#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/07/2010771.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2010771_Fobs loop_ _publ_author_name 'Freyhardt, Clemens C.' 'Wiebcke, Michael' 'Felsche, J\"urgen' _publ_section_title ; The monoclinic and cubic phases of metaboric acid (precise redeterminations) ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 276 _journal_page_last 278 _journal_volume 56 _journal_year 2000 _chemical_name_systematic 'metaboric acid, \g-phase' _space_group_IT_number 218 _symmetry_space_group_name_Hall 'P -4n 2 3' _symmetry_space_group_name_H-M 'P -4 3 n' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 8.8811(3) _cell_length_b 8.8811(3) _cell_length_c 8.8811(3) _exptl_absorpt_correction_type none _exptl_crystal_F_000 528.00 _refine_ls_extinction_coef 0.393(13) _refine_ls_extinction_method SHELXL97 _reflns_d_resolution_high 0.4649 _[local]_cod_data_source_file sk1343IIsup3.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title gbs _shelx_refln_list_code 4 _shelx_f_calc_maximum 92.46 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z' '-x, y, -z' 'x, -y, -z' 'z, x, y' 'z, -x, -y' '-z, -x, y' '-z, x, -y' 'y, z, x' '-y, z, -x' 'y, -z, -x' '-y, -z, x' 'y+1/2, x+1/2, z+1/2' '-y+1/2, -x+1/2, z+1/2' 'y+1/2, -x+1/2, -z+1/2' '-y+1/2, x+1/2, -z+1/2' 'x+1/2, z+1/2, y+1/2' '-x+1/2, z+1/2, -y+1/2' '-x+1/2, -z+1/2, y+1/2' 'x+1/2, -z+1/2, -y+1/2' 'z+1/2, y+1/2, x+1/2' 'z+1/2, -y+1/2, -x+1/2' '-z+1/2, y+1/2, -x+1/2' '-z+1/2, -y+1/2, x+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 1 1 1083.50 1165.57 32.40 o 0 0 2 8547.93 6639.14 523.98 o 0 1 2 1012.50 1030.39 31.27 o 1 1 2 1364.49 1421.70 10.77 o 0 2 2 1538.90 1648.87 21.08 o 2 2 2 4503.75 4108.34 61.94 o 0 1 3 2120.62 2118.49 46.42 o 0 2 3 136.33 133.13 4.17 o 1 2 3 1100.75 1163.57 25.26 o 0 3 3 6111.83 5735.87 529.88 o 2 3 3 2082.97 2207.46 9.92 o 0 0 4 6598.93 6044.28 506.69 o 0 1 4 598.22 631.29 10.34 o 1 1 4 549.43 622.06 18.40 o 0 2 4 447.17 500.35 5.52 o 1 2 4 5805.87 5749.88 158.11 o 2 2 4 457.64 504.27 4.47 o 0 3 4 150.52 167.22 2.97 o 1 3 4 160.95 158.23 2.89 o 2 3 4 54.78 60.93 1.73 o 3 3 4 1269.90 1359.87 8.38 o 0 4 4 111.05 105.55 2.16 o 2 4 4 96.25 99.88 1.95 o 4 4 4 2322.58 2299.16 12.41 o 0 1 5 278.54 271.70 5.56 o 0 2 5 93.36 88.69 3.37 o 1 2 5 414.15 443.06 4.47 o 0 3 5 1594.62 1707.70 48.84 o 1 3 5 510.55 533.82 7.32 o 2 3 5 409.56 433.47 10.33 o 0 4 5 273.64 288.86 4.48 o 1 4 5 57.55 63.77 1.29 o 2 4 5 1945.91 1960.83 45.71 o 3 4 5 228.80 233.43 4.50 o 0 5 5 540.80 540.39 11.31 o 2 5 5 141.07 147.32 5.09 o 4 5 5 884.25 837.38 12.00 o 0 0 6 248.61 249.66 3.66 o 0 1 6 0.60 1.33 2.10 o 1 1 6 617.59 656.09 5.84 o 0 2 6 1561.94 1626.05 25.28 o 1 2 6 371.29 379.00 4.59 o 2 2 6 2941.70 2987.06 24.08 o 0 3 6 190.90 203.80 3.64 o 1 3 6 897.17 907.79 13.17 o 2 3 6 74.77 78.44 1.59 o 3 3 6 1965.30 1949.55 47.37 o 0 4 6 96.78 104.82 2.04 o 1 4 6 317.25 316.05 4.58 o 2 4 6 7.91 7.13 1.02 o 3 4 6 112.62 106.69 2.83 o 4 4 6 1645.10 1654.73 15.82 o 0 5 6 13.21 15.15 1.73 o 1 5 6 331.20 314.26 5.89 o 2 5 6 212.33 193.38 7.11 o 3 5 6 869.54 834.32 12.69 o 4 5 6 346.51 326.28 5.73 o 5 5 6 238.01 245.82 5.71 o 0 6 6 1646.28 1512.37 18.57 o 2 6 6 1808.54 1767.65 16.68 o 4 6 6 52.83 54.27 1.67 o 6 6 6 1077.51 1083.49 10.62 o 0 1 7 2.77 3.01 1.95 o 0 2 7 32.55 32.19 1.13 o 1 2 7 174.72 172.15 4.73 o 0 3 7 3.18 4.07 0.99 o 1 3 7 1184.81 1186.40 23.00 o 2 3 7 5.20 7.39 2.39 o 0 4 7 739.85 682.14 9.67 o 1 4 7 19.49 16.65 1.13 o 2 4 7 1000.20 969.08 8.84 o 3 4 7 275.53 270.36 4.72 o 0 5 7 11.53 12.25 1.23 o 1 5 7 1021.98 1004.20 21.29 o 2 5 7 139.37 128.75 3.35 o 3 5 7 734.99 694.99 9.08 o 4 5 7 25.28 22.37 1.80 o 0 6 7 426.91 411.09 10.23 o 1 6 7 7.94 7.29 1.16 o 2 6 7 13.14 17.12 1.26 o 3 6 7 92.79 89.92 2.24 o 4 6 7 5.16 5.65 1.54 o 5 6 7 23.00 24.13 1.48 o 0 7 7 0.26 0.98 3.10 o 2 7 7 3.03 4.20 2.59 o 4 7 7 45.80 49.15 1.90 o 6 7 7 58.11 60.57 2.80 o 0 0 8 6963.34 6462.02 78.05 o 0 1 8 11.91 13.93 1.05 o 1 1 8 214.14 207.31 8.24 o 0 2 8 456.94 432.20 6.44 o 1 2 8 1200.44 1158.77 16.75 o 2 2 8 649.65 602.15 8.79 o 0 3 8 255.71 234.43 4.45 o 1 3 8 643.23 650.11 7.14 o 2 3 8 19.95 19.26 1.32 o 3 3 8 706.69 666.74 7.54 o 0 4 8 360.77 348.01 5.47 o 1 4 8 116.61 110.07 2.43 o 2 4 8 58.96 46.20 1.89 o 3 4 8 458.69 468.16 7.92 o 4 4 8 91.94 91.35 1.86 o 0 5 8 210.84 180.02 5.55 o 1 5 8 30.88 24.83 1.33 o 2 5 8 85.82 84.95 1.80 o 3 5 8 215.86 224.66 8.19 o 4 5 8 160.18 150.74 2.96 o 5 5 8 123.24 132.44 2.71 o 0 6 8 32.00 35.62 1.48 o 1 6 8 116.99 118.82 3.84 o 2 6 8 163.46 165.85 3.35 o 3 6 8 79.58 78.03 1.87 o 4 6 8 266.13 280.32 8.10 o 5 6 8 32.02 31.99 1.59 o 6 6 8 64.39 65.54 2.05 o 0 7 8 83.31 82.51 1.97 o 1 7 8 31.41 31.70 1.69 o 2 7 8 180.79 188.01 7.91 o 3 7 8 255.42 254.24 5.55 o 4 7 8 336.09 348.21 8.64 o 5 7 8 12.64 13.96 1.93 o 6 7 8 335.44 342.84 6.88 o 7 7 8 112.54 112.16 2.52 o 0 8 8 464.04 469.90 10.62 o 2 8 8 157.43 155.34 3.06 o 4 8 8 462.71 463.97 7.80 o 6 8 8 36.91 34.36 1.81 o 8 8 8 229.39 226.80 4.55 o 0 1 9 3.32 2.50 1.53 o 0 2 9 7.17 7.30 1.17 o 1 2 9 641.28 627.55 10.46 o 0 3 9 85.74 82.68 2.77 o 1 3 9 119.35 120.43 4.28 o 2 3 9 33.91 42.54 1.84 o 0 4 9 48.54 46.58 1.76 o 1 4 9 107.20 99.30 2.09 o 2 4 9 32.89 33.73 1.45 o 3 4 9 384.48 387.95 6.35 o 0 5 9 28.34 27.99 2.19 o 1 5 9 364.82 371.48 8.21 o 2 5 9 93.85 91.42 1.98 o 3 5 9 29.92 28.20 2.01 o 4 5 9 351.52 353.67 8.47 o 0 6 9 0.74 0.63 3.45 o 1 6 9 79.67 75.42 2.43 o 2 6 9 154.99 156.08 3.61 o 3 6 9 33.63 33.09 1.80 o 4 6 9 191.15 193.86 3.98 o 5 6 9 60.31 60.54 1.98 o 0 7 9 69.30 67.63 2.40 o 1 7 9 165.23 167.51 3.90 o 2 7 9 173.06 171.59 4.32 o 3 7 9 220.91 229.17 4.47 o 4 7 9 120.32 123.12 4.52 o 5 7 9 641.56 643.74 10.83 o 6 7 9 31.09 31.34 1.82 o 0 8 9 32.36 34.01 2.66 o 1 8 9 63.99 67.04 2.81 o 2 8 9 358.37 367.75 7.14 o 3 8 9 117.12 118.68 2.51 o 4 8 9 31.92 29.88 2.24 o 5 8 9 21.71 19.93 3.86 o 6 8 9 90.24 92.81 3.03 o 7 8 9 2.33 1.17 3.55 o 0 9 9 46.98 48.56 2.00 o 2 9 9 930.29 890.21 60.41 o 4 9 9 248.23 236.63 17.38 o 6 9 9 49.44 48.92 2.36 o 8 9 9 23.42 24.93 2.09 o 0 0 10 341.68 350.77 7.53 o 0 1 10 166.20 163.04 3.19 o 1 1 10 5.65 7.16 1.23 o 0 2 10 44.82 47.26 2.48 o 1 2 10 100.52 92.81 1.94 o 2 2 10 53.48 52.89 1.66 o 0 3 10 21.69 23.60 1.43 o 1 3 10 372.63 378.45 6.38 o 2 3 10 224.00 219.01 4.47 o 3 3 10 13.20 14.04 1.72 o 0 4 10 4.07 3.63 1.87 o 1 4 10 230.08 236.28 5.50 o 2 4 10 74.61 75.07 2.41 o 3 4 10 178.50 176.87 6.67 o 4 4 10 46.80 47.61 3.15 o 0 5 10 107.67 98.10 2.86 o 1 5 10 10.53 11.43 1.93 o 2 5 10 335.10 340.39 9.96 o 3 5 10 136.69 136.07 2.75 o 4 5 10 932.32 951.82 11.68 o 5 5 10 115.85 119.68 8.49 o 0 6 10 1.76 1.00 4.40 o 1 6 10 381.74 384.78 10.90 o 2 6 10 277.72 276.23 5.34 o 3 6 10 26.58 25.93 1.69 o 4 6 10 34.53 36.31 1.80 o 5 6 10 135.89 134.72 3.03 o 6 6 10 192.20 191.86 11.00 o 0 7 10 377.62 376.77 10.42 o 1 7 10 33.26 30.84 1.75 o 2 7 10 86.14 82.21 2.55 o 3 7 10 103.85 99.87 7.79 o 4 7 10 449.53 430.70 35.99 o 5 7 10 15.87 16.71 3.30 o 6 7 10 26.10 26.20 1.86 o 7 7 10 42.80 42.61 2.22 o 0 8 10 17.85 16.46 1.72 o 1 8 10 461.23 448.59 20.84 o 2 8 10 241.21 230.87 15.84 o 3 8 10 43.15 41.20 5.04 o 4 8 10 6.76 6.80 2.82 o 5 8 10 136.45 136.90 3.05 o 6 8 10 43.97 45.06 2.08 o 7 8 10 246.38 247.34 4.96 o 8 8 10 8.03 9.36 1.92 o 0 9 10 33.93 34.66 1.94 o 1 9 10 68.59 68.35 3.23 o 2 9 10 275.12 267.65 15.25 o 3 9 10 6.93 7.38 1.69 o 4 9 10 191.22 176.79 19.01 o 5 9 10 32.17 24.95 8.33 o 6 9 10 390.85 388.76 7.31 o 7 9 10 57.39 59.06 3.14 o 8 9 10 109.32 111.83 5.59 o 9 9 10 199.53 203.81 8.63 o 0 10 10 7.32 8.47 1.71 o 2 10 10 60.84 59.02 2.28 o 4 10 10 8.15 9.03 1.76 o 6 10 10 269.21 275.71 5.69 o 8 10 10 134.50 136.16 3.32 o 10 10 10 2.10 4.59 2.05 o 0 1 11 3.86 3.50 2.85 o 0 2 11 17.73 16.75 1.69 o 1 2 11 117.04 112.47 2.98 o 0 3 11 45.30 47.25 1.82 o 1 3 11 114.25 111.54 2.81 o 2 3 11 143.97 151.30 3.02 o 0 4 11 10.47 10.87 1.51 o 1 4 11 31.77 33.31 1.72 o 2 4 11 232.56 233.76 7.56 o 3 4 11 241.06 242.73 4.93 o 0 5 11 8.27 8.98 1.52 o 1 5 11 122.93 125.25 2.55 o 2 5 11 11.52 11.62 1.99 o 3 5 11 75.93 74.59 2.28 o 4 5 11 96.64 89.01 11.90 o 0 6 11 260.45 262.72 8.80 o 1 6 11 256.41 246.97 11.47 o 2 6 11 105.45 101.68 5.09 o 3 6 11 57.22 54.08 3.04 o 4 6 11 89.37 89.00 2.89 o 5 6 11 18.42 16.66 3.57 o 0 7 11 31.20 32.53 2.96 o 1 7 11 320.62 311.89 11.44 o 2 7 11 10.25 11.39 1.70 o 3 7 11 53.41 51.37 4.02 o 4 7 11 185.65 180.88 10.24 o 5 7 11 423.33 427.36 10.76 o 6 7 11 39.50 40.23 2.45 o 0 8 11 92.47 91.72 3.58 o 1 8 11 126.88 122.54 2.98 o 2 8 11 69.71 69.34 5.00 o 3 8 11 15.73 15.01 2.25 o 4 8 11 235.06 229.45 19.86 o 5 8 11 36.57 33.80 6.50 o 6 8 11 440.63 439.98 10.17 o 7 8 11 87.49 90.92 4.85 o 0 9 11 113.91 110.45 3.83 o 1 9 11 15.84 14.69 1.81 o 2 9 11 9.13 8.57 2.19 o 3 9 11 121.41 119.53 9.15 o 4 9 11 27.62 25.29 4.51 o 5 9 11 237.67 240.99 4.85 o 6 9 11 21.47 22.37 2.11 o 7 9 11 73.00 75.70 2.78 o 8 9 11 24.70 25.22 2.19 o 0 10 11 0.23 0.68 3.33 o 1 10 11 207.01 203.79 8.04 o 2 10 11 77.56 75.48 2.98 o 3 10 11 32.09 30.65 3.25 o 4 10 11 24.38 23.20 4.51 o 5 10 11 83.33 86.33 2.81 o 6 10 11 268.77 273.43 5.45 o 7 10 11 42.74 42.59 2.43 o 8 10 11 78.80 79.93 2.81 o 9 10 11 5.26 6.05 2.13 o 0 11 11 82.98 85.27 2.80 o 2 11 11 226.05 225.61 4.81 o 4 11 11 108.99 98.11 23.70 o 6 11 11 118.17 119.22 3.48 o 8 11 11 40.90 42.66 2.77 o 10 11 11 124.85 127.39 6.53 o 0 0 12 1018.60 1034.09 20.53 o 0 1 12 76.63 78.00 2.25 o 1 1 12 467.51 455.51 7.76 o 0 2 12 342.43 338.97 6.50 o 1 2 12 211.52 211.60 4.76 o 2 2 12 246.06 241.17 4.65 o 0 3 12 30.43 31.67 1.91 o 1 3 12 550.78 544.05 11.95 o 2 3 12 184.76 179.50 4.53 o 3 3 12 418.19 412.82 10.33 o 0 4 12 8.85 9.96 2.39 o 1 4 12 107.81 102.56 4.49 o 2 4 12 29.78 27.65 1.80 o 3 4 12 60.44 58.62 4.07 o 4 4 12 145.81 135.28 14.18 o 0 5 12 10.57 10.97 1.81 o 1 5 12 188.59 183.81 8.81 o 2 5 12 99.35 96.93 7.45 o 3 5 12 144.14 138.54 9.51 o 4 5 12 49.78 45.78 6.64 o 5 5 12 270.14 277.90 12.18 o 0 6 12 163.82 159.66 3.15 o 1 6 12 46.95 47.62 2.44 o 2 6 12 120.75 114.91 5.85 o 3 6 12 58.33 58.10 3.19 o 4 6 12 81.46 77.86 8.30 o 5 6 12 241.11 246.10 5.97 o 6 6 12 99.92 105.01 2.71 o 0 7 12 351.97 345.09 10.44 o 1 7 12 20.77 20.05 1.94 o 2 7 12 21.04 22.07 1.85 o 3 7 12 222.77 215.28 12.52 o 4 7 12 10.69 10.44 2.84 o 5 7 12 151.62 155.80 3.23 o 6 7 12 165.72 172.49 4.88 o 7 7 12 22.43 22.87 2.24 o 0 8 12 107.53 108.36 2.74 o 1 8 12 66.47 64.22 2.86 o 2 8 12 83.54 82.15 3.11 o 3 8 12 31.11 29.29 4.12 o 4 8 12 2.44 -0.38 5.50 o 5 8 12 48.89 45.77 10.21 o 6 8 12 56.47 57.54 2.53 o 7 8 12 256.69 258.77 6.63 o 8 8 12 32.98 32.67 2.36 o 0 9 12 68.29 70.35 2.46 o 1 9 12 340.49 329.93 13.15 o 2 9 12 15.31 15.59 3.08 o 3 9 12 53.01 52.74 3.80 o 4 9 12 97.91 98.30 5.82 o 5 9 12 39.36 35.94 13.06 o 6 9 12 46.87 49.64 2.49 o 7 9 12 94.87 98.72 3.20 o 8 9 12 57.52 59.13 3.04 o 9 9 12 48.77 47.75 2.61 o 0 10 12 17.36 18.42 3.52 o 1 10 12 35.76 35.34 2.96 o 2 10 12 57.25 53.17 4.13 o 3 10 12 19.53 19.20 2.12 o 4 10 12 1.15 -0.53 4.40 o 5 10 12 52.01 40.85 13.08 o 6 10 12 16.34 16.92 2.18 o 7 10 12 208.58 210.23 5.95 o 8 10 12 0.40 -0.18 5.25 o 9 10 12 101.25 103.35 4.24 o 10 10 12 41.82 41.87 2.85 o 0 11 12 39.30 40.24 2.78 o 1 11 12 82.78 82.00 3.83 o 2 11 12 121.14 121.64 5.52 o 3 11 12 71.13 71.32 4.95 o 4 11 12 35.37 34.53 8.81 o 5 11 12 25.47 21.99 7.07 o 6 11 12 22.47 24.62 2.26 o 7 11 12 18.36 18.68 2.28 o 8 11 12 2.62 2.21 3.27 o 9 11 12 13.89 14.69 2.51 o 0 12 12 28.58 26.82 3.16 o 2 12 12 14.39 14.00 3.26 o 4 12 12 63.59 59.83 10.78 o 6 12 12 20.74 22.47 2.25 o 8 12 12 39.74 42.35 2.66 o 0 1 13 39.67 39.74 1.90 o 0 2 13 24.08 22.64 2.25 o 1 2 13 16.24 16.66 2.17 o 0 3 13 3.04 2.84 3.20 o 1 3 13 347.28 344.60 8.36 o 2 3 13 4.87 5.60 1.84 o 0 4 13 33.45 34.11 2.18 o 1 4 13 14.78 15.57 3.27 o 2 4 13 129.13 126.60 5.17 o 3 4 13 49.54 48.14 3.97 o 0 5 13 27.08 25.88 1.90 o 1 5 13 331.36 322.85 11.42 o 2 5 13 88.16 88.01 3.79 o 3 5 13 53.16 51.50 4.07 o 4 5 13 46.66 42.36 4.20 o 0 6 13 10.24 10.44 1.78 o 1 6 13 10.82 11.02 2.63 o 2 6 13 128.05 124.44 4.43 o 3 6 13 23.79 23.03 1.93 o 4 6 13 203.75 200.40 4.11 o 5 6 13 14.60 13.20 2.12 o 0 7 13 5.32 4.06 3.10 o 1 7 13 311.01 300.61 15.23 o 2 7 13 39.71 38.81 2.99 o 3 7 13 392.20 390.92 10.40 o 4 7 13 13.90 13.02 2.02 o 5 7 13 98.35 102.39 4.02 o 6 7 13 21.31 21.57 2.14 o 0 8 13 92.64 90.83 3.75 o 1 8 13 13.52 14.00 2.00 o 2 8 13 19.01 18.35 2.06 o 3 8 13 52.84 53.21 3.65 o 4 8 13 151.86 147.10 8.12 o 5 8 13 12.74 14.33 3.44 o 6 8 13 22.97 23.70 2.21 o 7 8 13 13.15 13.29 2.14 o 0 9 13 9.99 11.63 2.05 o 1 9 13 244.00 238.93 8.95 o 2 9 13 67.40 62.30 2.66 o 3 9 13 44.70 44.49 2.43 o 4 9 13 30.98 31.13 6.72 o 5 9 13 157.48 161.13 6.17 o 6 9 13 2.12 1.28 2.59 o 7 9 13 435.00 451.87 8.42 o 8 9 13 6.53 6.67 2.15 o 0 10 13 76.29 73.90 2.78 o 1 10 13 18.61 17.14 2.72 o 2 10 13 92.17 93.30 2.98 o 3 10 13 9.59 10.43 2.83 o 4 10 13 9.27 7.56 2.17 o 5 10 13 14.72 13.21 2.16 o 6 10 13 88.97 89.33 3.07 o 7 10 13 27.65 28.81 2.36 o 8 10 13 43.80 45.81 2.54 o 9 10 13 29.80 29.92 2.50 o 0 11 13 14.25 15.16 2.21 o 1 11 13 86.25 84.73 2.97 o 2 11 13 68.54 66.60 2.83 o 3 11 13 49.10 48.17 2.82 o 4 11 13 28.19 27.19 4.31 o 5 11 13 40.23 35.72 8.62 o 6 11 13 124.04 128.94 4.55 o 7 11 13 268.13 276.01 6.21 o 8 11 13 52.13 53.71 2.77 o 0 12 13 2.29 1.01 3.46 o 1 12 13 31.48 29.78 3.20 o 2 12 13 80.31 79.81 5.54 o 3 12 13 38.85 39.30 2.50 o 4 12 13 4.21 4.34 2.26 o 5 12 13 24.58 24.33 5.90 o 6 12 13 250.38 263.25 8.10 o 7 12 13 9.83 9.17 2.29 o 0 13 13 199.06 198.70 5.03 o 2 13 13 25.91 25.97 2.29 o 4 13 13 25.28 25.04 3.47 o 0 0 14 523.15 516.46 9.27 o 0 1 14 17.23 17.04 1.83 o 1 1 14 519.46 519.03 20.29 o 0 2 14 218.80 219.01 4.81 o 1 2 14 2.60 3.15 2.18 o 2 2 14 48.94 50.09 2.21 o 0 3 14 4.95 3.18 5.55 o 1 3 14 21.51 21.31 1.96 o 2 3 14 14.64 15.00 2.08 o 3 3 14 531.88 522.77 23.38 o 0 4 14 10.96 9.32 3.92 o 1 4 14 84.45 84.85 2.55 o 2 4 14 50.61 49.07 3.69 o 3 4 14 42.10 41.43 3.55 o 4 4 14 155.60 149.92 10.28 o 0 5 14 31.27 30.94 2.65 o 1 5 14 83.65 83.25 2.68 o 2 5 14 178.28 172.35 8.04 o 3 5 14 305.36 296.54 21.87 o 4 5 14 64.61 60.23 3.46 o 5 5 14 83.32 82.53 9.45 o 0 6 14 272.78 273.93 9.63 o 1 6 14 36.87 38.13 2.27 o 2 6 14 53.88 55.12 3.77 o 3 6 14 41.14 40.12 3.14 o 4 6 14 56.48 54.31 3.84 o 5 6 14 25.61 25.02 2.17 o 6 6 14 25.02 24.90 2.21 o 0 7 14 83.38 86.01 3.51 o 1 7 14 16.22 17.06 2.46 o 2 7 14 53.07 53.31 3.56 o 3 7 14 129.83 127.64 6.08 o 4 7 14 14.40 15.65 2.11 o 5 7 14 77.83 76.84 9.75 o 6 7 14 24.09 25.13 2.24 o 7 7 14 132.24 133.81 3.42 o 0 8 14 225.47 225.14 6.91 o 1 8 14 40.82 39.37 2.63 o 2 8 14 13.97 13.31 2.10 o 3 8 14 109.09 105.27 5.42 o 4 8 14 12.24 11.42 2.15 o 5 8 14 29.12 29.47 3.68 o 6 8 14 2.95 -1.07 5.46 o 7 8 14 115.17 115.59 5.78 o 8 8 14 86.33 87.47 3.05 o 0 9 14 6.88 6.76 2.16 o 1 9 14 396.18 389.45 11.85 o 2 9 14 23.09 21.46 2.29 o 3 9 14 4.53 0.99 5.30 o 4 9 14 47.30 45.67 6.01 o 5 9 14 22.36 19.94 5.93 o 6 9 14 47.47 49.16 4.46 o 7 9 14 71.60 74.31 3.49 o 8 9 14 39.77 40.50 2.46 o 9 9 14 175.70 185.48 4.06 o 0 10 14 15.18 14.95 2.20 o 1 10 14 79.69 79.12 2.93 o 2 10 14 16.90 16.40 2.39 o 3 10 14 14.96 15.79 2.21 o 4 10 14 4.05 4.71 2.98 o 5 10 14 73.63 65.75 12.24 o 6 10 14 18.65 18.10 2.29 o 7 10 14 53.31 54.29 2.83 o 8 10 14 20.20 21.60 2.74 o 0 11 14 198.12 200.97 4.50 o 1 11 14 5.83 5.78 3.64 o 2 11 14 23.92 24.56 3.04 o 3 11 14 23.75 23.20 2.96 o 4 11 14 35.25 33.89 5.11 o 5 11 14 1.05 0.61 5.44 o 6 11 14 66.47 67.32 2.96 o 0 12 14 39.81 40.11 2.52 o 1 12 14 22.46 22.44 2.27 o 2 12 14 26.79 25.43 2.40 o 3 12 14 5.54 5.63 6.30 o 4 12 14 4.00 1.57 5.78 o 0 13 14 121.93 122.65 9.99 o 0 1 15 238.62 237.08 6.39 o 0 2 15 57.35 58.57 2.51 o 1 2 15 104.62 104.33 3.39 o 0 3 15 0.32 -1.21 9.89 o 1 3 15 255.12 256.02 7.80 o 2 3 15 96.24 95.16 2.94 o 0 4 15 133.33 130.27 3.26 o 1 4 15 47.57 47.79 2.43 o 2 4 15 8.63 9.53 2.05 o 3 4 15 231.66 223.55 12.40 o 0 5 15 187.46 188.60 6.22 o 1 5 15 83.16 83.01 2.85 o 2 5 15 148.48 146.38 5.56 o 3 5 15 92.03 89.86 4.88 o 4 5 15 8.17 8.61 2.08 o 0 6 15 3.78 3.38 4.04 o 1 6 15 117.89 119.55 5.28 o 2 6 15 14.47 15.01 2.08 o 3 6 15 3.64 2.10 3.64 o 4 6 15 48.65 47.66 3.88 o 5 6 15 73.13 74.83 7.93 o 0 7 15 114.87 115.70 3.20 o 1 7 15 12.80 14.03 2.14 o 2 7 15 91.11 89.29 4.06 o 3 7 15 72.40 70.28 2.80 o 4 7 15 26.79 24.40 2.32 o 5 7 15 8.89 8.77 5.87 o 6 7 15 47.73 48.53 2.57 o 0 8 15 57.80 55.22 3.31 o 1 8 15 74.54 76.62 4.03 o 2 8 15 13.07 12.87 2.17 o 3 8 15 53.50 54.43 4.17 o 4 8 15 142.75 134.90 14.41 o 5 8 15 10.92 12.48 2.19 o 6 8 15 20.40 21.60 2.49 o 7 8 15 17.66 19.10 2.24 o 0 9 15 26.52 27.75 2.37 o 1 9 15 134.65 136.00 3.45 o 2 9 15 14.74 13.43 2.23 o 3 9 15 36.83 37.66 2.47 o 4 9 15 9.82 8.00 5.46 o 5 9 15 50.41 43.69 8.62 o 6 9 15 14.69 15.75 2.76 o 7 9 15 34.67 35.33 3.06 o 0 10 15 155.72 155.24 4.90 o 1 10 15 17.05 17.34 2.34 o 2 10 15 92.75 91.70 5.17 o 3 10 15 3.82 5.59 3.94 o 4 10 15 86.24 81.96 11.17 o 5 10 15 2.64 0.59 7.18 o 6 10 15 9.24 12.14 2.24 o 0 11 15 30.39 33.31 2.40 o 1 11 15 190.83 196.84 6.27 o 2 11 15 111.39 115.16 4.58 o 3 11 15 3.85 4.22 2.41 o 4 11 15 195.88 197.87 11.37 o 0 0 16 0.04 -1.09 3.42 o 0 1 16 0.32 0.95 2.66 o 1 1 16 20.32 19.71 3.15 o 0 2 16 4.83 3.76 3.64 o 1 2 16 285.51 282.03 5.63 o 2 2 16 12.86 13.25 2.12 o 0 3 16 22.06 22.95 2.22 o 1 3 16 48.83 49.97 2.53 o 2 3 16 122.19 120.03 3.24 o 3 3 16 115.42 112.73 5.42 o 0 4 16 16.13 16.39 2.19 o 1 4 16 140.81 142.75 4.12 o 2 4 16 0.07 -4.91 6.72 o 3 4 16 226.68 226.91 7.37 o 4 4 16 90.06 90.22 3.00 o 0 5 16 7.65 9.34 2.15 o 1 5 16 31.21 30.53 2.37 o 2 5 16 4.49 2.49 3.75 o 3 5 16 4.22 4.91 2.98 o 4 5 16 45.53 42.94 5.21 o 5 5 16 174.06 169.93 16.24 o 0 6 16 0.01 -1.22 4.62 o 1 6 16 3.26 4.82 3.39 o 2 6 16 6.43 5.30 2.86 o 3 6 16 51.40 51.35 2.61 o 4 6 16 211.40 210.54 13.92 o 5 6 16 17.82 18.33 2.23 o 6 6 16 22.78 23.56 2.30 o 0 7 16 27.85 29.05 2.86 o 1 7 16 91.20 91.38 3.03 o 2 7 16 7.82 7.43 2.17 o 3 7 16 81.28 80.18 4.05 o 4 7 16 70.30 69.10 3.90 o 5 7 16 10.65 10.86 2.16 o 6 7 16 26.97 26.51 2.33 o 7 7 16 175.91 174.14 5.26 o 0 8 16 44.10 44.48 3.11 o 1 8 16 93.71 95.65 3.83 o 2 8 16 11.19 12.20 2.35 o 3 8 16 15.36 14.58 2.91 o 4 8 16 91.00 89.38 9.88 o 5 8 16 0.06 -0.75 4.94 o 6 8 16 36.81 36.91 2.53 o 0 9 16 36.76 38.92 2.47 o 1 9 16 29.63 30.10 2.37 o 2 9 16 113.61 116.16 4.47 o 3 9 16 29.63 30.48 2.35 o 4 9 16 98.25 95.15 10.14 o 5 9 16 58.04 53.10 6.82 o 0 10 16 63.19 63.31 2.93 o 1 10 16 110.99 111.05 4.06 o 2 10 16 2.41 1.05 4.41 o 0 1 17 123.98 124.77 3.36 o 0 2 17 13.22 13.35 2.22 o 1 2 17 37.95 39.05 2.44 o 0 3 17 0.01 -0.98 7.72 o 1 3 17 2.78 0.30 3.90 o 2 3 17 19.62 21.49 2.34 o 0 4 17 74.26 74.14 2.87 o 1 4 17 49.21 50.03 3.36 o 2 4 17 9.97 11.22 2.21 o 3 4 17 32.18 29.92 2.74 o 0 5 17 18.97 19.16 2.33 o 1 5 17 7.77 7.86 2.20 o 2 5 17 68.82 71.95 2.83 o 3 5 17 12.38 12.35 2.27 o 4 5 17 63.98 61.47 6.05 o 0 6 17 21.76 20.14 2.28 o 1 6 17 74.55 75.37 2.89 o 2 6 17 5.93 5.53 2.72 o 3 6 17 63.91 61.81 3.57 o 4 6 17 21.42 21.09 2.92 o 5 6 17 155.95 155.50 7.67 o 0 7 17 212.41 216.23 7.56 o 1 7 17 78.69 80.04 2.90 o 2 7 17 38.16 39.72 2.47 o 3 7 17 43.13 43.51 3.36 o 4 7 17 24.00 22.83 2.61 o 5 7 17 10.88 10.23 2.30 o 0 8 17 33.03 30.41 2.57 o 1 8 17 19.42 19.94 2.41 o 2 8 17 133.39 132.01 3.63 o 3 8 17 35.78 34.87 2.55 o 0 0 18 314.05 314.89 6.45 o 0 1 18 3.38 2.77 3.34 o 1 1 18 96.51 98.79 3.24 o 0 2 18 117.76 118.87 6.35 o 1 2 18 7.08 7.88 2.19 o 2 2 18 149.57 147.40 3.58 o 0 3 18 1.68 1.79 3.80 o 1 3 18 73.67 74.00 2.97 o 2 3 18 96.90 96.80 3.46 o 3 3 18 211.82 215.09 4.30 o 0 4 18 2.70 2.50 3.94 o 1 4 18 4.03 1.45 7.32 o 2 4 18 0.03 -1.11 5.62 o 3 4 18 25.72 26.58 2.54 o 4 4 18 8.17 8.57 2.30 o 0 5 18 25.73 26.29 4.00 o 1 5 18 3.82 2.41 7.40 o 2 5 18 106.07 108.48 5.24 o 3 5 18 401.92 404.40 14.90 o 0 6 18 91.44 92.34 3.20 o 1 6 18 2.43 2.97 3.20 o 2 6 18 40.38 38.79 3.28 o 0 1 19 1.51 0.47 5.02 o