#------------------------------------------------------------------------------ #$Date: 2016-04-02 21:17:15 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180776 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/07/2010760.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2010760_Fobs loop_ _publ_author_name 'Novoa de Armas, H\'ector' 'P\'erez, Hiram' 'Peeters, Oswald M.' 'Blaton, Norbert M.' 'De Ranter, Camiel J.' 'L\'opez, Jos\'e Manuel' _publ_section_title ; Tribenzylphosphine oxide ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first e98 _journal_page_last e99 _journal_volume 56 _journal_year 2000 _space_group_IT_number 146 _symmetry_space_group_name_Hall 'R 3' _symmetry_space_group_name_H-M 'R 3 :H' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 120.000 _cell_length_a 16.6850 _cell_length_b 16.6850 _cell_length_c 5.4680 _exptl_crystal_F_000 510.00 _reflns_d_resolution_high 0.8445 _cod_data_source_file qb0179Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' iran1 in R 3' _shelx_refln_list_code 4 _shelx_f_calc_maximum 131.03 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-y, x-y, z' '-x+y, -x, z' 'x+2/3, y+1/3, z+1/3' '-y+2/3, x-y+1/3, z+1/3' '-x+y+2/3, -x+1/3, z+1/3' 'x+1/3, y+2/3, z+2/3' '-y+1/3, x-y+2/3, z+2/3' '-x+y+1/3, -x+2/3, z+2/3' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 1 0 2439.08 2473.84 61.93 o -1 2 0 2449.20 2433.19 32.51 o 2 2 0 17167.72 16500.87 483.26 o -3 3 0 6081.60 6173.94 128.17 o 0 3 0 6165.79 6202.09 195.54 o 3 3 0 1896.79 2005.92 54.77 o -5 4 0 3375.72 3569.88 124.17 o -2 4 0 17119.58 16212.83 438.81 o 1 4 0 1172.34 1249.85 19.51 o 4 4 0 1591.01 1693.43 34.08 o -7 5 0 4596.19 4866.97 113.84 o -4 5 0 1137.87 1185.13 31.58 o -1 5 0 3332.38 3490.42 24.84 o 2 5 0 1518.11 1480.76 34.94 o 5 5 0 36.77 28.73 2.59 o -9 6 0 349.24 340.78 7.01 o -6 6 0 2477.09 2629.24 56.03 o -3 6 0 1901.91 1987.12 19.19 o 0 6 0 2442.70 2566.37 53.27 o 3 6 0 1229.89 1245.61 34.30 o 6 6 0 139.92 139.53 3.81 o -11 7 0 444.31 501.10 30.94 o -8 7 0 322.95 293.42 8.66 o -5 7 0 1527.39 1501.37 69.94 o -2 7 0 4552.69 4808.54 24.11 o 1 7 0 283.49 270.05 13.35 o 4 7 0 1854.19 1775.82 45.46 o 7 7 0 219.65 224.43 9.67 o -13 8 0 321.24 279.90 8.26 o -10 8 0 1179.26 1220.98 31.22 o -7 8 0 286.92 279.92 10.43 o -4 8 0 1570.80 1662.70 15.53 o -1 8 0 332.65 301.48 12.59 o 2 8 0 1730.94 1717.79 50.17 o 5 8 0 251.67 222.07 7.76 o 8 8 0 30.85 42.09 3.17 o -15 9 0 238.13 222.71 6.10 o -12 9 0 113.74 114.01 3.41 o -9 9 0 2949.01 3010.48 43.99 o -6 9 0 1213.51 1215.90 21.49 o -3 9 0 349.54 346.11 6.94 o 0 9 0 2946.95 2957.71 57.47 o 3 9 0 965.06 934.00 12.60 o 6 9 0 192.82 188.04 7.46 o 9 9 0 122.02 118.88 7.94 o -17 10 0 56.99 52.89 3.48 o -14 10 0 326.90 326.52 7.73 o -11 10 0 438.73 401.72 14.54 o -8 10 0 1730.40 1768.61 29.74 o -5 10 0 36.17 34.34 3.42 o -2 10 0 1188.84 1229.59 27.34 o 1 10 0 735.13 739.48 11.27 o 4 10 0 139.20 124.13 3.63 o 7 10 0 121.87 116.89 4.15 o -19 11 0 108.72 122.93 4.58 o -16 11 0 191.66 196.84 5.55 o -13 11 0 173.22 164.12 4.59 o -10 11 0 741.97 747.49 15.55 o -7 11 0 1856.57 1793.43 28.90 o -4 11 0 443.11 486.21 17.50 o -1 11 0 443.72 426.89 11.52 o 2 11 0 932.60 909.68 13.60 o 5 11 0 140.11 152.15 5.44 o 8 11 0 84.71 76.26 4.58 o -18 12 0 82.41 83.63 4.76 o -15 12 0 110.36 104.79 4.44 o -12 12 0 327.01 311.63 12.22 o -9 12 0 965.29 952.77 20.55 o -6 12 0 140.40 133.56 4.33 o -3 12 0 115.76 123.49 4.23 o 0 12 0 326.79 300.91 8.32 o 3 12 0 22.75 28.01 3.17 o 6 12 0 118.56 133.22 4.71 o -17 13 0 40.76 38.40 3.27 o -14 13 0 302.48 287.26 6.69 o -11 13 0 931.36 908.47 13.35 o -8 13 0 255.24 223.37 5.42 o -5 13 0 324.17 290.87 6.52 o -2 13 0 176.51 178.93 4.43 o 1 13 0 304.42 292.33 10.74 o 4 13 0 35.11 32.33 3.27 o -19 14 0 27.20 24.16 3.66 o -16 14 0 55.97 47.28 3.54 o -13 14 0 304.85 298.09 15.91 o -10 14 0 135.23 129.89 3.65 o -7 14 0 225.64 243.01 5.74 o -4 14 0 329.98 322.85 7.33 o -1 14 0 294.37 282.92 9.42 o 2 14 0 24.53 23.28 3.71 o 5 14 0 15.87 17.21 3.82 o -18 15 0 66.74 75.31 4.03 o -15 15 0 53.70 49.78 3.73 o -12 15 0 20.90 25.87 3.11 o -9 15 0 197.23 185.79 7.61 o -6 15 0 241.84 222.04 8.53 o -3 15 0 108.97 97.15 3.76 o 0 15 0 53.89 54.29 3.54 o 3 15 0 67.70 71.51 4.30 o -17 16 0 117.38 107.96 4.68 o -14 16 0 23.08 23.70 3.22 o -11 16 0 137.38 141.13 5.09 o -8 16 0 31.73 31.96 3.17 o -5 16 0 191.94 201.48 5.47 o -2 16 0 53.59 49.27 3.54 o 1 16 0 58.09 66.58 3.96 o -16 17 0 58.95 69.39 4.12 o -13 17 0 33.83 26.92 3.45 o -10 17 0 120.06 113.10 4.53 o -7 17 0 55.86 62.16 5.83 o -4 17 0 43.08 45.43 4.92 o -1 17 0 116.47 103.17 4.45 o -15 18 0 68.24 72.57 4.09 o -12 18 0 116.76 126.18 5.40 o -9 18 0 119.55 116.05 4.72 o -6 18 0 83.26 84.07 5.09 o -3 18 0 65.32 72.60 4.09 o -14 19 0 15.73 21.67 3.72 o -11 19 0 84.59 80.62 4.20 o -8 19 0 107.59 122.22 8.55 o -5 19 0 27.26 25.16 5.11 o -1 1 1 12086.20 11651.14 330.68 o -3 2 1 6306.34 6458.15 212.51 o 0 2 1 6514.81 6564.85 117.82 o -5 3 1 1736.23 1847.49 50.90 o -2 3 1 3720.77 3899.93 101.81 o 1 3 1 2442.76 2584.10 65.58 o -7 4 1 533.89 538.92 23.69 o -4 4 1 625.35 628.89 20.62 o -1 4 1 12612.18 12464.81 259.45 o 2 4 1 474.86 476.75 13.00 o -9 5 1 340.90 320.00 6.76 o -6 5 1 196.84 163.23 5.13 o -3 5 1 833.08 826.32 24.20 o 0 5 1 3766.11 3971.14 21.89 o 3 5 1 190.56 178.19 3.96 o -11 6 1 2.07 2.20 3.41 o -8 6 1 300.21 312.79 6.71 o -5 6 1 1047.05 1104.46 54.08 o -2 6 1 5739.19 5924.91 101.57 o 1 6 1 3794.41 4020.04 78.24 o 4 6 1 527.00 489.09 12.18 o -13 7 1 497.65 450.03 9.93 o -10 7 1 711.08 750.49 22.51 o -7 7 1 702.17 725.33 20.70 o -4 7 1 1370.26 1338.99 15.00 o -1 7 1 2418.10 2576.12 24.44 o 2 7 1 482.11 521.77 13.15 o 5 7 1 74.17 66.15 2.86 o -15 8 1 255.86 249.11 9.46 o -12 8 1 789.43 757.23 13.80 o -9 8 1 340.11 347.22 7.64 o -6 8 1 813.63 800.34 15.15 o -3 8 1 3376.65 3685.53 59.37 o 0 8 1 1234.38 1183.12 25.66 o 3 8 1 549.53 471.13 13.34 o 6 8 1 952.92 937.84 25.20 o -17 9 1 7.43 6.77 3.11 o -14 9 1 391.55 393.29 22.72 o -11 9 1 475.43 443.17 11.27 o -8 9 1 1264.78 1196.85 30.39 o -5 9 1 687.60 778.83 26.50 o -2 9 1 101.94 116.00 3.11 o 1 9 1 744.78 806.31 13.97 o 4 9 1 151.44 152.30 4.13 o 7 9 1 28.68 24.20 10.56 o -19 10 1 40.47 43.20 3.60 o -16 10 1 132.42 141.68 4.09 o -13 10 1 141.79 137.93 4.33 o -10 10 1 722.57 743.26 11.03 o -7 10 1 1358.86 1455.72 13.46 o -4 10 1 363.33 336.71 7.44 o -1 10 1 24.47 14.96 2.31 o 2 10 1 1549.37 1546.63 49.24 o 5 10 1 110.43 122.53 3.68 o 8 10 1 51.60 55.74 4.84 o -18 11 1 14.98 15.21 3.35 o -15 11 1 122.07 112.18 3.90 o -12 11 1 271.75 290.75 6.23 o -9 11 1 329.65 327.36 16.16 o -6 11 1 251.46 254.25 5.17 o -3 11 1 159.41 196.17 4.88 o 0 11 1 182.02 166.51 7.55 o 3 11 1 7.29 11.41 2.84 o 6 11 1 83.80 68.88 3.96 o -17 12 1 85.06 82.75 3.89 o -14 12 1 48.34 45.62 4.85 o -11 12 1 191.94 204.76 8.27 o -8 12 1 397.32 429.49 9.50 o -5 12 1 419.41 418.61 9.00 o -2 12 1 53.62 56.88 2.92 o 1 12 1 240.99 207.60 5.77 o 4 12 1 17.17 15.65 3.39 o 7 12 1 39.15 40.28 4.20 o -19 13 1 110.40 107.37 4.67 o -16 13 1 38.59 35.59 4.43 o -13 13 1 50.18 49.89 3.04 o -10 13 1 417.49 442.32 10.48 o -7 13 1 4.89 5.30 2.50 o -4 13 1 55.75 68.05 3.03 o -1 13 1 362.61 345.65 8.43 o 2 13 1 11.76 16.60 4.51 o 5 13 1 12.21 11.20 3.54 o -18 14 1 38.64 50.11 3.64 o -15 14 1 11.39 5.94 4.81 o -12 14 1 198.29 190.46 5.16 o -9 14 1 100.86 77.55 3.63 o -6 14 1 3.80 4.05 3.61 o -3 14 1 131.53 115.70 4.17 o 0 14 1 139.61 144.84 4.21 o 3 14 1 47.38 47.45 7.22 o -17 15 1 21.15 22.46 3.48 o -14 15 1 42.88 56.83 5.74 o -11 15 1 234.79 238.19 6.34 o -8 15 1 52.88 64.18 3.35 o -5 15 1 142.97 140.93 4.02 o -2 15 1 259.77 267.71 7.13 o 1 15 1 47.88 55.17 3.72 o -16 16 1 80.74 78.79 4.29 o -13 16 1 75.53 73.83 6.49 o -10 16 1 85.21 86.69 3.72 o -7 16 1 71.51 76.34 3.65 o -4 16 1 12.47 9.91 4.73 o -1 16 1 154.66 147.20 6.96 o -15 17 1 56.59 68.01 4.74 o -12 17 1 130.48 141.04 6.93 o -9 17 1 119.47 121.79 6.43 o -6 17 1 42.30 47.79 4.61 o -3 17 1 55.97 71.27 3.72 o -14 18 1 56.08 49.40 4.35 o -11 18 1 97.67 103.63 6.67 o -8 18 1 108.36 101.44 4.65 o -5 18 1 11.54 12.43 3.72 o -13 19 1 122.60 131.90 4.70 o -10 19 1 34.57 37.08 3.96 o -7 19 1 117.38 136.80 4.79 o 0 1 2 670.78 796.61 13.05 o -2 2 2 2137.59 2357.67 56.49 o 1 2 2 1602.26 1746.24 26.72 o -4 3 2 263.19 293.70 18.61 o -1 3 2 952.27 980.51 27.48 o 2 3 2 777.41 1013.29 20.17 o -6 4 2 39.45 32.85 2.25 o -3 4 2 259.38 229.89 7.34 o 0 4 2 26.68 29.12 2.01 o 3 4 2 443.27 513.15 13.32 o -8 5 2 180.98 183.83 4.39 o -5 5 2 1652.68 1862.98 40.28 o -2 5 2 623.45 618.57 10.63 o 1 5 2 590.04 608.46 9.84 o 4 5 2 146.49 126.89 3.67 o -10 6 2 52.74 54.43 2.61 o -7 6 2 10.91 5.38 5.46 o -4 6 2 283.65 297.37 6.65 o -1 6 2 2795.95 2964.50 81.97 o 2 6 2 332.66 364.33 13.48 o 5 6 2 23.32 20.44 2.73 o -12 7 2 168.57 149.14 6.15 o -9 7 2 335.34 302.91 8.60 o -6 7 2 73.87 63.00 2.44 o -3 7 2 1020.97 1126.49 20.46 o 0 7 2 1105.67 1090.57 16.85 o 3 7 2 51.96 36.57 3.04 o 6 7 2 273.43 271.86 12.49 o -14 8 2 541.47 598.01 12.44 o -11 8 2 671.49 630.36 22.91 o -8 8 2 35.12 40.82 4.66 o -5 8 2 344.29 301.88 15.38 o -2 8 2 281.50 262.40 9.47 o 1 8 2 593.39 584.20 10.23 o 4 8 2 209.50 228.91 5.85 o 7 8 2 189.75 167.37 4.76 o -16 9 2 27.98 33.17 3.15 o -13 9 2 627.89 560.90 13.71 o -10 9 2 42.17 43.16 2.73 o -7 9 2 291.43 317.40 8.13 o -4 9 2 500.12 494.39 17.25 o -1 9 2 72.09 72.47 3.48 o 2 9 2 1004.52 927.59 27.78 o 5 9 2 298.70 290.42 10.79 o 8 9 2 6.45 8.78 3.30 o -18 10 2 15.17 10.76 5.60 o -15 10 2 46.83 47.03 3.41 o -12 10 2 337.74 352.79 15.87 o -9 10 2 239.14 243.16 12.68 o -6 10 2 152.40 151.77 4.45 o -3 10 2 241.10 236.60 5.64 o 0 10 2 450.99 461.31 10.15 o 3 10 2 207.55 179.15 5.11 o 6 10 2 4.28 2.95 5.85 o -17 11 2 38.95 39.79 4.37 o -14 11 2 2.07 -0.13 4.10 o -11 11 2 351.17 334.20 19.49 o -8 11 2 288.06 271.96 5.97 o -5 11 2 429.28 432.25 9.48 o -2 11 2 9.13 0.62 4.00 o 1 11 2 232.32 253.15 8.21 o 4 11 2 20.28 18.81 3.21 o 7 11 2 30.18 31.48 4.06 o -16 12 2 108.06 112.74 4.03 o -13 12 2 24.40 25.24 3.05 o -10 12 2 288.43 234.62 5.23 o -7 12 2 15.16 3.03 4.74 o -4 12 2 2.60 -0.58 3.77 o -1 12 2 436.79 429.78 17.42 o 2 12 2 40.29 35.32 3.23 o 5 12 2 5.17 8.59 3.04 o -18 13 2 41.61 49.53 6.96 o -15 13 2 93.39 94.10 3.76 o -12 13 2 2.01 -6.73 6.73 o -9 13 2 58.45 75.31 3.17 o -6 13 2 45.03 54.45 3.11 o -3 13 2 82.10 81.05 3.29 o 0 13 2 84.69 88.17 3.75 o 3 13 2 22.69 30.60 5.57 o -17 14 2 26.24 29.12 3.48 o -14 14 2 37.27 27.99 3.41 o -11 14 2 92.51 81.97 3.54 o -8 14 2 80.73 93.23 3.45 o -5 14 2 36.33 34.15 3.41 o -2 14 2 140.55 139.96 4.32 o 1 14 2 61.31 55.32 3.65 o -16 15 2 5.29 10.61 4.07 o -13 15 2 99.28 108.26 5.51 o -10 15 2 94.35 108.78 4.09 o -7 15 2 28.41 31.05 3.17 o -4 15 2 23.55 26.61 3.35 o -1 15 2 154.21 148.39 4.57 o 2 15 2 42.61 47.59 4.09 o -15 16 2 19.56 22.69 3.85 o -12 16 2 220.89 198.84 5.96 o -9 16 2 24.87 25.59 3.31 o -6 16 2 34.68 36.36 3.54 o -3 16 2 45.44 45.06 4.04 o 0 16 2 121.51 138.37 4.64 o -14 17 2 48.87 48.37 3.96 o -11 17 2 41.76 50.23 3.78 o -8 17 2 148.57 145.26 4.45 o -5 17 2 4.35 2.56 3.93 o -2 17 2 48.72 49.19 4.15 o -13 18 2 82.65 78.06 4.15 o -10 18 2 54.53 54.42 4.02 o -7 18 2 37.38 43.75 3.87 o 0 0 3 84.90 90.08 4.76 o 1 1 3 593.28 616.63 15.69 o -1 2 3 1442.39 1567.36 13.05 o 2 2 3 256.02 238.79 5.24 o -3 3 3 847.69 963.09 22.91 o 0 3 3 1111.62 1097.60 15.28 o 3 3 3 403.46 364.39 18.75 o -5 4 3 744.14 783.50 14.34 o -2 4 3 645.65 695.85 9.55 o 1 4 3 313.68 259.92 8.34 o 4 4 3 289.61 243.45 9.08 o -7 5 3 497.11 534.03 16.42 o -4 5 3 1658.39 1714.55 14.81 o -1 5 3 576.57 527.05 9.52 o 2 5 3 720.75 693.45 18.12 o 5 5 3 93.67 96.87 3.63 o -9 6 3 340.76 321.10 8.33 o -6 6 3 238.39 213.21 6.34 o -3 6 3 1505.59 1464.39 14.17 o 0 6 3 621.55 629.02 10.31 o 3 6 3 275.04 312.74 7.64 o 6 6 3 147.48 130.41 3.66 o -11 7 3 237.09 239.23 6.15 o -8 7 3 273.11 249.11 7.82 o -5 7 3 533.11 540.32 11.18 o -2 7 3 611.43 598.44 19.38 o 1 7 3 874.03 789.83 27.79 o 4 7 3 53.30 57.03 3.11 o 7 7 3 171.40 186.54 11.88 o -13 8 3 525.91 523.00 18.77 o -10 8 3 288.74 274.60 8.47 o -7 8 3 74.52 66.46 3.25 o -4 8 3 892.82 875.46 29.96 o -1 8 3 468.22 481.24 10.15 o 2 8 3 143.57 130.20 4.60 o 5 8 3 293.22 324.62 20.22 o 8 8 3 46.23 54.40 3.85 o -15 9 3 108.90 109.59 4.45 o -12 9 3 425.65 488.29 21.12 o -9 9 3 186.65 172.36 9.53 o -6 9 3 58.70 54.46 3.57 o -3 9 3 914.70 856.07 28.03 o 0 9 3 14.51 18.03 6.04 o 3 9 3 217.94 221.16 7.57 o 6 9 3 96.92 95.83 4.87 o -17 10 3 34.44 40.60 4.00 o -14 10 3 97.35 88.18 4.11 o -11 10 3 288.00 290.33 16.17 o -8 10 3 126.44 110.60 3.66 o -5 10 3 832.30 861.54 21.78 o -2 10 3 141.99 144.79 4.33 o 1 10 3 336.18 301.95 9.79 o 4 10 3 130.27 107.61 4.76 o 7 10 3 76.37 83.28 7.67 o -16 11 3 93.07 91.52 4.39 o -13 11 3 5.85 9.20 2.93 o -10 11 3 261.51 281.28 13.64 o -7 11 3 327.29 315.87 8.61 o -4 11 3 110.99 117.57 6.11 o -1 11 3 220.59 192.91 5.31 o 2 11 3 3.28 1.73 3.70 o 5 11 3 30.63 28.80 3.76 o -15 12 3 174.76 201.17 5.84 o -12 12 3 26.03 24.33 9.02 o -9 12 3 245.28 258.79 7.85 o -6 12 3 293.32 335.12 8.76 o -3 12 3 78.16 74.14 4.32 o 0 12 3 166.85 166.46 6.42 o 3 12 3 23.40 41.46 3.35 o -14 13 3 113.82 105.47 4.15 o -11 13 3 49.54 58.42 3.65 o -8 13 3 61.28 53.40 3.60 o -5 13 3 156.89 152.36 5.34 o -2 13 3 190.46 185.12 4.73 o 1 13 3 85.19 85.57 5.14 o -16 14 3 39.65 41.44 3.86 o -13 14 3 206.68 234.93 12.76 o -10 14 3 47.49 36.24 4.50 o -7 14 3 82.28 87.33 4.58 o -4 14 3 115.13 121.80 5.38 o -1 14 3 153.32 150.83 4.70 o 2 14 3 56.78 47.32 4.08 o -15 15 3 23.27 20.19 3.60 o -12 15 3 257.33 239.26 7.13 o -9 15 3 52.58 49.84 3.60 o -6 15 3 31.92 37.58 3.50 o -3 15 3 94.95 89.87 5.63 o 0 15 3 120.04 127.23 4.85 o -14 16 3 66.64 68.28 4.50 o -11 16 3 133.14 137.48 10.50 o -8 16 3 87.92 87.82 4.27 o -5 16 3 29.86 32.83 3.96 o -2 16 3 37.38 44.57 7.07 o -10 17 3 56.80 68.12 4.15 o -7 17 3 79.84 78.04 4.09 o -1 1 4 45.58 48.23 2.75 o -3 2 4 488.14 477.51 10.05 o 0 2 4 237.15 213.32 5.55 o -5 3 4 259.35 227.56 5.72 o -2 3 4 798.02 783.85 19.34 o 1 3 4 763.88 744.14 11.82 o -7 4 4 237.75 245.31 6.15 o -4 4 4 690.47 670.01 16.71 o -1 4 4 169.36 153.96 6.32 o 2 4 4 729.72 736.59 12.61 o -9 5 4 228.64 214.15 12.80 o -6 5 4 341.24 331.93 12.97 o -3 5 4 718.20 684.08 11.84 o 0 5 4 338.22 347.15 8.00 o 3 5 4 487.52 493.32 22.90 o -11 6 4 88.26 98.09 7.05 o -8 6 4 391.29 377.82 12.13 o -5 6 4 382.19 390.59 9.94 o -2 6 4 144.86 158.20 5.59 o 1 6 4 493.09 458.00 11.02 o 4 6 4 164.33 183.88 6.71 o -13 7 4 59.08 57.64 5.06 o -10 7 4 303.82 263.47 10.14 o -7 7 4 127.93 99.19 5.29 o -4 7 4 497.05 464.41 10.74 o -1 7 4 306.86 294.21 7.52 o 2 7 4 58.54 66.92 3.74 o 5 7 4 217.71 206.72 11.12 o -15 8 4 46.08 54.99 4.44 o -12 8 4 96.89 112.22 9.11 o -9 8 4 297.39 307.58 8.50 o -6 8 4 234.80 232.63 6.21 o -3 8 4 370.10 389.43 13.92 o 0 8 4 215.68 218.50 6.13 o 3 8 4 28.62 32.22 3.71 o 6 8 4 80.25 82.29 4.01 o -14 9 4 82.00 68.50 4.07 o -11 9 4 115.22 116.01 7.68 o -8 9 4 130.16 117.70 3.96 o -5 9 4 141.87 119.14 4.03 o -2 9 4 276.44 272.13 7.33 o 1 9 4 12.32 13.36 2.97 o 4 9 4 69.38 70.23 5.13 o -13 10 4 72.20 85.12 4.21 o -10 10 4 116.24 141.77 7.40 o -7 10 4 52.09 59.71 5.62 o -4 10 4 258.20 269.39 7.20 o -1 10 4 64.57 64.02 3.65 o 2 10 4 21.28 30.67 3.45 o 5 10 4 47.07 52.17 5.12 o -15 11 4 88.36 88.24 4.55 o -12 11 4 66.93 68.37 3.66 o -9 11 4 14.28 5.35 3.86 o -6 11 4 615.55 580.45 13.63 o -3 11 4 63.70 67.47 3.72 o 0 11 4 76.36 86.81 5.51 o 3 11 4 30.95 32.61 3.54 o -14 12 4 81.95 98.82 4.37 o -11 12 4 7.26 4.76 4.19 o -8 12 4 116.41 133.53 4.45 o -5 12 4 170.52 185.51 5.24 o -2 12 4 125.05 123.15 5.96 o 1 12 4 50.39 48.18 3.96 o -13 13 4 73.46 78.08 4.32 o -10 13 4 24.07 22.76 2.95 o -7 13 4 67.88 69.53 3.89 o -4 13 4 190.29 189.22 7.89 o -1 13 4 68.99 62.88 3.90 o -12 14 4 107.58 115.10 4.92 o -9 14 4 34.03 31.24 3.90 o -6 14 4 68.58 68.70 3.85 o -3 14 4 81.29 83.56 4.97 o -11 15 4 68.93 75.91 4.21 o -8 15 4 69.77 70.58 5.12 o -5 15 4 37.60 46.90 3.87 o 0 1 5 11.11 11.77 4.48 o -2 2 5 244.99 230.18 8.50 o 1 2 5 247.61 247.03 6.47 o -4 3 5 148.44 146.74 4.81 o -1 3 5 80.62 91.32 3.72 o 2 3 5 145.32 132.66 4.20 o -6 4 5 29.91 24.29 8.48 o -3 4 5 225.01 209.84 5.71 o 0 4 5 152.02 150.29 4.33 o 3 4 5 119.03 117.65 10.98 o -8 5 5 71.36 75.77 3.90 o -5 5 5 68.56 82.10 3.70 o -2 5 5 34.43 38.75 3.34 o 1 5 5 183.87 170.68 4.75 o 4 5 5 116.37 110.54 4.60 o -10 6 5 50.06 49.20 3.78 o -7 6 5 93.43 76.61 3.85 o -4 6 5 51.97 46.26 3.45 o -1 6 5 17.34 14.61 3.30 o 2 6 5 69.12 59.68 3.82 o 5 6 5 61.38 68.05 4.08 o -12 7 5 5.54 4.61 4.67 o -9 7 5 109.20 118.64 6.88 o -6 7 5 102.08 114.91 5.06 o -3 7 5 19.67 11.10 3.30 o 0 7 5 86.23 96.58 4.07 o 3 7 5 11.25 12.26 3.68 o -11 8 5 13.51 12.77 3.64 o -8 8 5 105.04 103.18 4.09 o -5 8 5 16.50 5.18 7.88 o -2 8 5 23.39 19.34 3.48 o 1 8 5 17.88 23.88 3.39 o 4 8 5 18.42 17.00 3.86 o -10 9 5 38.16 40.63 3.96 o -7 9 5 64.92 61.08 3.89 o -4 9 5 44.98 53.86 4.09 o -1 9 5 32.06 32.34 3.72 o 2 9 5 35.78 29.17 4.56 o -9 10 5 29.93 32.71 3.56 o -6 10 5 78.80 83.32 3.89 o -3 10 5 34.04 34.59 3.78 o 0 10 5 51.61 54.31 5.03 o -8 11 5 6.27 3.57 6.18 o -5 11 5 90.17 78.23 5.73 o -2 11 5 65.87 68.19 4.71 o -7 12 5 30.89 28.31 4.88 o -4 12 5 85.41 103.67 6.49 o 0 0 6 15.45 19.35 5.71 o 1 1 6 34.80 33.55 3.58 o -1 2 6 39.62 39.62 5.01 o 2 2 6 78.10 70.62 4.26 o -3 3 6 102.04 99.23 4.27 o 0 3 6 52.80 53.36 5.44 o 3 3 6 37.61 49.14 5.98 o -5 4 6 43.59 52.66 4.11 o -2 4 6 76.30 75.71 4.39 o 1 4 6 46.62 52.70 4.12 o -7 5 6 22.12 35.50 3.60 o -4 5 6 19.93 25.02 3.65 o -1 5 6 16.46 19.40 4.40 o 2 5 6 58.11 60.79 4.27 o -6 6 6 55.31 59.83 4.15 o -3 6 6 4.61 5.81 5.14 o 0 6 6 39.73 44.57 3.92 o -5 7 6 19.75 23.55 3.66 o -2 7 6 2.15 -1.80 5.56 o