#------------------------------------------------------------------------------ #$Date: 2016-04-02 20:34:39 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180772 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/00/93/2009327.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2009327_Fobs loop_ _publ_author_name 'Faber, A.' 'Lemke, A.' 'Spangenberg, B.' 'Bolte, M.' _publ_section_title ; Three hydrohalogenides of organic nitrogen bases ; _journal_issue 12 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first IUC9900156 _journal_volume 55 _journal_year 1999 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 91.230 _cell_angle_gamma 90.000 _cell_length_a 7.3960 _cell_length_b 15.2770 _cell_length_c 12.3360 _exptl_crystal_F_000 544.00 _reflns_d_resolution_high 0.8000 _cod_data_source_file qb0137IIsup3.hkl _cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' he61 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 183.28 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 86.42 100.13 13.39 o 2 0 0 7595.77 7620.94 153.07 o 3 0 0 1473.58 1543.70 45.32 o 4 0 0 20.40 74.41 39.27 o 5 0 0 1195.76 1190.53 59.82 o 6 0 0 737.36 708.09 66.80 o 7 0 0 12.20 -6.60 61.03 o 8 0 0 253.71 329.41 78.75 o 9 0 0 6.89 -59.12 96.57 o 1 1 0 830.62 936.53 22.38 o 2 1 0 5562.87 5841.56 79.64 o 3 1 0 239.49 245.51 15.72 o 4 1 0 104.90 96.74 16.86 o 5 1 0 145.33 143.47 24.66 o 6 1 0 392.58 387.23 36.95 o 7 1 0 248.10 221.32 40.69 o 8 1 0 21.37 78.99 49.06 o 9 1 0 173.48 80.86 56.83 o 0 2 0 102.45 82.91 6.76 o 1 2 0 220.44 190.47 9.22 o 2 2 0 7527.86 7315.31 100.11 o 3 2 0 197.84 214.55 14.37 o 4 2 0 70.43 84.43 19.54 o 5 2 0 14.64 43.27 20.83 o 6 2 0 76.77 118.04 34.74 o 7 2 0 45.61 14.42 35.77 o 8 2 0 0.01 -10.53 46.61 o 9 2 0 0.21 -34.02 55.44 o 1 3 0 504.74 588.98 13.89 o 2 3 0 741.02 822.41 21.52 o 3 3 0 353.28 398.21 16.60 o 4 3 0 82.47 100.99 15.66 o 5 3 0 71.27 35.57 21.63 o 6 3 0 38.96 61.42 30.82 o 7 3 0 50.33 66.08 36.73 o 8 3 0 54.88 51.80 50.17 o 9 3 0 45.97 13.29 56.35 o 0 4 0 6436.89 6303.95 119.75 o 1 4 0 460.71 467.81 17.20 o 2 4 0 396.88 378.49 16.06 o 3 4 0 3229.26 3258.42 52.56 o 4 4 0 362.17 413.56 22.54 o 5 4 0 363.82 360.57 32.35 o 6 4 0 87.99 198.45 43.51 o 7 4 0 53.32 -5.87 37.67 o 8 4 0 337.61 309.96 50.40 o 9 4 0 0.30 27.54 97.30 o 1 5 0 3815.08 3677.75 55.72 o 2 5 0 17.63 21.54 10.65 o 3 5 0 881.17 855.67 25.28 o 4 5 0 745.34 720.22 25.39 o 5 5 0 42.87 44.44 27.17 o 6 5 0 84.05 48.64 32.79 o 7 5 0 540.61 515.11 50.39 o 8 5 0 17.22 65.04 48.47 o 0 6 0 2891.68 3066.99 65.54 o 1 6 0 3096.82 3159.46 47.25 o 2 6 0 232.31 212.76 15.31 o 3 6 0 348.56 314.14 15.30 o 4 6 0 158.87 107.00 19.74 o 5 6 0 503.97 511.31 36.35 o 6 6 0 353.07 345.76 39.89 o 7 6 0 19.40 43.26 43.67 o 8 6 0 0.52 54.39 56.50 o 1 7 0 514.66 466.07 17.95 o 2 7 0 2201.78 2378.85 45.56 o 3 7 0 14.70 48.69 14.89 o 4 7 0 875.96 905.48 34.67 o 5 7 0 699.78 708.83 39.99 o 6 7 0 118.68 216.30 36.05 o 7 7 0 48.72 61.75 46.86 o 8 7 0 116.78 23.39 58.25 o 0 8 0 255.53 233.07 21.58 o 1 8 0 614.65 600.11 21.40 o 2 8 0 7.20 6.21 13.98 o 3 8 0 317.70 338.58 21.35 o 4 8 0 127.96 66.81 32.43 o 5 8 0 3.24 19.50 29.56 o 6 8 0 11.99 67.16 35.93 o 7 8 0 176.19 103.32 50.35 o 8 8 0 73.45 93.68 70.95 o 1 9 0 132.42 172.28 20.85 o 2 9 0 473.46 432.38 24.28 o 3 9 0 431.89 513.37 29.83 o 4 9 0 145.13 158.92 29.57 o 5 9 0 75.67 81.98 33.04 o 6 9 0 468.64 491.40 47.45 o 7 9 0 33.84 74.86 56.87 o 8 9 0 0.00 38.50 72.39 o 0 10 0 179.67 191.94 32.68 o 1 10 0 903.23 913.17 35.53 o 2 10 0 347.25 331.27 24.16 o 3 10 0 137.30 99.27 24.48 o 4 10 0 550.69 539.15 55.69 o 5 10 0 54.05 77.01 38.82 o 6 10 0 131.81 117.09 63.25 o 7 10 0 18.75 6.52 69.98 o 1 11 0 20.11 9.69 20.68 o 2 11 0 0.99 14.50 25.64 o 3 11 0 44.75 82.70 26.84 o 4 11 0 109.28 101.91 33.62 o 5 11 0 419.31 448.33 49.53 o 6 11 0 70.00 22.14 36.57 o 7 11 0 26.29 74.35 59.76 o 0 12 0 711.23 643.17 54.15 o 1 12 0 1143.62 1122.71 42.78 o 2 12 0 855.23 764.11 42.49 o 3 12 0 70.28 97.81 48.06 o 4 12 0 784.86 827.30 52.82 o 5 12 0 89.35 140.60 39.06 o 6 12 0 17.28 70.66 48.85 o 7 12 0 72.45 109.24 81.68 o 1 13 0 196.62 182.64 45.76 o 2 13 0 601.80 630.26 44.28 o 3 13 0 206.81 191.71 48.28 o 4 13 0 145.59 20.23 39.82 o 5 13 0 137.72 140.59 47.48 o 6 13 0 0.57 31.31 46.82 o 0 14 0 728.43 624.69 57.53 o 1 14 0 1.90 -31.77 31.77 o 2 14 0 362.92 348.07 37.36 o 3 14 0 74.82 91.63 37.91 o 4 14 0 124.65 236.34 57.78 o 5 14 0 7.65 36.94 44.02 o 6 14 0 25.39 286.12 58.98 o 1 15 0 28.13 67.92 35.57 o 2 15 0 4.08 -21.91 53.03 o 3 15 0 57.98 -25.05 36.15 o 4 15 0 14.81 18.94 48.12 o 5 15 0 354.50 390.51 62.22 o 0 16 0 1.39 50.32 57.80 o 1 16 0 432.86 321.87 46.04 o 2 16 0 154.45 58.33 38.46 o 3 16 0 2.78 -46.01 46.01 o 4 16 0 611.35 659.97 70.70 o 5 16 0 34.09 69.20 183.22 o 1 17 0 80.22 82.64 49.88 o 2 17 0 88.45 26.70 59.36 o 3 17 0 8.12 128.58 53.98 o 4 17 0 9.82 30.38 111.26 o 0 18 0 29.87 114.98 79.08 o 1 18 0 32.06 73.70 47.82 o 2 18 0 83.57 80.40 64.92 o 3 18 0 0.45 -11.75 112.72 o -9 1 1 42.33 21.49 95.66 o -8 1 1 6.61 19.16 47.19 o -7 1 1 40.91 62.27 35.45 o -6 1 1 24.64 23.26 28.46 o -5 1 1 94.26 89.11 25.04 o -4 1 1 10776.16 11093.90 160.47 o -3 1 1 185.58 216.72 14.25 o -2 1 1 9599.07 9709.21 208.76 o -1 1 1 1645.96 1695.86 34.84 o 0 1 1 217.27 198.55 5.59 o 1 1 1 1583.41 1661.01 25.61 o 2 1 1 9520.67 9483.14 182.85 o 3 1 1 370.02 350.26 19.13 o 4 1 1 207.28 191.21 19.43 o 5 1 1 10.96 51.06 19.78 o 6 1 1 688.10 729.00 46.06 o 7 1 1 29.13 54.27 43.90 o 8 1 1 3.51 -27.62 57.72 o 9 1 1 0.18 -25.00 56.58 o -9 2 1 33.47 -54.79 54.79 o -8 2 1 356.30 246.48 55.46 o -7 2 1 97.66 69.62 38.03 o -6 2 1 39.50 59.97 29.74 o -5 2 1 819.70 823.57 37.48 o -4 2 1 385.32 426.40 22.43 o -3 2 1 2026.32 2035.45 46.45 o -2 2 1 1873.98 1988.05 39.69 o -1 2 1 1703.02 1823.47 28.11 o 0 2 1 5666.30 4585.19 61.93 o 1 2 1 142.04 134.36 11.28 o 2 2 1 15006.40 14645.50 188.52 o 3 2 1 2345.89 2394.05 44.07 o 4 2 1 39.09 31.94 20.23 o 5 2 1 1300.10 1319.81 37.73 o 6 2 1 657.43 629.19 45.69 o 7 2 1 13.27 22.14 37.08 o 8 2 1 141.96 181.14 53.83 o 9 2 1 5.72 -45.72 58.11 o -9 3 1 39.77 37.54 58.62 o -8 3 1 1.04 11.61 89.80 o -7 3 1 187.00 161.75 53.63 o -6 3 1 1352.46 1357.04 57.15 o -5 3 1 451.45 467.27 29.97 o -4 3 1 2801.71 2697.80 49.82 o -3 3 1 136.72 113.94 18.66 o -2 3 1 129.31 159.63 12.47 o -1 3 1 7318.39 7150.13 90.57 o 0 3 1 1156.69 1052.16 21.20 o 1 3 1 1578.95 1578.60 39.88 o 2 3 1 3873.20 4096.11 63.56 o 3 3 1 256.44 306.21 16.89 o 4 3 1 653.50 690.27 25.27 o 5 3 1 3.33 -16.31 27.74 o 6 3 1 406.02 386.39 40.97 o 7 3 1 88.91 45.42 42.51 o 8 3 1 163.35 210.16 56.92 o 9 3 1 25.66 -25.94 78.57 o -9 4 1 6.67 54.71 125.21 o -8 4 1 6.90 -35.80 42.69 o -7 4 1 39.22 -3.09 34.05 o -6 4 1 305.87 344.66 41.48 o -5 4 1 33.37 37.25 36.31 o -4 4 1 1139.24 1163.58 29.17 o -3 4 1 276.37 256.98 13.98 o -2 4 1 0.04 2.73 9.71 o -1 4 1 332.58 343.13 12.10 o 0 4 1 479.51 560.32 16.06 o 1 4 1 53.26 47.31 8.66 o 2 4 1 751.82 758.24 20.04 o 3 4 1 1081.70 1097.98 26.64 o 4 4 1 1856.28 1880.37 46.30 o 5 4 1 163.80 162.85 37.19 o 6 4 1 89.30 148.81 36.37 o 7 4 1 27.76 3.76 36.17 o 8 4 1 93.77 98.14 55.16 o 9 4 1 80.34 265.47 117.50 o -8 5 1 35.74 -17.17 42.28 o -7 5 1 28.96 45.25 37.88 o -6 5 1 28.31 59.49 33.57 o -5 5 1 88.01 91.73 25.28 o -4 5 1 32.88 11.69 15.01 o -3 5 1 562.86 593.33 21.66 o -2 5 1 7.67 13.98 9.67 o -1 5 1 1432.36 1487.02 25.54 o 0 5 1 2713.39 2695.47 48.55 o 1 5 1 11.59 12.21 14.67 o 2 5 1 440.80 505.63 18.88 o 3 5 1 598.69 614.41 22.41 o 4 5 1 1710.86 1819.17 69.39 o 5 5 1 10.20 44.30 32.88 o 6 5 1 463.83 456.88 41.83 o 7 5 1 21.22 3.14 44.41 o 8 5 1 11.35 -30.82 42.54 o -8 6 1 148.71 119.05 53.08 o -7 6 1 85.29 34.16 41.80 o -6 6 1 382.87 333.19 41.89 o -5 6 1 488.16 502.27 36.62 o -4 6 1 0.01 -14.78 16.43 o -3 6 1 1404.15 1488.49 29.65 o -2 6 1 1781.66 1868.38 31.59 o -1 6 1 1152.67 1134.06 24.11 o 0 6 1 3255.39 3419.68 69.01 o 1 6 1 1705.96 1812.30 39.75 o 2 6 1 159.52 170.58 15.26 o 3 6 1 1193.05 1190.78 29.73 o 4 6 1 107.64 83.06 28.58 o 5 6 1 778.38 683.69 35.87 o 6 6 1 100.67 93.05 32.27 o 7 6 1 12.21 32.43 37.21 o 8 6 1 21.25 -56.61 56.61 o -8 7 1 7.54 18.54 105.20 o -7 7 1 229.99 282.40 55.36 o -6 7 1 31.52 -26.74 29.45 o -5 7 1 271.60 235.74 29.57 o -4 7 1 883.79 936.34 36.22 o -3 7 1 190.15 183.74 15.55 o -2 7 1 384.90 372.31 17.05 o -1 7 1 2349.01 2260.18 38.64 o 0 7 1 30.00 39.74 13.56 o 1 7 1 1259.14 1282.15 33.63 o 2 7 1 414.39 397.51 16.18 o 3 7 1 229.68 228.16 22.24 o 4 7 1 275.46 320.09 27.20 o 5 7 1 16.23 -1.53 30.67 o 6 7 1 59.24 58.40 32.51 o 7 7 1 2.89 37.96 54.01 o 8 7 1 11.35 64.46 85.89 o -8 8 1 23.08 16.26 52.65 o -7 8 1 59.84 -6.74 83.05 o -6 8 1 23.67 48.09 46.74 o -5 8 1 5.38 47.28 42.40 o -4 8 1 65.50 87.96 26.01 o -3 8 1 110.64 126.74 18.20 o -2 8 1 411.79 380.84 22.99 o -1 8 1 293.83 314.07 18.93 o 0 8 1 3.09 -8.10 12.24 o 1 8 1 838.64 830.25 33.33 o 2 8 1 1821.97 1823.60 53.78 o 3 8 1 1278.02 1291.76 47.57 o 4 8 1 100.29 123.03 36.15 o 5 8 1 253.53 253.16 36.72 o 6 8 1 47.02 11.34 37.52 o 7 8 1 421.59 349.73 57.58 o 8 8 1 158.92 140.49 104.57 o -8 9 1 46.78 97.54 74.04 o -7 9 1 4.45 53.11 51.89 o -6 9 1 34.44 -0.72 37.08 o -5 9 1 1032.25 1071.63 49.88 o -4 9 1 42.47 31.44 32.03 o -3 9 1 1017.93 912.44 34.93 o -2 9 1 503.43 468.82 29.36 o -1 9 1 3.48 38.78 21.53 o 0 9 1 1244.87 1229.90 29.98 o 1 9 1 333.51 306.69 21.50 o 2 9 1 69.92 35.12 18.37 o 3 9 1 969.44 955.96 40.71 o 4 9 1 325.19 366.74 44.93 o 5 9 1 89.07 75.91 35.52 o 6 9 1 261.55 232.13 45.72 o 7 9 1 64.20 131.92 49.39 o 8 9 1 10.82 -55.77 78.77 o -7 10 1 0.14 45.38 79.47 o -6 10 1 210.01 239.18 43.06 o -5 10 1 62.29 15.47 39.15 o -4 10 1 105.50 127.67 33.36 o -3 10 1 19.14 35.64 22.78 o -2 10 1 138.12 92.27 27.35 o -1 10 1 84.11 94.78 19.28 o 0 10 1 0.28 17.76 18.49 o 1 10 1 2180.58 2117.87 47.38 o 2 10 1 227.94 191.27 31.89 o 3 10 1 87.55 36.31 26.66 o 4 10 1 576.89 564.41 39.43 o 5 10 1 3.33 7.40 37.81 o 6 10 1 13.44 9.42 39.16 o 7 10 1 87.30 135.29 50.86 o -7 11 1 9.95 21.69 65.29 o -6 11 1 40.81 48.91 39.95 o -5 11 1 8.79 100.40 45.51 o -4 11 1 377.26 410.64 43.01 o -3 11 1 348.99 332.12 34.70 o -2 11 1 186.68 219.66 40.31 o -1 11 1 547.93 499.81 35.14 o 0 11 1 269.64 272.93 28.68 o 1 11 1 223.82 228.52 26.63 o 2 11 1 135.74 147.48 26.27 o 3 11 1 6.75 19.90 25.26 o 4 11 1 3.38 -26.19 26.19 o 5 11 1 0.17 -44.39 44.39 o 6 11 1 111.71 128.24 46.66 o 7 11 1 41.53 2.73 50.44 o -7 12 1 15.34 16.71 67.87 o -6 12 1 9.05 -16.68 58.62 o -5 12 1 110.37 103.73 40.67 o -4 12 1 137.11 72.95 51.41 o -3 12 1 15.67 88.30 31.76 o -2 12 1 72.50 84.34 32.41 o -1 12 1 25.99 46.42 50.59 o 0 12 1 2113.59 2014.30 59.33 o 1 12 1 38.93 67.51 29.26 o 2 12 1 54.65 27.92 27.82 o 3 12 1 2.76 -3.30 28.42 o 4 12 1 67.63 83.91 35.41 o 5 12 1 89.88 98.11 42.33 o 6 12 1 30.98 -13.91 42.72 o 7 12 1 98.88 95.85 58.14 o -6 13 1 132.67 165.16 78.91 o -5 13 1 109.78 85.21 56.17 o -4 13 1 109.90 151.96 45.14 o -3 13 1 398.09 425.86 69.94 o -2 13 1 2336.41 2370.55 79.09 o -1 13 1 78.32 67.68 37.42 o 0 13 1 1270.65 1263.50 46.98 o 1 13 1 340.84 371.00 41.73 o 2 13 1 560.53 598.37 42.00 o 3 13 1 122.49 90.41 32.36 o 4 13 1 0.39 21.21 46.52 o 5 13 1 52.42 156.73 54.14 o 6 13 1 90.52 110.80 43.95 o -6 14 1 91.46 201.72 55.23 o -5 14 1 0.27 51.90 48.98 o -4 14 1 51.01 20.27 45.26 o -3 14 1 58.18 176.00 53.74 o -2 14 1 553.90 553.33 57.20 o -1 14 1 140.47 49.60 33.43 o 0 14 1 126.59 148.72 30.33 o 1 14 1 719.27 726.71 44.83 o 2 14 1 84.13 97.35 33.66 o 3 14 1 108.88 132.98 35.91 o 4 14 1 374.20 409.37 53.77 o 5 14 1 0.00 79.06 53.31 o 6 14 1 164.07 206.58 56.75 o -5 15 1 136.37 137.19 56.31 o -4 15 1 192.10 201.99 52.57 o -3 15 1 132.54 205.99 59.36 o -2 15 1 51.67 98.87 38.40 o -1 15 1 137.73 120.63 37.14 o 0 15 1 268.74 329.67 42.29 o 1 15 1 187.40 119.93 33.56 o 2 15 1 25.33 7.01 43.41 o 3 15 1 95.04 95.01 40.61 o 4 15 1 49.91 -46.63 46.63 o 5 15 1 0.86 2.65 56.59 o -4 16 1 33.47 68.59 51.20 o -3 16 1 1.80 -0.20 43.95 o -2 16 1 21.75 23.12 45.05 o -1 16 1 5.24 -13.34 60.54 o 0 16 1 12.74 60.61 41.61 o 1 16 1 5.34 9.10 36.17 o 2 16 1 14.26 88.57 43.80 o 3 16 1 7.28 76.53 46.09 o 4 16 1 31.16 33.48 63.49 o -4 17 1 8.74 -29.79 70.63 o -3 17 1 229.72 163.68 107.48 o -2 17 1 59.62 82.42 52.74 o -1 17 1 1.08 -18.11 41.04 o 0 17 1 148.45 156.58 63.17 o 1 17 1 1.46 -10.46 37.76 o 2 17 1 42.55 68.41 40.78 o 3 17 1 29.56 62.68 62.48 o 4 17 1 28.61 223.39 213.70 o -3 18 1 137.49 475.13 165.60 o -2 18 1 130.41 86.35 51.02 o -1 18 1 18.80 101.40 52.36 o 0 18 1 3.99 60.47 85.22 o 1 18 1 583.91 607.20 64.36 o 2 18 1 0.01 143.53 47.14 o 3 18 1 0.73 -8.45 118.60 o 0 19 1 84.70 177.17 73.94 o -9 0 2 79.38 -11.39 85.00 o -8 0 2 616.51 614.22 90.57 o -7 0 2 71.73 47.43 43.56 o -6 0 2 91.92 99.19 50.12 o -5 0 2 402.73 398.03 45.37 o -4 0 2 324.77 361.99 26.30 o -3 0 2 688.95 684.31 28.58 o -2 0 2 30633.71 30262.56 577.45 o -1 0 2 296.14 330.59 14.86 o 0 0 2 15822.87 12698.02 486.96 o 1 0 2 327.08 357.87 15.18 o 2 0 2 4701.03 4862.08 104.26 o 3 0 2 1185.06 1240.90 41.18 o 4 0 2 91.16 144.50 29.54 o 5 0 2 675.12 706.82 44.23 o 6 0 2 107.80 -13.95 46.75 o 7 0 2 613.09 717.03 87.43 o 8 0 2 626.97 592.02 108.06 o 9 0 2 4.68 -37.07 87.98 o -9 1 2 19.67 92.26 57.30 o -8 1 2 48.62 39.74 60.12 o -7 1 2 402.85 378.40 47.60 o -6 1 2 45.08 48.53 29.33 o -5 1 2 91.24 96.79 25.44 o -4 1 2 148.97 187.32 20.50 o -3 1 2 63.23 51.42 14.48 o -2 1 2 33592.09 30930.51 416.93 o -1 1 2 313.45 341.34 10.69 o 0 1 2 76.80 80.26 6.44 o 1 1 2 3351.76 3611.63 56.13 o 2 1 2 1199.46 1245.73 29.71 o 3 1 2 129.89 131.09 16.04 o 4 1 2 1124.11 997.90 30.56 o 5 1 2 182.97 179.84 22.20 o 6 1 2 222.05 256.73 44.19 o 7 1 2 366.86 423.93 53.82 o 8 1 2 0.02 62.54 51.49 o 9 1 2 10.11 -54.79 54.79 o -9 2 2 38.56 -49.29 53.61 o -8 2 2 0.11 33.41 55.20 o -7 2 2 12.30 6.75 35.59 o -6 2 2 2.83 27.50 32.08 o -5 2 2 79.71 142.30 26.78 o -4 2 2 3134.96 3467.94 66.94 o -3 2 2 5.99 14.90 13.35 o -2 2 2 2673.04 2571.34 40.08 o -1 2 2 0.03 4.96 9.42 o 0 2 2 138.47 130.22 8.53 o 1 2 2 298.94 364.30 13.65 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