#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/00/88/2008848.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2008848_Fobs loop_ _publ_author_name 'Petri, A.' 'Schwarz, T.' 'Schilling, J.' 'Lentz, A.' _publ_section_title ; Polymeric (cyclopropane-1,1-dicarboxylato)copper(II) ; _journal_issue 8 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 1247 _journal_page_last 1248 _journal_volume 55 _journal_year 1999 _space_group_IT_number 92 _symmetry_space_group_name_Hall 'P 4abw 2nw' _symmetry_space_group_name_H-M 'P 41 21 2' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 6.7940 _cell_length_b 6.7940 _cell_length_c 11.9557 _exptl_crystal_F_000 380.00 _reflns_d_resolution_high 0.8111 _[local]_cod_data_source_file sk1210sup2.hkl _[local]_cod_data_source_block pet145 #BEGIN Tags that were not found in dictionaries: _shelx_title ' PET145 -- Cu(C3H4(COO)2) -- IT-Nr. 92 P412121' _shelx_refln_list_code 4 _shelx_f_calc_maximum 135.70 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z+1/2' '-y+1/2, x+1/2, z+1/4' 'y+1/2, -x+1/2, z+3/4' '-x+1/2, y+1/2, -z+1/4' 'x+1/2, -y+1/2, -z+3/4' 'y, x, -z' '-y, -x, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 1 0 2560.91 2525.68 36.70 o 0 2 0 10819.37 10693.86 72.09 o 1 2 0 19.89 32.54 4.27 o 2 2 0 892.49 737.41 14.32 o 1 3 0 164.93 185.20 5.72 o 2 3 0 194.90 175.29 6.76 o 3 3 0 1218.85 1338.11 16.60 o 0 4 0 8407.10 8251.05 44.84 o 1 4 0 2319.28 2257.97 15.53 o 2 4 0 4749.31 4672.94 121.96 o 3 4 0 1113.99 1136.17 10.73 o 4 4 0 3418.26 3424.13 24.93 o 1 5 0 46.20 46.00 4.95 o 2 5 0 11.29 12.91 4.43 o 3 5 0 6.54 10.74 7.71 o 4 5 0 189.29 190.66 6.44 o 5 5 0 355.78 361.44 10.77 o 0 6 0 797.06 751.20 12.97 o 1 6 0 188.06 173.19 5.81 o 2 6 0 249.27 229.99 6.00 o 3 6 0 598.18 573.85 8.59 o 4 6 0 396.02 403.66 8.09 o 5 6 0 291.24 285.30 17.53 o 1 7 0 30.14 32.80 5.63 o 2 7 0 151.49 149.68 6.79 o 3 7 0 1.13 2.56 6.49 o 4 7 0 238.64 209.35 7.84 o 0 8 0 359.24 356.44 12.40 o 1 8 0 1191.12 1126.05 64.24 o 2 8 0 116.19 124.92 8.16 o 0 1 1 5579.13 5383.37 70.26 o 1 1 1 1060.68 1148.64 16.34 o -1 2 1 1140.68 1058.43 16.00 o 0 2 1 318.36 355.74 8.64 o 1 2 1 1363.09 1311.73 38.83 o 2 2 1 763.19 706.79 9.81 o -2 3 1 697.33 595.84 8.46 o -1 3 1 1462.64 1477.19 12.89 o 0 3 1 3752.03 3793.96 22.59 o 1 3 1 1446.21 1438.44 57.10 o 2 3 1 656.39 571.64 13.94 o 3 3 1 1729.17 1659.68 19.75 o -3 4 1 1465.55 1479.21 17.30 o -2 4 1 703.77 668.22 8.73 o -1 4 1 3677.86 3596.50 48.01 o 0 4 1 837.47 822.92 25.53 o 1 4 1 3810.55 3630.72 151.36 o 2 4 1 709.35 676.17 8.89 o 3 4 1 1412.23 1406.75 12.89 o 4 4 1 779.78 767.06 19.37 o -4 5 1 962.45 949.38 18.11 o -3 5 1 467.85 479.51 7.91 o -2 5 1 1502.03 1503.70 20.48 o -1 5 1 481.21 483.69 7.76 o 0 5 1 3175.38 3217.07 17.95 o 1 5 1 459.51 465.64 7.66 o 2 5 1 1412.09 1421.52 13.99 o 3 5 1 490.66 498.73 8.21 o 4 5 1 857.15 795.78 77.00 o 5 5 1 66.13 68.83 7.65 o -5 6 1 344.91 339.37 24.44 o -4 6 1 279.17 283.14 18.21 o -3 6 1 312.10 310.85 9.48 o -2 6 1 128.62 121.74 5.33 o -1 6 1 821.99 800.03 10.50 o 0 6 1 651.55 602.53 26.67 o 1 6 1 956.94 964.02 13.71 o 2 6 1 118.62 108.53 5.48 o 3 6 1 333.85 345.74 7.84 o 4 6 1 250.87 262.34 7.38 o 5 6 1 346.63 345.79 8.44 o -4 7 1 220.41 213.23 9.20 o -3 7 1 544.41 581.07 17.32 o -2 7 1 370.82 348.81 14.54 o -1 7 1 477.83 508.53 8.79 o 0 7 1 87.16 88.05 6.14 o 1 7 1 399.74 398.45 22.10 o 2 7 1 382.50 374.49 7.28 o 3 7 1 574.84 554.64 55.05 o 4 7 1 219.65 225.35 8.00 o -2 8 1 417.46 449.43 10.24 o -1 8 1 348.49 325.96 25.34 o 0 8 1 267.96 264.99 8.23 o 1 8 1 342.08 341.75 16.25 o 2 8 1 406.65 381.93 11.38 o 0 1 2 2319.27 2398.98 23.21 o 1 1 2 18415.17 18009.47 67.01 o -1 2 2 220.00 240.16 6.43 o 0 2 2 336.92 334.87 8.18 o 1 2 2 254.41 280.87 6.63 o 2 2 2 25.91 20.32 3.99 o -2 3 2 299.38 280.11 6.58 o -1 3 2 6313.84 6308.45 77.09 o 0 3 2 1649.75 1654.81 14.07 o 1 3 2 6344.41 6393.68 175.55 o 2 3 2 254.14 232.78 6.10 o 3 3 2 3812.36 3705.11 22.09 o -3 4 2 466.64 483.73 7.91 o -2 4 2 0.43 1.25 3.66 o -1 4 2 7.87 13.00 4.01 o 0 4 2 0.04 4.07 3.46 o 1 4 2 8.17 15.19 3.70 o 2 4 2 2.28 4.01 4.10 o 3 4 2 474.99 487.91 10.39 o 4 4 2 11.13 14.40 4.68 o -4 5 2 646.41 665.35 9.25 o -3 5 2 1665.31 1608.92 96.10 o -2 5 2 820.20 820.50 9.03 o -1 5 2 1666.30 1714.05 12.80 o 0 5 2 881.55 885.64 54.50 o 1 5 2 1783.59 1823.48 34.07 o 2 5 2 863.98 896.99 38.92 o 3 5 2 1556.72 1518.39 52.98 o 4 5 2 648.64 672.15 9.44 o 5 5 2 1030.17 1043.29 39.72 o -5 6 2 60.67 66.37 7.32 o -4 6 2 77.10 77.32 5.62 o -3 6 2 175.54 192.37 7.16 o -2 6 2 53.92 53.38 5.36 o -1 6 2 94.90 95.42 5.21 o 0 6 2 67.43 68.90 5.31 o 1 6 2 109.00 106.55 5.08 o 2 6 2 66.99 71.36 6.09 o 3 6 2 163.55 166.66 6.29 o 4 6 2 51.43 49.81 5.47 o 5 6 2 84.46 83.09 7.56 o -4 7 2 464.95 461.25 9.43 o -3 7 2 162.42 175.43 7.63 o -2 7 2 671.69 675.93 17.93 o -1 7 2 522.33 529.38 26.02 o 0 7 2 740.20 753.33 9.70 o 1 7 2 580.47 592.67 9.13 o 2 7 2 634.68 594.09 12.88 o 3 7 2 162.37 160.17 7.00 o 4 7 2 537.35 511.53 29.80 o -2 8 2 114.81 124.67 7.83 o -1 8 2 19.06 16.88 6.73 o 0 8 2 188.39 175.79 7.90 o 1 8 2 15.82 23.38 6.53 o 2 8 2 129.99 130.12 11.26 o 0 1 3 970.45 923.68 12.29 o 1 1 3 3713.33 4088.40 25.42 o -1 2 3 3159.25 3025.30 20.09 o 0 2 3 1628.75 1631.71 14.72 o 1 2 3 3419.17 3390.00 30.70 o 2 2 3 19.16 13.53 3.69 o -2 3 3 1926.24 1807.44 13.06 o -1 3 3 688.92 762.81 24.65 o 0 3 3 7055.12 7218.68 46.09 o 1 3 3 578.27 637.97 12.64 o 2 3 3 1987.76 1896.35 56.23 o 3 3 3 15.88 19.23 3.86 o -3 4 3 1637.52 1673.58 12.81 o -2 4 3 620.89 649.27 8.40 o -1 4 3 2071.10 1996.12 58.40 o 0 4 3 1581.69 1587.26 13.00 o 1 4 3 2019.61 1938.99 57.22 o 2 4 3 667.03 694.60 14.43 o 3 4 3 1489.38 1484.77 55.71 o 4 4 3 1436.14 1440.15 11.56 o -4 5 3 584.09 614.77 10.15 o -3 5 3 627.01 587.77 22.74 o -2 5 3 248.84 242.80 5.91 o -1 5 3 1060.09 1058.05 9.99 o 0 5 3 943.90 967.06 10.54 o 1 5 3 1008.68 1020.03 9.68 o 2 5 3 306.01 292.27 6.14 o 3 5 3 619.76 624.35 7.92 o 4 5 3 589.60 593.20 17.57 o 5 5 3 313.10 316.83 7.42 o -5 6 3 112.80 123.98 7.28 o -4 6 3 149.76 154.99 9.40 o -3 6 3 596.78 582.30 26.72 o -2 6 3 258.28 273.88 7.06 o -1 6 3 682.95 665.41 8.44 o 0 6 3 1089.62 1071.47 11.12 o 1 6 3 672.48 616.86 39.73 o 2 6 3 226.00 246.10 6.58 o 3 6 3 611.04 632.90 17.95 o 4 6 3 147.19 148.17 6.48 o 5 6 3 105.52 115.11 7.28 o -4 7 3 410.63 386.62 9.18 o -3 7 3 150.08 158.64 7.36 o -2 7 3 460.41 459.88 15.44 o -1 7 3 226.35 230.35 6.90 o 0 7 3 851.81 851.80 29.12 o 1 7 3 218.28 198.10 22.92 o 2 7 3 459.10 443.05 8.01 o 3 7 3 158.85 176.83 7.61 o 4 7 3 409.76 393.82 9.35 o -1 8 3 173.90 157.91 12.07 o 0 8 3 323.08 313.25 8.00 o 1 8 3 170.15 155.67 7.90 o 0 0 4 5462.35 5961.36 121.27 o 0 1 4 1448.46 1638.21 24.14 o 1 1 4 121.62 115.35 5.26 o -1 2 4 2560.34 2675.30 37.93 o 0 2 4 9158.28 9496.56 34.84 o 1 2 4 2409.99 2546.98 28.00 o 2 2 4 10555.76 10637.45 447.12 o -2 3 4 40.87 35.00 4.13 o -1 3 4 154.94 155.75 5.26 o 0 3 4 217.59 227.17 5.77 o 1 3 4 146.53 147.18 6.99 o 2 3 4 29.41 23.31 4.08 o 3 3 4 195.30 202.17 5.71 o -3 4 4 763.40 758.02 8.50 o -2 4 4 2425.60 2467.10 74.90 o -1 4 4 790.53 776.52 12.92 o 0 4 4 1327.40 1222.55 20.11 o 1 4 4 660.02 635.41 10.58 o 2 4 4 2417.49 2412.66 64.36 o 3 4 4 886.97 905.73 9.27 o 4 4 4 1459.09 1473.84 12.24 o -4 5 4 249.54 240.26 6.63 o -3 5 4 185.31 177.16 5.46 o -2 5 4 831.40 855.68 14.65 o -1 5 4 28.83 28.64 4.56 o 0 5 4 12.16 5.90 4.96 o 1 5 4 30.83 32.50 4.89 o 2 5 4 917.53 918.32 34.99 o 3 5 4 224.77 209.65 10.01 o 4 5 4 237.84 237.09 6.81 o 5 5 4 42.60 51.34 5.93 o -5 6 4 290.24 282.97 8.39 o -4 6 4 524.02 526.85 8.98 o -3 6 4 861.11 872.95 28.38 o -2 6 4 1141.38 1178.60 10.77 o -1 6 4 929.71 994.97 14.89 o 0 6 4 1032.13 1047.06 29.44 o 1 6 4 904.20 957.65 9.72 o 2 6 4 1082.71 1126.38 42.23 o 3 6 4 882.34 870.61 9.39 o 4 6 4 614.33 626.34 9.25 o 5 6 4 281.72 256.91 21.75 o -3 7 4 144.51 141.80 6.88 o -2 7 4 94.36 95.32 6.66 o -1 7 4 35.46 31.65 5.61 o 0 7 4 162.99 142.21 5.79 o 1 7 4 29.34 26.19 5.71 o 2 7 4 106.84 108.97 6.77 o 3 7 4 116.32 112.88 6.85 o 4 7 4 37.18 52.88 9.32 o 0 8 4 175.37 185.68 7.71 o 0 1 5 1594.78 1399.11 54.93 o 1 1 5 14.63 22.74 3.81 o -1 2 5 3808.20 3753.27 30.83 o 0 2 5 122.01 147.16 5.00 o 1 2 5 3850.84 3812.59 68.28 o 2 2 5 649.88 647.41 8.38 o -2 3 5 2888.07 2816.84 16.42 o -1 3 5 917.28 893.44 16.40 o 0 3 5 1176.11 1087.84 10.29 o 1 3 5 919.13 943.17 22.97 o 2 3 5 2926.13 2882.49 15.53 o 3 3 5 1316.52 1360.88 25.96 o -3 4 5 359.81 363.59 7.04 o -2 4 5 505.05 514.84 7.65 o -1 4 5 1194.95 1230.75 18.95 o 0 4 5 10.12 10.31 4.81 o 1 4 5 1182.02 1219.96 25.60 o 2 4 5 467.76 475.26 13.59 o 3 4 5 412.24 417.64 6.97 o 4 4 5 6.25 9.31 4.71 o -4 5 5 216.70 220.20 6.72 o -3 5 5 141.89 151.83 5.96 o -2 5 5 1520.88 1495.30 46.18 o -1 5 5 641.47 639.50 8.02 o 0 5 5 532.78 503.50 7.67 o 1 5 5 620.64 630.83 7.84 o 2 5 5 1473.66 1468.71 64.01 o 3 5 5 132.66 140.22 5.98 o 4 5 5 225.72 243.49 7.16 o 5 5 5 404.98 410.87 9.72 o -5 6 5 201.60 207.63 12.01 o -4 6 5 368.15 389.53 9.04 o -3 6 5 675.67 653.11 8.60 o -2 6 5 765.24 784.62 9.40 o -1 6 5 630.76 648.87 9.05 o 0 6 5 124.59 136.90 5.82 o 1 6 5 599.04 605.80 8.28 o 2 6 5 744.48 759.45 30.16 o 3 6 5 724.37 695.61 10.46 o 4 6 5 341.25 366.22 8.63 o 5 6 5 202.44 196.79 7.79 o -3 7 5 204.31 183.20 10.26 o -2 7 5 357.78 369.17 8.52 o -1 7 5 575.56 547.38 38.68 o 0 7 5 222.45 236.76 7.28 o 1 7 5 599.26 596.85 14.88 o 2 7 5 330.88 339.53 8.58 o 3 7 5 164.46 155.88 6.88 o 0 1 6 12.18 12.92 3.61 o 1 1 6 7357.77 7648.83 60.45 o -1 2 6 404.67 427.28 6.97 o 0 2 6 113.79 120.01 4.92 o 1 2 6 421.86 426.71 14.96 o 2 2 6 381.36 368.12 6.61 o -2 3 6 801.23 793.22 12.49 o -1 3 6 2735.41 2585.27 17.76 o 0 3 6 457.95 430.99 6.88 o 1 3 6 2782.32 2667.97 36.99 o 2 3 6 798.60 819.31 25.77 o 3 3 6 4413.82 4619.30 68.39 o -3 4 6 11.22 10.54 4.57 o -2 4 6 33.59 34.06 4.72 o -1 4 6 252.35 261.15 6.29 o 0 4 6 1.09 2.34 4.67 o 1 4 6 276.18 281.55 12.90 o 2 4 6 26.13 32.15 4.43 o 3 4 6 30.48 27.99 4.83 o 4 4 6 37.64 44.24 5.68 o -4 5 6 520.84 516.14 8.39 o -3 5 6 1018.31 1057.38 10.27 o -2 5 6 693.19 662.71 15.88 o -1 5 6 1321.53 1335.56 18.17 o 0 5 6 399.69 421.68 7.59 o 1 5 6 1336.92 1283.61 114.01 o 2 5 6 712.87 685.20 12.17 o 3 5 6 1006.69 1039.15 33.76 o 4 5 6 527.10 508.28 16.76 o 5 5 6 127.81 140.80 6.79 o -4 6 6 152.17 150.11 6.86 o -3 6 6 51.75 53.31 8.21 o -2 6 6 18.40 21.37 5.63 o -1 6 6 150.95 139.07 6.17 o 0 6 6 0.04 -0.80 5.15 o 1 6 6 156.09 151.04 6.04 o 2 6 6 15.84 17.85 5.01 o 3 6 6 52.07 61.01 8.24 o 4 6 6 153.90 156.18 7.30 o -3 7 6 342.87 373.47 12.36 o -2 7 6 522.54 514.99 9.20 o -1 7 6 491.26 488.57 14.37 o 0 7 6 535.41 562.40 9.01 o 1 7 6 499.03 484.48 19.40 o 2 7 6 568.49 587.90 20.44 o 3 7 6 343.32 347.73 12.61 o 0 1 7 983.94 895.29 22.84 o 1 1 7 145.10 152.90 4.96 o -1 2 7 3562.45 3434.50 46.13 o 0 2 7 134.06 131.83 4.72 o 1 2 7 3582.06 3374.91 44.86 o 2 2 7 1202.20 1119.60 94.64 o -2 3 7 2527.91 2546.77 17.13 o -1 3 7 155.48 149.57 5.51 o 0 3 7 621.58 580.60 8.00 o 1 3 7 146.85 145.36 5.65 o 2 3 7 2478.59 2531.80 14.22 o 3 3 7 470.50 451.76 7.28 o -3 4 7 298.29 305.50 6.74 o -2 4 7 535.55 535.05 7.45 o -1 4 7 737.51 728.34 8.75 o 0 4 7 286.94 299.92 6.51 o 1 4 7 789.90 813.74 37.43 o 2 4 7 567.17 573.69 7.61 o 3 4 7 239.55 244.94 6.31 o 4 4 7 2.83 4.71 5.43 o -4 5 7 172.79 185.60 7.86 o -3 5 7 130.91 130.86 5.95 o -2 5 7 1109.52 1137.73 12.78 o -1 5 7 183.56 189.87 9.70 o 0 5 7 293.97 305.48 7.02 o 1 5 7 179.95 185.13 8.22 o 2 5 7 1117.73 1148.67 12.84 o 3 5 7 89.29 89.74 5.55 o 4 5 7 151.63 151.97 7.22 o 5 5 7 536.28 559.77 21.74 o -4 6 7 298.06 287.99 8.32 o -3 6 7 611.83 624.41 15.68 o -2 6 7 813.34 808.75 9.82 o -1 6 7 547.50 531.54 20.89 o 0 6 7 533.61 526.00 11.87 o 1 6 7 600.94 594.70 8.33 o 2 6 7 785.47 781.64 17.09 o 3 6 7 565.82 569.00 35.08 o 4 6 7 276.78 278.94 8.67 o -2 7 7 176.55 175.33 8.29 o -1 7 7 357.55 347.10 8.29 o 0 7 7 107.97 95.22 6.51 o 1 7 7 331.24 321.88 9.72 o 2 7 7 198.55 180.29 10.69 o 0 0 8 1513.56 1495.27 53.44 o 0 1 8 68.74 69.60 4.28 o 1 1 8 37.34 44.60 4.57 o -1 2 8 671.78 700.28 8.47 o 0 2 8 3741.14 3902.55 17.92 o 1 2 8 710.07 747.45 8.66 o 2 2 8 5124.02 5108.87 188.31 o -2 3 8 176.13 171.59 6.05 o -1 3 8 18.22 22.97 4.92 o 0 3 8 383.73 410.86 7.13 o 1 3 8 20.91 18.69 4.66 o 2 3 8 226.29 216.54 6.47 o 3 3 8 472.45 441.74 9.02 o -3 4 8 376.97 369.58 13.70 o -2 4 8 1355.04 1327.62 11.28 o -1 4 8 372.70 359.55 10.25 o 0 4 8 746.72 770.28 8.84 o 1 4 8 459.86 455.73 7.27 o 2 4 8 1332.43 1307.41 10.36 o 3 4 8 309.05 308.15 6.94 o 4 4 8 829.22 798.79 11.04 o -4 5 8 233.81 244.39 7.79 o -3 5 8 201.07 207.40 6.77 o -2 5 8 182.95 173.28 11.96 o -1 5 8 43.26 43.88 5.67 o 0 5 8 71.15 64.21 6.10 o 1 5 8 40.51 39.61 5.93 o 2 5 8 160.58 158.91 6.24 o 3 5 8 171.80 173.19 6.50 o 4 5 8 240.53 242.10 13.80 o -3 6 8 522.28 513.20 9.28 o -2 6 8 821.67 790.62 34.79 o -1 6 8 657.71 633.64 43.14 o 0 6 8 1045.12 1085.77 20.26 o 1 6 8 707.88 717.55 9.44 o 2 6 8 876.86 886.54 10.17 o 3 6 8 555.04 562.33 9.62 o 0 1 9 1217.59 1238.48 26.66 o 1 1 9 667.00 699.25 8.48 o -1 2 9 2063.62 2053.39 13.71 o 0 2 9 90.95 92.40 5.03 o 1 2 9 1900.77 1871.88 12.40 o 2 2 9 2.86 4.32 4.34 o -2 3 9 804.81 779.77 12.85 o -1 3 9 127.77 128.14 5.39 o 0 3 9 2351.45 2386.40 18.32 o 1 3 9 144.85 143.44 5.36 o 2 3 9 801.82 781.33 12.75 o 3 3 9 141.30 148.13 9.53 o -3 4 9 460.59 461.68 12.06 o -2 4 9 156.71 156.61 6.38 o -1 4 9 757.17 803.50 9.46 o 0 4 9 116.59 107.32 6.14 o 1 4 9 730.41 783.99 12.40 o 2 4 9 128.45 128.05 6.84 o 3 4 9 497.88 504.58 8.54 o 4 4 9 526.89 528.34 11.24 o -4 5 9 335.36 309.94 8.30 o -3 5 9 338.28 348.39 8.18 o -2 5 9 173.44 191.30 6.39 o -1 5 9 663.91 644.97 8.47 o 0 5 9 594.69 557.93 23.09 o 1 5 9 674.24 661.88 8.94 o 2 5 9 165.80 174.42 6.25 o 3 5 9 342.97 359.10 8.28 o 4 5 9 381.25 342.17 17.96 o -2 6 9 97.60 98.22 6.77 o -1 6 9 202.81 201.15 7.89 o 0 6 9 293.76 306.85 7.92 o 1 6 9 196.43 182.68 7.77 o 2 6 9 98.63 100.38 6.59 o 0 1 10 135.03 138.49 5.22 o 1 1 10 2529.02 2635.22 74.94 o -1 2 10 12.70 12.15 4.47 o 0 2 10 3.42 5.83 4.38 o 1 2 10 18.54 18.79 4.44 o 2 2 10 56.89 57.30 4.83 o -2 3 10 245.43 253.27 7.16 o -1 3 10 1393.86 1455.34 11.46 o 0 3 10 525.57 513.17 8.05 o 1 3 10 1393.67 1467.29 24.26 o 2 3 10 242.90 247.94 10.07 o 3 3 10 834.77 856.53 9.45 o -3 4 10 220.93 228.84 7.60 o -2 4 10 78.02 82.64 5.69 o -1 4 10 64.98 63.62 5.92 o 0 4 10 10.60 12.16 6.03 o 1 4 10 74.95 74.13 5.90 o 2 4 10 79.31 85.21 9.18 o 3 4 10 229.79 237.24 7.42 o 4 4 10 74.36 69.30 7.04 o -3 5 10 747.22 758.21 22.54 o -2 5 10 373.79 388.49 8.74 o -1 5 10 1063.67 871.72 153.92 o 0 5 10 177.22 185.74 7.38 o 1 5 10 1011.42 1032.70 10.60 o 2 5 10 361.44 369.07 8.27 o 3 5 10 808.39 805.54 48.94 o -1 6 10 2.65 4.33 6.55 o 0 6 10 0.94 -0.86 6.62 o 1 6 10 1.71 -5.77 13.46 o 0 1 11 2119.13 2091.15 48.62 o 1 1 11 223.53 222.81 7.94 o -1 2 11 790.72 814.76 13.10 o 0 2 11 2.65 4.25 5.07 o 1 2 11 788.12 801.73 16.95 o 2 2 11 311.66 301.58 6.86 o -2 3 11 282.99 295.20 7.39 o -1 3 11 180.56 172.57 6.63 o 0 3 11 974.49 943.99 11.60 o 1 3 11 192.91 189.82 6.36 o 2 3 11 254.16 255.06 9.02 o 3 3 11 254.70 264.39 7.54 o -3 4 11 443.61 465.81 27.40 o -2 4 11 352.66 362.18 8.41 o -1 4 11 877.88 851.25 32.76 o 0 4 11 223.11 214.48 6.53 o 1 4 11 880.02 856.36 28.34 o 2 4 11 330.42 331.28 9.59 o 3 4 11 523.18 519.76 8.91 o -2 5 11 305.81 310.50 10.67 o -1 5 11 57.52 62.73 6.82 o 0 5 11 821.44 844.85 22.07 o 1 5 11 55.63 58.89 6.51 o 2 5 11 314.25 299.24 8.44 o 0 0 12 5213.00 5478.78 49.87 o 0 1 12 0.06 4.81 5.02 o 1 1 12 210.02 215.57 6.92 o -1 2 12 47.86 50.21 5.35 o 0 2 12 825.08 849.40 9.28 o 1 2 12 54.57 56.76 5.52 o 2 2 12 277.78 292.13 6.97 o -2 3 12 75.63 86.54 9.27 o -1 3 12 79.11 85.22 6.56 o 0 3 12 40.20 43.40 5.96 o 1 3 12 79.79 79.20 6.65 o 2 3 12 77.15 80.69 7.21 o 3 3 12 1.62 3.92 6.08 o -2 4 12 1011.53 946.97 11.13 o -1 4 12 428.09 422.77 8.60 o 0 4 12 1244.72 1253.28 13.32 o 1 4 12 422.08 402.51 8.27 o 2 4 12 1041.90 968.62 10.95 o 0 1 13 1070.95 1045.83 10.42 o 1 1 13 12.96 14.83 6.30 o -1 2 13 629.01 605.75 21.27 o 0 2 13 0.44 3.44 6.32 o 1 2 13 627.59 625.66 9.18 o 2 2 13 106.77 104.20 6.57 o -2 3 13 333.66 293.27 9.90 o -1 3 13 124.93 130.48 7.25 o 0 3 13 577.86 500.90 68.86 o 1 3 13 131.05 132.29 7.09 o 2 3 13 370.88 344.39 8.18 o 0 1 14 168.56 158.07 7.34 o 1 1 14 776.33 772.05 24.96 o -1 2 14 12.60 16.12 6.70 o 0 2 14 75.44 66.96 6.94 o 1 2 14 14.63 19.05 6.87 o