#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/07/2010749.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2010749_Fobs loop_ _publ_author_name 'Brewer, A. David' 'Ferguson, George' 'Znotins, Andrew A.' _publ_section_title ; 7,7-Dichloro-1,6-dimethyl-2-oxa-5-thiabicyclo[4.1.0]heptane 5,5-dioxide and 6-chloro-2,3-dihydro-7-methyl-5-methylene-2H,3H,5H-1,4-dithiepine 1,1,4,4-tetraoxide ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first e109 _journal_page_last e110 _journal_volume 56 _journal_year 2000 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 92.010 _cell_angle_beta 110.855 _cell_angle_gamma 119.210 _cell_length_a 8.0689 _cell_length_b 8.1209 _cell_length_c 9.9329 _exptl_crystal_F_000 264.00 _reflns_d_resolution_high 0.7836 _[local]_cod_data_source_file qa02222sup3.hkl _[local]_cod_data_source_block 2 #BEGIN Tags that were not found in dictionaries: _shelx_title ' UNIROYAL-2' _shelx_refln_list_code 4 _shelx_f_calc_maximum 111.08 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1091.76 1019.77 8.46 o 2 0 0 2176.49 2094.86 17.29 o 3 0 0 14.28 21.86 0.42 o 4 0 0 167.27 181.91 1.83 o 5 0 0 245.48 228.77 2.35 o 6 0 0 17.33 15.56 0.67 o 7 0 0 6.41 5.89 0.59 o 8 0 0 0.02 0.10 0.84 o -8 1 0 53.71 55.90 1.33 o -7 1 0 87.89 90.65 1.47 o -6 1 0 48.32 41.66 0.93 o -5 1 0 23.70 18.77 0.59 o -4 1 0 36.59 44.42 0.69 o -3 1 0 1659.12 1563.75 15.12 o -2 1 0 4257.67 4023.60 27.65 o -1 1 0 2987.53 3114.56 17.09 o 0 1 0 1003.76 935.40 8.21 o 1 1 0 245.76 233.78 1.61 o 2 1 0 5053.44 4756.91 37.46 o 3 1 0 779.58 764.65 4.27 o 4 1 0 0.01 0.05 0.54 o 5 1 0 71.67 76.58 1.18 o 6 1 0 15.30 15.61 0.71 o 7 1 0 0.50 0.74 0.92 o -8 2 0 10.61 8.43 0.71 o -7 2 0 0.82 0.80 0.70 o -6 2 0 44.44 54.33 0.99 o -5 2 0 1379.82 1387.81 6.50 o -4 2 0 137.28 158.38 1.57 o -3 2 0 961.73 984.90 4.03 o -2 2 0 192.25 170.41 1.43 o -1 2 0 597.79 533.83 5.53 o 0 2 0 5760.91 6024.70 33.52 o 1 2 0 972.04 1067.01 10.19 o 2 2 0 350.26 404.16 3.05 o 3 2 0 15.11 19.30 0.55 o 4 2 0 101.21 98.33 1.28 o 5 2 0 3.71 4.79 0.53 o 6 2 0 202.21 208.65 2.29 o -9 3 0 11.34 11.06 0.82 o -8 3 0 91.34 91.99 1.52 o -7 3 0 421.53 431.20 3.71 o -6 3 0 195.29 190.85 1.93 o -5 3 0 280.28 265.82 2.33 o -4 3 0 82.68 72.55 0.85 o -3 3 0 1614.36 1587.75 15.72 o -2 3 0 748.40 747.97 3.40 o -1 3 0 930.51 899.50 9.03 o 0 3 0 16.72 21.57 0.42 o 1 3 0 410.87 444.80 3.29 o 2 3 0 867.94 893.68 5.21 o 3 3 0 67.15 63.30 1.03 o 4 3 0 51.90 44.40 0.99 o 5 3 0 57.21 58.35 1.25 o 6 3 0 190.27 190.23 2.37 o -9 4 0 0.87 1.19 0.86 o -8 4 0 41.13 35.19 1.01 o -7 4 0 87.18 78.99 1.27 o -6 4 0 144.42 146.76 1.52 o -5 4 0 1489.11 1503.08 6.81 o -4 4 0 191.64 207.69 1.89 o -3 4 0 1188.54 1221.90 13.46 o -2 4 0 45.41 64.58 0.70 o -1 4 0 23.30 20.65 0.49 o 0 4 0 169.74 176.14 1.82 o 1 4 0 6.50 7.41 0.44 o 2 4 0 64.79 53.10 0.99 o 3 4 0 6.60 8.00 0.55 o 4 4 0 78.79 78.29 1.41 o 5 4 0 43.70 42.22 1.20 o -9 5 0 2.46 2.94 0.55 o -8 5 0 69.85 80.38 1.40 o -7 5 0 203.19 197.09 1.97 o -6 5 0 333.63 341.24 3.01 o -5 5 0 413.40 411.44 3.78 o -4 5 0 0.13 1.11 0.30 o -3 5 0 634.18 599.99 4.07 o -2 5 0 10.36 12.36 0.47 o -1 5 0 30.83 37.40 0.75 o 0 5 0 1.26 1.33 0.40 o 1 5 0 60.23 47.96 0.98 o 2 5 0 49.54 48.21 1.05 o 3 5 0 0.01 0.08 0.76 o 4 5 0 224.66 218.30 2.51 o -9 6 0 4.59 6.65 0.60 o -8 6 0 112.16 119.65 1.73 o -7 6 0 0.22 0.99 0.42 o -6 6 0 166.90 155.59 1.69 o -5 6 0 306.19 313.12 2.86 o -4 6 0 46.16 41.91 0.83 o -3 6 0 39.54 42.36 0.83 o -2 6 0 35.60 32.48 0.78 o -1 6 0 255.17 238.40 2.56 o 0 6 0 17.14 21.50 0.72 o 1 6 0 70.23 63.30 1.22 o 2 6 0 40.58 38.92 1.08 o 3 6 0 213.17 196.13 2.40 o -9 7 0 0.29 0.68 0.86 o -8 7 0 34.80 41.93 1.11 o -7 7 0 127.31 117.50 1.65 o -6 7 0 0.74 0.07 0.69 o -5 7 0 73.70 81.75 1.28 o -4 7 0 8.35 12.14 0.63 o -3 7 0 116.32 117.02 1.47 o -2 7 0 7.35 8.28 0.55 o -1 7 0 43.64 39.80 0.98 o 0 7 0 57.64 59.46 1.25 o 1 7 0 385.79 374.11 3.51 o 2 7 0 9.08 9.21 0.74 o -9 8 0 7.04 7.71 0.74 o -8 8 0 92.16 100.21 1.71 o -7 8 0 4.64 3.74 0.54 o -6 8 0 1.51 0.92 0.74 o -5 8 0 148.18 134.53 1.75 o -4 8 0 118.26 112.44 1.59 o -3 8 0 1.78 0.99 0.51 o -2 8 0 184.31 182.27 2.10 o -1 8 0 156.54 151.35 2.00 o 0 8 0 101.69 102.69 1.79 o 1 8 0 0.29 0.53 0.87 o -8 9 0 0.56 0.10 0.94 o -7 9 0 6.60 3.70 0.61 o -6 9 0 5.19 6.04 0.62 o -5 9 0 105.46 95.55 1.64 o -4 9 0 27.60 28.68 1.03 o -3 9 0 0.08 0.69 0.79 o -2 9 0 0.77 0.24 0.91 o -1 9 0 103.43 103.48 1.84 o -7 10 0 41.44 44.37 1.36 o -6 10 0 9.82 15.13 0.85 o -5 10 0 0.41 0.95 1.00 o -4 10 0 1.35 0.51 0.87 o -3 10 0 5.92 5.79 0.72 o 3 -10 1 1.40 1.56 0.58 o 4 -10 1 76.37 78.57 1.67 o 5 -10 1 1.63 1.23 1.04 o 6 -10 1 152.59 166.18 2.34 o 1 -9 1 11.72 10.82 0.82 o 2 -9 1 65.76 67.79 1.48 o 3 -9 1 108.49 111.25 1.79 o 4 -9 1 221.29 233.34 2.49 o 5 -9 1 19.69 19.42 0.86 o 6 -9 1 13.67 14.37 0.77 o 7 -9 1 18.40 20.57 0.91 o 8 -9 1 26.66 31.07 1.11 o -1 -8 1 21.58 24.87 1.04 o 0 -8 1 1.58 1.76 0.63 o 1 -8 1 312.73 320.01 3.20 o 2 -8 1 35.67 35.22 1.04 o 3 -8 1 85.90 90.04 1.45 o 4 -8 1 140.82 129.44 1.73 o 5 -8 1 8.42 8.81 0.62 o 6 -8 1 219.84 210.06 2.24 o 7 -8 1 2.40 1.08 0.83 o 8 -8 1 0.04 0.10 0.78 o -2 -7 1 8.74 10.73 0.80 o -1 -7 1 188.15 189.86 2.27 o 0 -7 1 5.98 4.05 0.57 o 1 -7 1 115.41 115.81 1.59 o 2 -7 1 115.26 118.59 1.53 o 3 -7 1 540.01 511.97 4.79 o 4 -7 1 859.39 810.15 6.02 o 5 -7 1 32.97 33.77 0.88 o 6 -7 1 3.22 2.71 0.48 o 7 -7 1 12.32 14.58 0.71 o 8 -7 1 1.58 2.49 0.53 o 9 -7 1 15.63 16.91 0.86 o -3 -6 1 43.55 43.97 1.24 o -2 -6 1 121.81 129.45 1.84 o -1 -6 1 25.65 26.43 0.84 o 0 -6 1 15.06 13.69 0.66 o 1 -6 1 1066.28 1041.39 6.49 o 2 -6 1 38.53 34.36 0.78 o 3 -6 1 50.32 44.09 0.87 o 4 -6 1 79.96 86.95 1.18 o 5 -6 1 29.13 21.93 0.69 o 6 -6 1 360.81 334.50 3.24 o 7 -6 1 24.43 24.60 0.78 o 8 -6 1 36.61 39.56 1.05 o 9 -6 1 2.05 2.33 0.59 o -4 -5 1 18.39 19.42 0.90 o -3 -5 1 57.21 63.39 1.27 o -2 -5 1 35.32 31.64 0.88 o -1 -5 1 693.35 694.31 5.36 o 0 -5 1 441.13 453.75 4.06 o 1 -5 1 49.28 50.07 0.85 o 2 -5 1 31.08 26.33 0.62 o 3 -5 1 257.46 232.78 2.15 o 4 -5 1 314.27 312.33 2.57 o 5 -5 1 7.40 2.34 0.40 o 6 -5 1 4.26 3.77 0.45 o 7 -5 1 9.48 6.73 0.57 o 8 -5 1 2.69 2.58 0.49 o 9 -5 1 23.71 23.19 0.95 o -5 -4 1 0.24 0.71 0.57 o -4 -4 1 160.63 168.57 2.00 o -3 -4 1 112.67 122.26 1.54 o -2 -4 1 528.99 512.29 4.50 o -1 -4 1 114.18 120.84 1.28 o 0 -4 1 561.70 552.37 3.89 o 1 -4 1 104.92 76.46 0.87 o 2 -4 1 21.43 36.39 0.60 o 3 -4 1 617.14 692.57 4.03 o 4 -4 1 75.33 76.34 0.95 o 5 -4 1 20.48 19.53 0.61 o 6 -4 1 229.34 207.61 2.06 o 7 -4 1 248.38 244.95 2.49 o 8 -4 1 85.58 85.91 1.49 o 9 -4 1 92.10 99.18 1.80 o -6 -3 1 168.20 173.45 2.27 o -5 -3 1 0.38 0.91 0.64 o -4 -3 1 31.09 32.38 0.89 o -3 -3 1 145.74 145.00 1.50 o -2 -3 1 260.73 281.54 2.39 o -1 -3 1 2804.66 2704.60 27.08 o 0 -3 1 594.91 633.23 3.50 o 1 -3 1 74.66 92.87 0.91 o 2 -3 1 177.58 180.64 1.75 o 3 -3 1 14.70 6.72 0.28 o 4 -3 1 31.01 26.60 0.58 o 5 -3 1 881.41 917.03 5.41 o 6 -3 1 55.57 54.96 0.99 o 7 -3 1 201.95 212.55 2.08 o 8 -3 1 36.80 33.77 1.03 o -7 -2 1 25.98 27.49 1.05 o -6 -2 1 2.76 1.45 0.51 o -5 -2 1 16.30 18.67 0.72 o -4 -2 1 984.48 948.04 6.04 o -3 -2 1 771.58 790.91 4.81 o -2 -2 1 992.77 1002.42 4.71 o -1 -2 1 348.19 361.34 2.45 o 0 -2 1 16.15 13.35 0.30 o 1 -2 1 2316.02 2120.56 20.29 o 2 -2 1 311.73 313.98 2.07 o 3 -2 1 619.41 732.99 3.68 o 4 -2 1 281.17 310.01 2.79 o 5 -2 1 100.86 117.68 1.26 o 6 -2 1 17.99 17.09 0.66 o 7 -2 1 113.74 116.71 1.62 o 8 -2 1 80.63 82.68 1.56 o -7 -1 1 11.12 10.48 0.75 o -6 -1 1 268.57 276.48 2.69 o -5 -1 1 256.64 237.26 2.56 o -4 -1 1 124.35 126.98 1.29 o -3 -1 1 267.29 289.23 2.60 o -2 -1 1 33.75 20.90 0.39 o -1 -1 1 1963.97 1863.81 18.27 o 0 -1 1 185.77 188.42 1.17 o 1 -1 1 162.85 179.29 1.22 o 2 -1 1 2308.12 2299.47 22.84 o 3 -1 1 307.27 330.89 2.52 o 4 -1 1 22.87 24.63 0.58 o 5 -1 1 1326.49 1346.62 6.90 o 6 -1 1 2.82 4.96 0.50 o 7 -1 1 271.02 278.21 2.85 o 8 -1 1 4.77 4.85 0.64 o -8 0 1 85.51 83.00 1.66 o -7 0 1 112.42 113.86 1.66 o -6 0 1 21.37 22.83 0.74 o -5 0 1 304.32 328.58 2.78 o -4 0 1 1556.90 1570.09 6.40 o -3 0 1 584.40 610.39 3.35 o -2 0 1 219.38 204.66 1.56 o -1 0 1 471.20 437.56 4.27 o 0 0 1 248.72 271.29 1.17 o 1 0 1 1433.78 1475.19 12.27 o 2 0 1 0.29 0.92 0.20 o 3 0 1 186.62 178.66 1.63 o 4 0 1 1224.44 1280.30 6.20 o 5 0 1 477.87 493.10 4.40 o 6 0 1 186.42 177.22 1.93 o 7 0 1 90.81 91.08 1.59 o -8 1 1 9.12 10.20 0.69 o -7 1 1 0.01 0.07 0.70 o -6 1 1 615.87 632.65 5.07 o -5 1 1 40.10 35.05 0.71 o -4 1 1 4.55 1.13 0.26 o -3 1 1 213.81 237.35 1.93 o -2 1 1 181.07 195.85 1.41 o -1 1 1 3895.40 3771.86 21.26 o 0 1 1 1588.60 1442.60 12.19 o 1 1 1 3192.17 3117.05 26.61 o 2 1 1 2618.09 2677.19 24.35 o 3 1 1 15.22 12.96 0.44 o 4 1 1 669.87 667.92 4.82 o 5 1 1 262.28 255.78 2.42 o 6 1 1 27.38 30.26 0.93 o 7 1 1 105.23 101.81 1.74 o -9 2 1 68.60 74.17 1.58 o -8 2 1 82.34 87.31 1.51 o -7 2 1 343.77 330.56 3.29 o -6 2 1 271.46 252.72 2.55 o -5 2 1 2.22 1.65 0.31 o -4 2 1 553.03 589.61 3.53 o -3 2 1 575.99 619.75 3.10 o -2 2 1 8.22 6.11 0.24 o -1 2 1 97.18 80.82 0.81 o 0 2 1 0.35 2.39 0.22 o 1 2 1 381.88 416.50 2.88 o 2 2 1 218.31 212.41 1.90 o 3 2 1 746.56 732.21 4.91 o 4 2 1 289.20 323.13 3.04 o 5 2 1 70.64 69.55 1.26 o 6 2 1 189.49 187.62 2.24 o -9 3 1 95.94 100.66 1.73 o -8 3 1 24.27 22.96 0.91 o -7 3 1 41.46 38.31 0.91 o -6 3 1 474.51 500.94 4.24 o -5 3 1 31.41 33.61 0.67 o -4 3 1 322.50 357.55 2.80 o -3 3 1 28.06 22.48 0.40 o -2 3 1 220.00 231.49 1.94 o -1 3 1 147.10 144.68 1.30 o 0 3 1 477.74 459.10 3.17 o 1 3 1 7.69 7.62 0.39 o 2 3 1 278.52 270.07 2.46 o 3 3 1 16.83 21.75 0.72 o 4 3 1 9.31 9.55 0.59 o 5 3 1 423.24 423.29 4.21 o -9 4 1 51.97 53.74 1.28 o -8 4 1 201.71 192.44 2.09 o -7 4 1 6.44 5.90 0.48 o -6 4 1 260.44 256.57 2.55 o -5 4 1 0.05 0.36 0.41 o -4 4 1 0.09 0.35 0.39 o -3 4 1 96.98 117.65 1.17 o -2 4 1 217.07 190.79 1.68 o -1 4 1 84.56 72.96 0.88 o 0 4 1 295.52 276.70 2.34 o 1 4 1 108.62 97.14 1.21 o 2 4 1 310.38 321.27 3.02 o 3 4 1 182.86 176.35 1.93 o 4 4 1 216.51 213.90 2.33 o 5 4 1 74.45 74.31 1.59 o -9 5 1 31.35 32.65 1.03 o -8 5 1 2.44 1.73 0.49 o -7 5 1 70.90 71.76 1.21 o -6 5 1 247.34 228.20 2.15 o -5 5 1 57.67 57.03 0.92 o -4 5 1 40.82 46.29 0.79 o -3 5 1 298.19 288.58 2.85 o -2 5 1 31.78 29.25 0.65 o -1 5 1 798.71 786.03 5.08 o 0 5 1 293.31 286.86 2.75 o 1 5 1 79.09 71.63 1.20 o 2 5 1 181.62 198.55 2.05 o 3 5 1 0.87 1.08 0.76 o 4 5 1 2.36 0.89 1.05 o -9 6 1 39.32 39.97 1.12 o -8 6 1 81.41 75.72 1.39 o -7 6 1 0.30 0.66 0.43 o -6 6 1 107.32 111.14 1.43 o -5 6 1 78.95 85.82 1.20 o -4 6 1 42.80 36.44 0.79 o -3 6 1 52.80 49.08 0.91 o -2 6 1 500.83 482.76 4.28 o -1 6 1 16.86 18.14 0.68 o 0 6 1 380.93 373.30 3.46 o 1 6 1 30.53 31.35 0.95 o 2 6 1 29.48 25.44 0.96 o 3 6 1 17.13 19.35 0.97 o -9 7 1 58.46 61.18 1.37 o -8 7 1 39.65 42.92 1.12 o -7 7 1 10.29 11.61 0.65 o -6 7 1 2.36 0.07 0.74 o -5 7 1 257.77 244.13 2.37 o -4 7 1 13.22 11.64 0.58 o -3 7 1 590.20 563.41 5.05 o -2 7 1 309.84 285.69 2.66 o -1 7 1 6.33 6.03 0.55 o 0 7 1 160.54 161.52 2.00 o 1 7 1 3.07 3.81 0.66 o 2 7 1 119.11 119.36 2.01 o -9 8 1 15.69 14.26 0.88 o -8 8 1 0.04 0.09 0.84 o -7 8 1 0.26 0.57 0.68 o -6 8 1 67.25 68.28 1.29 o -5 8 1 298.56 289.23 2.83 o -4 8 1 0.18 0.88 0.64 o -3 8 1 2.49 2.11 0.49 o -2 8 1 35.33 36.65 1.06 o -1 8 1 115.56 118.07 1.82 o 0 8 1 230.98 228.90 2.63 o -8 9 1 23.11 27.02 1.02 o -7 9 1 3.08 3.29 0.56 o -6 9 1 20.87 23.37 0.91 o -5 9 1 34.79 38.38 1.09 o -4 9 1 7.19 7.53 0.67 o -3 9 1 186.27 187.28 2.29 o -2 9 1 41.02 40.47 1.23 o -1 9 1 26.03 24.88 1.04 o -7 10 1 3.78 5.63 0.71 o -6 10 1 16.37 20.55 0.94 o -5 10 1 93.50 95.28 1.78 o -4 10 1 9.80 10.09 0.79 o 3 -10 2 32.96 34.47 1.18 o 4 -10 2 4.67 6.35 0.70 o 5 -10 2 2.62 4.17 0.72 o 6 -10 2 24.89 27.90 1.16 o 0 -9 2 205.77 211.33 2.68 o 1 -9 2 9.21 9.75 0.76 o 2 -9 2 2.58 3.07 0.59 o 3 -9 2 4.12 6.68 0.66 o 4 -9 2 0.48 1.70 0.51 o 5 -9 2 57.25 60.48 1.37 o 6 -9 2 62.59 60.25 1.38 o 7 -9 2 1.91 2.71 0.58 o -1 -8 2 147.12 148.54 2.14 o 0 -8 2 0.08 1.11 0.84 o 1 -8 2 15.79 16.07 0.81 o 2 -8 2 98.26 93.51 1.55 o 3 -8 2 131.70 136.71 1.79 o 4 -8 2 1.91 2.06 0.46 o 5 -8 2 19.22 17.20 0.76 o 6 -8 2 2.01 2.89 0.55 o 7 -8 2 6.66 6.64 0.67 o 8 -8 2 22.11 22.04 0.95 o -3 -7 2 73.66 75.35 1.66 o -2 -7 2 99.47 97.98 1.73 o -1 -7 2 18.76 18.00 0.84 o 0 -7 2 213.73 207.11 2.17 o 1 -7 2 0.88 0.84 0.45 o 2 -7 2 1.61 0.55 0.64 o 3 -7 2 43.00 40.51 0.95 o 4 -7 2 3.78 4.38 0.49 o 5 -7 2 39.11 34.74 0.91 o 6 -7 2 127.75 123.89 1.66 o 7 -7 2 0.69 0.42 0.77 o 8 -7 2 17.51 17.85 0.88 o -4 -6 2 141.95 144.18 2.19 o -3 -6 2 19.10 21.07 0.93 o -2 -6 2 172.27 170.42 2.03 o -1 -6 2 5.32 5.16 0.51 o 0 -6 2 238.95 234.53 2.32 o 1 -6 2 32.15 28.84 0.80 o 2 -6 2 129.52 123.41 1.40 o 3 -6 2 187.20 186.45 1.90 o 4 -6 2 203.43 223.30 2.12 o 5 -6 2 235.68 210.65 2.17 o 6 -6 2 78.13 78.03 1.29 o 7 -6 2 27.72 26.27 0.90 o 8 -6 2 1.92 1.94 0.51 o -5 -5 2 370.22 379.28 3.88 o -4 -5 2 16.05 15.62 0.84 o -3 -5 2 142.10 147.83 1.86 o -2 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73.81 74.73 1.41 o -6 2 9 9.05 9.64 0.60 o -5 2 9 11.39 9.92 0.61 o -4 2 9 99.40 101.69 1.47 o -3 2 9 201.66 204.36 2.06 o -2 2 9 590.77 567.83 5.44 o -1 2 9 2.89 3.87 0.56 o 0 2 9 28.09 29.53 1.01 o 1 2 9 5.94 4.87 0.64 o -9 3 9 32.02 33.39 1.14 o -8 3 9 9.97 13.33 0.77 o -7 3 9 0.06 0.09 0.75 o -6 3 9 4.89 4.92 0.56 o -5 3 9 210.05 211.67 2.14 o -4 3 9 29.89 28.15 0.90 o -3 3 9 216.36 210.13 2.15 o -2 3 9 6.17 6.94 0.64 o -1 3 9 28.04 30.14 0.99 o 0 3 9 14.90 15.55 0.86 o -9 4 9 7.37 7.34 0.79 o -8 4 9 6.96 7.94 0.68 o -7 4 9 131.51 131.58 1.85 o -6 4 9 11.53 10.44 0.68 o -5 4 9 2.00 1.09 0.77 o -4 4 9 49.98 42.81 1.12 o -3 4 9 14.65 16.37 0.78 o -2 4 9 110.99 108.35 1.68 o -1 4 9 4.61 4.47 0.66 o -9 5 9 54.54 60.00 1.45 o -8 5 9 15.44 18.99 0.90 o -7 5 9 3.23 1.87 0.57 o -6 5 9 4.53 4.23 0.64 o -5 5 9 127.87 122.88 1.79 o -4 5 9 30.74 28.42 0.95 o -3 5 9 1.93 0.96 0.77 o -2 5 9 12.86 12.65 0.80 o -8 6 9 10.55 11.28 0.79 o -7 6 9 113.48 111.40 1.84 o -6 6 9 0.38 1.16 0.57 o -5 6 9 26.66 18.53 0.88 o -4 6 9 3.19 3.19 0.64 o -3 6 9 10.10 9.82 0.82 o -6 7 9 0.47 0.10 0.98 o -2 -6 10 0.22 0.10 0.98 o -1 -6 10 165.78 169.96 2.30 o 0 -6 10 19.89 19.30 0.94 o 1 -6 10 7.75 5.09 0.71 o 2 -6 10 117.32 122.23 2.06 o -3 -5 10 62.78 66.22 1.49 o -2 -5 10 3.14 2.99 0.60 o -1 -5 10 50.79 49.59 1.30 o 0 -5 10 97.85 102.56 1.77 o 1 -5 10 183.99 185.94 2.34 o 2 -5 10 191.56 196.57 2.48 o -5 -4 10 0.86 3.20 0.63 o -4 -4 10 17.19 17.54 0.85 o -3 -4 10 33.16 32.74 1.05 o -2 -4 10 14.96 13.91 0.73 o -1 -4 10 167.27 173.10 2.16 o 0 -4 10 3.19 2.76 0.58 o 1 -4 10 8.44 7.73 0.70 o 2 -4 10 46.18 45.88 1.28 o 3 -4 10 4.34 3.46 0.70 o -6 -3 10 12.15 9.24 0.86 o -5 -3 10 133.12 127.73 2.00 o -4 -3 10 90.00 95.46 1.64 o -3 -3 10 90.59 97.94 1.66 o -2 -3 10 7.96 7.90 0.64 o -1 -3 10 38.29 38.33 1.05 o 0 -3 10 40.06 45.73 1.18 o 1 -3 10 31.35 33.99 1.06 o 2 -3 10 82.75 85.57 1.66 o -6 -2 10 288.53 288.32 2.96 o -5 -2 10 49.51 47.17 1.25 o -4 -2 10 18.59 23.97 0.90 o -3 -2 10 79.02 77.71 1.42 o 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46.06 42.59 1.10 o -5 2 10 18.50 15.65 0.78 o -4 2 10 3.26 2.94 0.59 o -3 2 10 21.41 21.67 0.83 o -2 2 10 19.06 16.64 0.79 o -1 2 10 3.01 3.61 0.62 o 0 2 10 62.98 67.21 1.52 o -8 3 10 11.48 12.45 0.78 o -7 3 10 11.13 8.52 0.68 o -6 3 10 3.51 3.53 0.54 o -5 3 10 2.66 3.24 0.53 o -4 3 10 0.34 0.16 0.77 o -3 3 10 15.06 13.67 0.78 o -2 3 10 72.95 76.98 1.51 o -1 3 10 4.32 4.02 0.66 o -8 4 10 6.76 7.03 0.72 o -7 4 10 3.80 5.30 0.63 o -6 4 10 0.93 0.11 0.79 o -5 4 10 25.81 29.50 1.01 o -4 4 10 8.65 10.72 0.75 o -3 4 10 50.14 50.03 1.30 o -2 4 10 0.34 0.10 0.98 o -8 5 10 9.92 8.68 0.78 o -7 5 10 32.73 38.65 1.18 o -6 5 10 0.05 0.48 0.51 o -5 5 10 74.49 80.56 1.58 o -4 5 10 1.27 0.92 0.57 o -3 5 10 2.42 1.44 0.69 o -6 6 10 2.44 4.82 0.71 o -2 -5 11 11.64 14.69 0.87 o -1 -5 11 78.93 80.31 1.67 o 0 -5 11 7.03 5.90 0.76 o -4 -4 11 52.54 53.37 1.37 o -3 -4 11 24.12 21.78 0.98 o -2 -4 11 0.00 0.76 0.78 o -1 -4 11 0.75 0.31 0.91 o 0 -4 11 14.28 14.29 0.81 o 1 -4 11 121.11 118.50 2.00 o -5 -3 11 1.47 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209.74 2.55 o 0 1 11 42.97 42.36 1.32 o -7 2 11 12.98 12.77 0.81 o -6 2 11 28.58 29.19 1.01 o -5 2 11 0.56 0.68 0.80 o -4 2 11 62.90 63.23 1.37 o -3 2 11 109.99 112.16 1.80 o -2 2 11 30.84 28.32 1.07 o -1 2 11 46.71 44.93 1.32 o -7 3 11 1.11 2.40 0.53 o -6 3 11 7.85 10.29 0.75 o -5 3 11 9.20 9.90 0.69 o -4 3 11 40.81 40.34 1.18 o -3 3 11 10.72 10.04 0.78 o -2 3 11 6.14 7.45 0.72 o -7 4 11 0.16 1.15 0.89 o -6 4 11 13.83 16.08 0.85 o -5 4 11 0.90 0.98 0.57 o -4 4 11 6.28 9.09 0.75 o -3 -3 12 84.10 81.00 1.71 o -2 -3 12 63.87 68.39 1.57 o -1 -3 12 4.41 3.93 0.71 o -4 -2 12 0.92 0.84 0.66 o -3 -2 12 3.90 4.13 0.64 o -2 -2 12 77.64 78.01 1.64 o -1 -2 12 0.67 0.40 0.98 o -5 -1 12 109.93 104.28 1.91 o -4 -1 12 52.96 47.82 1.36 o -3 -1 12 133.21 135.75 2.09 o -2 -1 12 87.79 89.92 1.73 o -1 -1 12 0.35 0.41 0.96 o -6 0 12 34.66 31.43 1.18 o -5 0 12 266.53 260.89 2.83 o -4 0 12 3.90 4.49 0.67 o -3 0 12 5.86 5.77 0.68 o -2 0 12 11.92 12.49 0.84 o -6 1 12 16.07 13.55 0.86 o -5 1 12 2.40 2.75 0.66 o 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