#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2009326.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2009326_Fobs loop_ _publ_author_name 'Faber, A.' 'Lemke, A.' 'Spangenberg, B.' 'Bolte, M.' _publ_section_title ; Three hydrohalogenides of organic nitrogen bases ; _journal_issue 12 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first IUC9900156 _journal_volume 55 _journal_year 1999 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 110.632 _cell_angle_gamma 90.000 _cell_length_a 7.8759 _cell_length_b 13.4002 _cell_length_c 7.2779 _exptl_crystal_F_000 272.00 _reflns_d_resolution_high 0.8005 _[local]_cod_data_source_file qb0137Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' he35 in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 165.78 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x, -y, z+1/2' 'x+1/2, y+1/2, z' 'x+1/2, -y+1/2, z+1/2' '-x, -y, -z' '-x, y, -z-1/2' '-x+1/2, -y+1/2, -z' '-x+1/2, y+1/2, -z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 6720.43 6249.47 166.92 o 4 0 0 1326.70 1312.87 22.42 o 6 0 0 2266.20 2440.41 56.23 o 8 0 0 493.65 576.55 17.63 o 1 1 0 3833.18 3429.22 61.02 o 3 1 0 1501.98 1496.31 18.45 o 5 1 0 0.31 0.72 0.94 o 7 1 0 120.62 128.37 3.57 o 9 1 0 46.26 43.68 3.61 o 0 2 0 458.05 406.66 22.06 o 2 2 0 3296.02 3202.98 37.98 o 4 2 0 1445.77 1513.33 18.76 o 6 2 0 0.07 0.57 1.15 o 8 2 0 20.59 21.16 2.18 o 1 3 0 2248.30 2338.39 30.30 o 3 3 0 1.16 7.83 0.90 o 5 3 0 338.92 325.00 5.18 o 7 3 0 371.41 446.40 10.27 o 9 3 0 19.67 15.64 3.54 o 0 4 0 567.86 551.56 12.34 o 2 4 0 1078.39 1046.01 13.01 o 4 4 0 870.10 953.02 12.27 o 6 4 0 58.16 56.27 1.95 o 8 4 0 57.92 60.58 3.21 o 1 5 0 1910.50 1995.44 24.05 o 3 5 0 1005.20 1037.27 13.23 o 5 5 0 375.76 384.06 6.59 o 7 5 0 198.18 183.94 5.32 o 0 6 0 36.66 61.82 2.29 o 2 6 0 604.77 532.22 7.14 o 4 6 0 416.97 401.00 6.38 o 6 6 0 76.88 88.91 3.00 o 8 6 0 26.67 34.84 2.61 o 1 7 0 1300.67 1344.09 16.60 o 3 7 0 4.37 7.06 1.13 o 5 7 0 80.40 74.11 2.32 o 7 7 0 162.87 158.91 4.08 o 0 8 0 1587.12 1619.81 28.10 o 2 8 0 60.44 61.91 1.82 o 4 8 0 0.19 0.72 1.41 o 6 8 0 257.10 259.09 5.59 o 8 8 0 62.97 55.66 3.95 o 1 9 0 914.14 935.50 13.58 o 3 9 0 2519.07 2545.49 36.03 o 5 9 0 560.80 616.27 13.10 o 7 9 0 49.04 51.95 4.11 o 0 10 0 41.93 44.83 2.52 o 2 10 0 191.81 184.65 3.68 o 4 10 0 303.11 314.96 7.49 o 6 10 0 18.31 16.11 1.88 o 1 11 0 352.84 364.11 6.93 o 3 11 0 4.48 2.88 1.26 o 5 11 0 63.78 69.65 4.84 o 0 12 0 34.81 40.55 2.57 o 2 12 0 251.74 275.89 5.24 o 4 12 0 276.06 263.85 5.73 o 6 12 0 11.20 9.12 2.89 o 1 13 0 52.31 35.52 1.82 o 3 13 0 0.22 1.48 1.72 o 5 13 0 17.74 20.26 2.60 o 0 14 0 249.65 235.29 7.32 o 2 14 0 151.34 151.99 3.61 o 4 14 0 110.46 107.91 4.75 o 1 15 0 39.99 39.19 2.34 o 3 15 0 20.26 15.71 2.56 o 0 16 0 5.73 1.50 2.46 o 2 16 0 20.01 19.66 3.74 o -9 1 1 70.16 75.80 2.87 o -7 1 1 184.03 208.05 5.85 o -5 1 1 438.79 400.60 6.09 o -3 1 1 890.99 809.01 17.40 o -1 1 1 1213.12 1208.02 24.68 o 1 1 1 1083.99 1070.71 15.23 o 3 1 1 756.06 678.60 15.05 o 5 1 1 362.22 360.47 7.40 o 7 1 1 154.08 172.82 6.36 o -8 2 1 118.85 140.58 3.87 o -6 2 1 342.53 353.26 6.97 o -4 2 1 892.44 893.18 11.40 o -2 2 1 1780.24 1713.50 23.63 o 0 2 1 2378.72 2682.22 36.27 o 2 2 1 1612.35 1679.06 26.56 o 4 2 1 639.20 619.48 8.40 o 6 2 1 241.05 261.34 7.66 o 8 2 1 90.16 92.29 5.57 o -9 3 1 0.02 -1.08 2.48 o -7 3 1 0.03 1.42 1.65 o -5 3 1 0.02 -0.15 1.08 o -3 3 1 40.46 36.40 1.38 o -1 3 1 417.64 390.77 6.30 o 1 3 1 200.33 197.63 3.52 o 3 3 1 2.46 1.89 0.81 o 5 3 1 0.28 1.02 1.04 o 7 3 1 0.28 -1.15 1.87 o -8 4 1 156.78 169.94 6.56 o -6 4 1 386.04 441.94 9.11 o -4 4 1 981.63 955.86 13.41 o -2 4 1 2664.10 2578.33 32.85 o 0 4 1 3452.49 3537.29 43.27 o 2 4 1 1840.14 1772.26 22.17 o 4 4 1 724.89 755.23 9.79 o 6 4 1 319.13 334.92 7.22 o 8 4 1 120.50 134.08 7.51 o -9 5 1 48.05 43.94 7.50 o -7 5 1 181.46 198.76 4.52 o -5 5 1 447.53 437.10 9.45 o -3 5 1 924.36 911.44 12.36 o -1 5 1 2177.54 2305.87 30.07 o 1 5 1 1580.19 1579.17 21.92 o 3 5 1 791.74 761.46 10.16 o 5 5 1 339.79 342.02 5.97 o 7 5 1 117.31 120.30 6.45 o -8 6 1 15.50 11.77 2.01 o -6 6 1 57.14 52.06 2.33 o -4 6 1 108.99 103.71 2.64 o -2 6 1 382.63 378.07 5.66 o 0 6 1 645.09 750.94 10.01 o 2 6 1 203.79 195.14 3.60 o 4 6 1 101.06 105.07 2.98 o 6 6 1 39.79 37.56 2.12 o 8 6 1 4.42 2.97 2.20 o -7 7 1 119.63 114.26 3.34 o -5 7 1 356.26 365.29 8.04 o -3 7 1 749.01 728.14 10.53 o -1 7 1 653.41 650.21 8.55 o 1 7 1 919.02 1022.07 17.90 o 3 7 1 612.22 594.54 8.41 o 5 7 1 228.86 224.12 5.05 o 7 7 1 113.40 107.70 3.68 o -8 8 1 47.38 48.98 3.57 o -6 8 1 88.78 97.85 2.80 o -4 8 1 56.77 56.80 2.05 o -2 8 1 217.94 220.06 3.87 o 0 8 1 321.60 317.44 4.90 o 2 8 1 80.03 82.41 2.10 o 4 8 1 106.61 118.82 3.04 o 6 8 1 100.48 108.76 3.97 o -7 9 1 19.17 12.62 1.93 o -5 9 1 0.25 0.59 1.31 o -3 9 1 0.60 -0.07 1.12 o -1 9 1 103.58 111.76 2.56 o 1 9 1 18.20 19.23 1.30 o 3 9 1 0.99 0.75 1.25 o 5 9 1 22.80 21.08 2.33 o 7 9 1 9.60 5.28 2.79 o -6 10 1 116.26 117.17 3.12 o -4 10 1 404.65 415.77 7.32 o -2 10 1 267.97 263.57 4.92 o 0 10 1 222.22 239.72 5.59 o 2 10 1 489.96 520.81 8.09 o 4 10 1 250.99 281.27 6.94 o 6 10 1 65.05 71.81 3.06 o -7 11 1 69.75 67.14 4.50 o -5 11 1 56.24 58.75 2.39 o -3 11 1 116.93 114.04 3.12 o -1 11 1 339.55 333.07 6.67 o 1 11 1 205.06 200.26 3.73 o 3 11 1 64.19 62.80 2.29 o 5 11 1 109.74 117.79 4.02 o -6 12 1 13.42 9.43 2.27 o -4 12 1 0.95 2.10 1.54 o -2 12 1 27.82 27.04 2.07 o 0 12 1 42.23 36.63 1.86 o 2 12 1 2.21 1.86 1.40 o 4 12 1 9.46 8.73 1.94 o -5 13 1 168.08 156.02 5.89 o -3 13 1 289.18 279.27 5.71 o -1 13 1 276.59 275.19 5.58 o 1 13 1 323.95 321.56 6.39 o 3 13 1 279.22 275.84 7.69 o 5 13 1 96.22 98.02 4.98 o -4 14 1 30.16 26.79 2.02 o -2 14 1 56.09 57.36 2.83 o 0 14 1 66.99 66.35 2.55 o 2 14 1 40.29 39.80 2.19 o 4 14 1 32.14 32.90 3.51 o -3 15 1 59.33 55.63 2.61 o -1 15 1 69.83 60.85 2.53 o 1 15 1 68.68 64.03 2.94 o 3 15 1 55.61 54.83 4.67 o -2 16 1 56.84 60.88 3.72 o 0 16 1 69.74 67.21 3.86 o 2 16 1 35.91 28.97 5.32 o -8 0 2 1106.49 1165.03 27.82 o -6 0 2 794.50 820.21 19.94 o -4 0 2 1129.74 1075.28 20.09 o -2 0 2 27483.84 24911.33 409.98 o 0 0 2 12501.20 11618.50 227.88 o 2 0 2 1254.81 1233.17 23.72 o 4 0 2 2747.90 2620.29 52.53 o 6 0 2 1277.66 1367.70 34.96 o -9 1 2 27.57 24.55 2.41 o -7 1 2 29.48 33.58 1.95 o -5 1 2 526.40 546.67 9.67 o -3 1 2 90.01 103.68 2.43 o -1 1 2 5452.55 5228.69 65.24 o 1 1 2 1243.75 1262.94 16.43 o 3 1 2 109.90 107.62 2.09 o 5 1 2 219.26 215.82 5.34 o 7 1 2 19.72 19.52 2.82 o -8 2 2 6.00 4.93 1.67 o -6 2 2 338.59 379.55 7.51 o -4 2 2 1671.31 1601.85 21.58 o -2 2 2 137.36 143.81 2.60 o 0 2 2 991.70 941.57 14.09 o 2 2 2 2757.32 2989.40 77.29 o 4 2 2 31.16 29.31 1.28 o 6 2 2 2.13 1.33 1.58 o 8 2 2 135.55 158.23 8.35 o -9 3 2 121.80 131.95 4.66 o -7 3 2 276.38 283.10 6.67 o -5 3 2 4.98 1.68 1.05 o -3 3 2 584.67 514.46 8.17 o -1 3 2 2524.79 2604.16 42.00 o 1 3 2 9.69 4.64 0.91 o 3 3 2 175.32 130.75 2.53 o 5 3 2 630.63 653.41 11.04 o 7 3 2 72.81 70.81 6.65 o -8 4 2 24.83 27.04 1.96 o -6 4 2 266.77 279.10 7.61 o -4 4 2 793.36 790.56 11.49 o -2 4 2 503.80 486.58 10.67 o 0 4 2 745.23 763.16 9.86 o 2 4 2 1327.03 1447.03 17.97 o 4 4 2 133.65 130.45 3.15 o 6 4 2 71.82 68.18 2.63 o -9 5 2 93.00 97.42 6.07 o -7 5 2 170.23 178.20 4.00 o -5 5 2 519.88 506.72 7.91 o -3 5 2 904.83 858.41 11.66 o -1 5 2 1877.98 1867.87 23.74 o 1 5 2 966.76 1052.07 13.34 o 3 5 2 608.31 664.23 9.81 o 5 5 2 275.29 251.59 5.16 o 7 5 2 132.55 120.67 9.83 o -8 6 2 17.38 15.59 1.75 o -6 6 2 189.95 185.63 3.79 o -4 6 2 447.96 398.32 6.44 o -2 6 2 3.06 1.72 0.84 o 0 6 2 298.59 276.09 4.23 o 2 6 2 548.78 514.89 7.56 o 4 6 2 171.67 190.20 3.94 o 6 6 2 32.03 38.05 2.07 o -7 7 2 78.86 82.40 2.76 o -5 7 2 0.78 0.93 1.13 o -3 7 2 328.39 338.61 6.09 o -1 7 2 1511.49 1608.62 19.97 o 1 7 2 24.16 30.21 1.36 o 3 7 2 45.27 38.60 1.73 o 5 7 2 243.03 220.00 5.07 o 7 7 2 22.21 10.92 2.61 o -8 8 2 152.10 152.99 4.47 o -6 8 2 10.41 7.70 1.44 o -4 8 2 1.40 2.16 1.16 o -2 8 2 1034.51 1095.19 21.08 o 0 8 2 281.60 304.49 5.90 o 2 8 2 7.20 5.96 1.16 o 4 8 2 229.78 234.08 5.02 o 6 8 2 177.85 157.46 4.58 o -7 9 2 152.92 159.82 5.21 o -5 9 2 1426.67 1430.56 21.10 o -3 9 2 927.03 927.10 15.43 o -1 9 2 480.65 510.38 8.71 o 1 9 2 2365.09 2448.39 31.94 o 3 9 2 1157.17 1205.45 26.66 o 5 9 2 78.08 86.10 3.09 o -6 10 2 84.37 79.19 2.58 o -4 10 2 271.40 276.20 5.58 o -2 10 2 16.95 18.66 1.39 o 0 10 2 47.30 47.53 1.62 o 2 10 2 492.52 515.20 8.63 o 4 10 2 1.14 2.17 1.46 o 6 10 2 6.00 3.16 2.78 o -7 11 2 69.96 66.22 3.11 o -5 11 2 6.62 6.27 1.56 o -3 11 2 120.64 110.71 3.09 o -1 11 2 414.39 433.78 9.25 o 1 11 2 0.96 1.13 1.21 o 3 11 2 17.41 20.65 1.77 o 5 11 2 185.36 210.14 7.23 o -6 12 2 104.29 94.70 3.11 o -4 12 2 252.15 248.14 5.22 o -2 12 2 30.88 32.10 1.87 o 0 12 2 137.89 147.57 3.62 o 2 12 2 385.50 399.72 7.66 o 4 12 2 31.31 28.29 2.23 o -5 13 2 0.10 0.24 1.54 o -3 13 2 21.36 17.73 1.75 o -1 13 2 68.72 54.85 2.55 o 1 13 2 0.32 1.44 1.61 o 3 13 2 7.60 8.22 1.81 o -4 14 2 91.55 81.57 3.99 o -2 14 2 196.08 184.54 4.33 o 0 14 2 166.84 161.84 4.62 o 2 14 2 112.14 114.53 3.95 o -3 15 2 27.26 22.27 2.29 o -1 15 2 34.35 38.27 2.49 o 1 15 2 24.95 21.16 3.19 o -2 16 2 5.17 5.26 3.46 o 0 16 2 13.44 13.12 5.25 o -9 1 3 63.85 67.39 2.75 o -7 1 3 153.86 162.39 4.08 o -5 1 3 345.06 323.21 6.70 o -3 1 3 718.51 694.52 9.39 o -1 1 3 847.56 809.38 13.93 o 1 1 3 654.81 628.62 8.66 o 3 1 3 413.15 407.63 7.75 o 5 1 3 216.16 199.39 5.14 o 7 1 3 84.21 81.36 4.93 o -8 2 3 129.22 139.29 3.83 o -6 2 3 328.78 345.57 6.64 o -4 2 3 591.34 610.68 9.58 o -2 2 3 889.76 887.32 11.84 o 0 2 3 1075.54 1092.67 15.42 o 2 2 3 697.11 680.80 10.07 o 4 2 3 314.41 305.85 7.37 o 6 2 3 132.19 122.13 5.39 o -9 3 3 0.04 0.27 2.09 o -7 3 3 0.29 -0.25 1.42 o -5 3 3 0.76 1.94 1.15 o -3 3 3 41.39 35.96 1.42 o -1 3 3 55.72 50.78 1.43 o 1 3 3 4.03 2.33 0.94 o 3 3 3 0.25 0.78 1.04 o 5 3 3 0.38 1.39 1.43 o 7 3 3 0.14 -0.24 3.04 o -8 4 3 132.15 143.91 3.94 o -6 4 3 340.61 344.75 7.77 o -4 4 3 883.30 824.48 11.95 o -2 4 3 1445.92 1408.24 17.46 o 0 4 3 1402.03 1453.11 19.61 o 2 4 3 764.76 775.80 11.61 o 4 4 3 407.74 388.08 8.05 o 6 4 3 186.18 168.23 4.97 o -9 5 3 60.17 56.51 4.34 o -7 5 3 172.42 173.79 4.01 o -5 5 3 328.30 300.44 5.18 o -3 5 3 692.55 648.06 9.41 o -1 5 3 905.10 880.31 11.15 o 1 5 3 690.34 695.68 14.67 o 3 5 3 392.08 386.64 6.48 o 5 5 3 172.63 177.97 6.90 o 7 5 3 58.05 60.55 5.19 o -8 6 3 21.55 17.56 1.79 o -6 6 3 37.36 38.35 1.98 o -4 6 3 92.74 82.96 2.39 o -2 6 3 304.14 309.58 4.80 o 0 6 3 163.73 169.39 3.45 o 2 6 3 100.81 106.58 2.65 o 4 6 3 54.72 53.89 2.02 o 6 6 3 11.12 5.11 1.90 o -7 7 3 134.53 125.44 3.24 o -5 7 3 360.23 332.38 5.68 o -3 7 3 344.32 322.98 5.45 o -1 7 3 468.27 482.40 7.84 o 1 7 3 584.54 636.77 17.11 o 3 7 3 288.53 281.58 5.25 o 5 7 3 134.94 142.24 4.03 o -8 8 3 43.98 45.43 3.91 o -6 8 3 28.43 26.87 1.61 o -4 8 3 80.32 80.02 2.28 o -2 8 3 256.37 259.28 4.56 o 0 8 3 95.54 100.04 2.57 o 2 8 3 71.40 75.35 2.33 o 4 8 3 118.39 120.36 3.95 o 6 8 3 40.66 50.08 5.37 o -7 9 3 2.28 0.67 1.58 o -5 9 3 1.25 3.35 1.36 o -3 9 3 33.86 33.17 1.72 o -1 9 3 30.52 28.35 1.52 o 1 9 3 2.15 2.00 1.20 o 3 9 3 10.46 9.29 1.41 o 5 9 3 19.08 13.37 1.89 o -6 10 3 184.86 188.46 6.79 o -4 10 3 213.32 220.61 5.49 o -2 10 3 140.41 146.80 3.80 o 0 10 3 333.38 359.94 7.17 o 2 10 3 321.49 359.59 6.49 o 4 10 3 83.46 82.33 3.05 o -7 11 3 34.63 37.14 3.20 o -5 11 3 40.68 40.90 2.06 o -3 11 3 195.90 198.91 4.28 o -1 11 3 210.62 223.13 5.06 o 1 11 3 59.01 64.18 2.28 o 3 11 3 96.88 101.13 3.10 o 5 11 3 71.31 74.87 4.66 o -6 12 3 1.00 1.49 1.87 o -4 12 3 10.05 8.44 1.63 o -2 12 3 40.95 42.72 2.35 o 0 12 3 6.96 6.70 1.66 o 2 12 3 2.85 4.74 1.61 o 4 12 3 25.28 23.91 2.82 o -5 13 3 154.98 163.34 4.64 o -3 13 3 175.14 167.93 4.43 o -1 13 3 220.84 220.62 6.08 o 1 13 3 269.42 275.71 5.83 o 3 13 3 126.47 133.67 5.00 o -4 14 3 29.82 29.44 2.53 o -2 14 3 48.10 41.99 4.07 o 0 14 3 35.93 38.47 2.38 o 2 14 3 29.62 27.45 3.70 o -3 15 3 44.82 35.14 5.75 o -1 15 3 51.52 51.29 8.60 o 1 15 3 52.42 52.91 6.21 o -8 0 4 399.27 441.80 14.47 o -6 0 4 213.45 198.50 6.42 o -4 0 4 4353.51 4076.92 75.49 o -2 0 4 6425.06 6703.55 111.28 o 0 0 4 633.07 572.37 14.49 o 2 0 4 1751.90 1641.31 38.44 o 4 0 4 1781.40 1619.85 115.20 o 6 0 4 102.67 90.47 5.35 o -9 1 4 46.90 43.71 2.29 o -7 1 4 119.86 122.62 3.45 o -5 1 4 44.19 39.10 1.82 o -3 1 4 1446.62 1475.00 18.92 o -1 1 4 126.05 124.23 2.46 o 1 1 4 299.99 308.30 6.13 o 3 1 4 161.49 147.35 4.29 o 5 1 4 1.38 -0.34 1.48 o -8 2 4 38.21 37.42 2.11 o -6 2 4 586.61 600.89 10.47 o -4 2 4 2.13 0.26 1.01 o -2 2 4 7.51 4.87 0.89 o 0 2 4 1674.43 1688.68 23.35 o 2 2 4 159.88 150.04 4.55 o 4 2 4 3.34 2.28 1.40 o 6 2 4 129.75 123.27 7.56 o -9 3 4 124.07 135.28 4.93 o -7 3 4 11.12 9.57 1.74 o -5 3 4 84.24 73.76 2.26 o -3 3 4 1019.06 928.01 16.17 o -1 3 4 118.95 106.78 2.45 o 1 3 4 30.61 18.02 1.51 o 3 3 4 557.63 564.34 11.05 o 5 3 4 148.41 132.60 3.98 o -8 4 4 57.33 64.22 2.61 o -6 4 4 307.96 316.63 10.78 o -4 4 4 216.17 224.41 4.41 o -2 4 4 313.45 311.88 8.78 o 0 4 4 802.85 892.57 13.51 o 2 4 4 199.47 231.37 7.48 o 4 4 4 55.64 50.03 2.51 o 6 4 4 78.81 76.23 5.67 o -9 5 4 64.22 63.16 4.59 o -7 5 4 169.96 165.41 4.47 o -5 5 4 331.52 322.33 5.84 o -3 5 4 781.82 742.91 12.25 o -1 5 4 563.68 628.13 9.90 o 1 5 4 521.98 564.09 9.05 o 3 5 4 248.37 247.43 5.54 o 5 5 4 171.94 160.08 8.50 o -8 6 4 45.49 44.61 2.48 o -6 6 4 166.09 173.36 3.84 o -4 6 4 36.71 37.34 1.61 o -2 6 4 59.71 57.87 2.28 o 0 6 4 401.41 422.82 7.12 o 2 6 4 182.25 199.70 4.33 o 4 6 4 27.69 35.46 2.10 o 6 6 4 65.09 71.19 8.20 o -7 7 4 0.53 0.21 1.38 o -5 7 4 45.27 43.01 1.75 o -3 7 4 690.59 712.98 11.08 o -1 7 4 66.06 71.78 2.55 o 1 7 4 9.66 6.40 1.24 o 3 7 4 199.31 181.54 6.34 o 5 7 4 64.56 46.07 3.40 o -8 8 4 16.61 11.41 2.20 o -6 8 4 4.62 2.79 1.41 o -4 8 4 308.10 296.78 8.72 o -2 8 4 377.48 407.35 8.43 o 0 8 4 6.53 5.62 1.28 o 2 8 4 87.90 88.90 2.56 o 4 8 4 249.50 235.46 5.77 o -7 9 4 500.89 500.55 10.15 o -5 9 4 617.44 623.85 10.05 o -3 9 4 176.39 169.11 4.48 o -1 9 4 1126.80 1328.26 38.40 o 1 9 4 1300.09 1425.39 20.67 o 3 9 4 114.90 120.66 3.39 o 5 9 4 117.58 153.38 8.23 o -6 10 4 184.25 177.05 4.26 o -4 10 4 0.02 0.02 1.66 o -2 10 4 0.59 0.20 1.50 o 0 10 4 379.47 413.61 7.52 o 2 10 4 17.67 18.31 1.69 o 4 10 4 19.78 16.15 3.09 o -7 11 4 1.69 0.76 2.51 o -5 11 4 10.16 7.22 1.49 o -3 11 4 254.79 249.38 5.94 o -1 11 4 15.52 15.51 1.89 o 1 11 4 0.15 -0.68 1.58 o 3 11 4 166.74 180.12 4.86 o -6 12 4 144.34 135.25 5.03 o -4 12 4 26.23 23.80 2.03 o -2 12 4 39.43 38.29 2.30 o 0 12 4 287.90 293.25 6.45 o 2 12 4 59.43 54.75 2.25 o -5 13 4 3.13 1.37 2.46 o -3 13 4 51.12 44.47 2.71 o -1 13 4 4.04 3.36 1.77 o 1 13 4 0.78 0.89 1.80 o -4 14 4 98.41 83.01 5.26 o -2 14 4 121.23 116.97 11.62 o 0 14 4 80.15 81.58 4.43 o -9 1 5 37.66 37.90 4.27 o -7 1 5 84.43 82.69 2.76 o -5 1 5 184.20 189.62 4.56 o -3 1 5 297.35 293.40 4.89 o -1 1 5 301.48 305.53 7.96 o 1 1 5 239.50 241.55 5.52 o 3 1 5 171.44 163.18 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