#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/00/93/2009331.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2009331_Fobs loop_ _publ_author_name 'Quiroga, J.' 'Cruz, S.' 'Insuasty, B.' 'Nogueras, M.' 'S\'anchez, A.' 'Cobo, J.' 'Low, J. N.' _publ_section_title ; Three 3-aryl-5-cyanopyrazolo[3,4-b]pyridines ; _journal_issue 12 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first IUC9900168 _journal_volume 55 _journal_year 1999 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 91.747 _cell_angle_beta 106.638 _cell_angle_gamma 99.610 _cell_length_a 12.4124 _cell_length_b 13.8275 _cell_length_c 14.3744 _exptl_crystal_F_000 960.00 _reflns_d_resolution_high 0.7732 _[local]_cod_data_source_file qb0140Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' iqsc10' _shelx_refln_list_code 4 _shelx_f_calc_maximum 382.84 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma 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22.06 o 7 1 0 409.72 371.25 24.45 o 8 1 0 771.25 747.15 35.53 o 9 1 0 407.04 360.04 30.88 o 10 1 0 746.41 834.97 52.93 o 11 1 0 194.29 154.11 53.52 o 12 1 0 85.30 51.10 42.64 o 13 1 0 63.46 43.95 40.25 o 14 1 0 6.56 41.00 76.52 o -15 2 0 96.53 122.53 71.51 o -14 2 0 16.69 0.00 56.03 o -13 2 0 87.64 18.92 45.57 o -12 2 0 3.32 -12.72 33.38 o -11 2 0 0.45 -10.73 24.15 o -10 2 0 180.04 183.25 24.95 o -9 2 0 76.50 94.76 16.77 o -8 2 0 534.33 494.83 23.00 o -7 2 0 579.47 602.19 19.43 o -6 2 0 4057.59 4197.99 71.91 o -5 2 0 253.31 239.13 10.24 o -4 2 0 2504.34 2341.10 43.95 o -3 2 0 915.29 874.54 21.42 o -2 2 0 250.46 288.73 11.50 o -1 2 0 2433.47 2551.42 55.10 o 1 2 0 844.71 809.28 18.18 o 2 2 0 203.46 187.55 10.36 o 3 2 0 3965.38 3924.86 92.99 o 4 2 0 1363.66 1430.77 42.76 o 5 2 0 449.52 419.06 24.92 o 6 2 0 736.37 708.86 34.22 o 7 2 0 43.74 31.02 16.42 o 8 2 0 18.79 42.20 18.64 o 9 2 0 6.95 -0.48 21.91 o 10 2 0 606.39 535.16 52.17 o 11 2 0 216.85 230.20 40.89 o 12 2 0 4.28 -5.99 44.18 o 13 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77.13 85.25 10.51 o -6 5 0 1652.60 1709.25 36.58 o -5 5 0 330.47 294.37 14.77 o -4 5 0 125.31 98.01 8.57 o -3 5 0 115.05 154.77 11.96 o -2 5 0 201.66 237.09 12.03 o -1 5 0 1010.45 929.37 23.54 o 0 5 0 61.05 38.42 6.87 o 1 5 0 460.39 427.34 17.36 o 2 5 0 422.86 435.49 21.50 o 3 5 0 1380.30 1295.61 33.45 o 4 5 0 2997.94 3287.41 80.93 o 5 5 0 1733.65 1689.76 43.20 o 6 5 0 449.78 538.89 24.96 o 7 5 0 10.89 15.02 9.25 o 8 5 0 320.08 415.96 82.65 o 9 5 0 674.34 691.83 63.64 o 10 5 0 1.58 7.97 40.00 o 11 5 0 0.46 -46.46 66.96 o 12 5 0 6.48 -41.00 71.97 o 13 5 0 16.37 61.49 82.45 o -15 6 0 56.08 20.95 62.40 o -14 6 0 2.51 -10.48 51.93 o -13 6 0 24.55 56.63 36.73 o -12 6 0 39.44 31.36 29.75 o -11 6 0 0.09 -15.58 15.58 o -10 6 0 0.02 8.35 14.60 o -9 6 0 108.24 79.50 15.26 o -8 6 0 0.78 -3.81 10.90 o -7 6 0 66.75 76.19 9.93 o -6 6 0 55.95 50.47 8.34 o -5 6 0 201.67 207.34 9.45 o -4 6 0 358.24 323.39 19.06 o -3 6 0 97.76 110.56 13.59 o -2 6 0 351.79 372.57 47.71 o -1 6 0 1972.60 1827.86 37.86 o 0 6 0 703.41 764.03 25.03 o 1 6 0 1941.53 2001.04 44.66 o 2 6 0 2152.40 2360.31 59.02 o 3 6 0 906.57 953.08 27.44 o 4 6 0 79.18 85.12 10.14 o 5 6 0 53.99 41.05 9.64 o 6 6 0 581.28 572.79 26.83 o 7 6 0 2.20 18.11 10.12 o 8 6 0 582.35 597.54 36.86 o 9 6 0 2.53 -4.38 18.14 o 10 6 0 103.41 120.33 23.67 o 11 6 0 0.44 -14.48 28.47 o 12 6 0 110.65 247.34 108.41 o 13 6 0 7.94 -20.50 92.47 o -15 7 0 2.64 -20.95 84.27 o -14 7 0 20.32 47.37 83.81 o -13 7 0 43.09 39.49 36.44 o -12 7 0 446.48 409.66 44.57 o -11 7 0 250.07 257.67 64.12 o -10 7 0 294.54 310.55 24.51 o -9 7 0 67.88 45.19 14.14 o -8 7 0 8.45 -3.28 16.44 o -7 7 0 73.15 77.01 10.47 o -6 7 0 10.42 22.13 7.58 o -5 7 0 19.79 25.16 14.64 o -4 7 0 264.65 268.54 31.36 o -3 7 0 14.29 5.59 8.16 o -2 7 0 24.97 26.25 3.41 o -1 7 0 1251.39 1278.37 36.02 o 0 7 0 274.21 282.70 16.01 o 1 7 0 427.75 399.60 18.16 o 2 7 0 3305.91 3307.09 74.15 o 3 7 0 831.43 803.49 29.02 o 4 7 0 636.75 651.71 26.49 o 5 7 0 17.99 27.77 12.43 o 6 7 0 30.91 27.67 12.36 o 7 7 0 278.80 312.07 21.42 o 8 7 0 0.13 5.55 11.95 o 9 7 0 6.10 0.15 14.59 o 10 7 0 163.25 137.88 22.78 o 11 7 0 73.19 211.81 103.40 o 12 7 0 55.76 66.96 97.93 o -13 8 0 68.13 5.47 36.90 o -12 8 0 37.94 46.25 26.22 o -11 8 0 17.41 1.78 24.43 o -10 8 0 2.14 -4.75 16.50 o -9 8 0 89.61 110.67 15.19 o -8 8 0 0.01 15.72 22.98 o -7 8 0 534.50 464.76 21.38 o -6 8 0 32.29 29.56 17.24 o -5 8 0 220.62 216.33 22.44 o -4 8 0 172.52 188.98 23.09 o -3 8 0 428.31 472.94 33.83 o -2 8 0 551.02 534.07 17.77 o -1 8 0 2.17 1.02 10.53 o 0 8 0 1219.17 1212.73 34.72 o 1 8 0 0.05 -4.30 9.39 o 2 8 0 577.95 562.26 19.77 o 3 8 0 510.49 532.77 22.71 o 4 8 0 617.47 646.15 30.70 o 5 8 0 1507.26 1544.43 59.24 o 6 8 0 143.98 137.60 17.80 o 7 8 0 0.06 -5.54 15.19 o 8 8 0 64.92 66.10 16.08 o 9 8 0 517.45 460.15 29.02 o 10 8 0 211.92 214.48 31.61 o 11 8 0 107.63 0.00 87.91 o 12 8 0 0.06 15.49 118.43 o -13 9 0 0.22 26.42 36.90 o -12 9 0 35.78 24.57 23.32 o -11 9 0 55.48 64.05 22.52 o -10 9 0 16.66 8.66 17.58 o -9 9 0 79.36 80.56 11.52 o -8 9 0 295.40 276.89 15.56 o -7 9 0 442.28 446.93 37.19 o -6 9 0 48.22 55.29 24.92 o -5 9 0 52.96 71.57 18.86 o -4 9 0 91.56 103.71 14.94 o -3 9 0 15.52 3.06 11.94 o -2 9 0 413.25 488.26 16.16 o -1 9 0 57.71 54.15 9.29 o 0 9 0 35.33 26.15 13.16 o 1 9 0 184.45 180.29 16.28 o 2 9 0 563.58 528.75 32.54 o 3 9 0 7.54 18.45 10.04 o 4 9 0 70.30 74.34 13.70 o 5 9 0 113.09 104.72 17.52 o 6 9 0 27.76 51.40 14.58 o 7 9 0 49.28 26.68 25.18 o 8 9 0 17.45 19.39 14.62 o 9 9 0 104.85 123.63 25.97 o 10 9 0 38.97 -41.45 82.90 o 11 9 0 0.34 123.90 108.41 o -12 10 0 14.44 4.61 24.62 o -11 10 0 11.90 11.75 12.18 o -10 10 0 49.17 35.16 10.63 o -9 10 0 0.60 -21.97 32.23 o -8 10 0 187.50 99.63 32.13 o -7 10 0 396.72 416.56 56.94 o -6 10 0 239.82 288.87 31.92 o -5 10 0 1782.42 2353.51 122.29 o -4 10 0 140.11 146.65 28.51 o -3 10 0 12.96 12.91 9.39 o -2 10 0 1377.90 1391.24 50.34 o -1 10 0 161.03 157.03 14.00 o 0 10 0 169.80 196.78 18.98 o 1 10 0 112.12 96.36 15.72 o 2 10 0 118.50 95.68 16.78 o 3 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61.94 72.03 49.37 o 6 13 0 252.93 155.37 45.88 o 7 13 0 15.26 -15.49 82.45 o 8 13 0 112.61 236.86 112.96 o -11 14 0 60.19 63.31 211.35 o -10 14 0 17.99 5.47 95.20 o -9 14 0 0.02 -10.48 84.27 o -8 14 0 163.61 114.76 49.15 o -7 14 0 14.45 -13.64 60.13 o -6 14 0 177.47 152.59 56.71 o -5 14 0 32.39 30.10 29.38 o -4 14 0 264.21 397.20 95.20 o -2 14 0 0.43 -12.59 30.21 o -1 14 0 330.84 317.90 33.40 o 0 14 0 49.75 80.35 22.35 o 1 14 0 1.11 -12.33 21.85 o 2 14 0 9.83 7.34 29.19 o 3 14 0 69.81 66.54 28.29 o 4 14 0 32.27 63.62 42.15 o 5 14 0 86.66 30.97 61.49 o 6 14 0 7.97 61.49 81.99 o 7 14 0 1.78 25.51 87.46 o -10 15 0 21.96 354.38 232.76 o -9 15 0 41.64 15.94 111.14 o -8 15 0 0.01 -52.84 73.79 o -7 15 0 34.93 -68.78 68.78 o -6 15 0 20.61 -73.79 73.79 o -5 15 0 281.02 327.96 100.67 o -4 15 0 1.29 26.42 68.78 o -2 15 0 307.72 279.22 41.45 o -1 15 0 55.86 53.05 30.76 o 0 15 0 126.54 165.67 46.15 o 1 15 0 8.25 17.06 29.66 o 2 15 0 14.17 -36.87 36.87 o 3 15 0 16.82 -5.24 36.87 o 4 15 0 11.17 -9.36 43.96 o 5 15 0 28.04 81.65 55.04 o -8 16 0 55.34 269.66 116.15 o -7 16 0 0.28 5.47 111.14 o -6 16 0 76.23 142.57 116.15 o -5 16 0 3.19 -105.68 121.62 o -4 16 0 0.01 -84.72 89.73 o 1 16 0 167.72 81.49 39.32 o 2 16 0 18.34 -25.94 36.90 o 3 16 0 27.28 -11.91 38.95 o 4 16 0 1.43 -51.47 76.98 o -6 17 0 138.73 95.20 137.56 o -5 17 0 83.83 116.15 84.72 o -4 17 0 51.79 100.21 100.21 o -3 17 0 332.00 396.29 121.62 o 3 -17 1 8.91 -58.30 79.26 o 4 -17 1 25.72 10.48 105.68 o 5 -17 1 107.98 195.41 132.10 o 6 -17 1 275.01 258.73 137.11 o -4 -16 1 3.28 -5.01 71.97 o -3 -16 1 0.24 61.95 66.96 o -2 -16 1 57.74 71.97 61.95 o -1 -16 1 0.42 0.00 51.47 o 3 -16 1 70.60 111.14 142.57 o 4 -16 1 40.40 -84.72 121.62 o 5 -16 1 1.39 -63.31 95.20 o 6 -16 1 3.90 -79.26 84.27 o 7 -16 1 9.27 0.00 95.20 o 8 -16 1 8.43 -26.42 116.15 o -6 -15 1 161.51 164.44 87.46 o -5 -15 1 0.94 -51.47 56.48 o -4 -15 1 31.22 61.49 92.47 o -3 -15 1 0.07 97.93 61.95 o -2 -15 1 58.14 41.00 41.00 o -1 -15 1 25.58 66.96 51.47 o 0 -15 1 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