN Tags that were not found in dictionaries: _shelx_title ' JJH971' _shelx_refln_list_code 4 _shelx_f_calc_maximum 359.90 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z+1/2' '-y+1/2, x+1/2, z+3/4' 'y+1/2, -x+1/2, z+1/4' '-x+1/2, y+1/2, -z+3/4' 'x+1/2, -y+1/2, -z+1/4' 'y, x, -z' '-y, -x, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 2 0 8415.97 8450.99 395.11 o 1 2 0 18952.94 21124.38 614.55 o 2 2 0 10275.49 10357.36 186.49 o 1 3 0 497.17 538.09 20.71 o 2 3 0 1006.26 852.09 23.97 o 3 3 0 8359.69 9275.43 210.42 o 0 4 0 28649.76 29547.00 2020.68 o 1 4 0 1803.66 2275.55 127.88 o 2 4 0 114.80 113.57 25.97 o 3 4 0 3086.07 3037.73 68.66 o 4 4 0 636.15 610.23 34.82 o 1 5 0 319.91 420.86 21.82 o 2 5 0 15447.51 15191.90 465.12 o 3 5 0 4833.58 4728.81 177.00 o 4 5 0 3039.85 2958.61 63.65 o 5 5 0 240.54 216.97 31.14 o 0 6 0 34681.79 35024.33 1367.14 o 1 6 0 8840.86 9259.02 174.57 o 2 6 0 737.08 781.86 57.33 o 3 6 0 174.91 159.03 21.50 o 4 6 0 4255.82 4076.87 179.22 o 5 6 0 4743.77 4800.51 136.65 o 6 6 0 8421.96 8272.39 192.31 o 1 7 0 1922.35 1939.23 165.89 o 2 7 0 4719.52 4929.06 99.29 o 3 7 0 291.52 311.89 22.83 o 4 7 0 283.78 303.58 46.15 o 5 7 0 2489.19 2546.34 51.21 o 6 7 0 4111.22 3877.65 83.77 o 7 7 0 2465.79 2219.82 66.41 o 0 8 0 1529.83 1377.64 35.19 o 1 8 0 562.31 657.05 81.81 o 2 8 0 5.13 20.99 21.63 o 3 8 0 304.89 254.62 24.81 o 4 8 0 172.79 134.53 24.14 o 5 8 0 1934.29 1855.36 48.60 o 6 8 0 1729.93 1688.30 41.93 o 7 8 0 1239.29 1080.54 261.08 o 8 8 0 313.14 280.18 44.83 o 1 9 0 334.48 349.24 28.13 o 2 9 0 220.45 217.97 26.13 o 5 9 0 160.76 226.03 26.39 o 6 9 0 142.22 173.08 25.36 o 7 9 0 840.47 816.47 82.18 o 8 9 0 62.96 70.93 35.62 o 9 9 0 108.83 60.10 37.15 o 0 10 0 6518.16 6421.41 382.98 o 3 10 0 58.82 126.37 30.90 o 6 10 0 861.70 883.03 39.89 o 7 10 0 33.01 63.43 33.12 o 8 10 0 178.63 172.78 30.47 o 9 10 0 15.98 62.87 34.65 o 1 11 0 97.11 82.02 32.55 o 2 11 0 3719.63 3713.61 81.83 o 4 11 0 983.35 1109.06 68.28 o 5 11 0 186.14 209.77 40.83 o 6 11 0 2101.67 2237.71 56.43 o 7 11 0 265.86 226.89 33.05 o 8 11 0 1246.95 1337.37 96.72 o 9 11 0 53.28 99.46 40.06 o 10 11 0 147.84 147.85 32.25 o 0 12 0 600.74 629.45 41.14 o 1 12 0 995.10 937.51 69.70 o 2 12 0 144.14 180.47 28.39 o 4 12 0 65.60 116.28 47.12 o 5 12 0 1459.80 1476.35 49.34 o 7 12 0 429.07 444.88 43.00 o 9 12 0 30.21 32.59 37.42 o 1 13 0 1063.08 1106.50 47.22 o 2 13 0 199.13 277.83 38.77 o 3 13 0 461.58 450.61 40.48 o 4 13 0 88.26 138.53 37.33 o 5 13 0 461.99 405.70 46.13 o 7 13 0 1203.70 1222.29 62.54 o 9 13 0 472.45 493.97 43.09 o 0 14 0 457.24 430.81 51.20 o 1 14 0 170.73 175.68 43.64 o 3 14 0 0.62 43.42 33.90 o 5 14 0 46.36 66.26 37.29 o 6 14 0 170.85 161.83 46.62 o 1 15 0 68.65 104.44 43.21 o 2 15 0 95.05 126.37 42.78 o 3 15 0 94.26 87.87 40.30 o 4 15 0 22.65 99.46 37.95 o 0 16 0 804.22 903.84 108.18 o 1 1 1 8838.41 7625.31 123.09 o -1 2 1 7430.09 6904.66 146.41 o 0 2 1 14439.73 14669.42 636.41 o 1 2 1 7922.20 8355.93 154.62 o 2 2 1 97.39 85.89 24.17 o -2 3 1 1258.19 1217.10 36.88 o -1 3 1 1148.29 1239.33 39.70 o 0 3 1 836.78 839.22 64.43 o 1 3 1 1098.85 1239.33 39.70 o 2 3 1 995.31 974.82 35.21 o 3 3 1 2445.97 2475.85 73.64 o -2 4 1 2342.74 2256.50 66.96 o -1 4 1 5455.32 5591.72 163.38 o 0 4 1 15538.92 16742.92 1265.33 o 1 4 1 5519.09 5660.44 116.66 o 2 4 1 2277.69 2643.42 76.10 o 4 4 1 3927.25 3855.38 113.78 o -4 5 1 563.53 596.38 34.42 o -3 5 1 782.25 759.40 36.90 o -2 5 1 5371.00 5450.33 124.88 o -1 5 1 5203.35 5228.89 122.31 o 0 5 1 26279.71 27237.96 1883.39 o 1 5 1 5276.61 5697.62 133.00 o 2 5 1 5339.20 5341.61 128.78 o 3 5 1 1003.75 1005.87 40.23 o 4 5 1 733.93 751.65 38.65 o -5 6 1 2022.90 2101.89 58.16 o -4 6 1 4078.12 4045.84 125.52 o -3 6 1 2444.32 2256.50 77.00 o -2 6 1 8377.19 8563.36 234.79 o -1 6 1 7085.00 7466.13 213.14 o 0 6 1 10808.70 11731.89 975.79 o 1 6 1 7206.47 8537.29 247.46 o 2 6 1 8245.21 8740.36 250.38 o 3 6 1 2400.67 2233.12 66.61 o 4 6 1 4213.00 3983.33 106.76 o 5 6 1 2270.63 2286.73 67.41 o 6 6 1 8714.53 8760.14 197.89 o -6 7 1 2438.89 2600.11 75.47 o -5 7 1 2445.56 2440.90 62.68 o -4 7 1 1010.51 1039.67 43.18 o -3 7 1 389.35 333.21 33.45 o -2 7 1 2794.88 2625.33 75.83 o -1 7 1 2554.28 2610.90 82.83 o 0 7 1 2184.72 2136.63 86.58 o 1 7 1 2460.50 2790.35 74.46 o 2 7 1 2960.77 3049.25 85.62 o 3 7 1 441.73 500.73 37.85 o 4 7 1 1074.02 1168.42 48.18 o 5 7 1 2432.96 2458.35 73.38 o 6 7 1 2464.32 2535.82 78.08 o 7 7 1 423.07 352.78 42.36 o -7 8 1 1091.47 1092.60 51.25 o -6 8 1 1101.90 1217.10 51.63 o -5 8 1 1215.77 1207.28 48.98 o -4 8 1 684.54 711.62 41.36 o -2 8 1 725.71 641.97 37.50 o -1 8 1 1896.00 1836.21 54.36 o 0 8 1 2657.80 2793.09 246.50 o 1 8 1 1852.76 1863.49 60.85 o 2 8 1 687.52 659.95 45.26 o 4 8 1 728.55 704.12 44.88 o 5 8 1 1213.23 1219.56 56.61 o 6 8 1 1093.59 1151.62 52.62 o 7 8 1 1081.04 1111.31 54.04 o 8 8 1 209.09 162.73 43.16 o -8 9 1 139.85 124.00 36.89 o -7 9 1 245.97 200.68 39.94 o -6 9 1 659.58 687.39 46.20 o -5 9 1 970.08 884.59 50.31 o -4 9 1 372.20 343.58 37.89 o -3 9 1 944.76 861.68 45.51 o -2 9 1 678.55 598.10 41.37 o 0 9 1 1215.00 1246.05 37.05 o 2 9 1 610.48 652.73 48.62 o 3 9 1 973.14 1120.73 54.27 o 4 9 1 418.52 445.56 46.12 o 5 9 1 959.32 952.93 54.39 o 6 9 1 602.32 629.53 47.75 o 7 9 1 192.74 93.23 41.51 o 8 9 1 123.74 141.87 38.62 o 9 9 1 11.98 36.31 32.28 o -9 10 1 134.43 129.56 41.71 o -8 10 1 146.14 69.16 38.68 o -7 10 1 139.30 110.28 37.75 o -6 10 1 1425.01 1427.07 61.24 o -5 10 1 101.32 100.87 36.81 o -4 10 1 973.86 970.42 48.30 o -3 10 1 201.93 108.80 33.82 o -2 10 1 1197.68 1212.18 51.53 o 0 10 1 471.99 454.40 81.54 o 2 10 1 1275.32 1440.41 64.20 o 4 10 1 869.29 784.85 55.29 o 6 10 1 1458.13 1369.09 67.80 o 7 10 1 116.84 107.34 43.08 o 8 10 1 109.71 42.96 36.96 o 9 10 1 139.49 160.94 44.71 o 10 10 1 143.54 212.84 45.24 o -9 11 1 611.39 650.93 55.74 o -8 11 1 396.50 368.85 46.02 o -7 11 1 962.81 972.62 57.15 o -6 11 1 882.78 882.49 54.44 o -5 11 1 182.49 82.02 38.30 o -4 11 1 308.49 317.95 41.47 o -3 11 1 346.74 366.15 43.16 o -1 11 1 660.11 694.80 44.59 o 0 11 1 3075.73 3281.86 94.87 o 1 11 1 641.70 658.14 61.47 o 3 11 1 386.33 399.23 52.10 o 4 11 1 328.64 368.85 52.79 o 6 11 1 816.01 771.09 60.67 o 7 11 1 956.43 867.90 64.37 o 8 11 1 417.65 265.06 55.08 o 9 11 1 664.92 717.27 58.51 o 10 11 1 296.14 316.69 50.17 o -10 12 1 369.77 374.28 54.54 o -9 12 1 273.89 274.32 49.03 o -7 12 1 809.73 812.74 56.26 o -6 12 1 1476.40 1390.04 68.32 o -5 12 1 364.25 254.83 46.13 o -4 12 1 289.79 225.36 43.38 o -3 12 1 768.80 738.18 51.70 o -1 12 1 831.89 855.48 53.60 o 0 12 1 2065.33 2039.94 92.70 o 1 12 1 811.98 828.89 68.99 o 3 12 1 845.76 804.72 61.98 o 4 12 1 323.87 340.97 50.76 o 5 12 1 413.41 343.58 57.48 o 6 12 1 1484.46 1353.49 75.19 o 7 12 1 800.35 724.84 62.62 o 9 12 1 300.84 326.81 52.24 o 10 12 1 360.82 354.11 54.38 o -8 13 1 506.80 492.87 56.33 o -6 13 1 412.12 478.89 47.81 o -5 13 1 610.51 570.84 55.57 o -4 13 1 423.21 417.74 48.98 o -3 13 1 252.91 207.73 43.68 o -2 13 1 985.38 1134.93 59.36 o 2 13 1 965.90 1012.58 74.01 o 3 13 1 236.71 258.22 55.49 o 4 13 1 422.78 344.89 61.52 o 5 13 1 611.70 681.85 62.57 o 6 13 1 416.10 375.65 58.74 o 8 13 1 532.13 605.01 58.94 o -7 14 1 69.91 86.55 41.31 o -5 14 1 148.37 110.28 45.15 o -2 14 1 200.16 185.02 39.31 o -1 14 1 164.94 127.96 42.25 o 0 14 1 153.75 34.22 36.28 o 1 14 1 150.59 95.97 58.69 o 2 14 1 180.54 69.75 51.80 o 5 14 1 131.65 92.55 50.17 o -4 15 1 57.49 100.16 40.20 o -3 15 1 40.18 109.54 36.14 o -1 15 1 70.81 171.85 37.88 o 0 15 1 446.10 387.70 44.30 o 2 15 1 168.88 184.07 60.24 o 0 1 2 7386.47 8970.22 614.65 o 1 1 2 4990.02 4741.37 121.32 o -1 2 2 4189.79 4204.27 91.40 o 0 2 2 2000.31 1974.96 127.59 o 1 2 2 4333.84 4553.99 133.17 o 2 2 2 15539.69 17046.34 248.45 o -2 3 2 1376.82 1304.68 43.28 o -1 3 2 1677.80 1824.15 45.15 o 0 3 2 5184.04 5247.63 769.67 o 1 3 2 1750.75 1909.41 61.59 o 2 3 2 1394.03 1488.96 38.07 o 3 3 2 1677.95 1541.08 47.03 o -3 4 2 627.64 670.86 31.03 o -2 4 2 5562.82 5983.07 174.45 o -1 4 2 2157.88 2082.54 64.33 o 0 4 2 4797.15 5197.88 277.14 o 1 4 2 2306.95 2344.38 71.66 o 2 4 2 5780.12 5912.41 130.06 o 3 4 2 634.05 694.80 33.44 o 4 4 2 2303.41 2310.38 67.75 o -4 5 2 597.22 638.40 33.83 o -3 5 2 1085.65 1204.83 39.14 o -2 5 2 2264.77 2196.64 62.76 o -1 5 2 172.98 114.01 24.83 o 0 5 2 578.97 594.08 35.36 o 1 5 2 158.58 165.44 29.01 o 2 5 2 2298.73 2276.63 60.53 o 3 5 2 1129.71 1259.26 42.52 o 4 5 2 618.23 634.84 35.52 o 5 5 2 7759.80 7631.46 172.39 o -5 6 2 1125.15 1094.93 44.31 o -4 6 2 4955.27 4799.78 141.60 o -3 6 2 1969.23 1993.46 53.49 o -2 6 2 5742.28 5591.72 142.30 o -1 6 2 1761.56 1622.36 48.26 o 0 6 2 305.31 315.19 22.76 o 1 6 2 1876.63 1915.57 61.69 o 2 6 2 5821.50 5983.07 152.64 o 3 6 2 2018.92 1993.46 56.64 o 4 6 2 4810.59 4587.35 143.21 o 5 6 2 1101.30 1071.73 46.15 o 6 6 2 1728.61 1662.35 54.60 o -6 7 2 5614.72 5419.16 166.02 o -5 7 2 141.63 152.99 29.64 o -4 7 2 2055.45 2044.13 63.73 o -3 7 2 2609.70 2636.17 75.99 o -1 7 2 418.73 347.51 31.53 o 0 7 2 10040.21 9801.83 493.33 o 1 7 2 363.44 381.13 37.15 o 2 7 2 31.77 56.34 28.57 o 3 7 2 2526.70 2532.28 78.03 o 4 7 2 1996.31 2050.51 57.45 o 5 7 2 180.53 178.37 36.71 o 6 7 2 5613.68 5761.64 171.19 o 7 7 2 46.03 56.87 29.76 o -7 8 2 465.67 364.80 43.08 o -6 8 2 1550.46 1574.46 55.93 o -5 8 2 436.21 450.04 38.87 o -4 8 2 1309.56 1231.89 49.47 o -3 8 2 1178.54 1085.62 46.44 o -2 8 2 1733.61 1563.29 50.16 o -1 8 2 789.24 711.62 39.48 o 0 8 2 229.48 239.31 23.54 o 1 8 2 797.80 830.92 46.73 o 2 8 2 1826.92 1746.72 58.91 o 3 8 2 1196.72 1163.60 50.49 o 4 8 2 1246.92 1185.34 50.96 o 5 8 2 448.31 471.21 41.31 o 6 8 2 1595.92 1588.47 58.99 o 7 8 2 487.50 579.29 44.10 o 8 8 2 230.24 343.58 41.80 o -7 9 2 294.78 248.12 44.41 o -6 9 2 1875.35 1848.31 60.60 o -4 9 2 604.68 680.01 42.27 o -3 9 2 267.65 301.82 34.28 o -2 9 2 242.89 271.99 32.55 o -1 9 2 467.27 439.63 35.47 o 0 9 2 7000.28 6968.95 336.50 o 1 9 2 564.27 577.60 49.12 o 2 9 2 211.47 293.31 43.45 o 3 9 2 257.38 207.73 41.65 o 4 9 2 685.27 767.18 46.85 o 5 9 2 156.76 153.87 41.09 o 6 9 2 1769.64 1714.47 64.20 o 7 9 2 339.31 281.36 47.29 o -9 10 2 194.70 169.09 43.07 o -8 10 2 148.14 203.69 42.25 o -7 10 2 963.27 1019.32 56.25 o -6 10 2 287.13 306.74 43.20 o -5 10 2 462.56 426.43 46.57 o -2 10 2 319.88 350.14 36.93 o -1 10 2 1190.48 1168.42 50.59 o 0 10 2 128.40 141.87 32.74 o 1 10 2 1350.23 1379.55 65.44 o 2 10 2 324.47 340.97 48.15 o 5 10 2 426.84 704.12 67.33 o 6 10 2 290.99 188.88 48.43 o 7 10 2 1051.99 1251.76 64.83 o 8 10 2 126.45 176.50 41.20 o 9 10 2 193.19 184.07 44.94 o -9 11 2 70.33 107.34 40.16 o -8 11 2 131.25 110.28 38.49 o -7 11 2 310.23 275.48 46.79 o -5 11 2 2235.60 2293.47 74.26 o -3 11 2 32.75 64.55 32.84 o -2 11 2 105.01 169.09 36.66 o -1 11 2 2770.53 2831.45 86.26 o 0 11 2 365.34 328.08 32.10 o 1 11 2 2707.24 3037.58 97.11 o 2 11 2 100.40 118.57 46.05 o 5 11 2 2209.34 2150.63 81.71 o 7 11 2 281.98 307.97 49.47 o 8 11 2 125.77 181.21 41.74 o 9 11 2 61.51 120.88 40.29 o 11 11 2 1100.37 1071.73 71.53 o -10 12 2 157.38 47.71 42.84 o -8 12 2 1126.42 1127.82 63.91 o -7 12 2 216.03 251.47 45.82 o -6 12 2 1155.90 1190.20 63.22 o -4 12 2 1670.65 1682.52 66.49 o -2 12 2 2290.19 2157.18 72.01 o 0 12 2 182.91 212.84 37.02 o 2 12 2 2369.36 2313.77 88.14 o 4 12 2 1655.57 1524.52 79.80 o 6 12 2 1180.78 1236.85 69.40 o 7 12 2 188.45 239.32 50.15 o 8 12 2 1169.43 1101.94 67.85 o 10 12 2 159.67 126.37 49.91 o -7 13 2 5.26 35.05 35.47 o -6 13 2 1601.77 1628.04 73.94 o -5 13 2 90.15 107.34 44.54 o -4 13 2 849.13 828.89 56.82 o -2 13 2 115.40 158.27 38.13 o -1 13 2 97.09 103.72 39.48 o 0 13 2 3197.03 3404.07 74.93 o 4 13 2 857.06 753.58 67.72 o 5 13 2 91.25 208.75 50.91 o 6 13 2 1612.38 1688.31 81.09 o 8 13 2 102.60 150.39 48.40 o -7 14 2 178.69 175.56 46.69 o -6 14 2 136.41 86.55 41.96 o -5 14 2 111.71 123.22 39.12 o -3 14 2 163.57 162.73 40.46 o -1 14 2 282.51 352.78 45.01 o 1 14 2 284.07 194.74 64.91 o 6 14 2 142.69 118.57 49.88 o 7 14 2 187.49 255.96 53.00 o -5 15 2 163.94 93.91 49.18 o -2 15 2 33.88 94.60 40.44 o -1 15 2 163.99 249.24 44.51 o 0 15 2 385.40 379.07 86.85 o 1 1 3 405.67 414.87 27.28 o -1 2 3 5529.11 5692.30 164.84 o 0 2 3 11309.73 11318.44 698.47 o 1 2 3 5157.42 5633.96 158.70 o 2 2 3 2612.67 2557.16 67.72 o -2 3 3 1737.20 1582.86 47.67 o -1 3 3 3177.85 3584.61 97.05 o 0 3 3 339.94 408.38 37.88 o 1 3 3 3197.60 3593.05 101.39 o 2 3 3 2081.94 2092.20 67.70 o 3 3 3 1564.94 1535.55 46.95 o -3 4 3 551.50 531.14 32.49 o -2 4 3 2966.50 2941.25 80.27 o -1 4 3 6710.87 6444.10 192.36 o 0 4 3 5492.66 6113.91 325.74 o 1 4 3 6812.06 7551.63 208.24 o 2 4 3 3152.34 3315.58 105.51 o 3 4 3 614.46 580.99 33.98 o 4 4 3 90.53 111.76 25.33 o -4 5 3 3582.06 3368.54 94.08 o -3 5 3 1241.21 1254.26 39.94 o -2 5 3 397.87 351.46 29.07 o -1 5 3 5209.69 5249.30 127.66 o 0 5 3 9298.96 9409.13 980.59 o 1 5 3 5455.87 6297.84 145.42 o 2 5 3 428.95 451.53 31.45 o 3 5 3 1120.84 1163.60 40.87 o 4 5 3 3615.32 3471.58 99.66 o 5 5 3 415.57 399.23 33.80 o -5 6 3 419.82 478.89 35.47 o -4 6 3 3251.72 3323.70 97.52 o -3 6 3 2685.04 2416.59 83.15 o -2 6 3 7535.57 7362.97 163.29 o -1 6 3 891.19 832.96 36.61 o 0 6 3 9461.84 9397.91 311.50 o 1 6 3 829.11 903.55 40.25 o 2 6 3 7549.02 7817.29 174.48 o 3 6 3 2529.74 2489.90 77.37 o 4 6 3 3078.64 3263.03 100.65 o 5 6 3 335.22 346.20 34.10 o 6 6 3 5894.12 5528.66 162.45 o -6 7 3 1460.30 1427.07 55.91 o -5 7 3 2641.56 2610.90 79.23 o -4 7 3 484.82 508.64 36.56 o -3 7 3 324.55 358.10 30.68 o -2 7 3 1058.01 1101.94 39.77 o -1 7 3 1852.70 1732.03 52.80 o 0 7 3 1530.77 1665.74 134.83 o 1 7 3 1964.12 2044.13 57.36 o 2 7 3 1042.14 1005.87 49.18 o 3 7 3 264.09 284.92 35.69 o 4 7 3 479.62 432.27 39.56 o 5 7 3 2533.84 2636.17 79.61 o 6 7 3 1411.30 1588.47 56.18 o 7 7 3 790.69 747.79 48.18 o -7 8 3 77.26 121.66 32.65 o -6 8 3 1657.90 1633.74 59.82 o -5 8 3 556.64 557.45 41.60 o -4 8 3 367.38 371.56 36.68 o -3 8 3 277.71 276.66 32.82 o -2 8 3 1172.43 1137.31 45.16 o -1 8 3 925.98 912.05 42.57 o 0 8 3 3361.18 3242.02 90.33 o 1 8 3 1045.03 1168.42 53.00 o 2 8 3 1253.31 1314.88 53.67 o 3 8 3 246.39 319.21 39.04 o 4 8 3 330.62 329.36 40.93 o 5 8 3 536.06 599.82 46.61 o 6 8 3 1740.52 1746.72 61.86 o 8 8 3 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