#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2008779.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2008779_Fobs loop_ _publ_author_name 'Luo, X.-M.' 'Chen, X.-H.' 'Shanmuga Sundara Raj, S.' 'Fun, H.-K.' 'Zhu, L.-G.' _publ_section_title ; Dichloro(ethylenediaminetetraacetic acid)palladium(II) hexahydrate ; _journal_issue 8 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 1220 _journal_page_last 1222 _journal_volume 55 _journal_year 1999 _space_group_IT_number 92 _symmetry_space_group_name_Hall 'P 4abw 2nw' _symmetry_space_group_name_H-M 'P 41 21 2' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 10.1962 _cell_length_b 10.1962 _cell_length_c 21.0571 _exptl_crystal_F_000 1176.00 _reflns_d_resolution_high 0.6464 _[local]_cod_data_source_file fr1173sup2.hkl _[local]_cod_data_source_block lxm01m #BEGIN Tags that were not found in dictionaries: _shelx_title ' lxm01m in P4(1)2(1)2' _shelx_refln_list_code 4 _shelx_f_calc_maximum 259.58 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z+1/2' '-y+1/2, x+1/2, z+1/4' 'y+1/2, -x+1/2, z+3/4' '-x+1/2, y+1/2, -z+1/4' 'x+1/2, -y+1/2, -z+3/4' 'y, x, -z' '-y, -x, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 2 0 4391.96 4994.99 122.09 o 1 2 0 21002.07 20626.17 261.25 o 2 2 0 1230.84 1233.05 28.06 o 1 3 0 14789.24 15352.60 195.40 o 2 3 0 1017.95 1044.90 16.98 o 3 3 0 10169.75 10872.74 184.34 o 0 4 0 67380.17 63170.36 1051.96 o 1 4 0 189.16 223.40 6.79 o 2 4 0 177.86 212.67 6.30 o 3 4 0 2423.02 2251.88 31.65 o 4 4 0 6670.28 6023.95 104.48 o 1 5 0 738.04 642.66 11.65 o 2 5 0 20050.88 19851.46 252.49 o 3 5 0 2635.18 2456.24 37.23 o 4 5 0 1.80 0.78 5.28 o 5 5 0 3310.93 3374.50 109.22 o 0 6 0 902.30 1008.08 25.36 o 1 6 0 7772.65 8075.37 104.95 o 2 6 0 3451.59 3956.42 53.41 o 3 6 0 480.02 478.20 10.29 o 4 6 0 159.15 161.52 6.93 o 5 6 0 9622.01 9070.51 127.73 o 6 6 0 1766.23 1747.86 40.69 o 1 7 0 1852.68 1904.85 27.89 o 2 7 0 226.03 297.40 9.06 o 3 7 0 2877.64 2716.69 38.26 o 4 7 0 69.90 71.04 5.96 o 5 7 0 925.56 909.59 17.62 o 6 7 0 829.66 837.89 16.97 o 7 7 0 1468.75 1497.59 36.72 o 0 8 0 1579.10 1393.92 34.95 o 1 8 0 1004.93 964.47 19.78 o 2 8 0 0.80 3.03 5.22 o 3 8 0 2299.76 2212.77 32.35 o 4 8 0 596.70 632.13 13.69 o 5 8 0 138.03 111.51 7.49 o 6 8 0 37.32 20.72 9.10 o 7 8 0 24.32 30.87 6.57 o 8 8 0 957.15 978.53 34.24 o 1 9 0 91.76 100.18 11.89 o 2 9 0 3292.51 3370.49 63.08 o 3 9 0 33.42 17.40 7.72 o 4 9 0 11.25 10.83 7.24 o 5 9 0 33.54 64.79 12.07 o 6 9 0 3825.49 3780.40 70.36 o 7 9 0 3.30 15.16 15.45 o 8 9 0 161.26 164.20 11.64 o 9 9 0 240.24 179.33 26.66 o 0 10 0 74.10 59.14 16.96 o 1 10 0 1664.95 1670.41 35.65 o 2 10 0 62.17 51.10 9.04 o 3 10 0 504.05 513.25 16.76 o 4 10 0 421.51 382.97 17.59 o 5 10 0 1589.79 1734.39 43.02 o 6 10 0 4.47 -6.00 8.73 o 7 10 0 232.87 265.25 13.31 o 8 10 0 332.33 367.83 18.07 o 9 10 0 1030.12 1033.79 38.12 o 10 10 0 57.07 109.66 24.84 o 1 11 0 804.87 777.05 22.40 o 2 11 0 521.09 490.24 19.70 o 3 11 0 1347.80 1263.66 29.56 o 4 11 0 226.72 212.10 14.79 o 5 11 0 529.08 500.45 20.25 o 6 11 0 261.55 294.34 17.11 o 7 11 0 958.96 948.18 38.84 o 8 11 0 6.52 49.07 21.81 o 9 11 0 71.96 66.04 21.81 o 10 11 0 40.41 81.79 24.23 o 11 11 0 336.90 375.63 35.75 o 0 12 0 774.20 745.73 30.41 o 1 12 0 190.80 203.29 12.61 o 2 12 0 0.02 1.09 10.25 o 3 12 0 274.89 294.29 20.51 o 4 12 0 503.18 497.80 20.75 o 5 12 0 156.00 170.29 14.44 o 6 12 0 48.28 47.24 12.04 o 7 12 0 3.12 6.58 13.55 o 8 12 0 297.70 258.56 27.57 o 9 12 0 165.02 138.14 28.48 o 10 12 0 101.10 144.80 27.87 o 1 13 0 39.10 42.29 9.92 o 2 13 0 655.60 676.62 21.20 o 3 13 0 12.27 13.53 11.40 o 4 13 0 96.97 53.40 15.44 o 5 13 0 7.97 5.41 10.81 o 6 13 0 475.08 503.13 22.12 o 7 13 0 9.48 34.72 23.95 o 8 13 0 173.62 201.15 30.90 o 0 14 0 193.30 173.22 18.63 o 1 14 0 217.68 220.83 14.51 o 2 14 0 10.08 1.50 10.74 o 3 14 0 74.40 58.42 13.15 o 4 14 0 437.42 442.43 26.67 o 5 14 0 120.09 126.42 14.97 o 6 14 0 8.85 19.48 14.92 o 7 14 0 12.13 42.45 26.96 o 1 15 0 330.55 348.26 21.86 o 2 15 0 7.20 57.80 13.64 o 3 15 0 461.60 443.20 22.21 o 4 15 0 79.93 99.44 14.79 o 1 1 1 3874.49 3858.96 67.21 o -1 2 1 9188.13 9254.61 140.37 o 0 2 1 30738.01 31463.78 470.35 o 1 2 1 8709.87 8887.42 114.14 o 2 2 1 872.38 830.14 14.41 o -2 3 1 3605.16 3392.36 45.56 o -1 3 1 4867.23 5117.67 67.07 o 0 3 1 5480.04 5763.41 89.08 o 1 3 1 5326.52 5638.52 73.62 o 2 3 1 3791.01 3571.69 47.83 o 3 3 1 104.91 73.02 4.24 o -3 4 1 559.41 452.95 9.25 o -2 4 1 3204.85 3050.65 41.50 o -1 4 1 11514.05 11855.71 177.26 o 0 4 1 1595.88 1314.02 18.26 o 1 4 1 11752.31 12011.25 153.75 o 2 4 1 3046.91 2824.35 38.67 o 3 4 1 662.95 558.97 9.74 o 4 4 1 882.30 864.31 14.54 o -4 5 1 7446.99 7197.38 111.68 o -3 5 1 2804.26 2444.64 34.30 o -2 5 1 2111.35 2016.45 28.77 o -1 5 1 3364.33 3332.91 45.21 o 0 5 1 15746.91 15877.44 189.26 o 1 5 1 3338.85 3242.07 52.94 o 2 5 1 2157.86 2113.44 30.10 o 3 5 1 2796.05 2446.67 34.37 o 4 5 1 7438.19 7312.27 95.46 o 5 5 1 4324.06 4251.01 69.16 o -5 6 1 1361.76 1324.54 22.94 o -4 6 1 7093.62 7030.16 92.17 o -3 6 1 2112.41 2149.15 30.86 o -2 6 1 445.63 435.33 9.57 o -1 6 1 6358.80 6128.35 80.54 o 0 6 1 16808.85 17166.98 204.56 o 1 6 1 6377.15 6134.94 80.67 o 2 6 1 441.05 435.58 9.71 o 3 6 1 1895.99 1958.03 28.54 o 4 6 1 7094.86 7081.52 92.82 o 5 6 1 1369.15 1332.51 23.06 o 6 6 1 227.13 274.73 9.51 o -6 7 1 2551.33 2480.49 38.96 o -5 7 1 2033.25 2077.72 33.27 o -4 7 1 151.65 160.39 8.67 o -3 7 1 1210.38 1238.32 19.85 o -2 7 1 2907.97 2828.84 56.66 o -1 7 1 3632.84 3463.47 47.44 o 0 7 1 1479.04 1352.46 19.51 o 1 7 1 3583.64 3484.47 47.71 o 2 7 1 2984.57 2911.52 40.64 o 3 7 1 1248.10 1298.15 21.68 o 4 7 1 142.98 126.34 11.29 o 5 7 1 1969.06 1931.93 31.31 o 6 7 1 2743.08 2634.50 41.02 o 7 7 1 69.10 70.79 7.09 o -7 8 1 131.35 123.40 8.77 o -6 8 1 1312.12 1312.43 25.82 o -5 8 1 1088.19 1097.73 22.45 o -4 8 1 906.42 970.02 26.22 o -3 8 1 317.06 313.96 10.99 o -2 8 1 391.22 437.51 13.41 o -1 8 1 385.89 429.38 16.70 o 0 8 1 966.04 937.60 22.13 o 1 8 1 355.59 388.62 13.29 o 2 8 1 331.02 348.63 10.11 o 3 8 1 355.60 355.81 10.23 o 4 8 1 943.83 972.22 19.39 o 5 8 1 1058.11 1099.88 20.42 o 6 8 1 1308.88 1355.17 24.14 o 7 8 1 144.30 148.17 8.34 o 8 8 1 432.42 446.62 13.75 o -8 9 1 1005.86 945.76 24.07 o -7 9 1 1139.20 1095.41 26.25 o -6 9 1 60.46 55.30 19.76 o -5 9 1 1252.64 1236.40 28.17 o -4 9 1 1635.39 1645.57 30.77 o -3 9 1 1667.69 1498.33 32.10 o -2 9 1 27.47 22.60 8.48 o -1 9 1 1501.09 1485.47 32.01 o 0 9 1 1070.34 1035.73 35.35 o 1 9 1 1528.57 1486.57 31.91 o 2 9 1 32.77 29.83 8.04 o 3 9 1 1604.41 1483.64 36.72 o 4 9 1 1695.31 1692.15 34.41 o 5 9 1 1288.34 1244.64 28.14 o 6 9 1 57.64 54.54 11.10 o 7 9 1 1119.71 1119.98 26.64 o 8 9 1 1024.96 959.95 32.76 o 9 9 1 375.32 401.35 23.35 o -9 10 1 50.63 63.97 51.20 o -8 10 1 469.15 463.99 16.94 o -7 10 1 371.50 378.71 15.07 o -6 10 1 139.95 180.56 16.92 o -5 10 1 669.96 710.97 23.78 o -4 10 1 1698.79 1605.66 40.45 o -3 10 1 751.98 754.07 20.67 o -2 10 1 321.26 338.72 17.93 o -1 10 1 2098.80 2008.15 41.19 o 0 10 1 2501.74 2430.68 48.13 o 1 10 1 2106.21 2010.97 41.33 o 2 10 1 315.09 319.31 15.48 o 3 10 1 781.00 770.38 21.02 o 4 10 1 1604.55 1518.28 38.69 o 5 10 1 699.62 740.02 24.13 o 6 10 1 147.03 160.86 13.44 o 7 10 1 377.50 391.43 15.18 o 8 10 1 455.64 467.62 19.70 o 9 10 1 54.76 77.96 27.26 o 10 10 1 110.74 113.98 17.35 o -10 11 1 189.52 236.28 29.69 o -9 11 1 410.31 431.37 35.75 o -8 11 1 49.97 61.10 14.83 o -7 11 1 57.16 87.40 16.32 o -6 11 1 556.18 550.24 21.36 o -5 11 1 738.91 766.29 25.49 o -4 11 1 178.04 173.28 39.68 o -3 11 1 793.04 822.75 30.13 o -2 11 1 1055.63 992.93 28.77 o -1 11 1 1119.07 1105.13 36.38 o 0 11 1 542.68 526.29 17.84 o 1 11 1 1082.46 1089.89 30.75 o 2 11 1 1038.67 977.19 24.83 o 3 11 1 810.33 828.55 30.43 o 4 11 1 184.96 198.12 14.31 o 5 11 1 726.37 725.71 24.45 o 6 11 1 574.32 565.09 22.12 o 7 11 1 48.83 48.75 17.36 o 8 11 1 52.24 25.45 20.60 o 9 11 1 410.05 480.45 37.56 o 10 11 1 176.30 147.83 27.26 o 11 11 1 0.42 31.50 20.60 o -10 12 1 115.02 93.91 26.05 o -9 12 1 249.90 253.25 29.69 o -8 12 1 120.75 106.23 17.25 o -7 12 1 170.76 164.26 18.44 o -6 12 1 261.44 243.67 18.59 o -5 12 1 248.99 233.75 15.79 o -4 12 1 174.12 135.89 18.95 o -3 12 1 288.19 291.62 16.69 o -2 12 1 273.06 239.20 17.14 o -1 12 1 171.75 152.16 13.70 o 0 12 1 111.76 116.18 11.41 o 1 12 1 175.82 161.32 12.06 o 2 12 1 263.05 250.08 13.76 o 3 12 1 298.98 328.46 18.40 o 4 12 1 171.73 175.72 14.67 o 5 12 1 255.58 226.19 20.60 o 6 12 1 247.98 249.03 17.00 o 7 12 1 176.09 190.84 15.03 o 8 12 1 116.66 98.76 26.05 o 9 12 1 252.68 182.97 28.48 o 10 12 1 107.58 97.54 24.84 o -8 13 1 296.46 305.84 22.66 o -7 13 1 326.20 340.19 19.21 o -6 13 1 58.99 69.22 19.39 o -5 13 1 30.10 30.05 12.02 o -4 13 1 370.65 353.42 37.18 o -3 13 1 415.41 413.80 24.84 o -2 13 1 24.45 25.18 13.29 o -1 13 1 81.02 95.43 11.43 o 0 13 1 224.32 222.42 15.62 o 1 13 1 87.44 88.51 11.47 o 2 13 1 24.90 27.57 11.28 o 3 13 1 387.03 375.51 18.77 o 4 13 1 386.14 412.81 38.17 o 5 13 1 29.32 13.15 36.05 o 6 13 1 59.54 53.78 13.82 o 7 13 1 321.62 303.39 31.81 o 8 13 1 296.87 350.19 36.96 o -7 14 1 124.65 156.28 19.49 o -6 14 1 85.14 96.37 14.67 o -5 14 1 129.81 145.95 17.01 o -4 14 1 138.86 166.11 15.94 o -3 14 1 218.31 186.27 16.67 o -2 14 1 219.37 217.93 17.14 o -1 14 1 293.72 296.21 16.53 o 0 14 1 216.10 242.99 14.65 o 1 14 1 291.57 282.40 15.14 o 2 14 1 214.94 252.42 17.69 o 3 14 1 234.00 210.03 16.96 o 4 14 1 128.87 135.75 14.98 o 5 14 1 131.93 135.08 15.36 o 6 14 1 83.13 88.20 15.08 o 7 14 1 133.43 119.35 27.26 o -4 15 1 14.14 21.55 12.06 o -3 15 1 174.48 182.32 20.98 o -2 15 1 500.86 476.89 27.26 o -1 15 1 148.98 173.45 13.93 o 0 15 1 24.40 38.50 13.55 o 1 15 1 148.11 195.94 14.53 o 2 15 1 486.67 481.29 28.62 o 3 15 1 180.31 197.21 17.22 o 4 15 1 15.51 57.18 16.62 o 0 1 2 18022.79 19584.61 378.52 o 1 1 2 10598.53 11156.41 188.49 o -1 2 2 2186.84 2218.71 36.19 o 0 2 2 899.39 908.20 18.52 o 1 2 2 2174.59 2179.23 30.13 o 2 2 2 4881.97 4793.39 58.82 o -2 3 2 2055.43 2237.75 33.55 o -1 3 2 3137.21 3325.59 52.93 o 0 3 2 1739.95 1924.23 29.28 o 1 3 2 2919.37 3212.43 43.25 o 2 3 2 2017.43 2242.46 33.66 o 3 3 2 86.84 79.83 4.85 o -3 4 2 3843.91 3586.25 48.38 o -2 4 2 2763.48 3022.19 41.16 o -1 4 2 22288.43 22243.21 282.10 o 0 4 2 2283.14 2412.04 33.36 o 1 4 2 21990.62 21906.51 278.05 o 2 4 2 2690.21 2997.10 40.94 o 3 4 2 3697.91 3477.92 47.06 o 4 4 2 2033.97 2037.12 27.16 o -4 5 2 4231.11 4220.73 52.89 o -3 5 2 3260.59 3177.43 44.82 o -2 5 2 60.13 69.62 6.36 o -1 5 2 7761.95 7962.59 96.40 o 0 5 2 12282.59 12667.00 151.57 o 1 5 2 7629.34 7830.60 123.71 o 2 5 2 53.33 59.43 5.06 o 3 5 2 3380.60 3339.72 45.61 o 4 5 2 4281.64 4124.62 60.75 o 5 5 2 5002.85 4647.92 130.52 o -5 6 2 16.21 15.21 5.31 o -4 6 2 1338.96 1304.19 20.59 o -3 6 2 1239.77 1264.49 19.81 o -2 6 2 6755.99 6242.51 81.96 o -1 6 2 882.79 872.14 13.67 o 0 6 2 133.86 105.40 6.52 o 1 6 2 914.84 901.05 15.17 o 2 6 2 6710.48 6350.05 83.50 o 3 6 2 1140.35 1198.07 19.16 o 4 6 2 1314.39 1266.40 20.17 o 5 6 2 15.90 19.12 6.86 o 6 6 2 6361.24 6483.09 92.94 o -6 7 2 461.53 442.35 15.99 o -5 7 2 551.58 545.65 13.92 o -4 7 2 4511.02 4356.09 58.93 o -3 7 2 527.02 491.32 10.62 o -2 7 2 1732.02 1637.16 26.18 o -1 7 2 298.19 290.20 9.03 o 0 7 2 4590.55 4744.41 59.19 o 1 7 2 253.78 243.08 8.12 o 2 7 2 1691.40 1611.11 26.55 o 3 7 2 553.81 525.91 11.26 o 4 7 2 4524.17 4357.14 59.13 o 5 7 2 533.40 507.84 12.48 o 6 7 2 450.28 466.68 12.08 o 7 7 2 394.21 376.12 11.19 o -7 8 2 1263.28 1184.90 27.26 o -6 8 2 367.02 325.51 16.75 o -5 8 2 468.46 488.02 15.38 o -4 8 2 311.67 284.46 11.97 o -3 8 2 1310.64 1347.17 28.74 o -2 8 2 1754.61 1717.95 28.36 o -1 8 2 2767.29 2714.15 45.94 o 0 8 2 12.73 12.65 6.77 o 1 8 2 2632.17 2580.64 43.87 o 2 8 2 1765.47 1785.86 29.23 o 3 8 2 1228.31 1229.53 22.63 o 4 8 2 324.89 296.33 9.03 o 5 8 2 426.79 440.50 11.71 o 6 8 2 400.44 376.73 12.67 o 7 8 2 1259.46 1165.64 21.78 o 8 8 2 0.32 7.26 7.71 o -8 9 2 7.87 0.27 7.99 o -7 9 2 457.81 485.37 16.47 o -6 9 2 95.23 95.26 13.03 o -5 9 2 2289.47 2253.62 55.79 o -4 9 2 405.73 432.74 14.57 o -3 9 2 942.16 898.51 22.44 o -2 9 2 262.51 270.06 12.27 o -1 9 2 2109.60 2099.06 42.00 o 0 9 2 345.04 339.61 19.92 o 1 9 2 2162.30 2156.01 43.01 o 2 9 2 260.82 264.02 12.17 o 3 9 2 954.98 925.12 26.34 o 4 9 2 412.53 418.68 11.55 o 5 9 2 2386.61 2342.06 41.16 o 6 9 2 102.33 95.73 8.83 o 7 9 2 456.54 486.53 14.56 o 8 9 2 10.93 9.82 9.48 o 9 9 2 1204.72 1180.99 41.12 o -9 10 2 165.29 160.82 29.08 o -8 10 2 77.86 78.98 10.80 o -7 10 2 553.34 530.40 17.85 o -6 10 2 1972.34 1957.51 47.45 o -5 10 2 339.94 348.60 16.99 o -4 10 2 229.00 219.51 17.12 o -3 10 2 577.23 629.65 21.61 o -2 10 2 3091.97 3047.72 58.35 o -1 10 2 89.28 69.53 9.55 o 0 10 2 672.42 625.46 21.57 o 1 10 2 90.20 64.82 9.77 o 2 10 2 3085.90 3049.12 58.46 o 3 10 2 548.38 568.27 17.70 o 4 10 2 239.86 238.64 29.58 o 5 10 2 341.72 354.32 19.54 o 6 10 2 1981.06 1951.28 47.19 o 7 10 2 558.74 544.99 17.70 o 8 10 2 75.41 70.75 15.63 o 9 10 2 165.57 184.50 18.42 o 10 10 2 589.23 598.23 28.27 o -10 11 2 137.00 150.86 28.48 o -9 11 2 202.21 200.54 28.48 o -8 11 2 756.65 732.10 25.63 o -7 11 2 106.22 118.00 14.25 o -6 11 2 169.87 192.40 14.76 o -5 11 2 227.20 244.26 15.24 o -4 11 2 2054.33 2025.07 49.20 o -3 11 2 163.85 187.89 12.36 o -2 11 2 99.64 88.74 10.37 o -1 11 2 71.95 65.88 9.83 o 0 11 2 2146.42 2103.44 58.72 o 1 11 2 70.00 49.54 9.51 o 2 11 2 101.74 72.41 11.31 o 3 11 2 171.21 178.55 13.75 o 4 11 2 2035.73 2033.72 49.31 o 5 11 2 228.49 225.71 15.11 o 6 11 2 173.74 168.51 18.12 o 7 11 2 109.27 125.42 14.71 o 8 11 2 733.32 776.71 46.65 o 9 11 2 201.50 189.03 27.26 o 10 11 2 136.92 222.35 30.29 o 11 11 2 15.67 67.86 23.63 o -10 12 2 44.62 89.06 26.05 o -9 12 2 13.39 56.95 23.63 o -8 12 2 55.63 49.06 16.85 o -7 12 2 262.40 261.42 17.00 o -6 12 2 59.57 74.77 13.34 o -5 12 2 114.66 112.05 13.58 o -4 12 2 0.59 7.10 22.42 o -3 12 2 612.56 602.70 22.96 o -2 12 2 565.39 579.23 19.08 o -1 12 2 681.17 708.61 21.12 o 0 12 2 5.16 10.45 11.39 o 1 12 2 683.55 674.37 23.77 o 2 12 2 573.31 573.48 19.95 o 3 12 2 570.62 545.33 22.29 o 4 12 2 0.80 2.75 9.65 o 5 12 2 116.68 120.20 13.76 o 6 12 2 68.96 45.14 11.73 o 7 12 2 251.47 263.38 17.38 o 8 12 2 55.31 55.13 22.42 o 9 12 2 13.97 7.88 19.39 o 10 12 2 45.31 88.46 26.05 o -8 13 2 10.42 6.58 22.11 o -7 13 2 76.82 66.01 13.07 o -6 13 2 8.23 25.85 11.53 o -5 13 2 583.12 584.41 23.47 o -4 13 2 5.97 19.32 11.50 o -3 13 2 188.27 194.81 15.53 o -2 13 2 12.32 12.45 9.38 o -1 13 2 371.36 373.38 18.76 o 0 13 2 22.89 26.00 13.75 o 1 13 2 368.42 343.65 15.81 o 2 13 2 12.53 23.94 9.98 o 3 13 2 200.81 182.76 16.19 o 4 13 2 4.93 9.83 15.68 o 5 13 2 598.85 592.49 23.32 o 6 13 2 8.06 15.75 11.54 o 7 13 2 78.01 71.70 16.92 o 8 13 2 10.35 60.59 23.02 o -7 14 2 256.51 302.39 26.35 o -6 14 2 234.21 245.36 18.27 o -5 14 2 97.59 63.65 30.00 o -4 14 2 13.88 4.45 11.14 o -3 14 2 308.89 334.75 23.56 o -2 14 2 372.94 345.48 36.96 o -1 14 2 63.33 73.37 13.73 o 0 14 2 125.32 140.78 13.79 o 1 14 2 62.76 84.37 11.59 o 2 14 2 376.23 380.20 20.39 o 3 14 2 305.64 304.82 19.98 o 4 14 2 16.73 27.11 12.34 o 5 14 2 103.36 110.88 14.81 o 6 14 2 240.19 221.27 17.34 o 7 14 2 256.56 242.34 30.29 o -4 15 2 556.20 559.44 40.29 o -3 15 2 15.00 47.77 18.73 o -2 15 2 6.41 5.03 16.47 o -1 15 2 16.45 35.10 10.76 o 0 15 2 629.29 610.98 21.49 o 1 15 2 16.78 37.40 11.63 o 2 15 2 7.87 22.87 15.89 o 3 15 2 15.49 15.34 11.95 o 4 15 2 548.60 499.91 48.17 o 0 1 3 6334.64 5979.56 91.80 o 1 1 3 5343.64 5276.57 117.36 o -1 2 3 78.69 120.17 6.83 o 0 2 3 9520.88 9575.29 132.68 o 1 2 3 55.59 84.33 6.07 o 2 2 3 10887.41 10883.23 130.28 o -2 3 3 720.44 743.80 11.61 o -1 3 3 5920.28 6224.53 125.59 o 0 3 3 360.50 304.52 7.11 o 1 3 3 6401.62 6630.51 86.17 o 2 3 3 552.67 562.90 10.37 o 3 3 3 11937.78 12209.51 146.17 o -3 4 3 2499.57 2482.10 32.24 o -2 4 3 4681.97 4435.70 58.83 o -1 4 3 11552.44 11558.80 159.72 o 0 4 3 10619.14 11626.63 148.91 o 1 4 3 11866.27 11786.35 151.14 o 2 4 3 4426.22 4160.65 55.54 o 3 4 3 2491.44 2444.07 34.20 o 4 4 3 729.59 843.04 13.33 o -4 5 3 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