#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/06/2010622.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2010622_Fobs loop_ _publ_author_name 'Camus, Fabrice' 'Norberg, Bernadette' 'Legrand, Anne' 'Rigo, Benoit' 'Durant, Fran\,cois' 'Wouters, Johan' _publ_section_title ; Structural analysis of pyrrolidinones ; _journal_issue 2 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 193 _journal_page_last 196 _journal_volume 56 _journal_year 2000 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 98.104 _cell_angle_gamma 90.000 _cell_length_a 9.9090 _cell_length_b 8.5190 _cell_length_c 23.7930 _exptl_crystal_F_000 824.00 _reflns_d_resolution_high .8110 _[local]_cod_data_source_file gs1054IIIsup4.hkl _[local]_cod_data_source_block III #BEGIN Tags that were not found in dictionaries: _shelx_title ' compoundIII P21/c z=4' _shelx_refln_list_code 4 _shelx_f_calc_maximum 185.83 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1722.15 1411.35 4.58 o 2 0 0 37.71 25.76 .21 o 3 0 0 228.35 202.73 .70 o 4 0 0 308.24 289.78 1.16 o 5 0 0 1651.05 1685.91 3.28 o 6 0 0 .05 .34 .06 o 7 0 0 55.68 55.84 .97 o 8 0 0 2.34 2.46 .19 o 9 0 0 113.90 94.26 1.44 o 10 0 0 4.03 2.75 .15 o 11 0 0 19.64 21.84 .45 o 12 0 0 7.68 6.86 .15 o 1 1 0 1608.96 1458.61 5.69 o 2 1 0 7910.62 8038.86 20.15 o 3 1 0 1850.43 1769.11 2.53 o 4 1 0 154.70 114.88 .76 o 5 1 0 3380.21 3681.63 4.98 o 6 1 0 75.87 76.97 .71 o 7 1 0 26.02 35.46 .57 o 8 1 0 114.73 109.57 1.49 o 9 1 0 5.95 4.58 .19 o 10 1 0 98.90 90.86 1.34 o 11 1 0 11.29 13.57 .30 o 12 1 0 4.06 4.34 .13 o 0 2 0 5451.12 5705.84 20.61 o 1 2 0 12.42 20.42 .25 o 2 2 0 643.82 632.47 1.46 o 3 2 0 1577.72 1627.29 2.68 o 4 2 0 572.78 513.29 1.72 o 5 2 0 69.72 71.71 .74 o 6 2 0 1.45 3.94 .09 o 7 2 0 151.64 137.81 1.55 o 8 2 0 111.44 112.30 1.54 o 9 2 0 146.40 140.58 1.74 o 10 2 0 2.70 3.12 .15 o 11 2 0 .86 1.82 .12 o 1 3 0 393.45 411.39 1.13 o 2 3 0 206.70 192.33 .82 o 3 3 0 1663.83 1699.83 3.10 o 4 3 0 .67 1.47 .07 o 5 3 0 19.76 27.02 .31 o 6 3 0 206.02 189.73 1.23 o 7 3 0 9.21 10.23 .26 o 8 3 0 113.58 114.25 1.58 o 9 3 0 44.83 41.40 .80 o 10 3 0 19.14 14.18 .29 o 11 3 0 .00 .02 .22 o 0 4 0 125.47 155.60 1.16 o 1 4 0 903.71 904.70 2.31 o 2 4 0 1.81 1.16 .06 o 3 4 0 148.40 150.95 .92 o 4 4 0 9.00 11.35 .18 o 5 4 0 516.72 502.03 2.28 o 6 4 0 64.25 64.90 1.14 o 7 4 0 7.19 6.38 .24 o 8 4 0 40.77 44.37 .71 o 9 4 0 2.97 2.61 .16 o 10 4 0 1.90 2.51 .14 o 11 4 0 1.67 1.35 .11 o 1 5 0 378.44 388.25 1.77 o 2 5 0 111.14 96.27 .92 o 3 5 0 773.33 798.47 2.76 o 4 5 0 31.07 28.89 .51 o 5 5 0 18.56 18.72 .38 o 6 5 0 111.37 103.92 1.50 o 7 5 0 149.04 149.09 1.80 o 8 5 0 27.17 32.00 .60 o 9 5 0 1.05 1.98 .14 o 10 5 0 1.34 1.68 .11 o 0 6 0 28.80 25.25 .48 o 1 6 0 38.73 42.13 .86 o 2 6 0 195.07 217.18 1.90 o 3 6 0 8.38 6.54 .21 o 4 6 0 68.79 63.21 1.15 o 5 6 0 17.69 19.14 .42 o 6 6 0 117.67 126.31 1.65 o 7 6 0 .17 1.57 .16 o 8 6 0 2.93 2.63 .15 o 9 6 0 5.73 5.53 .16 o 1 7 0 370.16 360.99 2.64 o 2 7 0 68.65 74.07 1.28 o 3 7 0 32.86 31.82 .63 o 4 7 0 .03 1.06 .18 o 5 7 0 102.87 104.75 1.52 o 6 7 0 .67 1.76 .16 o 7 7 0 37.96 39.46 .63 o 8 7 0 5.57 7.12 .18 o 9 7 0 4.25 4.25 .13 o 0 8 0 84.80 92.64 2.02 o 1 8 0 81.21 81.54 1.36 o 2 8 0 119.01 118.79 1.62 o 3 8 0 5.67 7.32 .21 o 4 8 0 8.94 9.04 .22 o 5 8 0 4.86 6.89 .19 o 6 8 0 7.39 5.74 .19 o 7 8 0 5.19 6.09 .16 o 1 9 0 22.44 20.65 .43 o 2 9 0 49.18 47.46 .97 o 3 9 0 149.24 142.73 1.55 o 4 9 0 .21 .18 .16 o 5 9 0 11.17 9.53 .19 o 6 9 0 22.23 18.10 .33 o 0 10 0 70.69 73.02 1.39 o 1 10 0 72.86 74.21 .97 o 2 10 0 2.43 2.45 .12 o 3 10 0 1.01 1.10 .10 o -12 1 1 15.15 22.98 .66 o -11 1 1 .09 .02 .35 o -10 1 1 9.97 9.62 .32 o -9 1 1 52.56 44.88 1.01 o -8 1 1 235.43 250.77 3.09 o -7 1 1 142.22 143.10 2.16 o -6 1 1 158.22 199.33 1.59 o -5 1 1 2290.21 2606.49 5.08 o -4 1 1 510.97 509.03 1.93 o -3 1 1 1773.36 1657.68 2.98 o -2 1 1 359.74 312.97 1.06 o -1 1 1 528.16 523.60 1.12 o 0 1 1 256.50 197.68 .61 o 1 1 1 3774.72 3456.78 13.09 o 2 1 1 253.82 224.24 .92 o 3 1 1 .39 1.51 .05 o 4 1 1 204.65 215.00 1.28 o 5 1 1 11.12 15.18 .32 o 6 1 1 99.38 79.36 1.03 o 7 1 1 6.07 5.45 .28 o 8 1 1 382.65 360.62 3.71 o 9 1 1 7.79 3.89 .27 o 10 1 1 2.90 1.82 .20 o 11 1 1 .13 .92 .16 o -11 2 1 3.83 5.59 .23 o -10 2 1 43.62 39.61 .90 o -9 2 1 .00 .22 .22 o -8 2 1 10.58 12.92 .42 o -7 2 1 163.69 165.52 2.39 o -6 2 1 26.83 25.47 .45 o -5 2 1 49.21 50.90 .77 o -4 2 1 251.76 239.85 1.43 o -3 2 1 978.39 1006.80 2.56 o -2 2 1 973.89 973.55 2.21 o -1 2 1 3792.78 4027.13 17.82 o 0 2 1 23980.55 22036.83 53.47 o 1 2 1 10363.22 11151.75 31.39 o 2 2 1 2064.70 1904.23 3.15 o 3 2 1 8.25 4.86 .11 o 4 2 1 3476.09 3730.93 5.76 o 5 2 1 199.87 207.53 1.53 o 6 2 1 2.48 2.99 .13 o 7 2 1 115.67 115.70 2.02 o 8 2 1 307.71 288.37 3.38 o 9 2 1 42.72 35.35 .93 o 10 2 1 12.99 11.04 .34 o 11 2 1 2.31 2.44 .19 o -11 3 1 3.24 5.70 .22 o -10 3 1 .07 .67 .18 o -9 3 1 86.82 84.12 1.90 o -8 3 1 688.37 737.52 5.47 o -7 3 1 .13 .78 .26 o -6 3 1 129.56 138.87 1.48 o -5 3 1 76.11 83.02 1.04 o -4 3 1 465.21 478.50 2.23 o -3 3 1 215.82 213.34 1.35 o -2 3 1 69.05 117.94 .91 o -1 3 1 32.05 27.06 .43 o 0 3 1 110.06 111.35 .82 o 1 3 1 772.00 636.77 2.00 o 2 3 1 715.41 700.57 2.24 o 3 3 1 898.37 923.91 2.81 o 4 3 1 2.86 3.65 .11 o 5 3 1 226.14 204.37 1.64 o 6 3 1 172.75 168.61 2.34 o 7 3 1 332.01 326.91 3.47 o 8 3 1 32.78 32.99 .92 o 9 3 1 5.73 8.94 .31 o 10 3 1 61.09 50.47 1.35 o 11 3 1 17.58 15.98 .47 o -11 4 1 3.16 4.55 .17 o -10 4 1 6.25 5.99 .25 o -9 4 1 102.03 101.13 2.03 o -8 4 1 37.20 33.89 .90 o -7 4 1 8.27 6.56 .34 o -6 4 1 37.21 31.35 .83 o -5 4 1 .12 1.06 .11 o -4 4 1 35.65 43.26 .78 o -3 4 1 772.43 809.26 2.99 o -2 4 1 730.52 743.24 2.68 o -1 4 1 2.37 5.01 .12 o 0 4 1 9.42 8.66 .18 o 1 4 1 30.18 32.17 .56 o 2 4 1 59.77 54.89 .75 o 3 4 1 157.84 161.22 1.35 o 4 4 1 152.86 151.33 1.42 o 5 4 1 106.51 115.67 1.37 o 6 4 1 124.36 129.20 2.18 o 7 4 1 31.69 29.91 .83 o 8 4 1 9.65 9.09 .31 o 9 4 1 22.85 24.77 .75 o 10 4 1 12.09 9.90 .32 o 11 4 1 4.41 6.29 .21 o -10 5 1 .08 .21 .33 o -9 5 1 1.04 .67 .19 o -8 5 1 4.16 5.54 .28 o -7 5 1 442.36 451.73 4.40 o -6 5 1 372.33 370.12 3.83 o -5 5 1 127.14 132.26 2.21 o -4 5 1 71.89 74.78 1.55 o -3 5 1 45.38 47.29 .85 o -2 5 1 47.74 61.77 .92 o -1 5 1 .20 1.08 .08 o 0 5 1 244.77 252.40 1.74 o 1 5 1 154.82 138.74 1.31 o 2 5 1 23.96 24.14 .43 o 3 5 1 42.36 34.64 .60 o 4 5 1 28.57 28.99 .74 o 5 5 1 .31 .98 .25 o 6 5 1 138.78 133.72 2.36 o 7 5 1 21.35 18.56 .52 o 8 5 1 .45 5.74 .25 o 9 5 1 2.66 3.84 .23 o 10 5 1 8.09 10.27 .28 o -9 6 1 9.00 9.45 .27 o -8 6 1 28.18 31.05 .83 o -7 6 1 4.22 3.23 .26 o -6 6 1 40.31 39.71 1.00 o -5 6 1 86.40 94.30 2.04 o -4 6 1 38.01 41.23 .95 o -3 6 1 15.74 13.56 .41 o -2 6 1 6.56 3.82 .26 o -1 6 1 155.89 135.62 2.10 o 0 6 1 46.33 49.16 .91 o 1 6 1 47.30 39.92 1.19 o 2 6 1 53.04 70.12 1.59 o 3 6 1 6.76 13.03 .37 o 4 6 1 174.28 177.37 2.62 o 5 6 1 3.38 3.49 .30 o 6 6 1 66.40 71.08 1.88 o 7 6 1 23.87 21.34 .75 o 8 6 1 78.28 75.57 1.65 o 9 6 1 1.36 1.66 .17 o -9 7 1 13.58 19.08 .45 o -8 7 1 3.91 5.46 .24 o -7 7 1 23.01 25.81 .73 o -6 7 1 4.50 5.98 .28 o -5 7 1 17.08 17.42 .49 o -4 7 1 1.19 2.17 .23 o -3 7 1 172.90 206.42 2.90 o -2 7 1 422.14 424.51 4.10 o -1 7 1 24.96 28.07 .85 o 0 7 1 77.98 78.35 1.78 o 1 7 1 96.61 91.90 1.98 o 2 7 1 81.38 83.26 1.87 o 3 7 1 86.35 83.98 1.91 o 4 7 1 4.94 4.40 .26 o 5 7 1 .09 1.64 .25 o 6 7 1 206.62 201.33 2.83 o 7 7 1 36.07 38.93 .87 o 8 7 1 2.48 3.30 .20 o -7 8 1 40.93 38.76 1.05 o -6 8 1 38.69 42.46 1.23 o -5 8 1 58.52 57.37 1.54 o -4 8 1 85.20 87.42 1.91 o -3 8 1 3.04 2.63 .24 o -2 8 1 83.99 78.54 1.87 o -1 8 1 345.21 363.03 3.93 o 0 8 1 38.00 38.21 .98 o 1 8 1 2.30 2.00 .25 o 2 8 1 160.43 166.78 2.67 o 3 8 1 103.97 101.24 2.11 o 4 8 1 12.43 14.87 .44 o 5 8 1 29.87 29.33 .80 o 6 8 1 25.10 27.91 .71 o 7 8 1 31.23 29.39 .63 o -6 9 1 34.02 34.29 .89 o -5 9 1 70.78 77.38 1.48 o -4 9 1 .00 .03 .39 o -3 9 1 2.83 2.56 .24 o -2 9 1 .00 1.16 .19 o -1 9 1 2.48 2.25 .21 o 0 9 1 19.42 20.36 .57 o 1 9 1 42.24 40.13 .91 o 2 9 1 .09 .19 .17 o 3 9 1 22.70 19.53 .53 o 4 9 1 20.39 17.10 .57 o 5 9 1 105.28 103.47 1.65 o 6 9 1 3.14 2.93 .18 o -3 10 1 21.63 21.55 .51 o -2 10 1 8.88 10.81 .29 o -1 10 1 2.00 1.49 .17 o 0 10 1 .18 .02 .34 o 1 10 1 7.87 6.20 .23 o 2 10 1 1.35 1.69 .16 o 3 10 1 9.02 8.62 .24 o -12 0 2 6.87 4.73 .18 o -11 0 2 2.69 2.21 .19 o -10 0 2 1.20 6.30 .28 o -9 0 2 143.47 123.17 2.30 o -8 0 2 24.10 22.98 .71 o -7 0 2 814.87 788.68 4.97 o -6 0 2 222.34 193.89 1.55 o -5 0 2 2343.01 2479.91 4.86 o -4 0 2 4201.68 4356.55 23.99 o -3 0 2 2770.79 2548.33 15.39 o -2 0 2 339.93 224.92 .85 o -1 0 2 865.30 842.03 5.37 o 0 0 2 2963.36 2839.74 8.68 o 1 0 2 13656.98 16942.02 30.12 o 2 0 2 2351.31 2082.33 11.92 o 3 0 2 .01 .51 .04 o 4 0 2 2866.79 2941.80 4.73 o 5 0 2 1429.89 1565.12 3.96 o 6 0 2 78.54 58.57 .89 o 7 0 2 112.43 101.90 1.85 o 8 0 2 1.21 5.54 .31 o 9 0 2 29.01 29.02 .84 o 10 0 2 11.70 10.81 .29 o 11 0 2 .00 .02 .37 o -12 1 2 .11 .22 .14 o -11 1 2 .56 1.28 .19 o -10 1 2 84.27 77.26 1.79 o -9 1 2 7.16 3.66 .24 o -8 1 2 76.66 78.77 1.80 o -7 1 2 .08 .07 .15 o -6 1 2 23.04 15.67 .34 o -5 1 2 2799.93 3093.67 5.54 o -4 1 2 2453.21 2603.69 4.41 o -3 1 2 178.98 161.52 .93 o -2 1 2 4156.23 3722.20 16.47 o -1 1 2 18128.85 21203.06 37.70 o 0 1 2 513.45 558.40 1.12 o 1 1 2 974.94 913.84 1.61 o 2 1 2 1311.56 1258.84 2.28 o 3 1 2 636.22 524.09 1.74 o 4 1 2 982.94 943.33 2.72 o 5 1 2 774.59 758.29 2.81 o 6 1 2 57.67 43.84 .79 o 7 1 2 .00 .70 .22 o 8 1 2 108.96 108.74 2.13 o 9 1 2 213.12 186.60 2.82 o 10 1 2 7.43 10.02 .30 o 11 1 2 3.12 2.70 .19 o -11 2 2 .63 .67 .17 o -10 2 2 12.43 11.95 .37 o -9 2 2 95.63 88.81 1.96 o -8 2 2 10.76 15.42 .45 o -7 2 2 .91 2.86 .28 o -6 2 2 58.15 63.45 .95 o -5 2 2 178.21 176.69 1.40 o -4 2 2 1450.38 1502.22 3.58 o -3 2 2 141.24 124.44 .90 o -2 2 2 284.41 271.66 1.18 o -1 2 2 2910.29 2663.31 14.63 o 0 2 2 287.44 281.98 1.06 o 1 2 2 18068.38 20050.37 45.05 o 2 2 2 291.38 288.09 1.24 o 3 2 2 598.56 591.26 2.02 o 4 2 2 292.39 272.25 1.56 o 5 2 2 44.10 50.06 .79 o 6 2 2 809.73 742.38 3.29 o 7 2 2 26.66 22.61 .71 o 8 2 2 104.70 98.97 2.06 o 9 2 2 22.29 17.64 .58 o 10 2 2 59.59 53.12 1.44 o 11 2 2 12.49 12.45 .38 o -11 3 2 3.12 4.38 .20 o -10 3 2 19.24 21.22 .67 o -9 3 2 65.30 58.60 1.64 o -8 3 2 361.81 372.36 3.91 o -7 3 2 45.37 41.75 .94 o -6 3 2 7.28 8.16 .16 o -5 3 2 32.14 38.45 .73 o -4 3 2 2469.43 2632.95 5.25 o -3 3 2 714.97 701.05 2.43 o -2 3 2 30.77 30.23 .49 o -1 3 2 783.87 796.80 2.25 o 0 3 2 4457.53 4366.52 22.67 o 1 3 2 102.61 126.58 .91 o 2 3 2 260.19 259.38 1.38 o 3 3 2 4.35 11.76 .25 o 4 3 2 745.49 683.20 2.72 o 5 3 2 180.70 180.55 1.56 o 6 3 2 3.31 2.70 .19 o 7 3 2 2.60 1.70 .27 o 8 3 2 47.21 47.09 1.05 o 9 3 2 18.09 15.97 .45 o 10 3 2 12.63 11.35 .33 o 11 3 2 16.91 12.22 .35 o -11 4 2 1.03 .35 .14 o -10 4 2 2.67 4.45 .23 o -9 4 2 .29 .92 .19 o -8 4 2 .12 .12 .57 o -7 4 2 138.67 142.21 2.41 o -6 4 2 6.70 4.74 .29 o -5 4 2 .07 .19 .26 o -4 4 2 308.44 333.35 2.08 o -3 4 2 214.48 257.30 1.69 o -2 4 2 3043.27 3359.05 5.77 o -1 4 2 19.80 44.98 .66 o 0 4 2 235.26 249.50 1.48 o 1 4 2 89.43 112.70 1.03 o 2 4 2 5.60 6.95 .15 o 3 4 2 8.23 2.99 .11 o 4 4 2 636.50 622.23 2.89 o 5 4 2 118.81 109.71 1.88 o 6 4 2 55.37 66.00 1.61 o 7 4 2 76.52 67.34 1.72 o 8 4 2 1.16 2.00 .22 o 9 4 2 20.64 22.26 .71 o 10 4 2 2.57 2.91 .21 o 11 4 2 .34 1.24 .14 o -10 5 2 2.15 2.46 .19 o -9 5 2 .20 1.17 .20 o -8 5 2 17.74 20.90 .60 o -7 5 2 54.79 69.93 1.82 o -6 5 2 23.79 26.37 .68 o -5 5 2 44.31 46.14 1.34 o -4 5 2 28.82 35.48 .80 o -3 5 2 13.47 14.85 .30 o -2 5 2 725.29 705.68 3.03 o -1 5 2 11.37 9.45 .20 o 0 5 2 23.40 30.05 .63 o 1 5 2 70.72 82.79 1.04 o 2 5 2 31.78 43.50 .79 o 3 5 2 8.15 8.08 .19 o 4 5 2 .82 1.81 .26 o 5 5 2 7.79 7.58 .33 o 6 5 2 304.94 341.65 3.72 o 7 5 2 244.76 221.83 3.10 o 8 5 2 9.03 6.73 .26 o 9 5 2 .05 .02 .39 o 10 5 2 .16 .19 .14 o -10 6 2 7.29 9.28 .27 o -9 6 2 .31 .54 .16 o -8 6 2 1.87 2.16 .22 o -7 6 2 390.68 397.90 4.07 o -6 6 2 27.53 23.91 .82 o -5 6 2 146.67 146.77 2.52 o -4 6 2 5.85 4.71 .33 o -3 6 2 84.84 80.16 1.72 o -2 6 2 45.79 44.13 1.25 o -1 6 2 123.18 122.87 2.00 o 0 6 2 25.63 25.31 .66 o 1 6 2 171.01 177.72 2.41 o 2 6 2 366.05 356.20 3.45 o 3 6 2 11.82 12.59 .38 o 4 6 2 10.09 9.40 .36 o 5 6 2 69.88 67.23 1.72 o 6 6 2 616.64 586.34 5.02 o 7 6 2 76.78 68.57 1.76 o 8 6 2 1.88 1.15 .22 o 9 6 2 8.39 9.50 .29 o -9 7 2 6.48 7.85 .24 o -8 7 2 70.70 73.56 1.48 o -7 7 2 3.58 4.72 .27 o -6 7 2 22.17 19.03 .57 o -5 7 2 4.82 7.11 .30 o -4 7 2 209.79 218.19 3.10 o -3 7 2 162.34 152.57 2.55 o -2 7 2 82.22 90.70 1.93 o -1 7 2 10.21 11.31 .39 o 0 7 2 .69 .04 .59 o 1 7 2 160.00 166.75 2.62 o 2 7 2 1.28 1.13 .31 o 3 7 2 11.10 9.98 .38 o 4 7 2 .18 1.02 .19 o 5 7 2 192.19 195.18 2.89 o 6 7 2 23.55 22.56 .64 o 7 7 2 75.42 66.25 1.52 o 8 7 2 7.04 6.03 .22 o -7 8 2 15.97 19.45 .57 o -6 8 2 14.36 14.75 .46 o -5 8 2 5.56 5.88 .26 o -4 8 2 128.94 128.70 2.31 o -3 8 2 35.48 35.05 .92 o -2 8 2 6.70 6.04 .30 o -1 8 2 196.07 194.87 2.91 o 0 8 2 86.51 87.13 1.97 o 1 8 2 .33 .50 .21 o 2 8 2 .36 1.21 .21 o 3 8 2 10.29 12.85 .36 o 4 8 2 2.29 2.99 .22 o 5 8 2 33.20 31.12 .81 o 6 8 2 1.08 .76 .19 o 7 8 2 10.99 11.75 .36 o -6 9 2 .75 .11 .33 o -5 9 2 .00 .88 .16 o -4 9 2 10.93 10.58 .34 o -3 9 2 20.48 20.14 .64 o -2 9 2 .00 .13 .41 o -1 9 2 .09 .07 .19 o 0 9 2 4.56 4.79 .24 o 1 9 2 2.35 2.52 .22 o 2 9 2 9.46 9.50 .31 o 3 9 2 8.51 9.17 .30 o 4 9 2 26.36 25.35 .67 o 5 9 2 18.51 18.31 .53 o 6 9 2 10.74 9.21 .28 o -3 10 2 1.65 1.50 .15 o -2 10 2 9.60 11.05 .34 o -1 10 2 1.92 1.82 .17 o 0 10 2 20.23 21.05 .55 o 1 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25 45.51 49.00 1.37 o -3 1 25 .08 1.19 .18 o -2 1 25 1.23 1.21 .19 o -1 1 25 23.05 25.35 .76 o 0 1 25 22.72 20.04 .55 o 1 1 25 .13 .06 .41 o 2 1 25 .86 .85 .18 o 3 1 25 .00 .07 .29 o 4 1 25 4.68 5.44 .20 o -7 2 25 8.00 8.07 .25 o -6 2 25 25.96 24.17 .60 o -5 2 25 .36 .05 .41 o -4 2 25 5.21 4.98 .26 o -3 2 25 4.27 4.29 .25 o -2 2 25 .48 .71 .21 o -1 2 25 .05 .09 .47 o 0 2 25 .16 .02 .46 o 1 2 25 23.16 23.69 .67 o 2 2 25 12.73 14.58 .43 o 3 2 25 2.17 3.01 .19 o 4 2 25 1.73 1.81 .15 o -6 3 25 23.75 16.85 .49 o -5 3 25 .81 .61 .17 o -4 3 25 8.37 6.96 .26 o -3 3 25 10.78 11.96 .36 o -2 3 25 .01 .20 .18 o -1 3 25 7.67 7.53 .29 o 0 3 25 12.10 14.37 .45 o 1 3 25 47.13 45.22 1.21 o 2 3 25 2.80 2.50 .21 o 3 3 25 18.46 16.85 .48 o -5 4 25 12.74 11.37 .33 o -4 4 25 .00 .02 .31 o -3 4 25 32.07 39.45 1.06 o -2 4 25 .37 .24 .17 o -1 4 25 17.16 18.29 .54 o 0 4 25 12.09 13.21 .40 o 1 4 25 71.69 78.03 1.40 o 2 4 25 1.21 .70 .15 o -4 5 25 10.37 12.29 .37 o -3 5 25 .07 .06 .29 o -2 5 25 11.50 10.17 .27 o 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41.54 1.10 o 1 3 26 13.47 18.79 .53 o 2 3 26 .06 .23 .14 o -4 4 26 4.86 4.58 .20 o -3 4 26 81.78 83.48 1.37 o -2 4 26 7.28 7.49 .26 o -1 4 26 .15 .05 .15 o 0 4 26 34.70 38.83 .95 o 1 4 26 4.30 4.08 .20 o -6 1 27 18.35 16.96 .45 o -5 1 27 7.65 6.94 .22 o -4 1 27 8.64 8.96 .26 o -3 1 27 1.73 2.10 .19 o -2 1 27 15.52 15.73 .43 o -1 1 27 1.04 1.24 .17 o 0 1 27 5.20 5.13 .22 o 1 1 27 .33 .95 .15 o 2 1 27 4.54 6.57 .24 o 3 1 27 8.49 10.06 .27 o -5 2 27 3.15 2.08 .16 o -4 2 27 .64 1.00 .16 o -3 2 27 2.36 4.26 .21 o -2 2 27 3.22 3.41 .20 o -1 2 27 6.89 8.16 .25 o 0 2 27 2.05 2.21 .18 o 1 2 27 .56 1.62 .15 o 2 2 27 6.30 6.99 .23 o -4 3 27 .02 .01 .29 o -3 3 27 1.76 3.77 .19 o -2 3 27 4.45 5.55 .21 o -1 3 27 3.44 3.32 .19 o 0 3 27 17.86 17.09 .48 o 1 3 27 24.63 28.65 .80 o -2 4 27 28.32 33.41 .79 o -1 4 27 38.17 39.76 .87 o -5 0 28 203.29 198.84 1.95 o -4 0 28 105.26 104.76 1.55 o -3 0 28 15.46 15.61 .49 o -2 0 28 .01 .21 .33 o -1 0 28 2.56 3.50 .19 o 0 0 28 46.19 46.52 1.06 o 1 0 28 14.28 14.62 .43 o -5 1 28 12.75 9.24 .24 o -4 1 28 21.18 23.39 .54 o -3 1 28 1.64 2.84 .19 o -2 1 28 4.23 5.53 .21 o -1 1 28 14.30 18.24 .50 o 0 1 28 3.26 3.54 .18 o 1 1 28 5.76 5.11 .19 o -4 2 28 9.83 10.64 .30 o -3 2 28 20.91 26.58 .56 o -2 2 28 .33 .56 .14 o -1 2 28 .20 .09 .28 o 0 2 28 7.14 7.08 .23 o 1 2 28 3.59 6.22 .22 o -2 3 28 11.50 13.20 .38 o -1 3 28 8.25 9.12 .27 o -3 1 29 2.32 1.77 .16 o -2 1 29 2.99 3.65 .18 o -1 1 29 12.17 11.47 .36 o