#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2008357.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2008357_Fobs loop_ _publ_author_name 'Fun, H.-K.' 'Chinnakali, K.' 'Razak, I. A.' 'Lu, Z.-L.' 'Kang, B.-S.' _publ_section_title ; p-Hydroxybenzaldehyde nicotinoylhydrazone monohydrate ; _journal_issue 4 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 574 _journal_page_last 576 _journal_volume 55 _journal_year 1999 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 91.126 _cell_angle_gamma 90.000 _cell_length_a 27.7745 _cell_length_b 7.3270 _cell_length_c 11.9575 _exptl_crystal_F_000 1088.00 _reflns_d_resolution_high 0.7108 _[local]_cod_data_source_file fr1156sup2.hkl _[local]_cod_data_source_block lg004m #BEGIN Tags that were not found in dictionaries: _shelx_title ' FR1156 in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 371.60 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 6 0 0 12615.65 12055.68 360.55 o 8 0 0 145.32 140.57 11.83 o 10 0 0 2739.47 2691.43 85.80 o 12 0 0 501.46 507.61 22.54 o 14 0 0 705.43 892.70 34.37 o 16 0 0 4337.03 4185.13 132.11 o 18 0 0 419.40 393.05 22.53 o 20 0 0 175.76 152.72 16.60 o 22 0 0 3998.42 3839.58 146.68 o 24 0 0 54.93 42.95 40.52 o 26 0 0 1021.85 975.41 52.43 o 28 0 0 518.17 484.34 29.69 o 30 0 0 657.46 620.35 48.63 o 32 0 0 1.85 -27.01 20.53 o 34 0 0 8.23 -10.80 21.61 o 36 0 0 290.41 284.19 39.98 o 38 0 0 68.30 43.22 25.93 o 3 1 0 160.24 184.98 10.70 o 5 1 0 12.12 6.54 8.39 o 7 1 0 1143.07 1148.80 32.84 o 9 1 0 1171.62 1016.03 25.67 o 11 1 0 24.18 24.91 6.54 o 13 1 0 82.85 89.97 8.31 o 15 1 0 4602.65 4509.82 100.01 o 17 1 0 1512.78 1552.21 38.98 o 19 1 0 1980.75 1956.07 59.79 o 21 1 0 2347.70 2266.73 54.96 o 23 1 0 1226.36 1118.42 31.92 o 25 1 0 397.68 372.67 20.77 o 27 1 0 224.84 188.25 17.38 o 29 1 0 9.31 9.45 17.89 o 31 1 0 82.28 107.00 18.34 o 33 1 0 2.17 28.95 16.76 o 35 1 0 320.30 389.20 32.06 o 37 1 0 132.44 173.51 25.59 o 0 2 0 6931.16 6709.79 290.02 o 2 2 0 28059.32 27529.69 670.98 o 4 2 0 3867.79 3964.34 100.23 o 6 2 0 1843.84 1919.11 43.98 o 8 2 0 10.36 16.46 6.79 o 10 2 0 719.28 776.83 21.29 o 12 2 0 457.02 427.59 12.88 o 14 2 0 1767.15 1850.75 44.60 o 16 2 0 1934.21 1881.20 60.58 o 18 2 0 812.96 818.26 24.69 o 20 2 0 795.20 797.61 32.89 o 22 2 0 1438.18 1433.28 46.01 o 24 2 0 2.16 11.16 12.14 o 26 2 0 46.91 26.01 19.34 o 28 2 0 3.03 9.25 12.19 o 30 2 0 131.15 119.42 16.75 o 32 2 0 1.15 35.88 14.01 o 34 2 0 61.61 82.19 22.53 o 36 2 0 0.07 15.13 30.25 o 38 2 0 55.16 64.83 34.58 o 1 3 0 2040.86 2047.46 66.94 o 3 3 0 5.99 3.51 6.31 o 5 3 0 2.44 3.69 6.58 o 7 3 0 176.65 168.91 9.83 o 9 3 0 82.11 88.16 8.66 o 11 3 0 22.86 19.74 7.45 o 13 3 0 225.92 220.02 12.41 o 15 3 0 1336.24 1274.75 33.84 o 17 3 0 1705.01 1637.69 49.03 o 19 3 0 1033.59 1034.56 39.48 o 21 3 0 4842.03 4604.83 121.25 o 23 3 0 85.62 108.50 15.31 o 25 3 0 6.68 3.58 15.87 o 27 3 0 50.98 68.11 14.59 o 29 3 0 469.19 492.55 37.28 o 31 3 0 0.00 16.70 18.15 o 33 3 0 121.47 157.16 26.61 o 35 3 0 169.16 167.63 27.51 o 37 3 0 157.55 218.74 65.91 o 0 4 0 3457.71 3787.19 170.03 o 2 4 0 3739.90 3678.38 95.18 o 4 4 0 3293.25 3546.13 92.41 o 6 4 0 1785.42 1801.21 50.78 o 8 4 0 1375.45 1451.54 36.78 o 10 4 0 75.25 55.64 9.73 o 12 4 0 0.03 20.24 19.42 o 14 4 0 267.65 269.90 14.44 o 16 4 0 363.99 339.44 19.37 o 18 4 0 10.93 -7.53 10.00 o 20 4 0 445.62 434.32 23.37 o 22 4 0 304.81 312.87 20.96 o 24 4 0 3.00 26.33 35.66 o 26 4 0 117.72 135.48 24.13 o 28 4 0 9.50 33.46 28.09 o 30 4 0 234.02 255.40 38.90 o 32 4 0 65.87 57.37 35.12 o 34 4 0 1.80 36.48 22.07 o 36 4 0 33.21 92.13 49.16 o 1 5 0 41.89 66.41 11.39 o 3 5 0 42.59 50.11 10.38 o 5 5 0 23.33 13.27 8.72 o 7 5 0 8.00 20.63 11.54 o 9 5 0 0.75 14.11 14.53 o 11 5 0 61.15 41.70 16.45 o 13 5 0 79.17 79.26 14.99 o 15 5 0 0.29 51.22 30.25 o 17 5 0 274.63 275.95 40.52 o 19 5 0 3530.12 3558.08 123.89 o 21 5 0 187.54 167.86 24.31 o 23 5 0 26.35 59.73 26.47 o 25 5 0 48.66 41.47 21.19 o 27 5 0 37.06 56.08 45.92 o 29 5 0 15.93 29.37 21.76 o 31 5 0 197.55 245.16 31.85 o 33 5 0 91.95 128.41 28.28 o 0 6 0 76.41 83.05 15.65 o 2 6 0 479.74 518.44 22.81 o 4 6 0 1652.75 1668.35 43.19 o 6 6 0 1365.95 1533.51 47.84 o 8 6 0 242.15 238.95 18.24 o 10 6 0 168.44 184.29 20.74 o 12 6 0 51.42 47.96 17.85 o 14 6 0 82.20 99.59 18.92 o 16 6 0 166.90 202.99 23.84 o 18 6 0 1220.00 1236.15 67.02 o 20 6 0 11.65 23.99 19.78 o 22 6 0 210.02 203.32 34.04 o 24 6 0 6.14 -3.24 32.41 o 26 6 0 0.53 3.70 20.75 o 28 6 0 87.29 132.70 56.19 o 30 6 0 0.06 -15.13 37.82 o 1 7 0 11.74 10.82 9.60 o 3 7 0 58.48 39.55 16.45 o 5 7 0 233.31 239.33 19.08 o 7 7 0 77.12 106.64 15.16 o 9 7 0 1.02 14.05 24.85 o 11 7 0 82.27 81.79 30.25 o 13 7 0 61.44 62.32 26.47 o 15 7 0 18.54 24.85 32.41 o 17 7 0 975.32 1068.86 78.90 o 19 7 0 40.12 12.59 44.84 o 21 7 0 76.01 76.14 24.31 o 23 7 0 3.93 -16.91 19.17 o 25 7 0 7.75 -12.97 20.75 o 27 7 0 28.15 36.86 27.01 o 2 8 0 16.74 16.42 17.08 o 4 8 0 189.54 194.59 18.70 o 6 8 0 28.96 18.71 13.45 o 8 8 0 11.38 47.54 24.85 o 10 8 0 92.51 69.72 35.12 o 12 8 0 0.58 -2.79 27.55 o 14 8 0 33.81 19.34 20.58 o 16 8 0 31.95 31.33 28.09 o 18 8 0 119.05 120.51 29.17 o 20 8 0 0.01 46.46 36.74 o 22 8 0 5.24 -10.12 20.75 o 24 8 0 19.86 12.84 37.28 o 1 9 0 0.09 7.56 17.57 o 9 9 0 0.59 56.19 30.25 o 11 9 0 0.37 -0.56 19.96 o 13 9 0 0.71 55.10 31.33 o 15 9 0 190.02 169.84 28.91 o 17 9 0 73.78 14.28 25.18 o 0 10 0 2.63 -12.97 27.01 o 2 10 0 20.43 5.40 30.25 o 4 10 0 0.32 34.58 31.33 o -37 1 1 396.45 409.55 46.47 o -35 1 1 1.67 46.15 18.15 o -33 1 1 30.13 42.89 14.43 o -31 1 1 18.76 29.84 12.53 o -29 1 1 119.43 129.33 17.17 o -27 1 1 89.60 108.58 15.85 o -25 1 1 3168.53 2941.48 70.36 o -23 1 1 10238.75 9671.62 210.45 o -21 1 1 72.65 80.62 11.61 o -19 1 1 323.71 290.09 19.19 o -17 1 1 506.56 468.03 17.21 o -15 1 1 190.04 211.51 12.02 o -13 1 1 49.57 49.47 9.36 o -11 1 1 10.91 14.63 9.58 o -9 1 1 1619.20 1737.91 40.97 o -7 1 1 106.20 148.30 13.43 o -5 1 1 224.91 233.78 10.32 o -3 1 1 2964.68 2977.85 93.32 o -1 1 1 41.71 117.78 11.89 o 1 1 1 118.27 167.52 15.13 o 3 1 1 50.89 49.22 6.31 o 5 1 1 1625.90 1533.98 43.58 o 7 1 1 3780.63 3537.30 89.77 o 9 1 1 21.07 18.59 7.56 o 11 1 1 461.90 470.07 14.90 o 13 1 1 11593.63 11580.37 247.04 o 15 1 1 92.83 110.99 9.40 o 17 1 1 151.90 136.53 10.22 o 19 1 1 394.78 316.42 14.21 o 21 1 1 113.66 110.05 10.87 o 23 1 1 877.10 816.14 30.91 o 25 1 1 1326.29 1226.26 41.04 o 27 1 1 1355.79 1229.07 41.78 o 29 1 1 164.19 174.43 18.35 o 31 1 1 33.68 77.21 16.08 o 33 1 1 16.71 64.08 47.00 o 35 1 1 672.34 777.16 42.77 o 37 1 1 188.08 172.28 25.59 o -38 2 1 139.97 188.01 41.06 o -36 2 1 17.07 33.50 25.93 o -34 2 1 9.24 -11.71 16.76 o -32 2 1 166.72 179.04 30.80 o -30 2 1 71.58 78.81 15.14 o -28 2 1 84.76 80.83 14.75 o -26 2 1 150.40 137.13 16.07 o -24 2 1 3147.05 3175.39 87.71 o -22 2 1 1466.45 1384.63 44.83 o -20 2 1 211.89 199.47 16.06 o -18 2 1 0.00 4.05 8.52 o -16 2 1 22.89 39.54 9.01 o -14 2 1 1.06 5.74 7.04 o -12 2 1 184.95 162.00 15.55 o -10 2 1 2185.55 2072.13 42.92 o -8 2 1 5815.89 6088.03 117.60 o -6 2 1 743.93 819.97 19.29 o -4 2 1 2006.96 1957.13 52.29 o -2 2 1 138082.89 153212.59 3737.96 o 0 2 1 20070.07 19334.65 472.36 o 2 2 1 48024.75 49303.14 1199.10 o 4 2 1 65.13 57.15 8.51 o 6 2 1 12206.91 11452.27 242.58 o 8 2 1 1339.66 1275.87 36.39 o 10 2 1 2084.36 2096.22 56.81 o 12 2 1 968.35 1127.36 34.49 o 14 2 1 3702.07 3579.45 80.32 o 16 2 1 189.94 194.63 10.87 o 18 2 1 964.42 1087.59 36.08 o 20 2 1 1092.30 1058.14 37.66 o 22 2 1 194.25 207.06 17.02 o 24 2 1 565.52 523.51 24.68 o 26 2 1 682.72 635.26 27.78 o 28 2 1 588.75 567.40 27.72 o 30 2 1 1.99 24.44 17.36 o 32 2 1 1.33 18.39 14.14 o 34 2 1 271.42 307.52 22.90 o 36 2 1 108.90 107.88 40.52 o 38 2 1 19.57 117.77 37.82 o -37 3 1 35.09 57.43 24.61 o -35 3 1 104.39 114.66 24.91 o -33 3 1 1.97 16.97 23.77 o -31 3 1 113.49 149.55 24.66 o -29 3 1 155.10 181.04 25.18 o -27 3 1 609.27 593.07 36.92 o -25 3 1 7.50 3.90 16.75 o -23 3 1 158.58 156.36 16.27 o -21 3 1 5284.02 5219.25 135.98 o -19 3 1 395.50 371.32 20.79 o -17 3 1 2.45 12.11 10.34 o -15 3 1 308.57 349.03 13.03 o -13 3 1 104.44 96.43 8.76 o -11 3 1 103.97 102.34 8.43 o -9 3 1 2365.66 2422.03 49.91 o -7 3 1 37.38 43.95 15.13 o -5 3 1 68.03 66.81 9.20 o -3 3 1 542.95 529.03 18.92 o -1 3 1 101.53 116.75 11.06 o 1 3 1 106.44 98.58 8.47 o 3 3 1 203.39 245.97 11.72 o 5 3 1 9.11 11.02 7.19 o 7 3 1 1629.62 1726.38 41.18 o 9 3 1 33.11 29.58 7.19 o 11 3 1 800.64 821.33 23.55 o 13 3 1 1345.22 1429.32 36.22 o 15 3 1 3659.76 3775.80 99.46 o 17 3 1 533.43 558.30 24.45 o 19 3 1 483.36 443.88 22.59 o 21 3 1 3693.04 3597.07 97.31 o 23 3 1 143.15 136.54 15.56 o 25 3 1 3.34 30.03 13.27 o 27 3 1 622.23 628.57 29.53 o 29 3 1 392.42 418.27 24.74 o 31 3 1 27.19 37.41 17.16 o 33 3 1 151.76 189.02 71.32 o 35 3 1 1.08 -9.76 20.18 o 37 3 1 6.85 69.15 35.66 o -34 4 1 7.92 15.98 20.97 o -32 4 1 13.45 55.03 22.55 o -30 4 1 112.79 170.34 28.91 o -28 4 1 63.51 72.00 20.97 o -26 4 1 89.94 117.44 23.73 o -24 4 1 183.45 167.21 40.52 o -22 4 1 24.82 47.00 28.63 o -20 4 1 2743.16 2787.47 98.66 o -18 4 1 847.77 793.23 33.09 o -16 4 1 6.68 10.46 8.70 o -14 4 1 1225.92 1224.47 33.30 o -12 4 1 218.68 237.22 16.75 o -10 4 1 701.34 772.23 23.51 o -8 4 1 36.09 77.97 10.45 o -6 4 1 1153.40 1263.16 33.03 o -4 4 1 40827.20 41502.47 876.66 o -2 4 1 1555.08 1621.33 56.21 o 0 4 1 81.26 61.29 9.05 o 2 4 1 0.65 6.23 14.97 o 4 4 1 591.11 664.23 23.22 o 6 4 1 49.74 29.84 9.61 o 8 4 1 73.29 80.12 9.03 o 10 4 1 52.02 78.08 11.28 o 12 4 1 87.37 67.23 10.14 o 14 4 1 494.25 476.60 22.22 o 16 4 1 2462.43 2506.26 70.48 o 18 4 1 31.34 21.21 13.32 o 20 4 1 296.96 297.08 23.92 o 22 4 1 1035.19 1079.51 39.25 o 24 4 1 35.94 28.19 14.02 o 26 4 1 237.45 230.71 27.22 o 28 4 1 1.27 13.53 18.69 o 30 4 1 48.47 16.06 20.15 o 32 4 1 16.17 34.47 25.93 o 34 4 1 0.04 -2.18 20.46 o -33 5 1 21.97 11.78 22.07 o -31 5 1 309.78 366.25 38.17 o -29 5 1 403.38 403.27 51.87 o -27 5 1 1.29 -16.21 15.46 o -25 5 1 0.60 12.48 29.17 o -23 5 1 28.71 20.04 19.72 o -21 5 1 2.31 -5.21 27.01 o -19 5 1 3067.91 3037.36 107.02 o -17 5 1 552.49 576.69 34.93 o -15 5 1 3.07 8.42 27.55 o -13 5 1 1.47 -0.30 11.99 o -11 5 1 22.83 33.97 13.13 o -9 5 1 62.24 74.72 14.10 o -7 5 1 295.22 306.42 15.98 o -5 5 1 6.50 4.18 9.37 o -3 5 1 145.63 177.79 17.95 o -1 5 1 343.85 339.36 16.61 o 1 5 1 13.54 43.86 10.59 o 3 5 1 106.38 82.16 13.76 o 5 5 1 237.03 237.28 15.58 o 7 5 1 13.03 18.35 18.59 o 9 5 1 341.28 374.00 19.22 o 11 5 1 95.35 86.24 13.96 o 13 5 1 42.59 50.78 17.08 o 15 5 1 699.68 726.05 51.88 o 17 5 1 964.44 971.04 35.45 o 19 5 1 2989.26 3202.31 89.77 o 21 5 1 1.18 -26.45 15.54 o 23 5 1 1.09 0.75 17.13 o 25 5 1 38.85 43.58 32.42 o 27 5 1 105.89 104.92 24.61 o 29 5 1 196.14 238.07 30.00 o 31 5 1 0.66 -11.89 27.55 o 33 5 1 112.84 136.36 27.26 o -30 6 1 0.32 -20.88 20.39 o -28 6 1 0.71 -5.65 21.26 o -26 6 1 23.38 55.20 24.36 o -24 6 1 1.03 -13.14 19.05 o -22 6 1 14.76 36.94 51.32 o -20 6 1 17.22 -3.24 19.45 o -18 6 1 73.18 72.50 22.58 o -16 6 1 316.81 378.68 30.88 o -14 6 1 1.43 -12.97 18.37 o -12 6 1 0.03 -12.67 15.13 o -10 6 1 24.62 10.20 14.15 o -8 6 1 26.34 12.23 12.91 o -6 6 1 54.86 45.48 15.00 o -4 6 1 33.38 29.82 10.60 o -2 6 1 14.44 -1.64 12.94 o 0 6 1 367.44 362.69 18.92 o 2 6 1 732.55 719.89 27.01 o 6 6 1 211.38 221.64 19.07 o 8 6 1 1332.97 1361.94 43.57 o 10 6 1 101.87 86.76 19.20 o 12 6 1 191.61 176.65 22.45 o 14 6 1 0.32 -1.38 16.60 o 16 6 1 33.90 19.45 26.47 o 18 6 1 244.82 249.32 27.55 o 20 6 1 115.33 108.01 25.39 o 22 6 1 104.90 83.70 22.85 o 24 6 1 4.93 17.53 20.25 o 26 6 1 11.32 -28.67 17.36 o 28 6 1 15.15 47.39 24.40 o 30 6 1 9.71 61.49 25.69 o -27 7 1 38.63 37.75 33.50 o -25 7 1 25.23 26.65 22.77 o -23 7 1 9.18 26.05 20.97 o -21 7 1 0.34 11.02 19.78 o -19 7 1 427.56 378.64 32.07 o -17 7 1 541.97 511.41 36.77 o -15 7 1 11.28 13.42 18.37 o -13 7 1 2.73 -21.92 14.28 o -11 7 1 19.96 15.98 13.17 o -9 7 1 17.11 13.48 13.07 o -7 7 1 6.68 2.49 17.14 o -5 7 1 1.13 7.09 14.88 o -3 7 1 2.39 -1.55 10.49 o -1 7 1 6.45 6.51 16.80 o 1 7 1 6.08 18.21 28.63 o 3 7 1 30.43 -3.70 24.31 o 5 7 1 4.11 3.60 11.85 o 7 7 1 13.37 11.68 41.06 o 9 7 1 32.90 17.95 21.07 o 11 7 1 26.12 -0.26 18.37 o 13 7 1 87.89 65.75 19.82 o 15 7 1 11.20 7.25 18.37 o 17 7 1 1410.67 1380.23 60.37 o 19 7 1 59.19 26.00 19.38 o 23 7 1 15.96 10.80 21.61 o 25 7 1 12.28 -22.53 18.63 o 27 7 1 4.68 56.89 25.69 o -24 8 1 1.23 -15.55 19.96 o -22 8 1 0.67 21.61 36.74 o -20 8 1 83.25 46.00 23.34 o -18 8 1 24.31 -19.17 17.52 o -16 8 1 0.52 2.06 20.53 o -14 8 1 24.60 32.53 52.94 o -12 8 1 22.87 35.15 18.71 o -10 8 1 52.84 32.51 41.06 o -8 8 1 278.31 297.46 26.30 o -6 8 1 200.77 194.19 19.50 o -4 8 1 302.07 271.50 20.57 o -2 8 1 0.01 -17.29 20.53 o 0 8 1 2.36 10.88 22.15 o 2 8 1 11.81 76.71 23.77 o 4 8 1 50.30 23.72 17.18 o 6 8 1 0.01 -0.06 14.28 o 8 8 1 59.98 49.37 18.61 o 10 8 1 318.36 259.52 49.71 o 12 8 1 29.66 20.18 30.79 o 14 8 1 63.51 80.35 23.22 o 16 8 1 201.90 232.78 35.66 o 18 8 1 21.09 -23.77 23.77 o 20 8 1 104.39 109.32 26.71 o 22 8 1 1.75 -13.00 22.19 o 24 8 1 41.17 12.22 38.36 o -17 9 1 0.20 86.44 35.66 o -15 9 1 105.19 103.32 26.92 o -13 9 1 29.68 53.87 24.13 o -11 9 1 12.07 25.65 20.15 o -9 9 1 6.08 15.13 27.01 o -5 9 1 16.15 -0.07 17.18 o -3 9 1 71.27 30.25 25.93 o -1 9 1 77.10 51.86 28.09 o 1 9 1 1.20 0.84 31.33 o 3 9 1 0.99 -0.09 17.94 o 7 9 1 66.96 22.69 30.25 o 9 9 1 1.39 15.13 25.93 o 11 9 1 10.33 71.31 33.50 o 13 9 1 77.69 39.75 23.07 o 15 9 1 468.79 436.54 37.82 o 17 9 1 16.26 -27.66 20.24 o -2 10 1 144.10 169.82 28.58 o 0 10 1 4.59 -15.13 24.85 o 2 10 1 77.43 142.63 36.74 o 4 10 1 6.99 -21.61 28.09 o 6 10 1 0.08 -32.41 25.93 o 8 10 1 1.98 -10.80 25.93 o -36 0 2 89.35 90.76 30.25 o -34 0 2 275.71 329.58 39.98 o -32 0 2 117.09 98.33 25.93 o -30 0 2 61.94 28.09 17.57 o -28 0 2 6.04 -0.61 27.55 o -26 0 2 1263.26 1227.88 49.96 o -24 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