#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/00/92/2009269.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2009269_Fobs loop_ _publ_author_name 'Kuhl, A.' 'Farrugia, L. J.' 'Kocienski, P. J.' _publ_section_title ; Absolute configuration of exo-syn-syn-dicarbonyl(\h^5^-cyclopentadienyl)[(1,2,3-\h)-(1R,2S,3S)-1-phenylbut-2-en-1-yl]molybdenum(II) ; _journal_issue 12 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 2041 _journal_page_last 2043 _journal_volume 55 _journal_year 1999 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _exptl_crystal_F_000 704.00 _[local]_cod_data_source_file gd1047sup2.hkl _[local]_cod_data_source_block pk4 #BEGIN Tags that were not found in dictionaries: _shelx_title ' Mo(C5H5)(CO)2{Ph(H).C.CH.C(H)Me} code pk4 in P212121' _shelx_refln_list_code 4 _shelx_f_calc_maximum 168.89 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 11120.14 10883.66 28.40 o 4 0 0 88.32 93.67 2.15 o 6 0 0 2181.60 2212.00 18.90 o 8 0 0 1667.18 1652.28 19.92 o 10 0 0 209.15 209.60 4.77 o 1 1 0 6365.42 5920.89 164.18 o 2 1 0 6518.97 6630.89 352.25 o 3 1 0 3206.21 3372.28 81.72 o 4 1 0 8035.47 8141.45 262.48 o 5 1 0 104.36 118.75 1.79 o 6 1 0 1879.54 1902.78 16.19 o 7 1 0 86.11 82.61 1.87 o 8 1 0 28.34 27.76 1.88 o 9 1 0 372.97 353.89 4.77 o 10 1 0 69.66 53.76 2.59 o 0 2 0 12532.91 12777.54 104.27 o 1 2 0 12884.21 11331.18 606.35 o 2 2 0 357.28 356.63 5.11 o 3 2 0 10737.42 10021.97 32.89 o 4 2 0 295.79 332.18 6.52 o 5 2 0 5472.27 5160.43 27.52 o 6 2 0 720.05 792.97 11.91 o 7 2 0 92.95 110.56 2.74 o 8 2 0 181.08 181.40 3.58 o 9 2 0 46.24 49.15 3.06 o 10 2 0 31.65 28.33 3.49 o 1 3 0 2110.26 2020.78 7.89 o 2 3 0 29.54 36.44 1.12 o 3 3 0 743.23 697.57 8.22 o 4 3 0 184.11 194.64 4.08 o 5 3 0 1660.50 1724.26 15.85 o 6 3 0 211.55 201.27 4.14 o 7 3 0 841.41 846.17 13.72 o 8 3 0 0.07 1.40 6.45 o 9 3 0 633.90 606.06 10.18 o 10 3 0 5.66 6.78 3.38 o 0 4 0 12189.91 12812.08 35.62 o 1 4 0 431.49 475.36 7.33 o 2 4 0 758.08 670.93 7.78 o 3 4 0 1554.07 1546.28 12.77 o 4 4 0 31.01 28.87 1.71 o 5 4 0 1701.19 1667.23 16.07 o 6 4 0 607.71 648.34 11.33 o 7 4 0 65.66 66.63 2.65 o 8 4 0 803.00 882.56 15.63 o 9 4 0 12.74 10.23 2.97 o 10 4 0 132.79 138.26 4.52 o 1 5 0 121.30 109.97 5.15 o 2 5 0 4418.77 4205.44 21.55 o 3 5 0 51.74 62.67 1.81 o 4 5 0 6564.40 6279.49 31.26 o 5 5 0 10.42 7.36 1.97 o 6 5 0 1377.78 1271.14 16.12 o 7 5 0 1.54 -0.74 5.90 o 8 5 0 4.72 -0.86 7.03 o 9 5 0 6.46 3.73 7.81 o 10 5 0 72.83 81.23 4.14 o 0 6 0 3957.84 3823.23 20.86 o 1 6 0 148.01 172.59 2.39 o 2 6 0 3225.17 3176.09 19.92 o 3 6 0 1629.22 1534.49 14.63 o 4 6 0 106.61 120.35 2.50 o 5 6 0 897.56 967.78 13.67 o 6 6 0 438.29 432.13 7.55 o 7 6 0 34.13 35.66 2.75 o 8 6 0 659.36 677.32 10.64 o 9 6 0 3.03 0.31 3.39 o 10 6 0 176.82 174.56 4.99 o 1 7 0 4610.92 4590.92 43.70 o 2 7 0 937.40 952.34 11.74 o 3 7 0 546.60 553.10 9.84 o 4 7 0 713.09 755.64 12.17 o 5 7 0 292.81 305.53 6.51 o 6 7 0 56.55 53.03 2.73 o 7 7 0 797.58 803.69 15.60 o 8 7 0 1.74 1.24 2.88 o 9 7 0 287.52 323.19 6.32 o 0 8 0 23.19 29.06 1.93 o 1 8 0 47.19 39.16 1.39 o 2 8 0 3.12 8.98 1.99 o 3 8 0 1856.43 1773.07 17.91 o 4 8 0 3.64 1.45 5.43 o 5 8 0 1721.47 1731.05 19.62 o 6 8 0 1.07 3.69 2.63 o 7 8 0 308.01 295.15 6.43 o 8 8 0 6.28 6.75 3.04 o 9 8 0 3.17 3.19 3.56 o 1 9 0 1567.37 1516.34 11.74 o 2 9 0 695.39 654.29 11.69 o 3 9 0 239.30 231.46 4.20 o 4 9 0 739.90 721.93 13.24 o 5 9 0 10.19 15.55 2.50 o 6 9 0 477.01 472.20 8.95 o 7 9 0 205.12 195.40 4.19 o 8 9 0 1.46 0.38 3.36 o 0 10 0 1322.48 1251.06 16.26 o 1 10 0 7.37 10.44 1.60 o 2 10 0 1049.56 998.99 15.10 o 3 10 0 12.05 11.61 2.50 o 4 10 0 36.98 42.87 2.75 o 5 10 0 25.56 21.56 2.89 o 6 10 0 54.70 66.09 3.26 o 7 10 0 10.69 10.05 3.33 o 8 10 0 217.99 226.45 5.28 o 1 11 0 525.20 500.63 6.78 o 2 11 0 234.16 210.41 4.00 o 3 11 0 4.25 -0.21 6.09 o 4 11 0 340.44 331.20 7.90 o 5 11 0 16.06 17.79 2.87 o 6 11 0 171.03 158.75 4.02 o 7 11 0 42.90 48.80 3.97 o 0 12 0 26.29 34.26 2.87 o 1 12 0 24.64 25.28 1.97 o 2 12 0 64.37 61.76 3.06 o 3 12 0 364.03 350.10 6.68 o 4 12 0 1.02 4.51 2.67 o 5 12 0 155.82 154.95 4.39 o 6 12 0 29.18 31.29 3.84 o 1 13 0 335.60 306.23 6.33 o 2 13 0 33.63 26.42 3.07 o 3 13 0 27.66 28.82 3.12 o 4 13 0 15.18 17.21 3.53 o 5 13 0 27.56 30.85 3.86 o 0 14 0 90.62 86.67 4.03 o 1 14 0 25.81 29.21 5.16 o 2 14 0 73.41 61.51 4.02 o 3 14 0 188.26 194.59 5.18 o 4 14 0 0.82 -2.33 8.12 o 1 15 0 10.20 8.56 3.53 o 1 0 1 9337.93 8563.70 423.82 o 2 0 1 3039.91 3180.61 71.28 o 3 0 1 9812.96 9810.78 361.91 o 4 0 1 680.23 660.70 8.94 o 5 0 1 6002.29 6156.91 113.84 o 6 0 1 153.97 159.62 2.21 o 7 0 1 229.67 224.92 2.89 o 8 0 1 14.33 17.30 1.85 o 9 0 1 26.54 27.30 5.88 o 10 0 1 24.66 9.27 8.53 o -10 1 1 39.76 37.98 2.54 o -9 1 1 591.14 544.70 6.86 o -8 1 1 313.93 306.79 6.08 o -7 1 1 977.26 994.45 10.47 o -6 1 1 1059.71 1034.53 9.34 o -5 1 1 1688.99 1742.28 10.75 o -4 1 1 4714.89 4555.13 44.09 o -3 1 1 2620.14 2740.82 16.09 o -2 1 1 5671.54 5664.24 91.31 o -1 1 1 16714.00 14131.67 680.39 o 1 1 1 16725.14 13819.64 497.02 o 2 1 1 5459.31 5749.84 193.47 o 3 1 1 2673.46 2806.72 34.04 o 4 1 1 4665.58 4531.46 36.78 o 5 1 1 1734.11 1831.15 17.99 o 6 1 1 1097.38 1057.64 16.87 o 7 1 1 965.47 970.16 27.95 o 8 1 1 313.41 305.43 5.01 o 9 1 1 593.67 538.61 6.75 o 10 1 1 39.80 43.29 2.48 o -10 2 1 191.81 189.64 4.73 o -9 2 1 166.67 168.04 3.83 o -8 2 1 1080.03 1168.15 17.09 o -7 2 1 138.54 136.59 2.98 o -6 2 1 687.03 704.58 11.27 o -5 2 1 578.18 601.60 9.61 o -4 2 1 323.69 337.30 4.72 o -3 2 1 2261.05 2216.83 13.70 o -2 2 1 408.05 421.34 5.46 o -1 2 1 11529.38 11472.80 277.18 o 0 2 1 28522.77 25915.89 647.55 o 1 2 1 11571.11 11291.66 79.54 o 2 2 1 404.15 416.97 5.47 o 3 2 1 2236.31 2204.13 13.75 o 4 2 1 338.08 362.87 6.89 o 5 2 1 604.70 669.04 9.93 o 6 2 1 683.87 697.69 11.42 o 7 2 1 158.46 153.50 3.06 o 8 2 1 1073.35 1055.60 16.78 o 9 2 1 170.50 163.53 3.92 o 10 2 1 191.62 199.46 4.66 o -10 3 1 92.03 92.79 4.02 o -9 3 1 70.10 77.19 3.39 o -8 3 1 20.79 21.66 2.76 o -7 3 1 180.91 179.94 3.96 o -6 3 1 1454.01 1416.73 15.94 o -5 3 1 1024.88 1028.22 12.42 o -4 3 1 6522.68 6197.22 28.48 o -3 3 1 3916.67 3751.16 19.30 o -2 3 1 4645.11 4630.53 19.49 o -1 3 1 886.42 847.14 5.19 o 0 3 1 2464.75 2371.51 30.36 o 1 3 1 935.92 907.48 11.59 o 2 3 1 4575.87 4416.55 19.02 o 3 3 1 3881.29 3626.48 19.04 o 4 3 1 6541.33 6195.07 28.48 o 5 3 1 1002.42 986.52 12.26 o 6 3 1 1448.44 1426.44 15.95 o 7 3 1 191.32 199.76 3.61 o 8 3 1 23.01 27.75 2.76 o 9 3 1 70.77 79.21 3.43 o 10 3 1 94.48 90.58 4.03 o -10 4 1 77.99 72.12 3.97 o -9 4 1 53.73 56.80 3.14 o -8 4 1 217.68 231.13 4.94 o -7 4 1 313.75 315.78 5.53 o -6 4 1 493.71 458.39 7.03 o -5 4 1 1981.34 1908.52 17.29 o -4 4 1 1064.78 1065.25 11.89 o -3 4 1 2343.18 2109.88 15.09 o -2 4 1 2783.63 2692.36 15.65 o -1 4 1 886.20 874.17 18.62 o 0 4 1 7753.37 8274.15 166.83 o 1 4 1 975.23 977.67 16.06 o 2 4 1 2767.56 2593.52 15.37 o 3 4 1 2384.47 2217.99 15.48 o 4 4 1 1054.21 1063.07 11.86 o 5 4 1 1987.12 1932.06 17.50 o 6 4 1 483.84 458.76 7.17 o 7 4 1 309.50 315.96 6.74 o 8 4 1 226.94 239.47 4.95 o 9 4 1 53.96 47.54 3.20 o 10 4 1 76.11 81.02 3.95 o -10 5 1 24.97 25.96 3.58 o -9 5 1 437.12 452.94 9.60 o -8 5 1 190.93 207.42 4.35 o -7 5 1 803.28 830.96 14.44 o -6 5 1 152.23 154.65 3.01 o -5 5 1 361.61 392.99 6.31 o -4 5 1 278.03 293.68 5.28 o -3 5 1 1444.36 1570.97 13.90 o -2 5 1 1081.10 1115.45 10.83 o -1 5 1 10325.03 10609.38 161.70 o 0 5 1 741.14 672.70 6.81 o 1 5 1 10234.93 10325.43 469.63 o 2 5 1 1086.47 1076.55 10.73 o 3 5 1 1456.12 1555.79 13.72 o 4 5 1 287.45 300.47 5.36 o 5 5 1 363.84 372.77 6.14 o 6 5 1 150.03 157.41 3.02 o 7 5 1 817.37 808.26 14.32 o 8 5 1 183.47 197.23 4.29 o 9 5 1 437.46 458.08 9.48 o 10 5 1 24.93 19.95 3.70 o -9 6 1 20.14 19.16 3.58 o -8 6 1 277.60 276.42 5.50 o -7 6 1 187.84 198.92 4.06 o -6 6 1 292.91 276.84 5.28 o -5 6 1 1729.56 1696.38 17.79 o -4 6 1 399.51 438.34 6.44 o -3 6 1 2489.69 2463.52 18.62 o -2 6 1 1111.57 1019.90 11.40 o -1 6 1 788.21 764.28 14.10 o 0 6 1 2470.00 2371.90 11.52 o 1 6 1 780.02 759.09 9.45 o 2 6 1 1143.86 1096.98 11.74 o 3 6 1 2485.69 2423.66 18.50 o 4 6 1 400.88 439.51 6.35 o 5 6 1 1753.22 1738.59 17.98 o 6 6 1 295.72 280.28 6.50 o 7 6 1 189.44 195.13 4.59 o 8 6 1 274.81 265.06 5.54 o 9 6 1 19.82 21.97 3.56 o -9 7 1 47.01 46.36 3.90 o -8 7 1 16.02 3.84 7.63 o -7 7 1 217.10 209.46 4.39 o -6 7 1 856.87 844.63 14.59 o -5 7 1 320.64 360.70 6.84 o -4 7 1 1905.95 1910.28 18.60 o -3 7 1 1002.68 999.27 12.75 o -2 7 1 1216.53 1173.70 13.08 o -1 7 1 1295.06 1282.52 9.39 o 0 7 1 287.92 272.88 3.45 o 1 7 1 1265.13 1247.63 9.26 o 2 7 1 1240.65 1209.71 13.25 o 3 7 1 1012.53 1002.37 12.74 o 4 7 1 1896.19 1909.33 18.48 o 5 7 1 325.31 356.58 6.88 o 6 7 1 860.50 861.44 14.72 o 7 7 1 224.84 218.64 4.37 o 8 7 1 14.86 21.24 3.01 o 9 7 1 46.19 43.52 3.91 o -9 8 1 30.82 35.36 3.77 o -8 8 1 375.63 399.52 7.50 o -7 8 1 100.04 97.49 3.45 o -6 8 1 312.80 329.04 6.22 o -5 8 1 70.90 74.93 2.90 o -4 8 1 23.70 25.15 2.35 o -3 8 1 252.98 242.46 4.62 o -2 8 1 1574.43 1515.68 16.06 o -1 8 1 595.22 570.62 7.64 o 0 8 1 2845.27 2636.84 14.35 o 1 8 1 618.11 598.96 7.26 o 2 8 1 1593.51 1553.10 16.13 o 3 8 1 246.68 237.61 4.55 o 4 8 1 24.95 24.91 2.41 o 5 8 1 73.77 82.46 2.91 o 6 8 1 307.21 322.21 6.22 o 7 8 1 99.33 93.14 3.41 o 8 8 1 383.64 385.14 7.55 o 9 8 1 30.78 37.13 3.77 o -8 9 1 25.73 33.36 3.61 o -7 9 1 108.55 109.96 3.61 o -6 9 1 286.12 291.00 5.36 o -5 9 1 96.74 84.07 3.05 o -4 9 1 757.95 734.65 13.58 o -3 9 1 274.52 250.29 4.92 o -2 9 1 443.82 429.83 7.13 o -1 9 1 647.74 655.20 16.31 o 0 9 1 362.49 334.31 4.37 o 1 9 1 627.01 635.40 8.00 o 2 9 1 452.07 435.07 7.08 o 3 9 1 272.51 237.91 4.92 o 4 9 1 761.62 765.86 13.54 o 5 9 1 108.23 99.08 3.10 o 6 9 1 284.51 278.59 5.40 o 7 9 1 107.38 112.83 3.58 o 8 9 1 25.21 5.44 8.28 o -8 10 1 1.82 -3.46 7.74 o -7 10 1 73.28 66.62 3.91 o -6 10 1 46.04 46.84 3.09 o -5 10 1 535.57 539.10 9.49 o -4 10 1 122.61 122.00 3.26 o -3 10 1 940.79 916.71 14.94 o -2 10 1 154.03 148.51 3.21 o -1 10 1 137.10 123.66 2.11 o 0 10 1 67.08 51.30 1.82 o 1 10 1 130.03 119.66 2.06 o 2 10 1 162.99 175.38 3.56 o 3 10 1 942.31 931.89 15.08 o 4 10 1 120.15 115.08 3.31 o 5 10 1 531.61 535.19 9.36 o 6 10 1 45.27 49.84 3.11 o 7 10 1 73.57 65.93 3.89 o 8 10 1 2.02 -4.33 7.75 o -7 11 1 145.20 153.45 4.78 o -6 11 1 93.12 90.50 3.67 o -5 11 1 35.15 35.76 3.07 o -4 11 1 90.15 87.96 3.28 o -3 11 1 95.40 92.17 3.11 o -2 11 1 118.26 112.72 3.16 o -1 11 1 335.94 321.73 4.58 o 0 11 1 265.83 254.76 3.83 o 1 11 1 344.19 335.19 5.30 o 2 11 1 117.67 117.33 3.11 o 3 11 1 94.40 82.23 3.14 o 4 11 1 92.91 85.08 3.30 o 5 11 1 32.65 35.13 3.06 o 6 11 1 92.35 85.79 3.62 o 7 11 1 145.31 145.95 4.71 o -6 12 1 93.88 97.05 4.41 o -5 12 1 29.33 30.03 3.53 o -4 12 1 48.34 45.65 3.15 o -3 12 1 47.02 48.38 2.97 o -2 12 1 261.03 238.10 5.09 o -1 12 1 143.02 133.98 2.47 o 0 12 1 540.36 489.16 6.36 o 1 12 1 139.44 125.74 2.44 o 2 12 1 259.70 248.11 5.02 o 3 12 1 45.23 43.46 3.04 o 4 12 1 44.91 47.14 3.11 o 5 12 1 28.77 30.13 3.52 o 6 12 1 92.42 97.26 4.47 o -5 13 1 67.12 67.98 4.18 o -4 13 1 231.95 228.73 5.03 o -3 13 1 34.33 35.77 3.07 o -2 13 1 154.47 149.68 3.90 o -1 13 1 30.57 25.13 2.13 o 0 13 1 3.81 1.69 3.81 o 1 13 1 29.20 26.78 2.15 o 2 13 1 156.05 148.90 3.85 o 3 13 1 31.04 26.68 3.07 o 4 13 1 232.54 225.71 5.12 o 5 13 1 65.77 80.64 4.09 o -4 14 1 9.70 4.37 8.82 o -3 14 1 92.35 82.97 4.34 o -2 14 1 140.51 128.66 4.61 o -1 14 1 31.96 32.31 2.54 o 0 14 1 202.76 187.19 3.34 o 1 14 1 32.37 33.27 4.36 o 2 14 1 137.18 129.12 4.43 o 3 14 1 91.68 85.64 4.27 o 4 14 1 9.58 16.97 3.68 o -1 15 1 143.58 144.35 3.41 o 0 15 1 25.42 25.42 3.09 o 1 15 1 142.90 152.96 4.05 o 0 0 2 13843.55 11393.38 92.87 o 1 0 2 18016.94 16080.99 683.52 o 2 0 2 11712.06 12486.44 118.84 o 3 0 2 1152.03 1215.11 9.84 o 4 0 2 22.27 18.46 1.45 o 5 0 2 1404.02 1496.44 14.16 o 6 0 2 696.58 700.44 10.99 o 7 0 2 595.30 602.45 11.82 o 8 0 2 851.24 815.53 14.69 o 9 0 2 646.45 595.41 7.09 o 10 0 2 119.58 114.93 2.89 o -10 1 2 70.16 72.47 3.49 o -9 1 2 114.27 119.20 2.57 o -8 1 2 457.30 463.50 8.33 o -7 1 2 754.06 749.30 12.85 o -6 1 2 757.05 802.46 11.80 o -5 1 2 1982.26 1973.41 16.36 o -4 1 2 2322.88 2331.86 15.84 o -3 1 2 5868.11 5851.40 23.34 o -2 1 2 669.05 633.03 6.35 o -1 1 2 5922.45 6050.82 33.16 o 0 1 2 4677.12 5123.33 134.70 o 1 1 2 6099.63 6687.79 117.39 o 2 1 2 797.63 762.34 6.95 o 3 1 2 6051.67 6166.96 24.03 o 4 1 2 2371.54 2380.29 16.08 o 5 1 2 2031.56 2007.97 16.49 o 6 1 2 735.95 759.88 11.67 o 7 1 2 783.13 794.94 13.20 o 8 1 2 468.07 444.30 8.19 o 9 1 2 115.48 113.29 3.66 o 10 1 2 71.27 76.27 5.09 o -10 2 2 60.61 49.95 3.80 o -9 2 2 49.87 43.83 3.08 o -8 2 2 116.19 121.06 3.24 o -7 2 2 409.12 432.58 7.35 o -6 2 2 1527.45 1473.28 15.87 o -5 2 2 2504.93 2656.63 19.37 o -4 2 2 4763.22 4558.38 23.40 o -3 2 2 5801.04 5447.48 23.26 o -2 2 2 4053.08 3822.21 16.79 o -1 2 2 3563.72 3724.20 14.68 o 0 2 2 1176.48 1201.73 7.55 o 1 2 2 3735.98 3875.21 15.06 o 9 2 2 51.29 34.64 3.07 o 10 2 2 60.76 59.61 3.73 o -10 3 2 104.62 94.03 4.17 o -9 3 2 281.29 296.60 5.64 o -8 3 2 872.23 888.88 15.67 o -7 3 2 461.62 462.50 7.84 o -6 3 2 325.66 315.66 6.09 o -5 3 2 252.98 259.80 5.07 o -4 3 2 118.80 127.83 2.56 o -3 3 2 1231.95 1261.32 11.14 o -2 3 2 3164.26 3304.04 16.42 o -1 3 2 2038.70 2051.24 11.71 o 0 3 2 7177.81 7991.09 24.60 o 1 3 2 1993.86 2031.47 11.63 o 8 3 2 870.57 910.86 15.78 o 9 3 2 283.99 290.66 5.61 o 10 3 2 105.68 95.55 4.19 o -10 4 2 94.43 92.83 4.17 o -9 4 2 229.05 240.90 4.86 o -8 4 2 384.42 377.86 8.11 o -7 4 2 336.70 335.70 7.00 o -6 4 2 427.62 422.31 6.85 o -5 4 2 1198.01 1261.14 14.23 o -4 4 2 1059.43 1137.21 12.28 o -3 4 2 2577.30 2552.16 16.80 o -2 4 2 364.35 318.05 5.82 o -1 4 2 4489.91 4609.12 20.17 o 0 4 2 398.91 434.40 6.02 o 1 4 2 4531.73 4731.08 20.37 o 8 4 2 378.67 369.10 8.21 o 9 4 2 228.25 242.86 4.89 o 10 4 2 94.92 88.61 4.20 o -10 5 2 52.90 49.58 3.92 o -9 5 2 19.78 28.53 3.11 o -8 5 2 4.23 -0.66 6.87 o -7 5 2 95.83 103.13 3.05 o -6 5 2 566.89 536.80 7.95 o -5 5 2 1579.26 1577.51 16.44 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234.83 250.85 4.87 o 9 7 2 161.37 156.75 4.67 o -9 8 2 5.61 8.04 3.54 o -8 8 2 7.88 12.95 3.03 o -7 8 2 114.33 117.75 3.59 o -6 8 2 448.14 421.63 8.32 o -5 8 2 897.26 897.27 14.78 o -4 8 2 1000.31 999.45 14.48 o -3 8 2 1127.70 1094.84 14.37 o -2 8 2 738.70 736.00 11.59 o -1 8 2 607.60 595.46 10.45 o 0 8 2 78.06 83.51 2.34 o 1 8 2 595.53 581.50 10.25 o 6 8 2 462.80 448.86 8.42 o 7 8 2 111.11 112.13 3.62 o 8 8 2 7.94 4.89 7.52 o 9 8 2 5.48 7.58 3.54 o -8 9 2 65.98 61.68 4.03 o -7 9 2 67.68 72.49 3.36 o -6 9 2 264.17 255.97 5.21 o -5 9 2 430.94 455.04 8.39 o -4 9 2 372.81 352.92 7.15 o -3 9 2 644.65 600.50 11.87 o -2 9 2 440.99 414.86 7.06 o -1 9 2 624.46 589.04 11.18 o 0 9 2 760.57 762.54 12.31 o 1 9 2 626.97 616.16 11.50 o 5 9 2 424.43 442.83 8.49 o 6 9 2 265.18 256.34 5.21 o 7 9 2 71.36 70.00 3.34 o 8 9 2 67.35 70.22 3.99 o -8 10 2 81.49 87.95 4.32 o -7 10 2 164.54 164.35 4.68 o -6 10 2 52.32 56.72 3.19 o -5 10 2 49.26 51.68 3.10 o -4 10 2 74.26 81.47 3.13 o -3 10 2 37.38 32.93 2.65 o 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