#------------------------------------------------------------------------------ #$Date: 2016-04-02 20:34:39 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180772 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/00/93/2009332.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2009332_Fobs loop_ _publ_author_name 'Quiroga, J.' 'Cruz, S.' 'Insuasty, B.' 'Nogueras, M.' 'S\'anchez, A.' 'Cobo, J.' 'Low, J. N.' _publ_section_title ; Three 3-aryl-5-cyanopyrazolo[3,4-b]pyridines ; _journal_issue 12 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first IUC9900168 _journal_volume 55 _journal_year 1999 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 91.437 _cell_angle_gamma 90.000 _cell_length_a 15.6264 _cell_length_b 12.4397 _cell_length_c 21.1296 _exptl_crystal_F_000 1696.00 _reflns_d_resolution_high 0.8398 _cod_data_source_file qb0140IIsup3.hkl _cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' iqsc3' _shelx_refln_list_code 4 _shelx_f_calc_maximum 412.33 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 6295.00 5321.96 299.37 o 4 0 0 52606.59 51221.38 2436.35 o 6 0 0 9358.94 8475.45 275.49 o 8 0 0 344.33 397.78 14.62 o 10 0 0 2149.30 2198.68 102.65 o 12 0 0 402.73 432.87 15.60 o 14 0 0 461.10 419.35 20.11 o 16 0 0 2.23 -3.75 12.68 o 18 0 0 509.51 501.33 31.07 o 1 1 0 19706.23 5617.96 1510.12 o 3 1 0 19199.19 16796.49 487.01 o 5 1 0 13517.75 12049.50 246.66 o 7 1 0 116.00 83.81 5.46 o 9 1 0 10972.26 11566.49 209.97 o 11 1 0 42.51 69.64 6.54 o 13 1 0 3486.42 3625.32 67.36 o 15 1 0 2673.20 2897.95 58.98 o 17 1 0 147.08 191.23 14.13 o 2 2 0 4659.32 4444.33 125.58 o 4 2 0 265.09 295.27 9.69 o 6 2 0 125.28 80.49 4.62 o 8 2 0 607.70 608.53 17.54 o 10 2 0 1548.01 1550.64 42.88 o 12 2 0 1012.10 1117.19 28.47 o 14 2 0 1080.39 1379.88 74.44 o 16 2 0 254.73 233.17 12.92 o 18 2 0 95.04 82.66 16.45 o 1 3 0 3894.46 3808.60 45.19 o 3 3 0 6018.66 6016.21 168.29 o 5 3 0 2097.68 1767.03 44.90 o 7 3 0 721.51 674.80 16.63 o 9 3 0 273.41 349.88 21.27 o 11 3 0 862.74 1006.01 37.45 o 13 3 0 865.91 942.94 21.39 o 15 3 0 1859.59 1963.73 44.73 o 17 3 0 408.01 335.85 17.43 o 0 4 0 82.89 110.59 4.56 o 2 4 0 1032.09 918.70 17.71 o 4 4 0 15231.85 15520.06 254.10 o 6 4 0 2954.52 3109.21 159.17 o 8 4 0 3049.52 2959.15 42.88 o 10 4 0 3261.46 3628.21 56.38 o 12 4 0 2493.58 2592.74 48.30 o 14 4 0 20.06 11.64 7.86 o 16 4 0 0.54 19.92 11.20 o 1 5 0 813.44 921.51 10.97 o 3 5 0 362.46 361.80 8.92 o 5 5 0 2083.67 2355.80 43.44 o 7 5 0 40.10 101.19 20.04 o 9 5 0 60.50 60.90 4.58 o 11 5 0 338.22 324.51 14.80 o 13 5 0 810.95 853.51 21.27 o 15 5 0 7.84 49.27 22.56 o 17 5 0 654.77 700.55 50.21 o 0 6 0 3792.03 3532.99 49.71 o 2 6 0 10457.65 10096.94 115.41 o 4 6 0 3.69 9.12 6.14 o 6 6 0 728.41 1045.12 33.10 o 8 6 0 1372.40 1600.83 41.46 o 10 6 0 1905.61 2154.11 58.30 o 12 6 0 325.86 456.50 54.81 o 14 6 0 3346.54 3941.65 87.39 o 16 6 0 163.47 138.27 18.74 o 1 7 0 7271.88 7255.92 73.67 o 3 7 0 2697.73 2636.73 33.44 o 5 7 0 196.92 233.13 28.53 o 7 7 0 245.04 227.14 13.63 o 9 7 0 208.24 314.34 47.80 o 11 7 0 222.81 242.49 12.67 o 13 7 0 766.36 813.08 40.90 o 15 7 0 1102.29 1326.16 58.38 o 0 8 0 159.30 130.03 6.64 o 2 8 0 137.54 207.58 27.91 o 4 8 0 28.62 66.53 4.12 o 6 8 0 5283.61 5702.47 101.84 o 8 8 0 173.45 148.47 8.89 o 10 8 0 603.75 585.17 23.62 o 12 8 0 341.09 392.28 22.31 o 14 8 0 52.33 49.27 16.03 o 1 9 0 600.02 712.04 55.89 o 3 9 0 933.04 1133.24 22.85 o 5 9 0 1.49 83.70 19.28 o 7 9 0 1232.44 1260.93 33.53 o 9 9 0 387.67 361.61 16.22 o 11 9 0 33.19 34.62 17.09 o 13 9 0 60.62 72.95 17.83 o 0 10 0 3488.58 4355.80 92.98 o 2 10 0 603.11 506.92 12.42 o 4 10 0 2886.66 3450.80 110.36 o 6 10 0 942.73 1168.67 48.35 o 8 10 0 6069.64 6767.95 175.37 o 10 10 0 6.59 33.68 15.53 o 12 10 0 45.49 58.30 16.14 o 1 11 0 700.31 681.28 18.32 o 3 11 0 31.69 51.70 8.35 o 5 11 0 144.02 215.78 19.24 o 7 11 0 303.39 321.56 15.01 o 9 11 0 7.54 23.53 23.05 o 11 11 0 207.92 140.59 18.99 o 0 12 0 737.96 1044.69 45.65 o 2 12 0 800.19 748.54 20.19 o 4 12 0 6.40 19.90 8.32 o 6 12 0 317.36 223.84 14.62 o 8 12 0 717.81 511.56 27.93 o 10 12 0 10.47 11.64 16.20 o 1 13 0 775.27 853.97 30.60 o 3 13 0 1.82 -2.92 8.83 o 5 13 0 470.87 479.13 22.67 o 7 13 0 999.75 1164.22 51.49 o 0 14 0 2207.27 2639.18 128.48 o 2 14 0 46.35 34.82 11.08 o 4 14 0 506.33 608.34 39.89 o 6 14 0 10.94 20.23 18.17 o -17 1 1 37.91 56.89 12.17 o -15 1 1 4.59 368.16 29.99 o -13 1 1 1146.87 1582.92 53.60 o -11 1 1 1009.89 998.73 19.85 o -9 1 1 23.26 47.34 57.75 o -7 1 1 1779.70 1817.98 46.48 o -5 1 1 23816.54 21641.82 611.08 o -3 1 1 12659.71 11205.93 218.90 o -1 1 1 3905.80 3180.44 259.70 o 1 1 1 1581.73 1476.80 86.14 o 3 1 1 517.40 459.49 10.65 o 5 1 1 1564.14 1461.10 31.44 o 7 1 1 152.69 135.58 5.76 o 9 1 1 84.53 92.68 9.98 o 11 1 1 366.93 408.17 14.12 o 13 1 1 79.52 94.53 8.45 o 15 1 1 728.14 851.59 29.05 o 17 1 1 447.29 489.73 23.34 o -18 2 1 146.37 142.83 18.66 o -16 2 1 21.82 56.60 10.54 o -14 2 1 932.79 1067.34 24.38 o -12 2 1 657.19 829.04 31.32 o -10 2 1 234.72 319.53 21.11 o -8 2 1 263.58 233.82 13.37 o -6 2 1 2632.86 2750.92 73.32 o -4 2 1 4427.50 4047.08 63.26 o -2 2 1 17205.27 16298.02 343.45 o 0 2 1 3724.64 3356.76 43.39 o 2 2 1 10245.17 10915.14 191.97 o 4 2 1 181.21 77.34 3.27 o 6 2 1 1031.29 877.95 24.45 o 8 2 1 30.41 40.31 4.96 o 10 2 1 483.65 524.36 15.75 o 12 2 1 131.00 211.50 18.77 o 14 2 1 4870.22 5000.81 101.35 o 16 2 1 75.75 114.27 13.22 o 18 2 1 20.37 38.02 20.25 o -17 3 1 155.42 150.60 16.11 o -15 3 1 856.09 1014.02 30.01 o -13 3 1 176.12 259.32 12.71 o -11 3 1 248.06 341.69 18.63 o -9 3 1 72.15 59.27 5.58 o -7 3 1 6682.22 6838.07 145.26 o -5 3 1 360.93 284.16 9.09 o -3 3 1 1883.19 1656.43 27.09 o -1 3 1 22980.28 22067.83 279.51 o 1 3 1 1575.46 1222.93 15.86 o 3 3 1 42616.48 45869.23 770.10 o 5 3 1 2036.93 2208.41 44.18 o 7 3 1 1608.99 1395.54 33.35 o 9 3 1 875.81 1106.57 18.97 o 11 3 1 1669.63 1622.40 29.28 o 13 3 1 1321.77 1257.81 28.06 o 15 3 1 1952.61 1984.70 43.62 o 17 3 1 224.03 233.50 15.11 o -16 4 1 1411.62 1324.54 41.61 o -14 4 1 755.27 814.26 20.68 o -12 4 1 1276.20 1464.94 59.13 o -10 4 1 3613.04 4021.24 82.28 o -8 4 1 227.86 242.23 31.24 o -6 4 1 694.45 862.64 32.75 o -4 4 1 6937.75 7097.93 125.57 o -2 4 1 4596.24 4149.76 57.33 o 0 4 1 3444.07 3028.86 35.98 o 2 4 1 126.95 69.80 3.75 o 4 4 1 2285.67 2745.58 54.86 o 6 4 1 17710.67 18663.22 333.94 o 8 4 1 612.03 490.99 13.35 o 10 4 1 15.11 54.97 13.26 o 12 4 1 475.58 425.74 14.22 o 14 4 1 76.89 45.92 8.82 o 16 4 1 500.03 445.85 19.67 o -17 5 1 2970.83 2899.05 114.69 o -15 5 1 78.26 92.47 10.16 o -13 5 1 30.46 38.49 12.10 o -11 5 1 273.96 287.77 12.04 o -9 5 1 1082.11 1154.21 22.79 o -7 5 1 368.12 406.89 8.60 o -5 5 1 8500.11 9381.19 161.92 o -3 5 1 1432.17 1559.81 26.74 o -1 5 1 1197.81 1114.19 14.15 o 1 5 1 1170.66 989.41 11.40 o 3 5 1 91.72 169.03 4.77 o 5 5 1 1394.58 2104.97 34.68 o 7 5 1 1267.80 1593.34 27.09 o 9 5 1 100.54 76.02 9.21 o 11 5 1 310.05 328.30 10.01 o 13 5 1 1440.42 1479.78 34.22 o 15 5 1 1794.14 1765.51 45.94 o 17 5 1 0.25 7.75 26.26 o -16 6 1 666.07 594.70 26.17 o -14 6 1 1259.19 1444.40 35.08 o -12 6 1 412.22 392.85 17.13 o -10 6 1 102.18 175.49 31.20 o -8 6 1 3595.58 3911.61 70.82 o -6 6 1 675.39 761.83 22.58 o -4 6 1 4040.81 4356.77 82.80 o -2 6 1 3632.50 4035.50 48.75 o 0 6 1 568.00 483.04 8.06 o 2 6 1 918.59 1072.55 18.09 o 4 6 1 2504.61 2567.84 47.50 o 6 6 1 1751.66 1997.47 47.74 o 8 6 1 578.19 544.82 49.24 o 10 6 1 770.74 866.71 23.27 o 12 6 1 4721.61 5337.58 109.93 o 14 6 1 728.29 755.01 22.95 o 16 6 1 89.06 84.54 20.32 o -15 7 1 51.34 61.85 20.40 o -13 7 1 104.13 93.71 13.25 o -11 7 1 33.27 37.10 9.52 o -9 7 1 776.38 852.54 24.28 o -7 7 1 118.17 93.85 6.61 o -5 7 1 142.64 205.58 5.90 o -3 7 1 3322.45 3661.79 60.13 o -1 7 1 2081.62 2363.24 37.85 o 1 7 1 2946.00 2773.69 40.40 o 3 7 1 229.71 198.52 5.02 o 5 7 1 1451.26 1761.59 32.71 o 7 7 1 1028.42 1196.85 86.91 o 9 7 1 2987.38 3256.63 90.39 o 11 7 1 232.38 236.24 21.51 o 13 7 1 377.81 371.06 24.03 o 15 7 1 743.86 796.45 74.40 o -14 8 1 44.59 61.34 35.48 o -12 8 1 2104.84 2251.92 62.75 o -10 8 1 50.31 58.48 11.45 o -8 8 1 7.99 31.12 8.89 o -6 8 1 63.76 330.02 102.35 o -4 8 1 156.12 163.70 5.35 o -2 8 1 2272.05 2590.77 36.50 o 0 8 1 46.01 42.33 4.10 o 2 8 1 2400.17 2509.22 56.80 o 4 8 1 266.25 266.61 10.16 o 6 8 1 155.22 224.07 36.07 o 8 8 1 143.01 127.30 12.47 o 10 8 1 5.91 58.66 31.20 o 12 8 1 1076.04 1094.81 51.35 o 14 8 1 15.01 35.41 13.04 o -13 9 1 239.08 333.08 22.64 o -11 9 1 796.97 822.92 34.36 o -9 9 1 14.99 5.04 7.60 o -7 9 1 922.18 923.49 23.87 o -5 9 1 427.50 463.73 11.54 o -3 9 1 1967.75 2060.03 33.70 o -1 9 1 68.86 86.04 7.83 o 1 9 1 3767.59 4074.23 62.05 o 3 9 1 987.09 1057.51 21.91 o 5 9 1 1152.66 1273.04 26.24 o 7 9 1 120.57 211.89 38.93 o 9 9 1 133.47 77.79 10.77 o 11 9 1 719.98 783.83 29.42 o 13 9 1 94.18 108.09 19.39 o -12 10 1 413.95 410.47 28.47 o -10 10 1 7.34 29.49 16.58 o -8 10 1 5319.54 5829.33 144.38 o -6 10 1 621.84 604.23 21.00 o -4 10 1 163.39 365.59 48.08 o -2 10 1 537.85 566.92 14.70 o 0 10 1 3372.36 3644.59 67.60 o 2 10 1 212.04 431.65 44.57 o 4 10 1 7781.82 7806.66 128.85 o 6 10 1 1644.21 1612.19 36.00 o 8 10 1 2919.76 3114.83 83.78 o 10 10 1 392.51 378.86 22.60 o 12 10 1 107.60 166.10 18.46 o -11 11 1 229.25 285.93 23.22 o -9 11 1 718.88 795.21 40.63 o -7 11 1 242.94 253.71 14.69 o -5 11 1 801.37 865.17 21.27 o -3 11 1 906.12 982.93 25.87 o -1 11 1 23.54 66.58 11.50 o 1 11 1 34.52 118.54 8.90 o 3 11 1 200.22 357.65 47.00 o 5 11 1 2158.82 2158.65 45.85 o 7 11 1 178.86 183.60 13.08 o 9 11 1 329.18 404.03 25.01 o 11 11 1 461.02 493.43 30.81 o -10 12 1 847.16 1021.15 63.61 o -8 12 1 298.80 261.96 20.34 o -6 12 1 1.87 16.60 10.02 o -4 12 1 510.74 446.12 12.40 o -2 12 1 0.43 61.70 12.37 o 0 12 1 2066.90 2021.93 48.32 o 2 12 1 46.73 98.48 15.05 o 4 12 1 142.32 142.67 9.94 o 6 12 1 0.33 -6.13 10.99 o 8 12 1 69.32 72.56 14.78 o 10 12 1 30.60 67.15 14.32 o -7 13 1 2.03 11.45 14.49 o -5 13 1 147.52 148.31 9.77 o -3 13 1 7.48 16.15 7.71 o -1 13 1 100.45 175.98 16.73 o 1 13 1 925.73 1094.10 31.33 o 3 13 1 76.67 83.35 10.35 o 5 13 1 53.59 95.90 15.84 o 7 13 1 326.34 369.61 33.44 o -6 14 1 276.45 296.89 31.07 o -4 14 1 388.64 353.49 20.41 o -2 14 1 67.20 46.42 12.17 o 0 14 1 672.31 678.31 39.08 o 2 14 1 0.35 14.42 13.35 o 4 14 1 98.79 121.57 17.87 o 6 14 1 1.25 -8.48 17.59 o -18 0 2 494.24 426.19 36.49 o -16 0 2 1552.54 1671.20 57.01 o -14 0 2 186.53 159.52 13.31 o -12 0 2 366.93 308.16 18.18 o -10 0 2 101.20 93.29 8.57 o -8 0 2 1929.40 2038.13 68.77 o -6 0 2 0.24 4.87 6.44 o -4 0 2 31748.10 29541.94 964.74 o -2 0 2 1099.05 897.38 18.14 o 0 0 2 3.30 5.04 4.98 o 2 0 2 23509.45 20218.65 382.31 o 4 0 2 58617.66 61051.82 1378.83 o 6 0 2 2453.78 2302.52 72.84 o 8 0 2 3281.24 3991.90 82.95 o 10 0 2 3682.99 3331.11 93.10 o 12 0 2 1154.13 1106.45 32.23 o 14 0 2 1537.86 1506.14 52.15 o 16 0 2 668.23 661.09 29.81 o 18 0 2 70.27 51.95 18.99 o -17 1 2 734.82 716.31 24.13 o -15 1 2 794.29 739.76 21.49 o -13 1 2 104.82 203.67 11.41 o -11 1 2 538.39 573.57 15.81 o -9 1 2 4804.18 4773.55 76.90 o -7 1 2 225.52 236.32 6.55 o -5 1 2 8850.21 8257.96 146.71 o -3 1 2 21674.70 20115.90 346.68 o -1 1 2 102.66 79.80 2.99 o 1 1 2 274.27 371.18 8.12 o 3 1 2 3877.57 3352.20 43.05 o 5 1 2 2594.68 2137.12 32.89 o 7 1 2 1867.91 1829.93 42.13 o 9 1 2 3929.66 4311.82 96.58 o 11 1 2 856.80 755.73 16.18 o 13 1 2 248.18 337.83 17.36 o 15 1 2 1909.29 1934.52 48.54 o 17 1 2 1054.07 1162.09 32.09 o -18 2 2 0.38 9.94 15.44 o -16 2 2 64.24 65.35 9.92 o -14 2 2 2.78 68.40 10.14 o -12 2 2 307.76 318.47 15.20 o -10 2 2 1148.56 1176.11 23.83 o -8 2 2 195.53 222.01 6.59 o -6 2 2 1204.16 1149.49 19.39 o -4 2 2 9711.21 9168.04 155.77 o -2 2 2 2209.95 2058.32 29.72 o 0 2 2 3781.69 3771.65 60.83 o 2 2 2 4213.87 4034.69 70.20 o 4 2 2 157.85 257.65 5.90 o 6 2 2 1343.93 1289.44 29.02 o 8 2 2 1186.98 1340.87 23.98 o 10 2 2 76.86 93.87 9.34 o 12 2 2 1539.36 1526.37 29.41 o 14 2 2 207.43 194.13 12.40 o 16 2 2 444.19 489.42 16.63 o 18 2 2 521.45 598.99 39.03 o -17 3 2 132.68 154.49 14.92 o -15 3 2 23.56 39.12 13.78 o -13 3 2 655.77 636.30 15.96 o -11 3 2 407.27 426.91 13.68 o -9 3 2 513.79 520.50 14.48 o -7 3 2 325.78 343.97 37.87 o -5 3 2 80.67 86.57 4.56 o -3 3 2 9.73 7.23 2.80 o -1 3 2 1034.68 1023.58 12.15 o 1 3 2 23399.52 22045.91 282.80 o 3 3 2 116.54 122.81 5.22 o 5 3 2 936.94 935.48 27.96 o 7 3 2 40.26 18.18 4.49 o 9 3 2 212.71 262.12 8.96 o 11 3 2 4.19 5.86 5.44 o 13 3 2 45.35 49.88 8.22 o 15 3 2 287.45 267.43 13.41 o 17 3 2 56.98 141.09 15.74 o -16 4 2 11.37 39.72 15.99 o -14 4 2 1405.75 1625.47 33.53 o -12 4 2 2919.59 2806.60 51.78 o -10 4 2 86.86 265.82 54.16 o -8 4 2 721.98 691.21 24.82 o -6 4 2 451.85 538.35 16.51 o -4 4 2 547.82 539.30 14.05 o -2 4 2 320.07 254.22 5.59 o 0 4 2 116.15 85.73 3.64 o 2 4 2 361.63 414.97 6.76 o 4 4 2 8190.63 8368.46 172.36 o 6 4 2 460.67 580.07 36.48 o 8 4 2 129.04 117.45 12.14 o 10 4 2 914.15 942.20 21.78 o 12 4 2 87.98 58.87 9.03 o 14 4 2 5.89 -2.58 8.56 o 16 4 2 443.84 413.44 19.37 o -17 5 2 0.28 162.07 59.54 o -15 5 2 19.55 35.67 11.04 o -13 5 2 2563.93 2449.41 49.95 o -11 5 2 2426.98 2537.57 44.85 o -9 5 2 50.55 105.76 14.81 o -7 5 2 85.93 142.93 6.44 o -5 5 2 8074.59 8307.50 193.43 o -3 5 2 2.66 7.61 4.03 o -1 5 2 107.29 100.03 3.61 o 1 5 2 543.45 625.78 9.19 o 3 5 2 1581.48 1690.62 23.96 o 5 5 2 692.24 862.54 17.65 o 7 5 2 584.06 539.06 15.79 o 9 5 2 477.17 480.39 15.36 o 11 5 2 482.85 429.86 14.31 o 13 5 2 83.20 104.81 8.61 o 15 5 2 49.29 68.91 15.92 o 17 5 2 1642.33 1667.85 80.83 o -16 6 2 68.32 83.25 19.66 o -14 6 2 753.10 847.40 28.69 o -12 6 2 12.40 11.20 7.29 o -10 6 2 514.25 569.33 12.56 o -8 6 2 106.19 284.10 51.32 o -6 6 2 1037.92 1011.85 19.05 o -4 6 2 5614.30 5932.76 91.38 o -2 6 2 1361.40 1142.86 30.41 o 0 6 2 963.52 909.28 12.72 o 2 6 2 3627.21 3430.87 40.74 o 4 6 2 246.02 285.02 12.28 o 6 6 2 2227.93 2771.96 61.95 o 8 6 2 2267.77 2605.96 52.00 o 10 6 2 177.94 163.78 11.13 o 12 6 2 26.21 31.17 5.80 o 14 6 2 94.13 119.75 15.79 o 16 6 2 103.79 103.85 22.58 o -15 7 2 1554.27 1763.62 69.26 o -13 7 2 11.64 15.17 10.51 o -11 7 2 490.08 535.48 16.87 o -9 7 2 298.96 309.63 10.79 o -7 7 2 84.94 110.79 6.10 o -5 7 2 1551.64 1651.01 26.07 o -3 7 2 831.64 1066.60 47.28 o -1 7 2 980.44 1147.81 20.64 o 1 7 2 2313.09 2323.90 28.10 o 3 7 2 94.34 80.43 9.33 o 5 7 2 247.78 203.04 31.64 o 7 7 2 4942.13 5307.63 118.01 o 9 7 2 77.86 82.73 20.16 o 11 7 2 1732.54 1908.77 54.02 o 13 7 2 310.85 312.60 22.35 o 15 7 2 653.88 686.01 41.76 o -14 8 2 0.57 -7.94 21.87 o -12 8 2 450.95 506.50 24.49 o -10 8 2 1.73 1.06 7.44 o -8 8 2 200.25 195.14 10.24 o -6 8 2 173.44 155.31 8.22 o -4 8 2 370.65 447.51 9.52 o -2 8 2 1064.20 1045.41 36.69 o 0 8 2 451.42 463.22 8.34 o 2 8 2 3965.65 3660.22 48.87 o 4 8 2 558.52 532.97 17.61 o 6 8 2 2187.73 2358.86 53.72 o 8 8 2 580.08 531.24 16.86 o 10 8 2 3815.46 4362.32 101.30 o 12 8 2 707.94 883.40 32.55 o 14 8 2 196.82 229.23 27.92 o -13 9 2 457.73 501.48 35.03 o -11 9 2 40.00 44.64 14.33 o -9 9 2 99.93 72.69 7.16 o -7 9 2 1351.06 1211.70 29.66 o -5 9 2 47.88 65.66 9.02 o -3 9 2 0.28 103.44 22.15 o -1 9 2 417.91 461.36 12.10 o 1 9 2 1514.86 1599.82 43.88 o 3 9 2 428.68 358.89 8.81 o 5 9 2 237.10 237.20 12.59 o 7 9 2 1743.50 1952.46 45.32 o 9 9 2 571.84 515.29 19.14 o 11 9 2 78.93 52.65 16.08 o 13 9 2 0.17 5.51 12.24 o -12 10 2 13.97 21.50 13.39 o -10 10 2 6.63 35.41 20.96 o -8 10 2 212.37 312.28 18.13 o -6 10 2 15.37 28.12 5.16 o -4 10 2 1873.81 1915.03 34.81 o -2 10 2 136.13 143.03 10.57 o 0 10 2 166.21 310.26 50.51 o 2 10 2 3371.14 3354.12 53.27 o 4 10 2 383.42 376.80 26.32 o 6 10 2 215.18 227.48 13.04 o 8 10 2 94.66 88.20 12.47 o 10 10 2 1224.85 1399.60 74.55 o 12 10 2 5.21 4.20 11.51 o -11 11 2 132.20 118.87 18.88 o -9 11 2 975.62 1051.37 43.09 o -7 11 2 59.86 52.99 11.52 o -5 11 2 3035.70 3321.97 60.52 o -3 11 2 601.97 611.03 24.67 o -1 11 2 291.35 321.40 9.23 o 1 11 2 926.95 982.25 25.00 o 3 11 2 4606.24 4997.53 97.54 o 5 11 2 360.84 424.20 25.44 o 7 11 2 556.82 563.82 20.95 o 9 11 2 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