#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/00/88/2008820.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2008820_Fobs loop_ _publ_author_name 'Govindasamy, L.' 'Velmurugan, D.' 'Rajendran, T. M.' _publ_section_title ; An N···H---O intramolecular strong hydrogen bond in N-(2-aminophenyl)naphthaldimine ; _journal_issue 8 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 1368 _journal_page_last 1369 _journal_volume 55 _journal_year 1999 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _cell_angle_alpha 90.000 _cell_angle_beta 99.100 _cell_angle_gamma 90.000 _cell_length_a 7.2030 _cell_length_b 7.6700 _cell_length_c 12.1970 _exptl_crystal_F_000 276.00 _reflns_d_resolution_high 0.8209 _[local]_cod_data_source_file os1054sup2.hkl _[local]_cod_data_source_block final1 #BEGIN Tags that were not found in dictionaries: _shelx_title ' TMR1 in P2(1) 22-11-97' _shelx_refln_list_code 4 _shelx_f_calc_maximum 74.50 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 931.63 911.41 7.60 o 2 0 0 425.67 407.28 1.38 o 3 0 0 34.84 27.46 0.46 o 4 0 0 34.29 34.21 0.64 o 5 0 0 17.06 17.21 0.49 o 6 0 0 17.37 18.44 0.53 o 7 0 0 3.93 4.44 0.29 o 8 0 0 0.08 0.23 0.18 o 1 1 0 1998.44 2055.59 13.95 o 2 1 0 411.85 393.68 1.44 o 3 1 0 141.18 141.57 1.07 o 4 1 0 16.98 19.50 0.50 o 5 1 0 26.29 23.57 0.65 o 6 1 0 16.65 17.03 0.51 o 7 1 0 14.10 14.58 0.43 o 8 1 0 0.03 -0.11 0.20 o 0 2 0 5549.98 5681.37 29.92 o 1 2 0 3986.16 4392.49 26.75 o 2 2 0 171.91 159.50 1.04 o 3 2 0 357.51 354.74 1.84 o 4 2 0 3.43 3.94 0.19 o 5 2 0 18.58 20.17 0.56 o 6 2 0 35.57 36.96 0.93 o 7 2 0 3.28 2.96 0.29 o 8 2 0 4.08 4.33 0.24 o 1 3 0 1440.58 1523.48 17..68 o 2 3 0 585.29 595.93 2.36 o 3 3 0 119.65 121.94 1.21 o 4 3 0 14.14 15.78 0.46 o 5 3 0 19.11 18.35 0.57 o 6 3 0 18.97 20.25 0.62 o 7 3 0 30.73 30.33 0.81 o 8 3 0 0.90 1.46 0.19 o 0 4 0 142.17 140.80 1.21 o 1 4 0 889.11 920.28 3.21 o 2 4 0 680.42 668.56 2.93 o 3 4 0 83.33 83.56 1.15 o 4 4 0 26.84 24.83 0.74 o 5 4 0 6.56 6.26 0.32 o 6 4 0 30.45 32.50 0.88 o 7 4 0 11.40 12.63 0.41 o 1 5 0 43.05 46.36 0.87 o 2 5 0 298.84 298.14 2.25 o 3 5 0 37.05 37.40 0.89 o 4 5 0 4.70 4.54 0.31 o 5 5 0 1.71 1.85 0.24 o 6 5 0 0.80 0.92 0.20 o 7 5 0 7.50 8.13 0.32 o 0 6 0 155.20 162.50 1.81 o 1 6 0 52.22 54.17 1.08 o 2 6 0 123.05 123.36 1.63 o 3 6 0 45.54 44.63 1.04 o 4 6 0 11.28 11.38 0.41 o 5 6 0 0.15 -0.02 0.26 o 6 6 0 3.56 3.31 0.24 o 1 7 0 9.98 11.10 0.41 o 2 7 0 70.45 70.88 1.32 o 3 7 0 23.68 22.31 0.65 o 4 7 0 17.51 15.94 0.48 o 5 7 0 0.48 0.69 0.22 o 0 8 0 17.88 17.41 0.50 o 1 8 0 4.79 4.94 0.34 o 2 8 0 11.66 10.92 0.42 o 3 8 0 73.14 67.88 1.11 o 4 8 0 0.43 0.58 0.20 o 1 9 0 0.87 1.20 0.21 o 2 9 0 5.27 4.55 0.26 o -8 0 1 0.41 0.30 0.23 o -7 0 1 12.32 11.93 0.39 o -6 0 1 8.69 9.62 0.36 o -5 0 1 0.71 1.05 0.16 o -4 0 1 228.79 239.66 1.64 o -3 0 1 403.04 408.42 1.76 o -2 0 1 317.16 261.24 1.10 o -1 0 1 62.76 56.03 0.36 o 0 0 1 91.57 85.59 0.64 o 1 0 1 585.88 560.98 6.43 o 2 0 1 307.32 290.49 1.22 o 3 0 1 313.38 297.26 1.56 o 4 0 1 50.42 42.65 0.73 o 5 0 1 12.92 13.25 0.40 o 6 0 1 171.87 174.54 1.96 o 7 0 1 0.40 0.39 0.27 o 8 0 1 0.30 -0.01 0.21 o -8 1 1 0.65 1.08 0.18 o -7 1 1 12.58 12.73 0.40 o -6 1 1 21.06 21.60 0.62 o -5 1 1 8.22 8.22 0.29 o -4 1 1 123.68 129.15 1.23 o -3 1 1 138.13 123.89 0.99 o -2 1 1 11.21 10.28 0.24 o -1 1 1 2253.93 2492.43 15.84 o 0 1 1 323.82 301.72 13.81 o 1 1 1 2130.44 2157.48 15.23 o 2 1 1 278.71 259.69 1.21 o 3 1 1 37.55 40.89 0.60 o 4 1 1 15.13 18.83 0.51 o 5 1 1 68.62 68.21 1.11 o 6 1 1 162.57 160.90 1.90 o 7 1 1 29.95 26.60 0.69 o 8 1 1 7.20 7.89 0.29 o -8 2 1 1.63 1.55 0.18 o -7 2 1 0.49 0.50 0.29 o -6 2 1 7.51 8.11 0.35 o -5 2 1 7.94 8.80 0.32 o -4 2 1 34.49 33.25 0.67 o -3 2 1 449.10 462.71 2.10 o -2 2 1 149.30 144.22 0.98 o -1 2 1 2888.05 3196.97 22.31 o 0 2 1 4779.14 5167.57 580.74 o 1 2 1 921.60 884.74 11.18 o 2 2 1 64.60 55.83 0.64 o 3 2 1 58.91 59.97 0.78 o 4 2 1 63.69 61.98 0.94 o 5 2 1 99.04 94.85 1.36 o 6 2 1 262.71 269.90 2.46 o 7 2 1 50.19 52.73 1.06 o 8 2 1 4.15 4.56 0.24 o -8 3 1 2.83 3.87 0.24 o -7 3 1 25.21 24.39 0.63 o -6 3 1 27.67 24.75 0.69 o -5 3 1 50.17 49.10 1.01 o -4 3 1 24.71 24.72 0.65 o -3 3 1 31.89 39.69 0.70 o -2 3 1 85.59 77.29 0.84 o -1 3 1 38.30 38.07 0.55 o 0 3 1 48.09 52.63 3.43 o 1 3 1 245.81 237.17 1.36 o 2 3 1 65.54 64.02 0.78 o 3 3 1 30.82 27.64 0.60 o 4 3 1 64.51 54.94 0.97 o 5 3 1 92.91 89.88 1.38 o 6 3 1 13.14 12.63 0.42 o 7 3 1 1.35 1.57 0.22 o 8 3 1 13.85 12.26 0.35 o -7 4 1 13.19 14.72 0.42 o -6 4 1 24.72 24.94 0.68 o -5 4 1 8.29 8.40 0.35 o -4 4 1 16.99 19.53 0.55 o -3 4 1 12.56 13.88 0.39 o -2 4 1 123.24 127.96 1.27 o -1 4 1 429.76 448.86 2.23 o 0 4 1 51.77 41.20 1.62 o 1 4 1 189.09 199.14 1.49 o 2 4 1 163.93 166.35 1.47 o 3 4 1 87.55 89.06 1.20 o 4 4 1 171.63 166.52 1.81 o 5 4 1 74.07 75.09 1.31 o 6 4 1 19.10 18.77 0.60 o 7 4 1 20.31 21.42 0.61 o -7 5 1 15.63 15.10 0.42 o -6 5 1 16.35 16.65 0.47 o -5 5 1 0.80 0.89 0.30 o -4 5 1 15.63 16.09 0.50 o -3 5 1 15.93 16.45 0.49 o -2 5 1 60.54 61.25 1.05 o -1 5 1 55.99 59.05 0.97 o 0 5 1 43.85 47.62 0.60 o 1 5 1 72.57 69.48 1.05 o 2 5 1 85.13 85.20 1.23 o 3 5 1 22.80 24.92 0.75 o 4 5 1 90.78 94.68 1.45 o 5 5 1 56.27 51.66 1.10 o 6 5 1 2.43 2.22 0.24 o 7 5 1 3.48 3.40 0.24 o -6 6 1 0.11 -0.10 0.23 o -5 6 1 11.14 12.16 0.42 o -4 6 1 15.27 15.50 0.46 o -3 6 1 69.51 70.34 1.29 o -2 6 1 36.16 37.00 0.93 o -1 6 1 28.59 30.28 0.83 o 0 6 1 11.45 12.58 0.40 o 1 6 1 0.49 0.63 0.31 o 2 6 1 85.03 88.23 1.41 o 3 6 1 126.32 123.65 1.68 o 4 6 1 57.41 58.65 1.18 o 5 6 1 0.33 0.53 0.25 o 6 6 1 2.72 2.75 0.21 o -5 7 1 0.12 -0.22 0.24 o -4 7 1 7.89 8.46 0.36 o -3 7 1 27.06 25.73 0.72 o -2 7 1 0.71 0.76 0.36 o -1 7 1 8.97 9.36 0.39 o 0 7 1 23.46 23.98 0.85 o 1 7 1 0.13 0.10 0.31 o 2 7 1 27.87 27.70 0.75 o 3 7 1 12.65 13.54 0.44 o 4 7 1 34.87 32.90 0.82 o 5 7 1 1.02 0.98 0.18 o -4 8 1 12.01 10.41 0.37 o -3 8 1 19.02 19.44 0.53 o -2 8 1 2.18 2.19 0.29 o -1 8 1 0.26 0.28 0.33 o 0 8 1 5.60 5.56 0.26 o 1 8 1 4.29 4.56 0.33 o 2 8 1 0.07 0.11 0.28 o 3 8 1 31.96 28.10 0.72 o 4 8 1 1.14 0.86 0.20 o -2 9 1 3.70 3.75 0.25 o -1 9 1 0.93 0.55 0.27 o 0 9 1 3.04 2.70 0.18 o 1 9 1 1.27 1.73 0.22 o 2 9 1 27.45 25.95 0.57 o -8 0 2 0.02 -0.21 0.21 o -7 0 2 13.02 13.04 0.41 o -6 0 2 9.33 9.31 0.35 o -5 0 2 3.31 3.23 0.21 o -4 0 2 90.47 104.40 1.10 o -3 0 2 1521.84 1513.24 17.96 o -2 0 2 9.87 10.21 0.24 o -1 0 2 1029.43 962.34 9.28 o 0 0 2 359.97 291.76 0.63 o 1 0 2 16.76 13.22 0.23 o 2 0 2 21.17 20.91 0.36 o 3 0 2 30.78 30.47 0.54 o 4 0 2 27.87 28.01 0.63 o 5 0 2 202.80 199.78 1.91 o 6 0 2 463.48 470.57 3.23 o 7 0 2 7.04 6.88 0.35 o 8 0 2 8.77 9.68 0.32 o -8 1 2 2.96 2.50 0.23 o -7 1 2 7.32 6.61 0.32 o -6 1 2 6.14 6.89 0.31 o -5 1 2 31.30 34.09 0.77 o -4 1 2 410.16 429.36 2.28 o -3 1 2 568.87 600.89 2.25 o -2 1 2 64.48 59.12 0.58 o -1 1 2 1155.37 1181.84 11.28 o 0 1 2 1008.31 899.20 42.19 o 1 1 2 201.61 172.33 0.87 o 2 1 2 235.06 234.62 1.23 o 3 1 2 154.43 145.82 1.18 o 4 1 2 35.45 31.37 0.67 o 5 1 2 85.75 78.65 1.23 o 6 1 2 22.25 24.95 0.69 o 7 1 2 24.66 25.65 0.76 o 8 1 2 1.92 1.77 0.18 o -8 2 2 0.37 0.65 0.15 o -7 2 2 3.07 2.80 0.25 o -6 2 2 3.08 2.87 0.26 o -5 2 2 16.39 16.27 0.49 o -4 2 2 235.57 236.67 1.78 o -3 2 2 181.46 192.79 1.37 o -2 2 2 607.46 604.61 2.09 o -1 2 2 1975.51 2126.21 18.45 o 0 2 2 1705.20 1566.82 45.85 o 1 2 2 72.44 62.81 0.62 o 2 2 2 14.43 12.83 0.34 o 3 2 2 163.05 172.45 1.37 o 4 2 2 3.13 3.07 0.19 o 5 2 2 242.92 242.00 2.18 o 6 2 2 28.82 29.83 0.88 o 7 2 2 20.77 21.80 0.61 o 8 2 2 2.58 3.48 0.23 o -8 3 2 1.71 1.39 0.18 o -7 3 2 3.21 2.67 0.25 o -6 3 2 23.66 23.86 0.67 o -5 3 2 23.98 27.51 0.77 o -4 3 2 25.49 30.75 0.71 o -3 3 2 245.14 254.36 1.76 o -2 3 2 221.31 229.61 1.48 o -1 3 2 147.80 153.19 1.11 o 0 3 2 168.86 163.18 5.75 o 1 3 2 8.43 9.21 0.26 o 2 3 2 115.89 107.20 1.05 o 3 3 2 6.80 6.95 0.23 o 4 3 2 54.32 53.69 0.97 o 5 3 2 78.37 77.09 1.30 o 6 3 2 16.99 17.53 0.53 o 7 3 2 11.62 11.49 0.40 o -7 4 2 7.81 9.34 0.36 o -6 4 2 2.97 4.26 0.29 o -5 4 2 5.50 6.68 0.32 o -4 4 2 32.94 36.52 0.85 o -3 4 2 5.64 6.30 0.24 o -2 4 2 106.07 110.40 1.19 o -1 4 2 681.49 702.35 2.86 o 0 4 2 94.36 104.50 3.68 o 1 4 2 121.52 115.08 1.17 o 2 4 2 92.72 92.57 1.13 o 3 4 2 90.14 93.45 1.26 o 4 4 2 45.53 44.24 0.98 o 5 4 2 90.61 92.52 1.45 o 6 4 2 10.67 9.34 0.39 o 7 4 2 14.49 15.27 0.43 o -7 5 2 3.55 4.17 0.23 o -6 5 2 0.27 0.02 0.25 o -5 5 2 17.84 17.78 0.54 o -4 5 2 18.98 20.48 0.62 o -3 5 2 17.81 17.06 0.49 o -2 5 2 51.96 50.50 0.97 o -1 5 2 54.56 53.79 0.95 o 0 5 2 75.99 79.16 1.55 o 1 5 2 4.07 4.53 0.25 o 2 5 2 50.76 48.42 0.96 o 3 5 2 17.26 17.55 0.56 o 4 5 2 44.51 43.40 1.00 o 5 5 2 3.08 3.38 0.28 o 6 5 2 4.54 4.94 0.29 o 7 5 2 0.19 -0.03 0.18 o -6 6 2 8.20 7.89 0.32 o -5 6 2 3.41 3.66 0.29 o -4 6 2 7.14 8.67 0.35 o -3 6 2 50.13 53.23 1.12 o -2 6 2 5.04 5.36 0.34 o -1 6 2 48.62 53.55 1.09 o 0 6 2 39.81 43.15 1.66 o 1 6 2 6.12 5.39 0.31 o 2 6 2 19.61 19.67 0.62 o 3 6 2 24.47 27.33 0.74 o 4 6 2 39.01 39.10 0.96 o 5 6 2 9.67 9.21 0.38 o 6 6 2 8.19 8.64 0.34 o -5 7 2 2.51 2.46 0.23 o -4 7 2 16.88 18.16 0.55 o -3 7 2 12.99 14.71 0.45 o -2 7 2 12.69 11.48 0.42 o -1 7 2 42.38 42.31 1.04 o 0 7 2 6.52 6.51 0.50 o 1 7 2 9.95 9.56 0.40 o 2 7 2 4.35 4.32 0.30 o 3 7 2 30.10 32.91 0.86 o 4 7 2 12.71 12.39 0.41 o 5 7 2 0.36 0.50 0.19 o -4 8 2 0.47 0.74 0.22 o -3 8 2 12.05 11.72 0.39 o -2 8 2 0.18 0.08 0.27 o -1 8 2 12.59 13.12 0.46 o 0 8 2 10.68 10.33 0.30 o 1 8 2 0.06 -0.02 0.31 o 2 8 2 1.26 1.49 0.25 o 3 8 2 43.05 44.09 0.85 o 4 8 2 0.53 0.51 0.19 o -2 9 2 3.99 3.35 0.25 o -1 9 2 10.29 8.72 0.35 o 0 9 2 5.31 4.66 0.27 o 1 9 2 4.06 4.71 0.26 o -8 0 3 4.63 3.88 0.25 o -7 0 3 14.52 13.68 0.43 o -6 0 3 2.13 1.95 0.21 o -5 0 3 1.81 2.67 0.21 o -4 0 3 247.28 245.07 1.72 o -3 0 3 9.61 12.41 0.34 o -2 0 3 310.92 285.59 1.30 o -1 0 3 120.96 94.14 0.64 o 0 0 3 642.10 562.28 8.26 o 1 0 3 276.16 258.22 1.15 o 2 0 3 3.99 3.91 0.13 o 3 0 3 906.68 973.96 3.22 o 4 0 3 0.50 0.39 0.19 o 5 0 3 360.03 343.91 2.59 o 6 0 3 14.76 14.95 0.45 o 7 0 3 0.44 0.21 0.26 o 8 0 3 0.36 0.61 0.19 o -8 1 3 0.77 0.62 0.20 o -7 1 3 9.08 7.88 0.35 o -6 1 3 4.71 4.50 0.29 o -5 1 3 20.48 22.49 0.64 o -4 1 3 89.06 96.57 1.11 o -3 1 3 4.85 5.49 0.17 o -2 1 3 21.77 18.78 0.36 o -1 1 3 338.34 333.46 1.29 o 0 1 3 215.91 187.09 1.35 o 1 1 3 110.26 93.37 0.72 o 2 1 3 759.18 743.87 2.43 o 3 1 3 43.33 33.52 0.61 o 4 1 3 22.72 24.20 0.62 o 5 1 3 92.45 86.94 1.32 o 6 1 3 6.65 7.31 0.34 o 7 1 3 3.24 3.20 0.27 o 8 1 3 0.82 0.42 0.19 o -8 2 3 2.88 3.77 0.23 o -7 2 3 0.78 0.77 0.27 o -6 2 3 5.62 4.98 0.28 o -5 2 3 13.04 14.34 0.42 o -4 2 3 23.30 23.85 0.60 o -3 2 3 58.32 69.54 0.85 o -2 2 3 98.44 86.73 0.83 o -1 2 3 484.84 456.28 1.73 o 0 2 3 179.45 154.32 2.63 o 1 2 3 45.42 47.21 0.58 o 2 2 3 385.27 399.45 1.91 o 3 2 3 366.53 388.53 2.18 o 4 2 3 92.05 91.64 1.24 o 5 2 3 15.91 14.71 0.43 o 6 2 3 66.93 62.46 1.20 o 7 2 3 4.79 5.02 0.29 o 8 2 3 3.79 4.09 0.22 o -8 3 3 0.04 0.15 0.18 o -7 3 3 2.17 2.21 0.23 o -6 3 3 15.24 15.00 0.45 o -5 3 3 17.55 17.39 0.50 o -4 3 3 65.89 67.10 1.05 o -3 3 3 4.64 5.73 0.21 o -2 3 3 134.02 145.03 1.22 o -1 3 3 477.83 492.75 2.11 o 0 3 3 35.44 36.64 0.97 o 1 3 3 356.46 322.53 1.76 o 2 3 3 379.80 405.85 2.17 o 3 3 3 78.00 75.80 1.06 o 4 3 3 17.76 17.63 0.53 o 5 3 3 16.98 16.09 0.46 o 6 3 3 3.19 3.60 0.27 o 7 3 3 2.23 2.33 0.22 o -7 4 3 3.19 3.08 0.25 o -6 4 3 1.20 0.80 0.33 o -5 4 3 24.42 24.02 0.67 o -4 4 3 21.87 20.20 0.58 o -3 4 3 6.07 5.46 0.27 o -2 4 3 175.32 189.49 1.61 o -1 4 3 93.24 91.88 1.07 o 0 4 3 212.03 216.47 3.49 o 1 4 3 194.44 189.84 1.57 o 2 4 3 20.16 20.59 0.58 o 3 4 3 19.11 18.25 0.53 o 4 4 3 42.63 39.60 0.95 o 5 4 3 7.49 7.75 0.35 o 6 4 3 2.87 2.81 0.27 o 7 4 3 4.22 4.28 0.26 o -7 5 3 4.58 4.23 0.24 o -6 5 3 5.76 5.56 0.33 o -5 5 3 3.93 3.64 0.26 o -4 5 3 45.62 48.47 1.05 o -3 5 3 17.24 19.52 0.58 o -2 5 3 62.25 70.26 1.13 o -1 5 3 72.49 75.29 1.14 o 0 5 3 33.83 33.47 0.64 o 1 5 3 41..63 44.53 0.90 o 2 5 3 3.28 4.20 0.28 o 3 5 3 26.58 29.37 0.81 o 4 5 3 23.40 25.25 0.69 o 5 5 3 7.67 8.29 0.38 o 6 5 3 1.05 0.90 0.19 o -6 6 3 0.36 0.19 0.23 o -5 6 3 1.69 1.62 0.23 o -4 6 3 6.70 7.05 0.33 o -3 6 3 12.38 14.06 0.44 o -2 6 3 22.01 24.80 0.68 o -1 6 3 9.99 11.41 0.41 o 0 6 3 33.58 31.13 0.60 o 1 6 3 46.56 46.66 1.04 o 2 6 3 11.05 12.36 0.43 o 3 6 3 3.79 3.73 0.29 o 4 6 3 0.46 0.57 0.31 o 5 6 3 26.12 25.02 0.70 o 6 6 3 3.25 2.48 0.22 o -5 7 3 0.91 1.04 0.18 o -4 7 3 14.47 13.93 0.44 o -3 7 3 7.61 9.07 0.41 o -2 7 3 0.53 0.73 0.29 o -1 7 3 33.91 36.40 0.96 o 0 7 3 4.74 4.87 0.22 o 1 7 3 0.16 0.06 0.30 o 2 7 3 0.07 0.10 0.31 o 3 7 3 7.70 7.58 0.37 o 4 7 3 1.15 1.33 0.21 o 5 7 3 5.81 5.64 0.26 o -4 8 3 0.16 0.05 0.19 o -3 8 3 5.78 5.36 0.30 o -2 8 3 4.19 3.96 0.30 o -1 8 3 3.48 3.51 0.31 o 0 8 3 25.48 23.99 0.46 o 1 8 3 2.55 2.33 0.24 o 2 8 3 14.49 14.48 0.43 o 3 8 3 3.53 3.36 0.25 o -1 9 3 7.66 5.83 0.29 o 0 9 3 0.23 -0.04 0.16 o 1 9 3 0.05 -0.21 0.21 o -8 0 4 3.21 3.23 0.23 o -7 0 4 0.40 0.64 0.27 o -6 0 4 2.89 2.31 0.23 o -5 0 4 7.94 6.88 0.28 o -4 0 4 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