#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/00/88/2008806.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2008806_Fobs loop_ _publ_author_name 'Shanmuga Sundara Raj, S.' 'Velmurugan, D.' 'Gunasekaran, K.' 'Fun, H.-K.' 'Manonmani, J.' 'Kandaswamy, M.' _publ_section_title ; {4,4'-Dimethyl-6'-morpholiniomethyl-6-mor-pholinomethyl-2,2'[1,2-ethanediylbis(iminomethylene)]diphenolato}copper(II) perchlorate dihydrate ; _journal_issue 8 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 1222 _journal_page_last 1224 _journal_volume 55 _journal_year 1999 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _cell_angle_alpha 90.000 _cell_angle_beta 99.750 _cell_angle_gamma 90.000 _cell_length_a 10.5460 _cell_length_b 14.2290 _cell_length_c 10.8070 _exptl_crystal_F_000 734.00 _reflns_d_resolution_high 0.7697 _[local]_cod_data_source_file na1413sup2.hkl _[local]_cod_data_source_block sha4 #BEGIN Tags that were not found in dictionaries: _shelx_title ' SHAIV in P2(1) ' _shelx_refln_list_code 4 _shelx_f_calc_maximum 150.32 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 -1 0 10464.71 10238.38 231.73 o 2 -1 0 6171.73 6019.91 36.27 o 3 -1 0 1300.96 1330.43 21.34 o 4 -1 0 5042.03 4969.93 46.41 o 5 -1 0 1260.69 1252.11 27.57 o 6 -1 0 151.99 146.54 5.72 o 7 -1 0 768.09 750.38 27.40 o 8 -1 0 574.89 569.26 26.79 o 9 -1 0 113.31 114.61 6.71 o 10 -1 0 201.96 206.43 8.03 o 11 -1 0 30.91 34.06 5.36 o 12 -1 0 54.04 55.48 5.90 o 13 -1 0 7.38 10.12 5.45 o 1 0 0 2701.90 2836.46 11.90 o 2 0 0 1857.19 1779.45 19.60 o 3 0 0 485.18 507.71 14.34 o 4 0 0 0.89 0.50 2.02 o 5 0 0 5223.99 4907.82 52.40 o 6 0 0 1163.89 1122.27 29.57 o 7 0 0 25.83 23.43 3.36 o 8 0 0 626.08 605.07 28.82 o 9 0 0 295.63 251.10 15.38 o 10 0 0 28.75 38.56 4.53 o 11 0 0 423.24 404.54 22.28 o 12 0 0 13.40 9.93 5.36 o 13 0 0 57.57 55.13 6.25 o 1 1 0 10374.43 10319.36 135.57 o 2 1 0 5857.44 5973.24 36.93 o 3 1 0 1279.71 1256.48 21.15 o 4 1 0 5255.86 5202.57 48.32 o 5 1 0 1204.71 1229.70 27.35 o 6 1 0 142.73 125.33 8.65 o 7 1 0 756.33 699.47 27.56 o 8 1 0 620.02 617.20 27.98 o 9 1 0 88.47 95.56 4.80 o 10 1 0 187.58 196.70 10.36 o 11 1 0 33.14 40.83 5.40 o 12 1 0 46.50 44.28 5.61 o 13 1 0 2.85 -2.43 5.75 o 0 2 0 8668.37 8423.76 195.34 o 1 2 0 1260.21 1482.63 14.18 o 2 2 0 10857.71 10792.54 287.40 o 3 2 0 2511.81 2593.26 31.44 o 4 2 0 1155.42 1117.59 24.06 o 5 2 0 2195.40 2253.20 37.29 o 6 2 0 466.31 470.38 20.72 o 7 2 0 97.16 88.90 4.44 o 8 2 0 220.27 226.44 10.25 o 9 2 0 16.20 17.16 4.30 o 10 2 0 91.90 100.74 5.43 o 11 2 0 646.54 667.25 32.49 o 12 2 0 71.60 70.00 6.13 o 13 2 0 10.28 4.69 5.86 o 1 3 0 5530.52 5818.12 96.72 o 2 3 0 610.57 583.84 15.72 o 3 3 0 1064.14 1088.95 22.54 o 4 3 0 3883.68 3913.39 45.41 o 5 3 0 254.14 308.16 16.88 o 6 3 0 955.19 916.26 28.33 o 7 3 0 309.41 339.96 15.77 o 8 3 0 607.13 653.10 30.45 o 9 3 0 623.70 601.52 29.97 o 10 3 0 537.43 462.33 25.23 o 11 3 0 26.31 30.41 5.51 o 12 3 0 167.98 163.74 7.00 o 13 3 0 29.04 30.19 6.20 o 0 4 0 888.18 920.61 19.12 o 1 4 0 285.66 280.01 9.14 o 2 4 0 1413.41 1486.85 26.06 o 3 4 0 104.77 94.82 4.00 o 4 4 0 970.60 1153.32 27.13 o 5 4 0 498.96 440.82 20.70 o 6 4 0 1432.49 1491.90 36.74 o 7 4 0 1.97 1.60 3.59 o 8 4 0 450.08 448.63 24.73 o 9 4 0 817.45 832.86 35.18 o 10 4 0 14.47 16.43 4.87 o 11 4 0 278.55 272.66 10.30 o 12 4 0 50.60 44.22 6.02 o 13 4 0 88.21 97.76 7.03 o 1 5 0 1776.41 1842.83 20.73 o 2 5 0 144.62 164.77 7.73 o 3 5 0 798.56 845.38 23.98 o 4 5 0 1098.26 1125.13 28.73 o 5 5 0 1251.75 1258.69 32.84 o 6 5 0 208.37 190.95 8.99 o 7 5 0 472.84 481.21 24.04 o 8 5 0 117.67 122.45 5.12 o 9 5 0 25.42 29.91 4.60 o 10 5 0 390.49 379.95 18.90 o 11 5 0 4.49 6.32 5.31 o 12 5 0 127.03 131.38 6.96 o 13 5 0 75.59 62.71 6.87 o 0 6 0 1542.73 1340.73 27.81 o 1 6 0 3907.35 3962.18 32.55 o 2 6 0 114.16 104.11 4.83 o 3 6 0 1116.88 1066.34 28.61 o 4 6 0 4708.63 4758.78 59.31 o 5 6 0 318.10 298.98 17.16 o 6 6 0 990.68 1008.19 33.88 o 7 6 0 78.94 87.92 5.40 o 8 6 0 131.43 128.67 5.65 o 9 6 0 35.87 32.25 4.69 o 10 6 0 5.64 2.40 5.01 o 11 6 0 335.34 336.93 18.60 o 12 6 0 84.90 86.89 6.86 o 1 7 0 1133.18 1091.15 29.39 o 2 7 0 476.29 523.07 20.82 o 3 7 0 180.38 207.72 11.60 o 4 7 0 346.48 339.78 16.65 o 5 7 0 681.63 663.84 28.45 o 6 7 0 268.10 269.12 12.19 o 7 7 0 83.73 79.93 4.83 o 8 7 0 2.80 6.87 4.44 o 9 7 0 131.62 138.63 6.91 o 10 7 0 181.73 159.96 10.85 o 11 7 0 35.78 28.19 5.79 o 12 7 0 95.57 103.53 7.14 o 0 8 0 2461.64 2471.89 43.11 o 1 8 0 54.26 69.88 3.35 o 2 8 0 720.34 709.26 25.16 o 3 8 0 737.01 729.17 27.97 o 4 8 0 12.97 12.70 3.69 o 5 8 0 1351.91 1353.67 39.29 o 6 8 0 761.49 832.20 34.93 o 7 8 0 129.31 128.81 7.41 o 8 8 0 78.67 79.57 5.38 o 9 8 0 76.25 88.68 5.63 o 10 8 0 76.77 71.97 5.86 o 11 8 0 87.77 78.20 6.46 o 12 8 0 11.10 10.99 6.27 o 1 9 0 1400.27 1410.84 25.93 o 2 9 0 557.95 525.32 25.53 o 3 9 0 79.46 84.83 4.44 o 4 9 0 270.93 241.76 12.20 o 5 9 0 53.61 50.94 4.74 o 6 9 0 402.30 387.02 16.54 o 7 9 0 837.92 845.50 36.91 o 8 9 0 5.33 -0.53 4.80 o 9 9 0 8.74 8.06 5.06 o 10 9 0 92.17 88.45 6.27 o 11 9 0 0.94 6.52 5.70 o 0 10 0 1401.39 1332.29 37.67 o 1 10 0 626.52 667.69 20.76 o 2 10 0 624.56 612.63 29.28 o 3 10 0 1169.85 1088.34 38.25 o 4 10 0 18.64 25.45 4.67 o 5 10 0 850.87 862.96 35.98 o 6 10 0 64.96 70.49 5.01 o 7 10 0 51.48 40.16 5.15 o 8 10 0 328.37 299.45 19.13 o 9 10 0 106.33 111.33 6.15 o 10 10 0 9.45 8.05 5.61 o 11 10 0 72.78 73.30 6.93 o 1 11 0 1168.53 1173.76 27.65 o 2 11 0 495.63 428.29 23.20 o 3 11 0 347.92 351.95 17.44 o 4 11 0 926.64 906.39 36.96 o 5 11 0 690.52 662.78 32.46 o 6 11 0 46.78 42.27 4.99 o 7 11 0 280.10 265.04 14.90 o 8 11 0 59.79 56.30 5.70 o 9 11 0 25.08 19.89 5.49 o 10 11 0 103.85 102.37 7.03 o 0 12 0 892.22 873.72 36.61 o 1 12 0 480.10 483.24 16.30 o 2 12 0 457.39 458.65 22.76 o 3 12 0 1380.77 1256.37 44.53 o 4 12 0 122.89 122.64 5.65 o 5 12 0 81.66 76.71 5.49 o 6 12 0 289.16 267.40 16.00 o 7 12 0 101.52 100.74 6.13 o 8 12 0 60.73 57.54 6.20 o 9 12 0 93.64 88.15 6.43 o 10 12 0 28.62 25.95 6.29 o 1 13 0 744.29 690.35 23.97 o 2 13 0 159.51 152.11 6.04 o 3 13 0 94.01 77.49 5.56 o 4 13 0 321.57 351.93 17.48 o 5 13 0 104.65 102.39 5.97 o 6 13 0 30.59 28.06 5.42 o 7 13 0 351.54 341.66 14.51 o 8 13 0 130.68 135.29 8.83 o 9 13 0 22.32 20.64 6.23 o 0 14 0 417.59 437.48 19.93 o 1 14 0 144.37 140.02 4.43 o 2 14 0 93.59 102.62 6.64 o 3 14 0 253.05 246.30 14.37 o 4 14 0 156.33 149.87 9.13 o 5 14 0 104.01 96.64 6.31 o 6 14 0 122.25 118.24 6.64 o 7 14 0 3.75 3.75 5.58 o 8 14 0 109.60 120.51 7.35 o 1 15 0 144.17 152.23 6.55 o 2 15 0 94.58 89.44 6.11 o 3 15 0 29.50 32.11 5.42 o 4 15 0 131.46 135.36 6.62 o 5 15 0 82.64 80.65 6.46 o 6 15 0 11.43 9.36 5.67 o 7 15 0 46.20 45.72 6.59 o 0 16 0 2.77 -3.30 5.08 o 1 16 0 9.45 11.42 3.80 o 2 16 0 108.37 102.59 6.57 o 3 16 0 191.30 198.93 7.98 o 4 16 0 6.13 7.14 5.54 o 5 16 0 57.14 56.21 6.61 o 6 16 0 27.86 28.75 6.41 o 1 17 0 84.23 81.02 4.60 o 2 17 0 90.86 82.55 6.70 o 3 17 0 22.44 22.48 6.29 o 4 17 0 32.25 30.51 6.38 o 5 17 0 18.13 22.36 6.54 o 0 18 0 120.18 140.90 7.76 o 1 18 0 8.61 6.40 4.43 o 2 18 0 25.22 17.33 6.34 o 3 18 0 60.72 57.58 6.94 o -13 -1 1 30.06 28.10 6.04 o -12 -1 1 51.05 55.08 5.70 o -11 -1 1 303.32 322.90 15.93 o -10 -1 1 139.96 143.90 7.42 o -9 -1 1 739.50 712.87 32.55 o -8 -1 1 116.53 112.24 8.44 o -7 -1 1 1615.18 1460.09 35.76 o -6 -1 1 270.84 217.17 14.76 o -5 -1 1 585.25 525.42 18.98 o -4 -1 1 8108.91 7626.69 57.22 o -3 -1 1 574.25 537.04 15.08 o -2 -1 1 8187.37 8013.06 42.64 o -1 -1 1 6703.45 6880.37 203.67 o 0 -1 1 1398.40 1469.59 10.34 o 1 -1 1 303.83 282.94 5.82 o 2 -1 1 2949.88 2713.87 26.65 o 3 -1 1 494.21 458.20 14.01 o 4 -1 1 1526.59 1463.03 26.74 o 5 -1 1 2254.26 2181.40 36.33 o 6 -1 1 819.36 794.82 26.80 o 7 -1 1 355.93 284.56 17.75 o 8 -1 1 34.89 22.84 4.01 o 9 -1 1 68.63 69.41 4.71 o 10 -1 1 562.31 577.10 27.70 o 11 -1 1 31.30 35.82 5.31 o 12 -1 1 36.35 29.43 5.70 o 13 -1 1 60.80 72.82 6.55 o -13 0 1 0.83 0.39 5.59 o -12 0 1 41.68 43.92 5.65 o -11 0 1 468.11 466.32 25.46 o -10 0 1 96.64 87.30 5.31 o -9 0 1 947.43 899.15 36.11 o -8 0 1 3528.42 3349.74 58.22 o -7 0 1 330.97 311.05 15.49 o -6 0 1 1282.59 1326.65 31.01 o -5 0 1 2540.34 2675.08 38.93 o -4 0 1 748.38 728.01 19.33 o -3 0 1 6290.24 6130.92 43.88 o -2 0 1 806.48 920.75 14.74 o -1 0 1 848.71 794.78 7.37 o 0 0 1 7549.50 6835.91 102.66 o 1 0 1 364.03 348.64 5.79 o 2 0 1 6210.36 5899.37 37.96 o 3 0 1 162.15 134.28 6.09 o 4 0 1 6.59 7.03 2.02 o 5 0 1 958.15 890.71 24.71 o 6 0 1 1078.69 970.18 28.75 o 7 0 1 434.12 395.90 21.99 o 8 0 1 7.40 5.88 3.82 o 9 0 1 394.21 405.94 16.70 o 10 0 1 38.77 40.55 4.99 o 11 0 1 480.80 530.36 24.02 o 12 0 1 81.87 91.79 6.20 o 13 0 1 10.22 9.79 6.00 o -13 1 1 38.77 43.16 6.07 o -12 1 1 63.11 58.43 5.84 o -11 1 1 303.17 296.29 16.48 o -10 1 1 82.76 91.27 5.17 o -9 1 1 663.99 658.29 32.89 o -8 1 1 132.48 140.67 8.31 o -7 1 1 1592.29 1488.36 37.66 o -6 1 1 290.43 292.04 15.72 o -5 1 1 646.13 605.50 20.65 o -4 1 1 8253.76 8068.02 59.62 o -3 1 1 581.95 595.68 15.86 o -2 1 1 7571.71 7514.02 42.43 o -1 1 1 6846.19 7154.53 122.75 o 0 1 1 1412.96 1473.64 12.01 o 1 1 1 261.88 281.94 15.06 o 2 1 1 3329.74 3215.79 29.66 o 3 1 1 446.85 412.45 14.06 o 4 1 1 1359.75 1282.35 25.64 o 5 1 1 2245.47 2143.94 36.62 o 6 1 1 848.28 818.75 27.03 o 7 1 1 387.42 381.66 19.60 o 8 1 1 30.25 27.39 4.10 o 9 1 1 109.49 120.71 4.97 o 10 1 1 595.81 682.82 27.64 o 11 1 1 33.35 39.41 5.47 o 12 1 1 32.57 29.52 5.75 o 13 1 1 56.70 59.82 6.62 o -13 2 1 9.25 8.79 5.65 o -12 2 1 64.37 71.29 5.95 o -11 2 1 573.21 563.63 30.08 o -10 2 1 90.22 93.83 6.80 o -9 2 1 89.60 85.48 4.97 o -8 2 1 324.71 321.07 17.05 o -7 2 1 33.55 28.15 3.52 o -6 2 1 2080.57 2057.25 39.43 o -5 2 1 2678.47 2735.99 40.50 o -4 2 1 159.03 178.42 8.65 o -3 2 1 7735.88 8114.39 54.54 o -2 2 1 3157.16 3405.65 31.65 o -1 2 1 1139.03 1258.35 14.45 o 0 2 1 4151.67 4204.52 48.07 o 1 2 1 3761.16 3667.52 40.55 o 2 2 1 2125.86 2173.97 26.68 o 3 2 1 485.20 475.39 15.71 o 4 2 1 519.52 523.08 17.74 o 5 2 1 803.89 825.32 24.76 o 6 2 1 1118.41 1195.29 31.52 o 7 2 1 99.98 111.63 5.40 o 8 2 1 796.91 788.76 32.09 o 9 2 1 228.06 229.37 11.26 o 10 2 1 82.72 86.00 5.43 o 11 2 1 142.17 157.01 7.96 o 12 2 1 90.96 88.86 6.48 o 13 2 1 10.90 13.76 6.02 o -13 3 1 71.58 66.27 6.52 o -12 3 1 160.13 157.10 7.64 o -11 3 1 13.79 13.73 5.01 o -10 3 1 152.32 157.37 8.76 o -9 3 1 193.64 188.35 7.39 o -8 3 1 216.72 232.53 14.05 o -7 3 1 753.90 757.86 29.25 o -6 3 1 180.56 176.21 10.09 o -5 3 1 1908.59 2013.11 36.87 o -4 3 1 4569.70 4496.86 48.64 o -3 3 1 1660.38 1794.72 28.00 o -2 3 1 3071.91 3287.40 34.50 o -1 3 1 1485.56 1663.30 16.03 o 0 3 1 22597.06 22914.89 739.75 o 1 3 1 5467.11 5772.92 29.75 o 2 3 1 1805.31 1814.65 26.86 o 3 3 1 124.34 120.42 6.61 o 4 3 1 4080.25 3946.71 47.12 o 5 3 1 1203.25 1320.54 31.13 o 6 3 1 882.75 897.41 28.53 o 7 3 1 1216.83 1131.68 34.98 o 8 3 1 564.65 567.92 27.24 o 9 3 1 97.84 104.84 5.13 o 10 3 1 580.81 576.09 27.24 o 11 3 1 27.01 29.61 5.58 o 12 3 1 80.83 87.70 6.43 o 13 3 1 15.62 16.46 5.79 o -12 4 1 53.82 56.53 5.93 o -11 4 1 240.82 253.20 13.36 o -10 4 1 49.22 49.29 5.06 o -9 4 1 70.72 83.46 4.96 o -8 4 1 222.66 237.05 13.55 o -7 4 1 170.90 177.45 8.51 o -6 4 1 61.63 56.39 3.52 o -5 4 1 1778.18 2032.39 38.96 o -4 4 1 5.41 2.81 2.43 o -3 4 1 989.92 1023.68 23.33 o -2 4 1 452.10 507.13 17.31 o -1 4 1 891.20 1029.26 14.73 o 0 4 1 6254.50 6878.00 35.25 o 1 4 1 4011.75 4225.72 79.47 o 2 4 1 2487.91 2658.69 34.83 o 3 4 1 1199.31 1223.05 26.07 o 4 4 1 3148.55 3592.37 47.51 o 5 4 1 1716.15 1590.57 35.90 o 6 4 1 2847.21 2815.55 50.36 o 7 4 1 36.98 42.68 4.08 o 8 4 1 1013.98 980.75 37.48 o 9 4 1 450.00 388.61 19.84 o 10 4 1 111.92 117.03 6.71 o 11 4 1 348.15 343.29 19.74 o 12 4 1 31.05 34.26 5.81 o -13 5 1 66.15 80.12 6.66 o -12 5 1 107.49 113.35 6.68 o -11 5 1 18.47 18.72 5.31 o -10 5 1 716.75 784.81 38.80 o -9 5 1 262.45 305.03 15.10 o -8 5 1 233.05 240.51 10.92 o -7 5 1 1573.58 1579.59 41.94 o -6 5 1 558.36 560.30 25.50 o -5 5 1 194.50 224.92 10.85 o -4 5 1 91.03 83.37 4.78 o -3 5 1 38.99 43.73 2.65 o -2 5 1 1647.11 1653.75 30.27 o -1 5 1 4564.73 4556.08 135.80 o 0 5 1 301.81 286.00 9.84 o 1 5 1 1430.60 1578.54 31.70 o 2 5 1 689.68 672.39 21.05 o 3 5 1 418.72 396.24 18.35 o 4 5 1 2121.46 2047.10 37.93 o 5 5 1 725.62 711.46 26.57 o 6 5 1 434.63 456.04 22.05 o 7 5 1 699.82 704.62 30.65 o 8 5 1 240.72 255.84 14.64 o 9 5 1 354.56 328.95 17.91 o 10 5 1 260.88 232.02 13.89 o 11 5 1 21.53 24.24 5.54 o 12 5 1 213.18 232.98 12.52 o -12 6 1 58.83 69.09 6.48 o -11 6 1 281.40 263.74 16.15 o -10 6 1 59.18 70.76 5.59 o -9 6 1 138.69 152.73 5.97 o -8 6 1 612.00 596.88 30.06 o -7 6 1 59.67 72.22 5.56 o -6 6 1 879.12 840.76 31.92 o -5 6 1 1112.33 1125.21 33.47 o -4 6 1 386.46 415.10 20.43 o -3 6 1 1016.62 994.90 27.33 o -2 6 1 3038.40 3031.27 43.34 o -1 6 1 967.10 1049.09 17.73 o 0 6 1 1388.33 1439.30 20.68 o 1 6 1 609.93 696.61 35.45 o 2 6 1 2670.00 2807.31 42.13 o 3 6 1 1388.53 1387.71 32.08 o 4 6 1 802.74 836.20 27.89 o 5 6 1 543.67 536.27 25.41 o 6 6 1 476.49 535.16 25.65 o 7 6 1 430.54 344.90 22.63 o 8 6 1 750.89 775.37 36.98 o 9 6 1 488.83 475.57 25.87 o 10 6 1 4.90 -0.80 4.83 o 11 6 1 223.85 219.86 10.69 o 12 6 1 4.95 2.08 6.00 o -12 7 1 149.75 158.18 7.53 o -11 7 1 28.45 28.70 5.75 o -10 7 1 178.58 157.90 9.96 o -9 7 1 289.96 265.11 13.36 o -8 7 1 192.21 189.22 8.88 o -7 7 1 577.67 535.51 29.24 o -6 7 1 459.01 344.66 25.10 o -5 7 1 232.78 252.92 12.61 o -4 7 1 569.72 501.84 23.69 o -3 7 1 415.58 460.68 19.93 o -2 7 1 332.44 346.31 17.69 o -1 7 1 883.95 940.47 18.70 o 0 7 1 262.46 214.34 17.43 o 1 7 1 5176.19 4997.91 43.19 o 2 7 1 1457.69 1338.43 32.14 o 3 7 1 538.84 512.08 22.53 o 4 7 1 645.13 639.25 26.03 o 5 7 1 49.85 57.46 4.21 o 6 7 1 318.17 289.57 17.59 o 7 7 1 424.73 430.25 20.07 o 8 7 1 94.93 86.35 5.19 o 9 7 1 649.85 592.32 33.47 o 10 7 1 289.99 286.14 12.65 o 11 7 1 42.37 38.19 6.04 o 12 7 1 130.89 138.98 8.03 o -12 8 1 31.06 23.05 6.41 o -11 8 1 67.95 60.64 6.23 o -10 8 1 20.65 22.54 5.27 o -9 8 1 277.65 266.23 14.48 o -8 8 1 586.38 601.19 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