#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/07/2010757.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2010757_Fobs loop_ _publ_author_name 'Perez-Lourido, P.' 'Garc\'ia-V\'azquez, J. A.' 'Romero, J.' 'Fernandez, P.' 'Sousa-Pedrares, A.' 'Sousa, A.' _publ_section_title ; Bis[2-(diphenylphosphinoyl)benzene] disulfide ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first e101 _journal_page_last e102 _journal_volume 56 _journal_year 2000 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 104.498 _cell_angle_gamma 90.000 _cell_length_a 13.2492 _cell_length_b 10.8014 _cell_length_c 21.1925 _exptl_crystal_F_000 1288.00 _reflns_d_resolution_high 0.8418 _[local]_cod_data_source_file qb0174Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' pf98 in C 2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 234.60 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 3565.24 3783.09 58.89 o 4 0 0 3408.06 3524.78 76.85 o 6 0 0 2960.25 3012.42 84.08 o 8 0 0 17983.76 18298.36 189.96 o 10 0 0 1588.27 1507.22 96.52 o 12 0 0 5484.16 5503.54 148.61 o 14 0 0 1846.80 1995.13 124.58 o 1 1 0 9616.46 9275.36 66.54 o 3 1 0 50701.75 51702.91 192.30 o 5 1 0 576.29 830.30 59.21 o 7 1 0 3945.88 3917.98 96.20 o 9 1 0 2084.85 2006.93 96.09 o 11 1 0 303.23 237.79 82.70 o 13 1 0 1006.55 1086.27 104.81 o 15 1 0 279.23 273.51 96.20 o 0 2 0 50470.36 50826.80 162.74 o 2 2 0 2967.79 2735.61 70.16 o 4 2 0 714.66 727.72 59.74 o 6 2 0 2058.16 2327.53 78.13 o 8 2 0 819.29 709.76 74.94 o 10 2 0 2420.06 2275.76 107.15 o 12 2 0 147.46 154.03 85.89 o 14 2 0 1791.96 1790.51 120.33 o 1 3 0 592.26 480.37 59.53 o 3 3 0 139.51 170.82 54.21 o 5 3 0 8515.79 8802.01 121.29 o 7 3 0 2806.07 2854.99 93.33 o 9 3 0 1249.60 1187.58 88.23 o 11 3 0 4936.55 4893.17 144.67 o 13 3 0 1153.66 1154.41 110.13 o 0 4 0 1678.72 1409.32 64.52 o 2 4 0 456.58 520.44 58.15 o 4 4 0 1115.77 1007.40 66.65 o 6 4 0 663.53 679.57 68.14 o 8 4 0 1815.96 1833.88 92.37 o 10 4 0 235.00 300.61 81.85 o 12 4 0 2783.11 2926.31 126.28 o 14 4 0 104.92 29.66 88.12 o 1 5 0 14.70 -14.78 55.17 o 3 5 0 8403.16 8217.15 122.67 o 5 5 0 2087.79 2124.50 83.55 o 7 5 0 723.84 756.00 79.94 o 9 5 0 2022.93 2023.19 107.89 o 11 5 0 1242.42 1133.04 104.28 o 13 5 0 58.15 88.23 86.53 o 0 6 0 799.13 906.52 67.50 o 2 6 0 7148.74 7150.22 122.35 o 4 6 0 2260.15 2435.53 90.57 o 6 6 0 1523.47 1253.38 89.40 o 8 6 0 140.88 161.04 79.19 o 10 6 0 7404.50 7606.78 176.03 o 12 6 0 810.17 692.75 99.60 o 1 7 0 44.17 -66.33 66.33 o 3 7 0 3111.88 3361.18 103.75 o 5 7 0 4007.77 3984.52 121.93 o 7 7 0 355.16 286.37 88.97 o 9 7 0 1686.71 1723.22 104.60 o 11 7 0 409.37 405.96 89.72 o 0 8 0 22.86 240.56 70.05 o 2 8 0 2116.08 2011.40 98.96 o 4 8 0 115.22 100.77 81.21 o 6 8 0 165.98 120.01 74.73 o 8 8 0 93.10 -49.43 84.08 o 10 8 0 598.95 718.48 102.26 o 1 9 0 309.38 368.75 84.83 o 3 9 0 3197.42 3354.06 122.14 o 5 9 0 63.77 -21.79 79.30 o 7 9 0 188.58 190.38 84.30 o 9 9 0 257.36 362.37 98.96 o 0 10 0 5206.71 5132.45 147.01 o 2 10 0 3950.70 4003.55 134.79 o 4 10 0 142.28 100.13 85.57 o 6 10 0 113.74 153.28 86.10 o 8 10 0 58.62 -24.77 94.50 o 1 11 0 11.49 171.99 78.98 o 3 11 0 25.49 9.67 77.60 o 5 11 0 0.49 10.31 87.80 o 7 11 0 1195.88 1107.32 121.71 o 0 12 0 3196.38 3465.57 145.95 o 2 12 0 34.87 17.86 93.12 o 4 12 0 18.53 137.23 88.12 o -15 1 1 1291.08 1210.01 117.46 o -13 1 1 439.17 355.68 92.37 o -11 1 1 1885.05 2047.54 104.60 o -9 1 1 12.61 75.26 65.91 o -7 1 1 11001.77 10919.17 138.19 o -5 1 1 2840.85 2986.90 76.85 o -3 1 1 5835.06 5801.60 82.70 o -1 1 1 248.00 231.63 40.61 o 1 1 1 9595.70 9598.83 72.39 o 3 1 1 3050.59 3050.26 73.67 o 5 1 1 9402.57 9968.32 119.06 o 7 1 1 123.37 152.22 59.00 o 9 1 1 3410.91 3250.21 110.44 o 11 1 1 5.39 102.15 75.26 o 13 1 1 1835.57 2065.29 123.31 o 15 1 1 492.45 447.73 102.37 o -14 2 1 2316.56 2117.16 131.49 o -12 2 1 1677.85 1727.90 110.44 o -10 2 1 3.20 13.50 71.33 o -8 2 1 1683.93 1483.51 80.15 o -6 2 1 2988.94 2846.80 83.76 o -4 2 1 2625.45 2629.10 72.92 o -2 2 1 23454.11 22699.04 131.07 o 0 2 1 39034.52 40111.51 141.38 o 2 2 1 33765.56 33174.21 159.98 o 4 2 1 2870.58 3139.23 76.43 o 6 2 1 2.96 68.56 54.00 o 8 2 1 11475.10 11090.95 158.28 o 10 2 1 357.98 491.53 82.17 o 12 2 1 0.46 -83.66 83.66 o 14 2 1 86.03 81.74 87.48 o -13 3 1 464.67 448.90 94.07 o -11 3 1 744.57 788.21 88.65 o -9 3 1 894.97 1018.56 84.19 o -7 3 1 85.35 130.54 63.67 o -5 3 1 2629.01 2387.16 78.56 o -3 3 1 1.41 149.14 52.62 o -1 3 1 4025.47 3907.14 78.24 o 1 3 1 2582.24 2489.10 70.80 o 3 3 1 4744.80 4711.19 85.04 o 5 3 1 3197.11 3281.03 85.57 o 7 3 1 57.98 163.06 59.00 o 9 3 1 8.80 -64.95 77.17 o 11 3 1 1887.98 1826.86 106.94 o 13 3 1 559.57 575.40 98.86 o -14 4 1 92.21 69.41 92.69 o -12 4 1 161.99 217.59 88.23 o -10 4 1 3679.89 3694.75 121.50 o -8 4 1 4216.25 4361.04 118.63 o -6 4 1 610.94 587.20 65.48 o -4 4 1 2206.24 2201.99 77.17 o -2 4 1 764.64 740.48 60.70 o 0 4 1 5196.58 5035.96 106.09 o 2 4 1 9513.50 10082.81 117.35 o 4 4 1 2870.80 3364.90 88.12 o 6 4 1 42.24 36.25 60.27 o 8 4 1 3.74 -14.46 74.09 o 10 4 1 5177.61 5117.78 142.44 o 12 4 1 161.64 165.19 86.95 o 14 4 1 1051.30 1158.34 117.35 o -13 5 1 18.58 87.06 83.66 o -11 5 1 26.00 -14.46 79.41 o -9 5 1 3328.37 3022.30 120.54 o -7 5 1 2506.58 2757.40 100.45 o -5 5 1 5209.95 5047.94 108.96 o -3 5 1 93.67 164.13 58.04 o -1 5 1 9206.66 9825.99 124.48 o 1 5 1 1560.42 1996.41 74.73 o 3 5 1 4389.46 4488.70 98.43 o 5 5 1 177.93 175.07 63.46 o 7 5 1 1266.86 1172.91 87.27 o 9 5 1 147.67 268.72 77.39 o 11 5 1 2793.21 2807.36 123.31 o 13 5 1 230.94 128.94 95.35 o -12 6 1 453.18 552.86 92.80 o -10 6 1 199.23 246.40 83.34 o -8 6 1 151.04 90.25 80.68 o -6 6 1 856.32 1019.94 80.47 o -4 6 1 296.20 234.28 65.91 o -2 6 1 4434.12 4385.06 99.82 o 0 6 1 1673.28 1904.38 55.70 o 2 6 1 3.10 -56.66 56.66 o 4 6 1 74.51 -22.85 65.80 o 6 6 1 170.61 220.04 74.30 o 8 6 1 136.49 68.35 82.81 o 10 6 1 161.09 186.24 88.65 o 12 6 1 187.69 259.80 90.35 o -11 7 1 343.78 404.79 92.06 o -9 7 1 1079.20 1026.21 99.71 o -7 7 1 77.56 79.94 79.72 o -5 7 1 1551.22 1477.14 92.16 o -3 7 1 1470.16 1386.46 85.25 o -1 7 1 6347.58 6284.20 126.82 o 1 7 1 959.62 1002.30 76.43 o 3 7 1 6916.88 6812.83 135.53 o 5 7 1 359.11 228.22 79.41 o 7 7 1 47.00 12.44 80.15 o 9 7 1 193.76 257.99 87.80 o 11 7 1 3127.27 3208.54 140.21 o -12 8 1 1316.04 1170.99 121.82 o -10 8 1 1902.24 1837.81 122.14 o -8 8 1 376.36 400.75 88.02 o -6 8 1 3.97 182.41 72.39 o -4 8 1 4700.99 4612.86 127.98 o -2 8 1 14420.89 14487.96 195.38 o 0 8 1 599.51 566.13 57.31 o 2 8 1 4263.99 4368.69 125.96 o 4 8 1 2536.50 2611.03 109.70 o 6 8 1 2297.82 2089.53 109.70 o 8 8 1 824.10 830.94 95.78 o 10 8 1 2419.06 2523.12 133.94 o -11 9 1 1317.30 1504.35 120.86 o -9 9 1 89.10 132.13 92.59 o -7 9 1 43.58 63.04 81.00 o -5 9 1 974.14 976.47 96.52 o -3 9 1 2632.66 2702.66 113.00 o -1 9 1 1413.98 1284.95 101.20 o 1 9 1 70.69 149.99 74.52 o 3 9 1 456.97 430.41 86.63 o 5 9 1 94.87 260.75 79.51 o 7 9 1 64.67 274.89 81.64 o 9 9 1 335.22 369.92 98.33 o -8 10 1 826.77 849.97 105.87 o -6 10 1 41.96 -38.06 85.25 o -4 10 1 93.49 70.37 83.23 o -2 10 1 533.80 521.82 86.00 o 0 10 1 4343.61 4490.68 100.01 o 2 10 1 18.01 -42.09 81.53 o 4 10 1 71.15 59.32 79.72 o 6 10 1 1155.27 1111.68 108.32 o 8 10 1 675.13 882.60 98.33 o -7 11 1 6.93 48.05 86.85 o -5 11 1 54.69 119.27 84.72 o -3 11 1 1893.15 2070.29 115.97 o -1 11 1 343.47 378.53 96.09 o 1 11 1 4.99 25.09 86.74 o 3 11 1 262.58 256.18 87.48 o 5 11 1 1041.41 1082.45 107.26 o 7 11 1 3.40 -37.52 90.14 o -4 12 1 57.56 162.74 91.63 o -2 12 1 673.52 562.54 99.60 o 0 12 1 125.99 283.04 154.88 o 2 12 1 469.40 379.06 97.37 o 4 12 1 36.54 26.15 94.07 o -14 0 2 2318.39 2591.68 126.28 o -12 0 2 95.72 37.84 81.21 o -10 0 2 38.10 117.89 72.18 o -8 0 2 2436.01 2490.27 88.76 o -6 0 2 20092.96 19436.93 163.70 o -4 0 2 1004.65 948.61 60.91 o -2 0 2 304.84 365.46 45.50 o 0 0 2 7639.50 7727.55 39.76 o 2 0 2 16563.64 17749.75 109.70 o 4 0 2 6546.05 7038.82 97.05 o 6 0 2 3584.25 3601.31 89.19 o 8 0 2 2330.51 2242.70 90.14 o 10 0 2 2906.28 2862.11 113.21 o 12 0 2 815.15 715.18 93.86 o 14 0 2 12.72 -17.75 93.44 o -15 1 2 0.09 18.50 90.67 o -13 1 2 503.74 487.91 88.44 o -11 1 2 2962.92 2874.76 118.52 o -9 1 2 1067.69 1059.49 80.68 o -7 1 2 3334.73 3160.81 87.91 o -5 1 2 5932.80 5991.13 93.86 o -3 1 2 25473.92 25574.33 140.10 o -1 1 2 9969.30 9594.57 72.50 o 1 1 2 34654.66 33742.38 129.47 o 3 1 2 21831.34 21793.80 140.95 o 5 1 2 2762.63 2772.71 79.51 o 7 1 2 5844.23 6035.78 113.85 o 9 1 2 1783.38 1732.15 92.59 o 11 1 2 2263.64 2302.02 112.25 o 13 1 2 1679.39 1655.08 116.19 o -14 2 2 42.00 170.40 88.87 o -12 2 2 129.53 163.81 83.02 o -10 2 2 613.14 648.11 87.06 o -8 2 2 0.35 -12.12 63.46 o -6 2 2 1265.16 1330.23 68.14 o -4 2 2 108.67 316.98 54.11 o -2 2 2 3981.44 3667.01 74.62 o 0 2 2 2730.41 2695.74 45.62 o 2 2 2 1189.44 1205.75 64.42 o 4 2 2 2702.98 3016.35 77.81 o 6 2 2 303.79 271.81 61.12 o 8 2 2 1946.33 2107.49 93.01 o 10 2 2 2139.61 2128.75 107.89 o 12 2 2 27.21 20.73 83.55 o 14 2 2 233.28 86.95 100.03 o -15 3 2 686.64 637.37 99.82 o -13 3 2 0.02 44.43 80.79 o -11 3 2 1531.33 1587.15 100.45 o -9 3 2 414.81 396.39 76.22 o -7 3 2 5333.67 5225.14 109.91 o -5 3 2 2145.32 2272.04 77.60 o -3 3 2 1861.19 1949.74 68.35 o -1 3 2 526.78 560.52 58.78 o 1 3 2 8928.70 8502.88 100.03 o 3 3 2 1243.42 1290.90 64.20 o 5 3 2 1957.39 2117.80 76.75 o 7 3 2 49.63 92.69 62.08 o 9 3 2 1228.64 1069.48 91.95 o 11 3 2 1258.52 1100.09 102.05 o 13 3 2 1801.47 1486.81 121.50 o -14 4 2 287.55 448.37 91.84 o -12 4 2 359.14 245.13 84.08 o -10 4 2 983.28 1014.31 91.63 o -8 4 2 567.51 505.24 79.51 o -6 4 2 1811.44 1821.76 77.07 o -4 4 2 647.60 598.36 61.65 o -2 4 2 587.38 632.91 59.95 o 0 4 2 465.05 481.47 66.97 o 2 4 2 1742.59 2056.36 71.75 o 4 4 2 226.62 353.45 58.46 o 6 4 2 979.28 881.75 72.07 o 8 4 2 2451.52 2501.86 104.07 o 10 4 2 163.95 88.65 82.91 o 12 4 2 253.67 320.92 93.01 o 14 4 2 29.17 -15.31 100.67 o -13 5 2 598.84 524.16 101.09 o -11 5 2 27.79 106.09 75.69 o -9 5 2 3901.55 3729.30 125.01 o -7 5 2 0.10 130.64 65.91 o -5 5 2 363.07 374.07 63.14 o -3 5 2 109.06 61.76 58.89 o -1 5 2 6164.08 5788.74 102.37 o 1 5 2 164.21 195.06 58.78 o 3 5 2 11930.84 11967.81 146.06 o 5 5 2 140.92 82.06 63.57 o 7 5 2 1534.06 1577.27 90.78 o 9 5 2 264.39 289.45 79.51 o 11 5 2 5419.75 5488.98 161.79 o 13 5 2 710.56 554.35 106.94 o -12 6 2 17.51 96.84 81.32 o -10 6 2 252.41 143.19 83.23 o -8 6 2 7870.69 7953.10 160.72 o -6 6 2 1747.14 1654.87 94.29 o -4 6 2 3669.64 3698.15 101.30 o -2 6 2 7588.10 7654.61 125.54 o 0 6 2 4607.21 4784.50 173.53 o 2 6 2 611.39 631.74 68.24 o 4 6 2 3208.72 3000.19 100.13 o 6 6 2 5413.84 5219.51 129.05 o 8 6 2 750.75 756.85 89.19 o 10 6 2 952.39 1061.29 101.62 o 12 6 2 197.45 229.07 94.93 o -13 7 2 4.20 -81.00 94.29 o -11 7 2 24.43 105.24 81.96 o -9 7 2 440.44 541.59 87.48 o -7 7 2 1104.95 947.13 94.71 o -5 7 2 917.35 856.56 84.72 o -3 7 2 898.46 781.83 78.45 o -1 7 2 6210.14 6425.69 128.09 o 1 7 2 42.07 9.14 65.16 o 3 7 2 151.05 198.99 73.24 o 5 7 2 597.87 725.07 85.04 o 7 7 2 3775.80 3565.07 125.33 o 9 7 2 6.26 -85.36 85.36 o 11 7 2 862.10 792.14 107.26 o -12 8 2 10.54 137.55 90.25 o -10 8 2 692.19 758.87 103.00 o -8 8 2 1.59 77.39 76.75 o -6 8 2 1809.70 1931.56 103.96 o -4 8 2 2188.02 2104.83 103.64 o -2 8 2 108.54 46.88 77.28 o 0 8 2 2844.17 2861.73 106.62 o 2 8 2 2090.80 1985.14 100.77 o 4 8 2 1236.88 1130.28 99.07 o 6 8 2 561.94 477.18 85.04 o 8 8 2 46.93 113.74 79.72 o 10 8 2 153.92 20.73 92.69 o -11 9 2 14.37 180.50 93.54 o -9 9 2 4328.31 4796.33 159.66 o -7 9 2 333.70 400.32 87.59 o -5 9 2 6.10 97.16 73.67 o -3 9 2 1680.25 1443.23 101.94 o -1 9 2 5463.93 5304.02 139.78 o 1 9 2 13.02 -26.79 79.72 o 3 9 2 6286.95 6228.71 152.75 o 5 9 2 840.96 939.58 95.67 o 7 9 2 823.26 882.60 99.60 o 9 9 2 368.63 182.30 97.05 o -8 10 2 305.08 321.66 93.97 o -6 10 2 249.86 373.64 88.65 o -4 10 2 1379.23 1466.51 100.13 o -2 10 2 792.74 850.50 93.65 o 0 10 2 0.60 -31.22 57.59 o 2 10 2 278.72 285.84 85.15 o 4 10 2 1127.47 1096.58 104.28 o 6 10 2 550.37 629.19 98.54 o 8 10 2 484.69 615.15 104.60 o -7 11 2 206.05 231.95 93.01 o -5 11 2 328.97 292.75 91.84 o -3 11 2 1640.49 1740.23 115.23 o -1 11 2 270.58 254.27 90.78 o 1 11 2 1380.86 1438.65 108.43 o 3 11 2 220.62 340.05 86.00 o 5 11 2 132.88 184.54 91.74 o 7 11 2 60.53 166.68 93.86 o -4 12 2 28.88 29.55 86.10 o -2 12 2 7.53 -28.49 92.69 o 0 12 2 965.03 985.85 77.48 o 2 12 2 644.42 788.00 104.49 o 4 12 2 122.29 101.52 93.65 o -15 1 3 6.63 14.67 88.87 o -13 1 3 307.83 315.39 86.63 o -11 1 3 4614.13 4491.25 134.79 o -9 1 3 2666.09 2690.22 100.67 o -7 1 3 3523.74 3650.96 91.74 o -5 1 3 4568.50 4620.62 87.27 o -3 1 3 42191.75 44256.97 181.98 o -1 1 3 3571.52 3674.98 61.76 o 1 1 3 15789.47 15578.59 104.81 o 3 1 3 35675.43 35866.87 182.83 o 5 1 3 5394.58 5713.27 100.67 o 7 1 3 112.82 196.87 60.59 o 9 1 3 1694.47 1631.80 92.91 o 11 1 3 496.44 394.26 86.32 o 13 1 3 1016.78 1081.38 109.17 o -14 2 3 51.77 -16.90 92.27 o -12 2 3 743.29 655.44 90.67 o -10 2 3 3245.66 3358.21 113.74 o -8 2 3 460.55 548.40 66.65 o -6 2 3 23560.45 23488.00 184.64 o -4 2 3 2681.11 2677.36 75.58 o -2 2 3 3044.44 2943.64 73.24 o 0 2 3 42239.21 43703.80 122.74 o 2 2 3 44696.48 42175.73 193.15 o 4 2 3 2364.57 2157.13 73.24 o 6 2 3 3086.07 2865.94 88.55 o 8 2 3 2482.30 2351.98 98.86 o 10 2 3 6599.95 6373.71 151.90 o 12 2 3 71.80 179.22 80.04 o 14 2 3 1123.87 1309.82 109.91 o -15 3 3 1138.20 1027.81 115.76 o -13 3 3 110.41 179.22 84.51 o -11 3 3 1940.30 1818.67 104.49 o -9 3 3 1288.12 1301.21 90.99 o -7 3 3 2282.58 2451.16 84.08 o -5 3 3 3026.70 3015.18 83.98 o -3 3 3 58.19 105.02 52.51 o -1 3 3 796.51 993.69 60.59 o 1 3 3 19871.82 20474.41 146.16 o 3 3 3 4.86 -15.09 54.21 o 5 3 3 911.50 785.45 65.91 o 7 3 3 324.90 342.18 68.24 o 9 3 3 1692.65 1529.54 101.83 o 11 3 3 1671.03 1604.91 109.81 o 13 3 3 583.70 399.69 101.41 o -14 4 3 598.27 509.17 104.17 o -12 4 3 145.85 151.37 85.57 o -10 4 3 223.43 38.91 83.44 o -8 4 3 3547.84 3333.65 108.21 o -6 4 3 227.08 250.76 61.65 o -4 4 3 1186.51 1079.04 68.14 o -2 4 3 1225.88 1307.27 65.48 o 0 4 3 14080.63 14764.62 96.77 o 2 4 3 754.78 720.92 63.04 o 4 4 3 595.06 431.04 61.23 o 6 4 3 453.84 432.32 66.97 o 8 4 3 120.79 26.04 77.17 o 10 4 3 419.97 547.76 84.61 o 12 4 3 1194.48 1386.78 108.21 o -13 5 3 71.90 147.12 86.42 o -11 5 3 2.99 62.72 81.00 o -9 5 3 1115.09 1013.88 93.22 o -7 5 3 1043.53 953.61 84.83 o -5 5 3 48.79 79.30 58.15 o -3 5 3 297.32 315.28 60.70 o -1 5 3 1944.52 2119.71 76.96 o 1 5 3 577.55 502.48 61.65 o 3 5 3 3017.78 3101.28 89.82 o 5 5 3 31.80 -1.81 63.35 o 7 5 3 1173.45 1098.92 86.21 o 9 5 3 1230.86 1323.00 99.18 o 11 5 3 231.63 195.80 94.07 o 13 5 3 201.28 130.22 99.71 o -12 6 3 188.22 96.20 91.52 o -10 6 3 318.84 198.25 86.95 o -8 6 3 402.52 371.41 83.55 o -6 6 3 7.73 -19.98 70.05 o -4 6 3 3021.14 2889.21 94.61 o -2 6 3 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