#------------------------------------------------------------------------------ #$Date: 2016-04-02 20:34:39 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180772 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/00/93/2009333.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2009333_Fobs loop_ _publ_author_name 'Quiroga, J.' 'Cruz, S.' 'Insuasty, B.' 'Nogueras, M.' 'S\'anchez, A.' 'Cobo, J.' 'Low, J. N.' _publ_section_title ; Three 3-aryl-5-cyanopyrazolo[3,4-b]pyridines ; _journal_issue 12 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first IUC9900168 _journal_volume 55 _journal_year 1999 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 96.248 _cell_angle_gamma 90.000 _cell_length_a 6.6222 _cell_length_b 11.0791 _cell_length_c 28.2635 _exptl_crystal_F_000 876.00 _reflns_d_resolution_high 0.8008 _cod_data_source_file qb0140IIIsup4.hkl _cod_data_source_block III #BEGIN Tags that were not found in dictionaries: _shelx_title ' iqsc8' _shelx_refln_list_code 4 _shelx_f_calc_maximum 185.87 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1930.11 1836.73 56.73 o 4 0 0 384.29 310.48 31.13 o 6 0 0 267.52 220.93 38.51 o 8 0 0 228.88 234.37 129.67 o 1 1 0 183.66 196.69 8.64 o 2 1 0 1641.11 1600.05 31.63 o 3 1 0 1327.86 1374.24 32.94 o 4 1 0 17.88 37.27 11.85 o 5 1 0 5.82 9.45 16.33 o 6 1 0 67.22 88.50 24.46 o 7 1 0 334.48 299.67 49.35 o 8 1 0 73.11 76.83 103.13 o 0 2 0 1994.27 1871.64 73.04 o 1 2 0 533.33 577.70 20.07 o 2 2 0 351.52 384.63 14.25 o 3 2 0 4552.88 4813.04 104.67 o 4 2 0 789.78 829.35 26.93 o 5 2 0 239.52 204.58 21.14 o 6 2 0 10.35 53.40 26.01 o 7 2 0 180.84 173.60 59.81 o 8 2 0 25.72 22.10 101.28 o 1 3 0 3.41 7.92 11.64 o 2 3 0 258.40 314.38 19.87 o 3 3 0 393.97 405.63 24.10 o 4 3 0 1173.74 1184.62 45.34 o 5 3 0 2350.86 2467.48 204.26 o 6 3 0 1.85 -23.40 40.25 o 7 3 0 7.29 130.38 64.43 o 8 3 0 15.57 -71.08 96.79 o 0 4 0 4471.02 4203.44 149.62 o 1 4 0 3027.94 3138.66 88.68 o 2 4 0 4.06 -0.22 8.61 o 3 4 0 30.76 32.29 16.96 o 4 4 0 78.27 130.01 27.84 o 5 4 0 1.65 30.75 35.00 o 6 4 0 17.45 11.42 45.23 o 7 4 0 9.66 74.09 67.14 o 1 5 0 2922.06 3182.81 107.10 o 2 5 0 6840.50 7700.18 207.55 o 3 5 0 382.95 387.43 47.72 o 4 5 0 10.89 17.71 24.62 o 5 5 0 49.76 69.98 51.38 o 6 5 0 2.71 -14.56 83.33 o 7 5 0 17.13 -120.55 125.83 o 0 6 0 584.19 542.71 71.08 o 1 6 0 1435.51 1380.39 59.38 o 2 6 0 467.15 418.02 25.65 o 3 6 0 496.28 478.52 32.93 o 4 6 0 14.91 56.93 34.60 o 5 6 0 306.58 239.26 91.01 o 6 6 0 434.40 139.76 120.07 o 7 6 0 62.66 -10.09 120.55 o 1 7 0 828.06 768.10 41.36 o 2 7 0 882.98 936.83 44.70 o 3 7 0 1.69 -15.44 32.72 o 4 7 0 311.35 375.45 43.41 o 5 7 0 135.82 52.06 69.91 o 7 7 0 0.01 105.18 135.44 o 0 8 0 82.34 204.82 49.71 o 1 8 0 1082.10 1115.20 61.35 o 2 8 0 0.53 29.90 41.66 o 3 8 0 483.82 487.03 37.96 o 4 8 0 175.34 198.29 61.72 o 5 8 0 35.21 20.52 66.23 o 6 8 0 1.08 -14.89 110.46 o 1 9 0 438.88 497.88 44.18 o 2 9 0 188.05 197.21 53.20 o 3 9 0 89.67 89.33 69.64 o 5 9 0 0.66 -41.31 70.08 o 6 9 0 0.32 24.97 89.81 o 0 10 0 114.44 30.26 90.77 o 1 10 0 937.40 968.91 186.11 o 2 10 0 870.04 1057.55 75.16 o 3 10 0 190.08 248.78 89.33 o 4 10 0 2.28 10.09 74.92 o 1 11 0 145.18 98.74 71.99 o 2 11 0 0.02 49.47 89.33 o 4 11 0 452.21 696.88 149.37 o 1 12 0 37.12 104.22 99.42 o 2 12 0 29.54 -64.36 109.50 o 3 12 0 14.19 99.42 104.22 o 2 13 0 38.22 -79.73 124.39 o -7 0 1 1113.39 1315.56 118.77 o -5 0 1 235.77 253.54 31.71 o -3 0 1 5.78 3.97 18.20 o -1 0 1 1116.21 1092.20 36.52 o 1 0 1 5211.40 4941.53 130.96 o 3 0 1 0.59 8.57 13.62 o 5 0 1 1933.65 1875.49 84.92 o 7 0 1 667.29 772.18 93.98 o -8 1 1 0.04 -9.51 94.63 o -7 1 1 54.92 37.05 45.94 o -6 1 1 116.15 79.22 24.62 o -5 1 1 369.24 363.74 22.03 o -4 1 1 52.74 45.44 11.99 o -3 1 1 1051.94 1185.16 32.82 o -2 1 1 3651.72 3682.29 70.88 o -1 1 1 15863.87 14825.36 300.32 o 1 1 1 59.38 66.68 3.38 o 2 1 1 160.78 151.25 6.91 o 3 1 1 4676.00 5007.88 96.53 o 4 1 1 1384.98 1571.95 44.88 o 5 1 1 2.78 18.63 17.14 o 6 1 1 358.94 428.08 35.50 o 7 1 1 13.97 -23.31 48.50 o 8 1 1 0.12 127.16 155.13 o -8 2 1 28.47 120.07 124.87 o -7 2 1 186.90 140.31 56.02 o -6 2 1 129.14 160.07 24.92 o -5 2 1 1.28 6.07 15.49 o -4 2 1 182.37 158.94 16.21 o -3 2 1 93.67 90.01 12.31 o -2 2 1 2315.96 2192.25 51.54 o -1 2 1 1643.48 1571.96 46.81 o 0 2 1 197.25 200.25 9.70 o 1 2 1 406.18 377.25 19.76 o 2 2 1 554.94 524.95 22.19 o 3 2 1 1195.98 1286.58 31.29 o 4 2 1 823.41 831.95 28.44 o 5 2 1 1122.02 1153.50 40.15 o 6 2 1 977.49 932.46 78.41 o 7 2 1 26.42 -11.12 56.17 o 8 2 1 318.07 464.08 192.11 o -8 3 1 65.64 65.86 96.12 o -7 3 1 60.39 196.53 54.16 o -6 3 1 470.07 504.85 59.71 o -5 3 1 3077.04 3340.50 140.74 o -4 3 1 125.65 151.10 17.91 o -3 3 1 2458.61 2558.94 73.41 o -2 3 1 2286.31 2280.14 95.58 o -1 3 1 452.41 375.71 29.60 o 0 3 1 2.08 12.81 9.28 o 1 3 1 3476.90 3558.48 115.19 o 2 3 1 1282.99 1360.31 35.33 o 3 3 1 387.75 353.38 19.68 o 4 3 1 165.98 147.85 18.90 o 5 3 1 3.18 52.39 28.93 o 6 3 1 337.32 395.02 50.16 o 7 3 1 178.95 186.72 65.21 o -7 4 1 146.75 14.31 84.70 o -6 4 1 45.41 102.35 38.58 o -5 4 1 118.52 122.63 41.39 o -4 4 1 193.26 163.26 24.43 o -3 4 1 80.85 46.11 21.80 o -2 4 1 1287.13 1391.78 47.23 o -1 4 1 41.71 53.82 12.77 o 0 4 1 342.95 348.56 15.71 o 1 4 1 3648.33 3544.25 89.71 o 2 4 1 2050.08 2079.67 98.13 o 3 4 1 1388.14 1432.91 53.33 o 4 4 1 199.03 171.63 47.76 o 5 4 1 1060.63 1019.83 69.81 o 6 4 1 25.52 -7.01 46.14 o 7 4 1 8.04 54.08 97.42 o -7 5 1 3.01 -30.26 135.44 o -6 5 1 355.84 251.78 81.13 o -5 5 1 57.34 85.03 49.41 o -4 5 1 3.78 -15.99 30.32 o -3 5 1 346.30 336.55 31.10 o -2 5 1 1020.67 1129.79 38.01 o -1 5 1 292.81 300.19 24.22 o 0 5 1 64.82 54.75 14.56 o 1 5 1 131.07 130.15 22.53 o 2 5 1 0.22 21.92 28.96 o 3 5 1 1321.81 1300.78 63.47 o 4 5 1 194.23 243.72 29.90 o 5 5 1 297.60 300.67 74.20 o 6 5 1 95.96 -4.80 85.49 o 7 5 1 4.31 55.23 125.83 o -7 6 1 55.53 -30.26 135.44 o -6 6 1 3.74 48.82 68.21 o -5 6 1 635.62 707.95 90.05 o -4 6 1 1.50 21.78 36.75 o -3 6 1 247.83 214.15 18.78 o -2 6 1 35.81 19.35 16.59 o -1 6 1 143.84 108.76 19.77 o 0 6 1 17.62 44.22 15.93 o 1 6 1 156.63 133.06 20.14 o 2 6 1 95.74 87.03 20.21 o 3 6 1 21.46 21.70 16.16 o 4 6 1 0.42 20.88 35.23 o 5 6 1 418.13 369.44 69.69 o 6 6 1 38.40 -35.06 115.27 o 7 6 1 51.17 195.95 115.27 o -7 7 1 5.28 10.09 134.96 o -6 7 1 1.91 -29.78 139.28 o -5 7 1 51.48 65.28 47.99 o -4 7 1 0.23 0.48 33.98 o -3 7 1 458.13 395.67 30.22 o -2 7 1 82.75 113.12 27.96 o -1 7 1 125.57 133.56 23.82 o 0 7 1 638.44 635.19 33.20 o 1 7 1 10.69 10.13 20.21 o 2 7 1 154.92 133.27 26.29 o 3 7 1 21.35 4.77 21.42 o 4 7 1 559.51 538.61 60.00 o 5 7 1 41.44 119.43 110.22 o 7 7 1 364.16 516.30 150.33 o -6 8 1 331.57 265.59 130.15 o -5 8 1 324.91 211.80 156.09 o -4 8 1 95.86 147.20 62.32 o -3 8 1 49.27 59.09 34.24 o -2 8 1 81.03 60.24 35.95 o -1 8 1 2556.31 2877.47 113.97 o 0 8 1 450.93 459.70 37.08 o 1 8 1 693.87 607.78 47.56 o 2 8 1 1844.31 1900.11 84.64 o 3 8 1 2.14 -13.10 26.62 o 4 8 1 2.33 88.81 90.05 o 5 8 1 137.77 166.12 72.02 o 6 8 1 163.88 275.68 115.27 o -6 9 1 0.10 149.30 97.09 o -5 9 1 3.74 -60.03 99.90 o -4 9 1 136.61 129.32 61.96 o -3 9 1 226.57 234.43 42.26 o -2 9 1 445.43 460.91 71.85 o -1 9 1 30.43 62.48 42.82 o 0 9 1 1577.05 1693.84 91.22 o 1 9 1 296.10 285.02 38.38 o 2 9 1 178.87 222.23 45.28 o 3 9 1 0.02 46.65 42.19 o 4 9 1 203.96 264.15 94.61 o 5 9 1 189.52 85.01 89.81 o -5 10 1 93.65 169.54 94.61 o -4 10 1 50.13 179.14 94.61 o -3 10 1 0.01 24.97 74.44 o -2 10 1 343.37 406.65 53.79 o -1 10 1 782.01 860.53 95.93 o 0 10 1 54.31 54.54 72.41 o 1 10 1 0.97 -56.38 56.38 o 2 10 1 1266.85 1472.46 96.13 o 3 10 1 15.80 -50.85 109.98 o -4 11 1 54.49 94.61 109.50 o -2 11 1 87.44 56.85 65.77 o -1 11 1 2.29 -12.44 85.49 o 0 11 1 36.76 10.09 56.37 o 1 11 1 196.33 158.90 69.24 o 2 11 1 52.16 19.69 84.53 o 4 11 1 0.78 -24.97 94.61 o -3 12 1 163.94 34.58 99.42 o -2 12 1 61.35 59.55 94.61 o -1 12 1 8.20 88.79 74.20 o 0 12 1 117.31 146.40 84.17 o 1 12 1 141.35 139.76 114.79 o 3 12 1 6.67 104.22 114.31 o 4 12 1 0.16 10.09 104.02 o -2 13 1 35.06 -29.78 129.19 o -1 13 1 0.01 134.48 129.19 o 0 13 1 232.83 353.00 158.97 o 1 13 1 17.24 138.80 123.91 o -8 0 2 286.81 384.22 134.96 o -6 0 2 215.09 241.65 39.55 o -4 0 2 351.77 308.12 23.74 o -2 0 2 12718.52 12974.96 374.87 o 2 0 2 118.61 127.69 11.87 o 4 0 2 1245.54 1174.98 46.20 o 6 0 2 22.44 53.64 37.50 o 8 0 2 1.09 142.64 172.90 o -8 1 2 99.93 124.18 94.50 o -7 1 2 13.15 23.26 42.76 o -6 1 2 98.09 121.90 28.62 o -5 1 2 271.68 275.27 19.44 o -4 1 2 165.78 157.24 13.09 o -3 1 2 1901.15 2055.86 48.32 o -2 1 2 957.99 891.23 23.68 o -1 1 2 6105.75 5510.70 131.29 o 0 1 2 7355.20 5487.15 1290.74 o 1 1 2 167.60 158.50 6.03 o 2 1 2 893.60 887.14 17.66 o 3 1 2 469.31 397.42 14.78 o 4 1 2 996.64 952.92 32.74 o 5 1 2 45.78 47.29 17.40 o 6 1 2 64.85 100.57 25.24 o 7 1 2 11.68 -24.65 45.03 o 8 1 2 21.06 -25.45 137.36 o -8 2 2 2.82 89.81 145.04 o -7 2 2 102.59 110.53 56.36 o -6 2 2 124.73 101.31 29.29 o -5 2 2 747.67 729.45 35.72 o -4 2 2 465.24 473.67 32.25 o -3 2 2 3633.42 3902.91 83.29 o -2 2 2 18.36 16.54 6.13 o -1 2 2 18201.25 17091.94 466.88 o 0 2 2 511.70 511.39 17.53 o 1 2 2 10252.80 9946.20 217.24 o 2 2 2 23.79 26.61 5.39 o 3 2 2 603.98 600.40 16.20 o 4 2 2 149.59 117.36 16.12 o 5 2 2 261.52 249.29 22.20 o 6 2 2 38.47 55.14 32.65 o 7 2 2 24.52 -41.71 54.60 o 8 2 2 0.85 107.99 101.46 o -8 3 2 7.89 215.64 170.50 o -7 3 2 98.83 77.72 81.87 o -6 3 2 131.19 151.16 39.75 o -5 3 2 232.53 222.54 58.23 o -4 3 2 24.45 -2.58 17.68 o -3 3 2 799.21 858.70 47.21 o -2 3 2 107.63 67.49 20.88 o -1 3 2 2812.82 2717.04 71.58 o 0 3 2 1250.46 1301.25 44.62 o 1 3 2 140.26 176.59 13.37 o 2 3 2 221.19 226.80 12.92 o 3 3 2 1685.65 1725.33 46.60 o 4 3 2 49.53 23.36 17.71 o 5 3 2 437.06 423.44 46.05 o 6 3 2 59.76 84.60 43.70 o 7 3 2 184.56 147.81 60.93 o -7 4 2 18.43 15.31 67.72 o -6 4 2 159.50 109.11 111.18 o -5 4 2 18.93 17.96 30.32 o -4 4 2 327.31 314.72 25.54 o -3 4 2 30.05 11.64 21.84 o -2 4 2 3346.28 3452.90 84.43 o -1 4 2 11291.13 11387.70 266.68 o 0 4 2 99.42 85.92 12.11 o 1 4 2 1526.70 1725.72 74.40 o 2 4 2 303.79 355.28 27.51 o 3 4 2 692.38 662.35 28.07 o 4 4 2 53.32 25.31 24.69 o 5 4 2 79.61 50.78 37.62 o 6 4 2 406.40 403.18 60.17 o 7 4 2 132.12 103.47 63.55 o -7 5 2 2.99 35.06 125.35 o -6 5 2 184.96 151.74 80.11 o -5 5 2 157.85 198.60 45.40 o -4 5 2 304.01 307.32 60.99 o -3 5 2 859.21 845.39 76.32 o -2 5 2 202.40 192.55 17.78 o -1 5 2 794.83 863.55 32.08 o 0 5 2 884.55 817.60 27.05 o 1 5 2 956.54 1082.90 55.29 o 2 5 2 4268.03 4558.97 144.05 o 3 5 2 244.46 223.16 29.07 o 4 5 2 45.55 8.07 29.58 o 5 5 2 25.09 76.47 49.16 o 6 5 2 20.05 150.81 115.75 o 7 5 2 13.47 -30.26 150.81 o -7 6 2 85.99 10.09 130.15 o -6 6 2 71.99 119.59 119.59 o -5 6 2 162.25 169.75 60.55 o -4 6 2 138.64 137.17 43.96 o -3 6 2 692.71 706.09 34.20 o -2 6 2 1006.41 967.58 43.29 o -1 6 2 277.65 233.19 22.28 o 0 6 2 51.34 64.15 18.05 o 1 6 2 218.69 194.82 23.74 o 2 6 2 1.24 26.44 17.23 o 3 6 2 56.53 64.70 13.20 o 4 6 2 1217.10 1077.62 97.78 o 5 6 2 7.97 62.18 55.26 o 7 6 2 52.60 220.93 125.35 o -7 7 2 48.07 14.89 170.02 o -6 7 2 229.71 288.39 82.30 o -5 7 2 15.37 -12.73 70.98 o -4 7 2 250.13 182.97 38.56 o -3 7 2 183.23 154.41 25.59 o -2 7 2 92.64 115.70 26.94 o -1 7 2 19.29 19.24 19.47 o 0 7 2 356.37 341.81 27.33 o 1 7 2 31.35 44.67 26.72 o 2 7 2 631.43 597.86 32.55 o 3 7 2 29.00 12.90 16.92 o 4 7 2 19.44 123.13 58.01 o 5 7 2 0.94 124.87 85.01 o 7 7 2 5.27 10.09 105.18 o -6 8 2 28.03 80.95 99.90 o -5 8 2 421.08 282.40 151.29 o -4 8 2 0.12 -12.62 40.26 o -3 8 2 0.16 8.03 76.27 o -2 8 2 433.28 452.91 39.25 o -1 8 2 730.40 798.81 70.27 o 0 8 2 18.27 18.57 29.19 o 1 8 2 792.13 809.87 48.74 o 2 8 2 758.90 693.02 62.58 o 3 8 2 1225.09 1260.85 136.84 o 4 8 2 0.46 28.42 40.22 o 5 8 2 169.78 44.40 90.29 o 6 8 2 82.03 130.15 125.35 o -3 9 2 2.78 55.40 39.65 o -2 9 2 158.97 237.96 60.99 o -1 9 2 10.46 -9.13 30.02 o 0 9 2 81.47 152.97 38.76 o 1 9 2 10.11 68.95 37.57 o 2 9 2 48.37 57.50 38.59 o 3 9 2 4.44 -46.77 48.55 o 4 9 2 36.71 -64.84 69.64 o 5 9 2 179.72 289.61 99.90 o 6 9 2 109.86 74.92 95.09 o -5 10 2 58.55 209.40 139.76 o -2 10 2 4.19 101.34 60.99 o -1 10 2 14.32 -25.69 44.56 o 0 10 2 1345.65 1385.66 107.18 o 1 10 2 120.58 36.41 59.79 o 2 10 2 386.99 473.20 68.82 o 3 10 2 67.23 1.47 65.89 o 4 10 2 29.60 -94.61 94.61 o 5 10 2 26.26 144.56 109.50 o -5 11 2 4.48 99.90 154.65 o -4 11 2 5.33 -39.86 94.61 o -2 11 2 22.22 139.28 94.61 o 0 11 2 6.13 21.68 61.40 o 1 11 2 888.30 975.54 162.81 o 2 11 2 69.55 230.53 99.90 o 3 11 2 279.82 341.95 78.84 o 4 11 2 0.68 -34.58 94.61 o -3 12 2 27.10 109.50 119.59 o -2 12 2 139.68 74.44 119.59 o -1 12 2 1.48 -39.86 94.61 o 0 12 2 168.20 244.77 87.72 o 1 12 2 24.74 159.93 124.87 o 2 12 2 34.14 190.19 134.96 o 4 12 2 8.25 -4.80 124.39 o -1 13 2 56.43 233.89 144.56 o 0 13 2 28.10 29.78 124.39 o -7 0 3 9.53 12.69 60.27 o -5 0 3 460.92 447.65 47.33 o -3 0 3 137.70 186.99 28.82 o -1 0 3 7999.81 7869.07 323.93 o 1 0 3 9907.89 9489.25 231.54 o 3 0 3 1242.66 1223.21 37.38 o 5 0 3 58.85 70.22 26.77 o 7 0 3 3.93 167.75 79.01 o -8 1 3 105.38 24.48 102.39 o -7 1 3 37.68 26.76 46.77 o -6 1 3 141.37 109.22 28.03 o -5 1 3 21.23 22.46 16.07 o -4 1 3 838.46 838.98 27.19 o -3 1 3 84.43 111.65 10.90 o -2 1 3 1794.93 1828.37 46.04 o -1 1 3 2496.45 2400.98 54.47 o 0 1 3 895.89 807.78 23.86 o 1 1 3 2233.34 2238.38 39.25 o 2 1 3 264.05 276.80 9.77 o 3 1 3 10.28 36.06 10.54 o 4 1 3 1257.06 1280.60 34.97 o 5 1 3 4.27 -7.05 17.46 o 6 1 3 153.82 182.27 29.78 o 7 1 3 78.56 45.76 46.29 o 8 1 3 1.21 -1.77 100.50 o -8 2 3 28.97 -14.89 145.04 o -7 2 3 330.37 284.41 51.36 o -6 2 3 769.55 853.90 67.34 o -5 2 3 41.71 30.47 18.36 o -4 2 3 219.32 212.66 15.41 o -3 2 3 3669.89 3847.15 77.61 o -2 2 3 5827.49 5956.18 160.49 o -1 2 3 15666.81 15236.49 369.76 o 0 2 3 80.11 100.97 8.12 o 1 2 3 7169.83 7045.87 151.38 o 2 2 3 5896.97 5794.75 96.20 o 3 2 3 365.75 442.75 16.35 o 4 2 3 608.00 642.71 31.89 o 5 2 3 1.07 1.37 68.35 o 6 2 3 1225.60 1188.72 54.97 o 7 2 3 100.48 128.10 56.27 o 8 2 3 11.20 121.99 162.33 o -8 3 3 11.01 49.95 125.35 o -7 3 3 22.56 89.87 47.92 o -6 3 3 44.87 18.15 30.08 o -5 3 3 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