#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2010615.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2010615_Fobs loop_ _publ_author_name 'Boryczka, Stanis\/law' 'Schreurs, Antoine M. M.' 'Kroon, Jan' 'Steiner, Thomas' _publ_section_title ; C[tripleC---H···N hydrogen bonding in 3-methylthio-4-propargylthioquinoline ; _journal_issue 2 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 263 _journal_page_last 264 _journal_volume 56 _journal_year 2000 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 107.569 _cell_angle_beta 100.986 _cell_angle_gamma 94.567 _cell_length_a 7.4477 _cell_length_b 8.5135 _cell_length_c 9.7860 _exptl_crystal_F_000 256.00 _reflns_d_resolution_high 0.7697 _[local]_cod_data_source_file de1124Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title DE1124 _shelx_refln_list_code 4 _shelx_f_calc_maximum 88.13 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 588.02 591.19 3.59 o 2 0 0 7522.71 8297.71 5.25 o 3 0 0 1413.59 1500.58 51.44 o 4 0 0 94.16 77.98 0.87 o 5 0 0 67.94 85.15 1.07 o 6 0 0 13.87 17.95 1.02 o 7 0 0 126.37 132.96 1.70 o 8 0 0 86.68 91.19 1.88 o 9 0 0 43.50 59.41 2.10 o -9 1 0 11.61 25.48 1.84 o -8 1 0 157.22 150.94 2.04 o -7 1 0 223.08 243.21 2.07 o -6 1 0 94.29 103.83 1.34 o -5 1 0 72.66 66.49 0.98 o -4 1 0 53.42 85.55 0.91 o -3 1 0 287.34 271.65 6.24 o -2 1 0 7767.59 8141.97 5.24 o -1 1 0 313.36 322.98 12.80 o 1 1 0 447.47 413.81 1.27 o 2 1 0 87.85 93.38 5.17 o 3 1 0 431.96 436.69 4.63 o 4 1 0 297.01 368.11 1.75 o 5 1 0 2.44 4.32 0.65 o 6 1 0 0.47 0.00 0.94 o 7 1 0 0.01 5.07 1.25 o 8 1 0 188.64 191.82 2.22 o 9 1 0 0.40 0.00 1.82 o -9 2 0 0.52 0.00 1.70 o -8 2 0 10.67 7.82 1.28 o -7 2 0 3.24 5.49 1.03 o -6 2 0 0.00 0.67 0.79 o -5 2 0 0.05 0.00 0.54 o -4 2 0 21.12 20.48 0.59 o -3 2 0 143.88 123.09 1.86 o -2 2 0 495.31 508.62 1.57 o -1 2 0 88.68 65.48 3.26 o 0 2 0 1501.69 1497.44 21.84 o 1 2 0 325.55 351.54 5.45 o 2 2 0 24.65 20.89 0.82 o 3 2 0 1070.11 1125.99 2.77 o 4 2 0 138.47 126.24 1.18 o 5 2 0 2.29 1.97 0.72 o 6 2 0 34.65 24.87 1.16 o 7 2 0 274.73 279.53 2.34 o 8 2 0 12.71 8.94 1.64 o -9 3 0 29.85 26.87 1.94 o -8 3 0 194.29 213.63 2.31 o -7 3 0 253.02 270.05 2.18 o -6 3 0 5.59 9.94 0.89 o -5 3 0 74.97 71.22 1.02 o -4 3 0 374.75 332.10 1.67 o -3 3 0 319.64 285.71 1.39 o -2 3 0 4.26 4.23 0.27 o -1 3 0 747.04 672.41 10.38 o 0 3 0 1798.87 1752.75 24.58 o 1 3 0 159.64 124.38 6.82 o 2 3 0 180.37 203.23 1.22 o 3 3 0 449.64 436.50 1.94 o 4 3 0 460.96 454.98 2.21 o 5 3 0 30.81 27.56 0.97 o 6 3 0 220.60 241.59 2.20 o 7 3 0 212.08 196.21 2.35 o 8 3 0 0.07 1.34 1.85 o -9 4 0 0.53 0.00 1.71 o -8 4 0 153.10 145.61 2.10 o -7 4 0 235.97 264.27 2.27 o -6 4 0 108.93 115.15 1.48 o -5 4 0 98.31 96.32 1.23 o -4 4 0 520.95 481.96 2.15 o -3 4 0 359.47 349.59 1.71 o -2 4 0 0.49 0.00 0.39 o -1 4 0 350.58 355.95 1.58 o 0 4 0 1.41 1.78 0.42 o 1 4 0 0.55 0.84 0.46 o 2 4 0 157.50 165.16 1.25 o 3 4 0 79.41 90.48 1.14 o 4 4 0 0.21 5.61 0.98 o 5 4 0 126.25 127.22 1.59 o 6 4 0 16.39 11.07 1.17 o 7 4 0 3.43 3.95 1.64 o 8 4 0 28.26 24.02 2.32 o -8 5 0 1.14 1.34 1.40 o -7 5 0 6.37 5.53 1.22 o -6 5 0 2.71 8.33 1.04 o -5 5 0 20.02 19.91 1.03 o -4 5 0 224.38 204.43 1.63 o -3 5 0 168.71 158.05 1.33 o -2 5 0 0.04 0.00 0.52 o -1 5 0 628.69 592.96 2.27 o 0 5 0 655.88 715.08 2.51 o 1 5 0 63.59 65.75 0.96 o 2 5 0 40.32 45.67 0.92 o 3 5 0 534.38 509.70 2.52 o 4 5 0 288.30 255.99 2.05 o 5 5 0 2.17 1.09 0.99 o 6 5 0 68.59 67.83 1.81 o 7 5 0 101.32 94.44 2.11 o -8 6 0 27.72 32.65 1.87 o -7 6 0 69.92 70.87 1.75 o -6 6 0 321.30 311.87 2.42 o -5 6 0 38.36 37.69 1.14 o -4 6 0 832.56 847.48 3.29 o -3 6 0 1431.41 1382.92 3.95 o -2 6 0 2.87 8.36 0.80 o -1 6 0 1487.06 1360.10 3.76 o 0 6 0 265.22 244.61 1.77 o 1 6 0 77.25 88.70 1.23 o 2 6 0 25.14 25.58 1.09 o 3 6 0 14.74 3.72 1.01 o 4 6 0 26.70 20.72 1.62 o 5 6 0 3.69 7.90 1.46 o 6 6 0 22.06 26.60 1.77 o -7 7 0 5.44 5.51 1.62 o -6 7 0 80.34 77.59 1.68 o -5 7 0 78.67 79.79 1.65 o -4 7 0 49.94 56.32 1.46 o -3 7 0 726.39 674.84 3.10 o -2 7 0 4.69 5.81 0.96 o -1 7 0 576.66 577.04 2.80 o 0 7 0 0.00 3.12 0.95 o 1 7 0 62.71 52.54 1.60 o 2 7 0 13.14 8.60 1.39 o 3 7 0 18.36 9.34 1.17 o 4 7 0 35.94 31.10 1.56 o 5 7 0 0.66 5.25 1.65 o 6 7 0 0.76 3.38 3.74 o -7 8 0 26.15 27.46 2.04 o -6 8 0 36.55 36.74 1.76 o -5 8 0 144.76 150.16 2.11 o -4 8 0 58.16 67.46 1.52 o -3 8 0 0.44 0.00 1.15 o -2 8 0 1.60 0.80 1.19 o -1 8 0 272.91 304.21 2.35 o 0 8 0 95.09 97.77 1.65 o 1 8 0 2.68 4.11 1.10 o 2 8 0 48.20 49.32 1.56 o 3 8 0 193.36 173.38 2.31 o 4 8 0 7.48 9.04 1.52 o 5 8 0 3.94 14.32 3.75 o -6 9 0 4.03 0.00 2.28 o -5 9 0 22.34 32.95 2.14 o -4 9 0 132.91 142.93 2.34 o -3 9 0 297.55 288.00 2.63 o -2 9 0 13.19 14.99 1.43 o -1 9 0 124.30 134.60 2.15 o 0 9 0 152.77 167.48 2.28 o 1 9 0 41.58 43.52 1.84 o 2 9 0 65.08 52.22 1.93 o 3 9 0 9.19 9.22 1.79 o -4 10 0 13.87 20.03 2.18 o -3 10 0 6.06 11.94 2.02 o -2 10 0 0.08 0.00 1.71 o -1 10 0 24.06 21.69 1.93 o 0 10 0 10.69 5.69 1.85 o 1 10 0 1.04 4.41 2.01 o -2 -10 1 4.39 3.91 2.21 o -1 -10 1 8.77 12.18 1.85 o 0 -10 1 29.85 28.27 2.77 o 1 -10 1 5.15 0.00 2.46 o 2 -10 1 6.51 2.83 1.92 o 3 -10 1 4.49 12.52 2.01 o 4 -10 1 10.28 14.64 2.10 o -4 -9 1 3.00 6.06 1.73 o -3 -9 1 8.79 6.02 1.80 o -2 -9 1 120.03 108.78 2.05 o -1 -9 1 0.10 0.41 1.36 o 0 -9 1 2.78 4.04 1.46 o 1 -9 1 135.52 150.05 2.17 o 2 -9 1 227.47 270.71 2.55 o 3 -9 1 0.53 10.46 1.47 o 4 -9 1 68.11 74.29 1.89 o 5 -9 1 285.37 308.49 2.90 o 6 -9 1 31.77 32.06 1.87 o -5 -8 1 71.77 75.41 2.46 o -4 -8 1 2.17 3.95 1.47 o -3 -8 1 195.61 170.14 2.15 o -2 -8 1 103.01 98.40 1.67 o -1 -8 1 25.61 36.70 1.44 o 0 -8 1 7.21 6.16 1.21 o 1 -8 1 146.70 152.55 1.79 o 2 -8 1 50.72 54.62 1.37 o 3 -8 1 10.57 14.04 1.13 o 4 -8 1 35.08 35.25 1.47 o 5 -8 1 10.98 10.07 1.41 o 6 -8 1 0.21 0.00 1.62 o 7 -8 1 43.38 50.92 2.14 o -6 -7 1 31.95 27.30 1.85 o -5 -7 1 21.66 24.51 1.72 o -4 -7 1 10.55 9.16 1.40 o -3 -7 1 41.06 36.07 1.43 o -2 -7 1 2.71 0.00 0.95 o -1 -7 1 0.11 1.04 0.86 o 0 -7 1 14.30 10.33 0.92 o 1 -7 1 13.75 10.49 0.91 o 2 -7 1 40.84 45.29 1.14 o 3 -7 1 178.09 195.68 1.84 o 4 -7 1 8.67 9.72 1.05 o 5 -7 1 600.89 608.49 3.13 o 6 -7 1 26.75 27.50 1.56 o 7 -7 1 314.70 320.94 2.84 o -7 -6 1 2.34 1.27 2.00 o -6 -6 1 3.50 2.47 1.67 o -5 -6 1 12.90 7.01 1.31 o -4 -6 1 14.49 7.19 1.38 o -3 -6 1 113.90 86.85 1.34 o -2 -6 1 203.43 206.82 1.73 o -1 -6 1 0.03 3.10 0.68 o 0 -6 1 94.57 85.97 1.15 o 1 -6 1 190.15 152.18 1.34 o 2 -6 1 135.15 127.28 1.28 o 3 -6 1 62.98 65.37 1.11 o 4 -6 1 206.45 202.81 1.73 o 5 -6 1 1058.97 1097.53 3.80 o 6 -6 1 64.76 72.74 1.54 o 7 -6 1 320.96 329.35 2.65 o 8 -6 1 275.99 287.15 2.78 o -7 -5 1 66.75 67.52 1.86 o -6 -5 1 139.56 126.31 1.86 o -5 -5 1 93.54 75.21 1.70 o -4 -5 1 13.55 8.32 0.87 o -3 -5 1 179.57 144.88 1.44 o -2 -5 1 517.39 470.95 2.18 o -1 -5 1 416.48 464.38 2.04 o 0 -5 1 250.31 233.28 1.44 o 1 -5 1 1055.68 1064.40 2.85 o 2 -5 1 252.16 253.15 1.46 o 3 -5 1 3.43 0.49 0.61 o 4 -5 1 153.80 149.30 1.36 o 5 -5 1 59.29 54.84 1.16 o 6 -5 1 4.58 7.69 0.99 o 7 -5 1 1.21 1.39 1.25 o 8 -5 1 1.92 5.58 1.53 o -8 -4 1 15.25 23.03 1.77 o -7 -4 1 108.02 95.70 2.07 o -6 -4 1 109.05 91.80 1.62 o -5 -4 1 37.11 44.36 1.20 o -4 -4 1 6.58 5.96 0.73 o -3 -4 1 247.74 301.08 1.75 o -2 -4 1 48.33 68.86 0.85 o -1 -4 1 439.96 542.93 1.93 o 0 -4 1 526.77 624.98 49.42 o 1 -4 1 7.85 4.88 0.68 o 2 -4 1 0.78 1.19 0.84 o 3 -4 1 22.25 25.35 0.64 o 4 -4 1 106.33 99.93 1.05 o 5 -4 1 403.57 380.28 2.02 o 6 -4 1 61.37 57.70 1.17 o 7 -4 1 48.93 51.88 1.35 o 8 -4 1 156.47 170.01 2.19 o 9 -4 1 70.46 80.06 3.36 o -8 -3 1 15.62 5.18 1.69 o -7 -3 1 8.44 13.37 1.30 o -6 -3 1 106.59 105.13 1.60 o -5 -3 1 271.62 278.06 1.96 o -4 -3 1 98.13 123.67 1.28 o -3 -3 1 1084.16 1043.56 2.85 o -2 -3 1 1649.13 1595.56 130.44 o -1 -3 1 12.30 12.77 0.87 o 0 -3 1 100.31 62.56 4.69 o 1 -3 1 1781.31 1625.16 41.22 o 2 -3 1 677.18 658.52 4.07 o 3 -3 1 62.56 64.95 2.87 o 4 -3 1 513.71 466.24 1.89 o 5 -3 1 340.38 319.37 1.78 o 6 -3 1 3.80 16.83 0.95 o 7 -3 1 48.12 55.22 1.41 o 8 -3 1 38.08 50.22 1.66 o 9 -3 1 30.63 28.25 2.05 o -9 -2 1 70.79 78.97 2.43 o -8 -2 1 10.90 15.57 1.59 o -7 -2 1 118.86 104.70 1.60 o -6 -2 1 121.83 124.80 1.56 o -5 -2 1 381.58 361.74 2.04 o -4 -2 1 213.39 223.16 1.45 o -3 -2 1 618.77 614.58 2.02 o -2 -2 1 27.68 55.87 0.78 o -1 -2 1 914.12 958.90 15.26 o 0 -2 1 856.26 810.43 26.20 o 1 -2 1 924.65 907.57 12.17 o 2 -2 1 51.86 41.71 0.82 o 3 -2 1 5.69 4.23 1.31 o 4 -2 1 353.53 379.77 1.64 o 5 -2 1 3.54 5.31 0.65 o 6 -2 1 5.06 12.65 0.90 o 7 -2 1 1.89 6.05 1.07 o 8 -2 1 28.35 24.25 1.47 o 9 -2 1 15.13 7.21 1.90 o -9 -1 1 50.76 56.46 2.27 o -8 -1 1 16.25 15.92 1.50 o -7 -1 1 12.54 13.68 1.10 o -6 -1 1 362.32 405.87 2.34 o -5 -1 1 9.68 9.70 0.71 o -4 -1 1 364.26 367.38 1.71 o -3 -1 1 343.60 333.89 21.04 o -2 -1 1 512.83 566.95 5.57 o -1 -1 1 194.36 206.16 0.55 o 0 -1 1 115.17 130.41 3.16 o 1 -1 1 2461.97 2463.54 50.16 o 2 -1 1 638.30 651.33 14.38 o 3 -1 1 1.73 2.02 0.52 o 4 -1 1 4302.81 4896.92 5.68 o 5 -1 1 396.62 420.52 1.99 o 6 -1 1 804.95 934.24 3.28 o 7 -1 1 74.02 86.09 1.56 o 8 -1 1 24.92 30.35 1.56 o 9 -1 1 12.60 24.08 1.92 o -9 0 1 33.93 24.20 1.65 o -8 0 1 8.43 12.88 1.40 o -7 0 1 13.78 12.16 1.10 o -6 0 1 210.13 215.56 1.78 o -5 0 1 313.68 360.10 1.91 o -4 0 1 598.25 599.52 2.12 o -3 0 1 674.87 591.84 28.06 o -2 0 1 506.43 460.14 5.76 o -1 0 1 750.54 796.33 12.55 o 0 0 1 58.97 95.34 1.94 o 1 0 1 1762.46 1890.10 11.13 o 3 0 1 46.63 48.37 1.98 o 5 0 1 373.55 367.86 1.93 o 6 0 1 146.47 168.69 1.71 o 7 0 1 274.30 299.84 2.30 o 8 0 1 0.40 0.00 1.32 o 9 0 1 7.21 8.24 2.06 o -9 1 1 94.03 121.94 2.24 o -8 1 1 6.53 14.36 1.50 o -7 1 1 77.98 75.36 1.42 o -6 1 1 477.18 491.26 2.46 o -5 1 1 299.80 282.34 1.67 o -4 1 1 17.97 14.93 0.55 o -3 1 1 823.02 700.38 1.38 o -2 1 1 134.58 110.27 1.82 o -1 1 1 3.66 5.06 0.15 o 0 1 1 1497.92 1561.24 28.66 o 1 1 1 13.88 28.03 0.77 o 2 1 1 958.50 979.30 13.66 o 3 1 1 4.35 5.74 0.26 o 4 1 1 23.78 22.05 0.63 o 5 1 1 25.48 24.94 0.88 o 6 1 1 62.93 69.82 1.40 o 7 1 1 0.16 0.00 0.92 o 8 1 1 53.83 63.56 1.80 o -9 2 1 0.71 0.00 1.48 o -8 2 1 87.06 76.59 1.69 o -7 2 1 0.76 0.00 1.01 o -6 2 1 128.45 124.47 1.43 o -5 2 1 23.14 27.49 0.78 o -4 2 1 206.64 192.97 1.29 o -3 2 1 224.67 208.09 9.15 o -2 2 1 88.03 84.54 0.69 o -1 2 1 132.21 106.68 4.84 o 0 2 1 47.33 54.03 2.30 o 1 2 1 440.66 430.02 4.64 o 2 2 1 530.50 572.68 29.06 o 3 2 1 8.32 5.60 0.49 o 4 2 1 579.32 568.55 40.70 o 5 2 1 313.13 306.46 15.49 o 6 2 1 7.04 7.71 1.61 o 7 2 1 138.52 145.08 2.02 o 8 2 1 73.76 74.39 2.07 o -9 3 1 46.07 52.55 1.96 o -8 3 1 131.41 128.62 1.90 o -7 3 1 14.28 9.95 1.10 o -6 3 1 859.41 848.37 3.28 o -5 3 1 322.01 328.10 1.92 o -4 3 1 712.99 719.24 2.50 o -3 3 1 1111.38 1045.74 2.72 o -2 3 1 325.46 300.64 8.04 o -1 3 1 118.64 102.01 0.78 o 0 3 1 1379.14 1400.51 11.47 o 1 3 1 639.92 600.37 13.26 o 2 3 1 188.53 193.21 1.27 o 3 3 1 193.80 224.85 1.50 o 4 3 1 431.77 409.68 2.15 o 5 3 1 65.52 62.66 1.23 o 6 3 1 12.34 15.84 1.38 o 7 3 1 24.25 17.56 1.65 o 8 3 1 84.17 96.00 2.37 o -9 4 1 57.47 67.89 2.14 o -8 4 1 8.70 5.26 1.28 o -7 4 1 138.50 128.89 1.73 o -6 4 1 475.93 431.52 2.58 o -5 4 1 58.44 63.37 1.12 o -4 4 1 62.06 60.86 0.94 o -3 4 1 356.10 328.35 1.74 o -2 4 1 647.12 563.55 2.10 o -1 4 1 19.76 13.75 0.52 o 0 4 1 99.33 99.08 0.95 o 1 4 1 175.76 173.56 1.27 o 2 4 1 0.54 0.00 0.57 o 3 4 1 7.20 4.93 0.72 o 4 4 1 96.74 103.15 1.43 o 5 4 1 27.02 23.64 1.39 o 6 4 1 13.16 14.96 1.47 o 7 4 1 68.79 71.88 2.10 o -8 5 1 1.57 1.69 1.62 o -7 5 1 4.55 6.19 1.21 o -6 5 1 9.66 10.38 1.10 o -5 5 1 70.24 74.52 1.34 o -4 5 1 59.43 51.89 1.02 o -3 5 1 273.17 237.39 1.67 o -2 5 1 287.59 270.68 1.70 o -1 5 1 29.16 26.42 0.72 o 0 5 1 594.17 582.09 2.36 o 1 5 1 944.12 867.79 2.96 o 2 5 1 81.01 72.48 1.13 o 3 5 1 277.35 283.74 2.05 o 4 5 1 340.30 312.07 2.23 o 5 5 1 35.39 35.16 1.45 o 6 5 1 1.60 1.47 1.50 o 7 5 1 33.60 32.33 1.92 o -8 6 1 0.26 6.29 1.53 o -7 6 1 21.76 15.09 1.43 o -6 6 1 319.77 319.96 2.45 o -5 6 1 43.56 35.48 1.31 o -4 6 1 5.86 11.37 0.97 o -3 6 1 33.19 33.67 1.06 o -2 6 1 1032.45 978.40 3.39 o -1 6 1 299.45 257.19 1.84 o 0 6 1 478.20 539.01 2.59 o 1 6 1 1408.18 1452.64 4.23 o 2 6 1 43.83 34.74 1.21 o 3 6 1 777.37 773.72 3.52 o 4 6 1 69.54 64.30 1.55 o 5 6 1 48.34 41.19 1.80 o 6 6 1 3.44 1.25 1.93 o -7 7 1 162.37 168.01 2.45 o -6 7 1 35.38 35.99 1.56 o -5 7 1 92.95 89.21 1.65 o -4 7 1 10.38 11.54 1.14 o -3 7 1 1.97 3.47 1.17 o -2 7 1 12.97 11.50 0.98 o -1 7 1 226.12 234.36 2.09 o 0 7 1 1.14 7.42 1.50 o 1 7 1 509.65 499.06 2.95 o 2 7 1 11.80 13.53 1.54 o 3 7 1 73.63 55.66 1.46 o 4 7 1 7.81 11.45 1.55 o 5 7 1 9.37 9.46 1.91 o -7 8 1 0.00 1.58 1.92 o -6 8 1 34.78 34.02 1.83 o -5 8 1 0.00 0.00 1.53 o -4 8 1 0.06 5.53 1.44 o -3 8 1 179.24 168.70 1.99 o -2 8 1 116.75 105.46 1.73 o -1 8 1 104.08 110.94 1.79 o 0 8 1 78.93 76.10 1.69 o 1 8 1 241.42 225.33 2.31 o 2 8 1 5.88 2.51 1.37 o 3 8 1 153.34 135.45 2.36 o 4 8 1 62.70 63.94 2.20 o -5 9 1 1.13 10.18 1.69 o -4 9 1 81.82 87.36 2.13 o -3 9 1 154.15 145.84 2.17 o -2 9 1 46.77 47.55 1.69 o -1 9 1 17.95 21.47 1.74 o 0 9 1 115.44 116.78 2.10 o 1 9 1 145.42 128.32 2.24 o 2 9 1 4.21 0.88 1.81 o 3 9 1 1.02 0.00 2.16 o -3 10 1 1.93 3.65 2.04 o -2 10 1 0.20 0.00 1.96 o -1 10 1 6.51 0.00 1.85 o 0 10 1 3.10 2.31 2.02 o -2 -10 2 34.22 41.83 2.05 o -1 -10 2 37.35 53.34 2.76 o 0 -10 2 2.31 1.76 1.75 o 1 -10 2 43.35 50.09 2.02 o 2 -10 2 14.05 24.78 2.00 o 3 -10 2 0.92 1.03 1.96 o 4 -10 2 15.48 23.79 2.02 o -4 -9 2 0.77 0.00 2.10 o -3 -9 2 7.39 3.44 1.61 o -2 -9 2 31.16 32.87 1.68 o -1 -9 2 29.46 29.35 1.70 o 0 -9 2 44.84 51.44 1.62 o 1 -9 2 57.66 65.68 1.67 o 2 -9 2 159.35 193.40 2.24 o 3 -9 2 50.95 69.59 1.79 o 4 -9 2 15.83 14.59 1.64 o 5 -9 2 80.29 99.41 2.12 o 6 -9 2 123.14 140.19 2.77 o -5 -8 2 143.51 129.39 2.45 o -4 -8 2 75.13 65.32 1.87 o -3 -8 2 2.42 1.93 1.28 o -2 -8 2 115.77 113.26 1.78 o -1 -8 2 254.92 277.11 2.28 o 0 -8 2 36.45 39.12 7.46 o 1 -8 2 107.07 106.55 1.54 o 2 -8 2 103.98 105.01 2.35 o 3 -8 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178.99 4.27 o 4 -2 10 4.25 5.55 1.82 o -7 -1 10 191.26 190.12 2.65 o -6 -1 10 12.70 14.98 1.59 o -5 -1 10 298.78 325.96 2.45 o -4 -1 10 64.01 63.97 1.12 o -3 -1 10 78.23 66.41 1.60 o -2 -1 10 41.48 31.90 1.37 o -1 -1 10 186.31 167.27 1.97 o 0 -1 10 14.08 16.07 1.39 o 1 -1 10 0.55 9.85 1.49 o 2 -1 10 63.61 62.85 3.81 o 3 -1 10 13.27 5.97 1.91 o -7 0 10 14.41 13.86 2.15 o -6 0 10 0.50 4.16 1.76 o -5 0 10 17.82 13.43 1.55 o -4 0 10 24.74 29.70 2.40 o -3 0 10 0.91 2.24 0.84 o -2 0 10 82.98 91.73 1.81 o -1 0 10 121.81 126.76 1.96 o 0 0 10 9.35 11.01 1.46 o 1 0 10 2.36 0.00 1.41 o 2 0 10 137.01 134.47 2.24 o 3 0 10 47.82 47.07 2.12 o -6 1 10 20.25 13.74 1.81 o -5 1 10 162.44 162.93 2.20 o -4 1 10 218.59 238.17 2.18 o -3 1 10 8.92 5.53 2.00 o -2 1 10 152.54 149.14 2.12 o -1 1 10 229.09 203.39 4.03 o 0 1 10 68.65 61.83 2.01 o 1 1 10 107.26 96.42 2.08 o 2 1 10 201.19 193.43 2.55 o -6 2 10 26.67 33.34 2.22 o -5 2 10 288.13 281.84 2.76 o -4 2 10 39.19 43.09 1.73 o -3 2 10 16.24 14.84 2.46 o -2 2 10 105.48 105.55 1.99 o -1 2 10 5.48 0.00 1.58 o 0 2 10 41.26 37.24 1.90 o 1 2 10 17.70 15.77 1.85 o 2 2 10 3.41 0.00 1.94 o -5 3 10 6.84 2.76 2.05 o -4 3 10 2.44 0.00 1.85 o -3 3 10 18.16 18.94 1.28 o -2 3 10 3.93 3.25 1.79 o -1 3 10 397.47 392.59 3.15 o 0 3 10 165.60 183.87 2.57 o -2 -8 11 18.70 11.43 1.78 o -1 -8 11 22.52 38.19 1.96 o 0 -8 11 103.07 129.23 2.51 o -4 -7 11 16.88 15.94 1.74 o -3 -7 11 73.28 88.33 2.00 o -2 -7 11 53.83 84.92 2.14 o -1 -7 11 17.05 20.31 1.66 o 0 -7 11 191.39 218.73 2.73 o 1 -7 11 29.91 23.59 2.31 o -4 -6 11 13.14 13.13 1.71 o -3 -6 11 0.08 1.07 1.74 o -2 -6 11 59.06 63.73 1.88 o -1 -6 11 29.82 26.43 1.50 o 0 -6 11 0.01 0.64 1.56 o 1 -6 11 0.56 0.00 1.64 o 2 -6 11 3.31 0.00 1.31 o -5 -5 11 1.32 4.17 1.70 o -4 -5 11 159.11 186.37 2.38 o -3 -5 11 220.55 230.30 2.39 o -2 -5 11 4.77 7.09 1.50 o -1 -5 11 80.13 76.67 1.88 o 0 -5 11 157.15 160.87 2.23 o 1 -5 11 59.00 52.30 1.77 o 2 -5 11 21.06 22.93 1.78 o 3 -5 11 74.23 64.29 3.49 o -6 -4 11 67.59 53.59 1.84 o 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10.05 2.09 o -5 0 11 42.71 49.75 1.84 o -4 0 11 36.50 35.79 1.87 o -3 0 11 1.35 0.00 1.41 o -2 0 11 0.90 0.00 1.39 o -1 0 11 9.29 13.61 1.67 o 0 0 11 140.00 145.08 4.07 o 1 0 11 24.90 32.14 2.00 o -4 1 11 275.63 257.24 2.79 o -3 1 11 37.38 33.80 1.77 o -2 1 11 0.71 0.00 1.69 o -1 1 11 221.51 225.02 2.73 o 0 1 11 169.93 168.63 2.53 o 1 1 11 1.16 10.24 2.14 o -4 2 11 92.42 100.71 2.36 o -3 2 11 96.77 100.44 2.24 o -2 2 11 2.92 5.43 1.75 o -1 2 11 93.04 96.22 2.31 o -3 -6 12 0.02 0.02 1.74 o -2 -6 12 4.49 6.43 1.76 o -1 -6 12 3.18 10.98 1.85 o 0 -6 12 34.69 37.82 2.45 o -4 -5 12 23.83 43.39 2.05 o -3 -5 12 127.56 157.27 2.55 o -2 -5 12 68.09 73.85 2.23 o -1 -5 12 40.86 36.73 2.09 o 0 -5 12 140.36 139.60 2.53 o 1 -5 12 164.14 141.98 3.07 o -4 -4 12 31.17 58.40 2.18 o -3 -4 12 31.33 25.66 2.00 o -2 -4 12 169.67 138.34 2.33 o -1 -4 12 0.24 7.70 1.61 o 0 -4 12 66.81 59.31 1.95 o 1 -4 12 22.33 29.92 2.46 o -4 -3 12 8.75 13.40 1.93 o -3 -3 12 0.63 0.00 1.66 o -2 -3 12 1.14 3.08 1.44 o -1 -3 12 0.59 0.10 1.51 o 0 -3 12 38.90 29.84 1.81 o 1 -3 12 10.90 9.47 1.90 o -4 -2 12 9.27 5.67 1.86 o -3 -2 12 198.95 205.73 2.75 o -2 -2 12 161.14 132.24 2.26 o -1 -2 12 1.74 0.00 1.71 o 0 -2 12 108.97 109.44 2.33 o 1 -2 12 313.40 293.77 3.19 o -4 -1 12 11.78 14.80 2.52 o -3 -1 12 5.12 0.00 1.55 o -2 -1 12 93.97 88.21 2.34 o -1 -1 12 57.24 66.35 2.13 o 0 -1 12 25.91 20.89 1.99 o -3 0 12 115.85 122.36 2.95 o -2 0 12 38.60 37.28 1.99 o -1 0 12 16.09 13.39 1.88 o