#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2008584.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2008584_Fobs loop_ _publ_author_name 'Clegg, W.' 'Elsegood, M. R. J.' 'Dyer, P. W.' 'Gibson, V. C.' 'Marshall, E. L.' _publ_section_title ; Dibenzylbis(tert-butylimido)molybdenum(VI), containing both \h^1^- and \h^2^-benzyl ligands ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 916 _journal_page_last 918 _journal_volume 55 _journal_year 1999 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 97.120 _cell_angle_gamma 90.000 _cell_length_a 9.7330 _cell_length_b 17.5790 _cell_length_c 13.0160 _exptl_crystal_F_000 880.00 _reflns_d_resolution_high 0.8405 _[local]_cod_data_source_file ln1081sup2.hkl _[local]_cod_data_source_block vcg35 #BEGIN Tags that were not found in dictionaries: _shelx_title ' VCG35 in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 226.54 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 51320.82 51274.87 673.69 o 4 0 0 13322.19 12806.17 169.00 o 6 0 0 892.30 1010.10 15.04 o 8 0 0 2903.21 2899.24 85.74 o 10 0 0 907.78 883.67 14.73 o 2 1 0 13712.51 12896.02 171.06 o 3 1 0 107.43 119.37 4.00 o 4 1 0 5319.52 5569.70 74.22 o 5 1 0 13.01 7.89 1.19 o 6 1 0 5060.04 4973.67 67.01 o 7 1 0 0.50 3.69 1.63 o 8 1 0 137.42 145.28 4.08 o 9 1 0 32.14 23.45 1.26 o 10 1 0 2065.37 2074.53 54.03 o 11 1 0 46.94 54.86 2.19 o 1 2 0 1.70 15.89 11.26 o 2 2 0 1565.47 1573.75 21.69 o 3 2 0 857.84 836.86 12.92 o 4 2 0 4415.42 3934.80 53.55 o 5 2 0 3067.60 3224.66 44.49 o 6 2 0 651.14 659.42 10.61 o 7 2 0 377.06 405.67 8.30 o 8 2 0 2557.07 2534.54 74.27 o 9 2 0 25.21 13.28 1.78 o 10 2 0 964.03 975.32 38.70 o 11 2 0 27.11 17.90 1.48 o 1 3 0 237.63 248.60 4.06 o 2 3 0 17174.04 17668.79 240.11 o 3 3 0 8.32 2.44 0.53 o 4 3 0 37.18 29.83 2.52 o 5 3 0 1128.77 1225.01 18.12 o 6 3 0 6106.14 6180.63 84.79 o 7 3 0 1239.12 1216.52 46.29 o 8 3 0 26.28 33.50 1.26 o 9 3 0 178.73 168.30 4.71 o 10 3 0 1070.36 1068.66 47.16 o 11 3 0 28.84 36.12 1.56 o 0 4 0 1068.37 1080.83 20.97 o 1 4 0 872.91 814.57 11.84 o 2 4 0 1.76 14.42 7.11 o 3 4 0 1337.47 1408.96 20.20 o 4 4 0 4955.81 4831.31 67.47 o 5 4 0 1869.31 1920.57 27.84 o 6 4 0 2584.58 2581.05 37.28 o 7 4 0 22.15 19.86 1.48 o 8 4 0 586.05 542.32 12.45 o 9 4 0 102.50 90.99 3.56 o 10 4 0 346.51 349.79 10.37 o 11 4 0 1.29 5.63 3.26 o 1 5 0 573.23 569.54 10.98 o 2 5 0 18216.23 19134.25 334.47 o 3 5 0 400.39 326.82 7.12 o 4 5 0 3687.73 3882.78 68.86 o 5 5 0 2160.95 2471.65 44.58 o 6 5 0 4765.26 4725.35 84.34 o 7 5 0 2613.16 2559.43 47.84 o 8 5 0 824.58 771.99 16.61 o 9 5 0 15.79 15.11 1.48 o 10 5 0 761.50 766.22 17.79 o 11 5 0 103.84 106.69 4.45 o 0 6 0 27044.45 27564.16 488.58 o 1 6 0 1630.77 1567.10 28.55 o 2 6 0 962.20 1155.58 21.97 o 3 6 0 3842.42 4004.76 71.89 o 4 6 0 11246.62 11503.48 203.67 o 5 6 0 3210.87 3412.06 62.49 o 6 6 0 506.03 520.09 11.56 o 7 6 0 47.52 54.83 2.67 o 8 6 0 1067.87 1084.81 22.25 o 9 6 0 520.59 567.16 13.93 o 10 6 0 247.39 265.28 8.89 o 11 6 0 0.06 -1.19 3.56 o 1 7 0 1636.60 1631.48 30.62 o 2 7 0 5291.63 5097.54 91.83 o 3 7 0 557.65 461.22 10.08 o 4 7 0 2519.08 2589.36 47.58 o 5 7 0 2513.32 2673.02 49.94 o 6 7 0 3594.66 3675.86 68.13 o 7 7 0 1897.37 1975.01 37.71 o 8 7 0 611.70 610.51 14.23 o 9 7 0 292.40 281.60 8.60 o 10 7 0 540.69 562.40 14.23 o 0 8 0 3770.06 3535.11 65.03 o 1 8 0 4363.17 4412.23 80.91 o 2 8 0 760.63 857.18 17.21 o 3 8 0 2351.60 2413.66 45.50 o 4 8 0 3794.92 3845.39 71.48 o 5 8 0 3839.59 4143.73 77.40 o 6 8 0 69.68 66.09 2.96 o 7 8 0 97.04 99.29 5.04 o 8 8 0 1098.24 1143.52 26.40 o 9 8 0 1100.47 1087.38 23.43 o 10 8 0 263.02 265.28 9.19 o 1 9 0 2705.51 2756.11 52.08 o 2 9 0 6581.46 6610.95 121.76 o 3 9 0 4125.31 4194.73 78.07 o 4 9 0 66.32 60.16 2.67 o 5 9 0 166.16 153.54 5.63 o 6 9 0 3669.78 3799.66 71.39 o 7 9 0 776.85 802.79 17.79 o 8 9 0 312.35 313.62 9.19 o 9 9 0 38.05 44.16 2.37 o 10 9 0 5.74 6.82 3.85 o 0 10 0 5926.35 5983.77 112.06 o 1 10 0 3513.87 3537.44 67.30 o 2 10 0 37.11 32.60 1.48 o 3 10 0 1896.95 1882.68 37.72 o 4 10 0 3622.31 3512.66 67.25 o 5 10 0 4529.08 4487.68 85.46 o 6 10 0 2424.43 2366.58 46.64 o 7 10 0 29.33 32.01 2.07 o 8 10 0 141.77 151.45 4.45 o 9 10 0 1048.51 1000.69 22.84 o 10 10 0 172.25 170.42 7.71 o 1 11 0 2229.10 2228.89 43.98 o 2 11 0 2374.46 2394.01 47.26 o 3 11 0 3822.70 3738.01 71.74 o 4 11 0 349.52 349.52 9.19 o 5 11 0 106.59 100.47 5.04 o 6 11 0 1100.47 1144.48 24.33 o 7 11 0 1227.05 1194.37 25.81 o 8 11 0 189.29 196.21 9.19 o 9 11 0 51.89 49.20 2.67 o 0 12 0 435.44 419.84 10.38 o 1 12 0 5462.55 5400.56 104.68 o 2 12 0 743.20 756.91 16.91 o 3 12 0 720.96 710.90 16.31 o 4 12 0 1408.40 1393.65 31.16 o 5 12 0 1613.80 1620.86 33.84 o 6 12 0 43.17 41.19 2.37 o 7 12 0 190.27 213.11 7.71 o 8 12 0 237.08 237.71 8.60 o 9 12 0 850.18 856.69 20.76 o 1 13 0 3235.42 3189.82 63.94 o 2 13 0 49.87 51.57 2.67 o 3 13 0 5239.56 5320.13 104.57 o 4 13 0 117.44 125.96 5.63 o 5 13 0 1066.32 1084.21 23.73 o 6 13 0 77.49 88.61 3.85 o 7 13 0 3855.19 3843.20 76.70 o 8 13 0 0.12 -0.30 3.85 o 9 13 0 76.34 79.43 4.45 o 0 14 0 1179.83 1173.17 25.52 o 1 14 0 5545.63 5587.28 111.76 o 2 14 0 212.14 235.64 7.71 o 3 14 0 429.98 479.39 12.45 o 4 14 0 122.35 128.92 5.93 o 5 14 0 1075.83 1091.58 24.62 o 6 14 0 36.29 36.75 2.37 o 7 14 0 442.44 456.24 13.04 o 8 14 0 0.18 0.89 4.15 o 1 15 0 2348.98 2379.38 49.60 o 2 15 0 273.77 261.15 8.30 o 3 15 0 3480.47 3549.92 72.54 o 4 15 0 212.08 189.10 7.41 o 5 15 0 383.20 400.49 11.56 o 6 15 0 4.78 4.15 3.85 o 7 15 0 1054.03 1082.53 25.51 o 8 15 0 65.34 60.16 3.56 o 0 16 0 372.35 372.93 10.67 o 1 16 0 2865.25 2793.19 58.83 o 2 16 0 47.59 47.42 2.37 o 3 16 0 842.62 896.81 21.35 o 4 16 0 3.10 3.85 3.56 o 5 16 0 2330.09 2408.49 53.74 o 6 16 0 10.81 5.33 4.45 o 7 16 0 195.51 207.47 8.60 o 1 17 0 840.61 849.65 20.46 o 2 17 0 158.76 153.23 6.82 o 3 17 0 615.73 652.29 16.60 o 4 17 0 61.84 57.49 3.26 o 5 17 0 623.44 602.76 16.31 o 6 17 0 57.50 64.90 3.26 o 0 18 0 266.23 274.48 9.19 o 1 18 0 1039.84 1028.01 24.62 o 2 18 0 238.93 238.60 8.89 o 3 18 0 1543.32 1504.02 34.42 o 4 18 0 79.58 86.83 4.45 o 5 18 0 2321.19 2344.61 51.95 o 1 19 0 1131.06 1153.21 27.58 o 2 19 0 214.70 196.51 8.30 o 3 19 0 2232.46 2406.86 55.21 o 4 19 0 47.07 39.71 2.67 o 0 20 0 132.58 143.15 7.11 o 1 20 0 939.29 955.20 24.02 o 2 20 0 2.79 8.89 2.07 o 3 20 0 664.00 625.30 17.49 o -11 0 1 1341.97 1357.06 30.85 o -9 0 1 1422.27 1447.96 22.47 o -7 0 1 292.69 274.59 5.61 o -5 0 1 6.64 57.90 1.85 o -3 0 1 14885.48 14635.10 227.92 o 1 0 1 2078.12 1980.89 34.19 o 3 0 1 17153.85 16948.02 223.57 o 5 0 1 305.83 343.67 5.83 o 7 0 1 5537.46 5525.50 74.57 o 9 0 1 423.09 449.45 8.44 o 11 0 1 729.17 672.77 20.90 o -11 1 1 578.10 570.25 10.93 o -10 1 1 33.86 30.86 1.78 o -9 1 1 2001.94 2005.24 29.53 o -8 1 1 86.63 91.64 3.24 o -7 1 1 6367.30 6337.90 85.91 o -6 1 1 1.42 5.20 2.07 o -5 1 1 6939.69 7396.85 99.09 o -4 1 1 166.16 166.06 5.19 o -3 1 1 29533.70 28028.71 373.58 o -2 1 1 1522.52 1553.97 21.12 o -1 1 1 6105.84 6294.67 83.88 o 1 1 1 48736.77 45496.10 603.94 o 2 1 1 754.66 721.10 10.35 o 3 1 1 7.48 10.81 2.07 o 4 1 1 645.90 682.38 10.12 o 5 1 1 10633.41 10264.83 188.89 o 6 1 1 231.19 220.10 6.82 o 7 1 1 189.23 178.93 5.04 o 8 1 1 36.12 46.40 1.77 o 9 1 1 1445.30 1488.25 40.65 o 10 1 1 17.16 16.19 8.00 o 11 1 1 229.01 199.29 5.76 o -11 2 1 573.72 594.89 11.27 o -10 2 1 137.99 113.47 4.00 o -9 2 1 1524.16 1557.81 24.41 o -8 2 1 207.97 204.18 10.37 o -7 2 1 332.34 335.20 6.46 o -6 2 1 371.74 390.85 6.88 o -5 2 1 6052.59 5954.09 80.55 o -4 2 1 909.72 979.58 14.19 o -3 2 1 2484.11 2522.78 34.45 o -2 2 1 417.15 422.22 6.41 o -1 2 1 23464.12 23047.47 311.00 o 0 2 1 207.32 216.48 4.75 o 1 2 1 6126.89 6169.10 83.04 o 2 2 1 3709.45 3875.89 57.69 o 3 2 1 13571.86 13024.40 175.25 o 4 2 1 5810.18 6104.56 124.70 o 5 2 1 757.05 813.53 15.13 o 6 2 1 121.06 157.96 3.76 o 7 2 1 4592.84 4424.56 61.66 o 8 2 1 526.20 516.20 9.24 o 9 2 1 655.77 649.18 11.31 o 10 2 1 62.04 75.35 4.89 o 11 2 1 722.13 729.54 30.84 o -11 3 1 587.87 603.56 16.90 o -10 3 1 0.04 -0.52 2.19 o -9 3 1 1456.85 1466.28 22.66 o -8 3 1 76.21 86.50 3.85 o -7 3 1 4278.33 4318.99 60.88 o -6 3 1 82.57 83.82 2.96 o -5 3 1 213.89 173.88 3.76 o -4 3 1 2709.84 2890.47 40.42 o -3 3 1 1644.69 1451.55 20.57 o -2 3 1 7679.43 7825.92 106.85 o -1 3 1 12742.74 13183.92 179.41 o 0 3 1 924.66 1000.55 14.08 o 1 3 1 1680.34 1562.24 35.18 o 2 3 1 2071.57 2109.77 96.41 o 3 3 1 537.31 556.00 8.34 o 4 3 1 147.68 170.78 3.42 o 5 3 1 9020.39 8299.29 226.77 o 6 3 1 1.65 2.76 1.35 o 7 3 1 359.73 371.27 9.78 o 8 3 1 144.44 151.81 5.78 o 9 3 1 1131.74 1116.15 40.64 o 10 3 1 74.09 64.83 2.67 o 11 3 1 415.44 386.77 8.44 o -11 4 1 266.45 290.28 7.21 o -10 4 1 0.50 0.03 5.63 o -9 4 1 607.92 616.56 11.02 o -8 4 1 239.37 220.83 10.52 o -7 4 1 992.65 983.71 15.47 o -6 4 1 819.36 802.99 12.83 o -5 4 1 10574.87 10761.45 148.11 o -4 4 1 42.43 44.99 6.22 o -3 4 1 400.77 354.73 5.77 o -2 4 1 3940.06 3901.96 54.03 o -1 4 1 6289.35 6351.76 87.94 o 0 4 1 87.92 71.97 2.52 o 1 4 1 21782.35 21638.02 299.52 o 2 4 1 4912.81 5166.65 108.86 o 3 4 1 16716.44 16397.71 227.48 o 4 4 1 1073.48 1035.79 15.33 o 5 4 1 801.51 864.87 13.96 o 6 4 1 425.65 447.62 14.08 o 7 4 1 5189.52 5232.94 93.26 o 8 4 1 482.60 431.38 10.67 o 9 4 1 1020.44 969.31 20.76 o 10 4 1 4.81 -2.96 2.96 o 11 4 1 828.57 814.26 19.27 o -11 5 1 508.70 497.46 13.93 o -10 5 1 0.70 -1.19 3.26 o -9 5 1 76.19 83.58 3.56 o -8 5 1 1267.15 1215.00 24.92 o -7 5 1 1024.33 978.11 20.17 o -6 5 1 276.92 294.07 7.71 o -5 5 1 2857.50 2927.13 53.55 o -4 5 1 3788.16 3972.62 70.96 o -3 5 1 2649.85 2517.22 45.27 o -2 5 1 3091.17 3304.33 58.48 o -1 5 1 5611.72 5539.22 96.78 o 0 5 1 114.03 175.79 5.34 o 1 5 1 33188.02 33339.60 582.19 o 2 5 1 74.21 46.24 2.07 o 3 5 1 12.85 12.74 0.89 o 4 5 1 897.82 983.16 19.29 o 5 5 1 8408.73 8146.87 142.63 o 6 5 1 1479.56 1514.56 29.39 o 7 5 1 71.69 89.80 4.45 o 8 5 1 21.48 24.30 1.78 o 9 5 1 1425.94 1320.04 26.70 o 10 5 1 101.54 105.51 4.15 o 11 5 1 258.15 254.61 9.19 o -11 6 1 668.17 700.61 17.49 o -10 6 1 558.92 571.01 14.53 o -9 6 1 226.31 242.16 8.00 o -8 6 1 16.39 23.71 1.78 o -7 6 1 1725.74 1699.00 32.95 o -6 6 1 687.01 635.28 13.64 o -5 6 1 2964.30 2838.96 52.06 o -4 6 1 54.92 89.21 3.56 o -3 6 1 1823.18 1836.28 33.59 o -2 6 1 4705.16 4663.43 82.85 o -1 6 1 15526.94 15657.24 277.47 o 0 6 1 341.57 293.31 6.52 o 1 6 1 33.41 37.93 1.48 o 2 6 1 3977.77 4115.50 73.46 o 3 6 1 7862.05 7898.41 139.91 o 4 6 1 168.86 135.17 4.45 o 5 6 1 363.00 362.90 8.60 o 6 6 1 2133.91 2175.36 40.70 o 7 6 1 4547.12 4578.09 84.25 o 8 6 1 914.17 885.63 19.28 o 9 6 1 624.00 580.25 14.23 o 10 6 1 23.76 17.78 1.78 o -10 7 1 9.24 1.19 3.85 o -9 7 1 453.20 458.62 12.15 o -8 7 1 2111.01 2059.70 40.38 o -7 7 1 3342.48 3347.69 62.74 o -6 7 1 198.38 185.85 6.22 o -5 7 1 1038.84 1078.61 22.55 o -4 7 1 4505.28 4766.33 87.08 o -3 7 1 4154.64 4051.65 73.68 o -2 7 1 306.37 304.81 7.12 o -1 7 1 550.59 487.41 10.09 o 0 7 1 10270.93 10272.59 184.07 o 1 7 1 4115.36 4235.63 76.45 o 2 7 1 2403.18 2267.54 41.96 o 3 7 1 1086.98 1301.66 25.23 o 4 7 1 1667.48 1662.73 31.19 o 5 7 1 4509.41 4763.60 86.11 o 6 7 1 1544.02 1559.02 29.98 o 7 7 1 1.73 2.07 2.96 o 8 7 1 123.53 126.85 5.33 o 9 7 1 1041.13 1054.71 25.21 o 10 7 1 506.17 534.81 13.93 o -10 8 1 632.45 628.85 16.31 o -9 8 1 444.18 443.20 12.15 o -8 8 1 107.05 106.69 5.63 o -7 8 1 737.15 761.26 16.90 o -6 8 1 1957.12 2004.80 38.90 o -5 8 1 4766.37 4790.81 88.21 o -4 8 1 307.71 325.22 8.00 o -3 8 1 190.56 195.64 5.63 o -2 8 1 4918.48 4768.96 87.21 o -1 8 1 14631.27 15204.03 275.06 o 0 8 1 1150.23 1015.22 20.49 o 1 8 1 387.57 445.99 9.79 o 2 8 1 3733.96 3751.29 69.15 o 3 8 1 1573.79 1508.52 29.70 o 4 8 1 3022.94 2997.58 56.52 o 5 8 1 26.17 24.60 1.48 o 6 8 1 405.69 424.84 10.67 o 7 8 1 1852.53 1860.77 38.00 o 8 8 1 1215.15 1164.10 24.62 o 9 8 1 406.92 404.05 11.26 o 10 8 1 109.63 107.58 4.45 o -10 9 1 0.03 0.59 3.85 o -9 9 1 430.21 415.32 11.86 o -8 9 1 1104.74 1112.36 24.32 o -7 9 1 483.29 476.74 12.16 o -6 9 1 28.94 30.23 1.78 o -5 9 1 1963.55 2009.79 40.09 o -4 9 1 2181.39 2281.44 44.57 o -3 9 1 1208.94 1134.18 22.56 o -2 9 1 276.02 280.16 7.12 o -1 9 1 113.95 113.82 4.15 o 0 9 1 8828.93 9217.80 169.10 o 1 9 1 3218.04 3002.25 56.28 o 2 9 1 5738.89 6066.49 111.74 o 3 9 1 104.44 103.44 3.85 o 4 9 1 985.63 926.00 18.99 o 5 9 1 3733.29 3803.76 71.12 o 6 9 1 503.78 499.89 12.16 o 7 9 1 295.00 299.69 8.60 o 8 9 1 1208.79 1159.61 24.62 o 9 9 1 258.18 262.91 8.60 o 10 9 1 826.96 822.57 19.87 o -10 10 1 525.52 493.01 14.23 o -9 10 1 98.43 102.25 4.45 o -8 10 1 139.46 120.03 5.93 o -7 10 1 240.84 238.91 8.00 o -6 10 1 1213.45 1240.79 26.11 o -5 10 1 2121.67 2139.10 43.07 o -4 10 1 199.86 199.49 6.22 o -3 10 1 286.88 267.99 7.41 o -2 10 1 5053.98 4890.17 91.88 o -1 10 1 2431.40 2302.60 44.60 o 0 10 1 2072.21 1973.43 38.64 o 1 10 1 3508.41 3832.61 72.36 o 2 10 1 3145.23 3316.69 63.38 o 3 10 1 2486.72 2555.17 49.34 o 4 10 1 4708.91 4804.45 91.47 o 5 10 1 133.96 126.85 5.33 o 6 10 1 3.94 5.93 3.26 o 7 10 1 493.28 501.64 12.75 o 8 10 1 702.56 721.43 21.05 o 9 10 1 25.73 31.71 2.07 o -9 11 1 162.06 163.90 7.71 o -8 11 1 1818.03 1764.69 37.40 o -7 11 1 396.75 376.49 10.97 o -6 11 1 444.28 423.06 11.27 o -5 11 1 879.17 899.02 19.87 o -4 11 1 2494.11 2450.59 49.33 o -3 11 1 1840.08 1903.04 39.20 o -2 11 1 827.34 819.93 17.50 o -1 11 1 8.46 10.08 1.19 o 0 11 1 5476.92 5426.69 103.25 o 1 11 1 4477.24 4625.18 88.21 o 2 11 1 6048.50 6178.95 117.32 o 3 11 1 16.10 19.86 1.78 o 4 11 1 1300.82 1357.97 27.90 o 5 11 1 4077.85 4112.77 79.15 o 6 11 1 3120.96 3094.79 60.63 o 7 11 1 225.44 203.04 7.41 o 8 11 1 153.81 168.35 7.11 o 9 11 1 179.27 192.35 8.00 o -9 12 1 69.38 60.75 2.96 o -8 12 1 78.04 69.05 3.26 o -7 12 1 23.68 26.08 2.07 o -6 12 1 2595.03 2603.86 54.06 o -5 12 1 177.57 178.73 6.52 o -4 12 1 580.11 577.92 13.94 o -3 12 1 30.97 34.38 1.78 o -2 12 1 5219.52 5400.09 104.63 o -1 12 1 273.43 253.75 7.41 o 0 12 1 2849.46 2873.50 57.09 o 1 12 1 251.17 238.33 7.11 o 2 12 1 4411.49 4416.06 85.77 o 3 12 1 817.65 829.02 18.39 o 4 12 1 3659.54 3798.99 74.66 o 5 12 1 431.83 434.62 11.56 o 6 12 1 1019.40 1017.98 22.84 o 7 12 1 225.45 243.64 8.30 o 8 12 1 1908.23 1825.26 38.58 o 9 12 1 1.95 -3.85 3.85 o -9 13 1 19.56 25.19 2.37 o -8 13 1 1569.88 1594.20 35.31 o -7 13 1 452.48 434.31 16.60 o -6 13 1 258.91 260.25 8.60 o -5 13 1 2.97 2.96 2.96 o -4 13 1 3743.92 3670.22 74.36 o -3 13 1 102.36 95.43 4.74 o -2 13 1 979.05 911.02 20.17 o -1 13 1 3.22 0.30 2.67 o 0 13 1 3940.54 3936.97 78.28 o 1 13 1 674.55 637.31 14.83 o 2 13 1 2180.90 2130.88 43.37 o 3 13 1 26.03 22.52 1.78 o 4 13 1 740.35 745.84 17.20 o 5 13 1 158.34 153.23 6.22 o 6 13 1 1124.97 1151.82 25.51 o 7 13 1 9.77 16.60 2.07 o 8 13 1 200.04 177.83 7.71 o -8 14 1 12.58 15.41 2.37 o -7 14 1 341.77 357.49 11.26 o -6 14 1 1847.77 1887.37 42.44 o -5 14 1 7.44 5.63 1.48 o -4 14 1 49.32 40.90 2.07 o -3 14 1 4.79 5.63 2.96 o -2 14 1 8607.67 8531.56 168.27 o -1 14 1 295.79 294.36 8.60 o 0 14 1 2886.24 2876.21 59.74 o 1 14 1 0.18 2.96 2.96 o 2 14 1 3074.31 3111.30 63.31 o 3 14 1 137.67 150.86 6.22 o 4 14 1 2231.30 2200.71 46.03 o 5 14 1 41.49 49.79 2.37 o 6 14 1 1370.85 1358.51 30.26 o 7 14 1 89.77 90.69 4.15 o 8 14 1 1414.86 1375.31 31.15 o -8 15 1 969.40 969.44 28.47 o -7 15 1 76.00 80.02 8.89 o -6 15 1 26.84 23.41 2.07 o -5 15 1 132.58 141.37 6.52 o -4 15 1 2166.83 2166.26 46.02 o -3 15 1 628.69 612.01 15.42 o -2 15 1 387.44 391.91 10.97 o -1 15 1 691.01 668.11 16.31 o 0 15 1 3259.84 3310.16 67.78 o 1 15 1 518.77 524.20 13.34 o 2 15 1 1303.00 1327.17 29.08 o 3 15 1 173.28 163.31 6.52 o 4 15 1 1561.20 1599.19 34.72 o 5 15 1 28.02 33.49 2.37 o 6 15 1 926.58 993.49 23.43 o 7 15 1 13.35 7.71 2.07 o -7 16 1 30.09 32.90 2.67 o -6 16 1 951.97 953.75 23.13 o -5 16 1 8.72 11.26 2.07 o -4 16 1 164.77 153.53 6.82 o -3 16 1 416.50 408.51 11.56 o -2 16 1 2576.01 2510.46 52.87 o -1 16 1 782.07 759.48 18.39 o 0 16 1 484.85 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