#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/07/2010775.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2010775_Fobs loop_ _publ_author_name 'Matos Beja, A.' 'Paix\~ao, J. A.' 'Ramos Silva, M.' 'Alte da Veiga, L.' 'd Rocha Gonsalves, A. M.' 'Serra, A. C.' _publ_section_title ; 2-Bromo-5-hydroxybenzaldehyde ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 354 _journal_page_last 355 _journal_volume 56 _journal_year 2000 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 3.9740 _cell_length_b 9.1640 _cell_length_c 19.1720 _exptl_crystal_F_000 392.00 _reflns_d_resolution_high 0.8418 _[local]_cod_data_source_file sk1352Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' BZALN' _shelx_refln_list_code 4 _shelx_f_calc_maximum 144.88 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 311.98 303.82 9.50 o 4 0 0 313.42 309.98 11.84 o 1 1 0 7337.32 7572.77 58.16 o 2 1 0 5092.61 5284.30 26.66 o 3 1 0 94.27 88.85 11.13 o 4 1 0 24.27 35.14 13.98 o 0 2 0 653.45 671.10 4.34 o 1 2 0 6269.45 6509.55 97.39 o 2 2 0 239.55 242.35 4.83 o 3 2 0 1040.32 1056.51 8.22 o 4 2 0 0.17 -2.80 17.43 o 1 3 0 4445.71 4533.94 91.81 o 2 3 0 1509.80 1505.42 36.72 o 3 3 0 419.17 394.74 7.56 o 4 3 0 10.35 0.81 20.88 o 0 4 0 14897.05 14961.14 62.57 o 1 4 0 27.99 23.52 4.61 o 2 4 0 93.91 98.24 7.52 o 3 4 0 519.78 557.34 8.03 o 4 4 0 454.67 456.63 10.39 o 1 5 0 862.37 860.87 5.87 o 2 5 0 2509.98 2577.56 35.32 o 3 5 0 166.51 138.41 7.44 o 4 5 0 20.70 -34.84 34.84 o 0 6 0 205.85 196.40 5.38 o 1 6 0 1652.52 1646.56 19.46 o 2 6 0 26.12 50.21 9.59 o 3 6 0 381.54 378.06 8.51 o 1 7 0 1735.29 1699.79 20.07 o 2 7 0 121.26 120.66 6.82 o 3 7 0 197.42 210.82 15.32 o 0 8 0 1093.79 1086.30 9.11 o 1 8 0 155.34 152.27 7.77 o 2 8 0 2.42 0.20 12.42 o 3 8 0 314.28 329.52 10.63 o 1 9 0 11.44 12.08 18.39 o 2 9 0 552.82 559.30 9.64 o 0 10 0 279.52 278.45 8.21 o 1 10 0 266.33 277.36 11.30 o 1 0 1 4109.93 4352.08 38.76 o 2 0 1 2981.46 3080.10 52.87 o 3 0 1 1059.85 1102.54 11.32 o 4 0 1 4.95 -14.89 14.89 o -4 1 1 189.77 175.75 26.36 o -3 1 1 413.44 422.91 9.64 o -2 1 1 1188.36 1213.59 8.78 o -1 1 1 2294.08 2387.77 37.21 o 1 1 1 1669.56 1720.90 42.55 o 2 1 1 1036.92 1020.09 20.84 o 3 1 1 409.38 442.91 13.40 o 4 1 1 221.31 203.88 11.74 o -4 2 1 271.64 262.28 12.06 o -3 2 1 188.06 182.50 10.38 o -2 2 1 187.24 189.01 6.78 o -1 2 1 2159.52 2194.25 15.05 o 0 2 1 958.26 922.00 4.62 o 1 2 1 2128.83 2173.22 45.15 o 2 2 1 225.28 225.35 6.95 o 3 2 1 202.34 192.75 9.11 o 4 2 1 280.03 290.68 21.51 o -4 3 1 176.59 161.78 15.93 o -3 3 1 537.72 519.86 11.14 o -2 3 1 1257.80 1281.87 10.11 o -1 3 1 1051.47 1018.77 25.54 o 0 3 1 2510.19 2389.97 11.86 o 1 3 1 1135.57 1107.86 52.96 o 2 3 1 1117.98 1132.11 9.44 o 3 3 1 570.36 581.51 18.61 o 4 3 1 181.09 168.33 14.36 o -4 4 1 87.87 101.90 12.70 o -3 4 1 554.09 553.30 12.58 o -2 4 1 1424.95 1417.20 66.17 o -1 4 1 1561.42 1593.36 26.51 o 0 4 1 164.47 174.21 6.06 o 1 4 1 1746.73 1793.78 48.53 o 2 4 1 1529.63 1512.33 30.05 o 3 4 1 583.99 601.25 11.39 o 4 4 1 101.28 96.51 12.57 o -4 5 1 18.24 7.49 48.48 o -3 5 1 166.71 161.76 10.43 o -2 5 1 442.33 422.01 17.58 o -1 5 1 348.55 325.53 20.78 o 0 5 1 4231.43 4182.03 35.05 o 1 5 1 298.78 275.21 6.95 o 2 5 1 425.99 421.43 16.11 o 3 5 1 203.20 213.10 10.50 o 4 5 1 40.76 -24.79 47.55 o -3 6 1 94.09 80.07 23.11 o -2 6 1 141.78 153.70 14.28 o -1 6 1 444.16 447.50 12.37 o 0 6 1 896.99 858.80 12.44 o 1 6 1 433.56 422.55 23.31 o 2 6 1 175.03 184.99 9.54 o 3 6 1 123.64 104.89 26.54 o -3 7 1 190.03 189.06 17.81 o -2 7 1 521.83 543.06 11.08 o -1 7 1 458.50 442.86 9.60 o 0 7 1 72.94 53.56 20.67 o 1 7 1 463.98 451.78 7.90 o 2 7 1 509.16 521.09 9.19 o 3 7 1 194.83 178.77 14.35 o -3 8 1 162.14 121.40 72.27 o -2 8 1 298.99 291.19 15.37 o -1 8 1 175.82 194.10 9.24 o 0 8 1 351.06 332.36 6.03 o 1 8 1 159.48 165.30 7.58 o 2 8 1 236.91 239.73 10.93 o 3 8 1 153.42 156.96 13.33 o -2 9 1 30.60 47.96 11.41 o -1 9 1 389.12 388.92 24.71 o 0 9 1 251.80 240.67 7.25 o 1 9 1 400.55 388.34 11.39 o 2 9 1 23.73 33.40 27.70 o -1 10 1 105.88 91.98 11.73 o 0 10 1 164.36 166.94 8.19 o 1 10 1 102.78 107.93 39.33 o 1 0 2 746.52 747.90 6.28 o 2 0 2 118.96 110.08 6.24 o 3 0 2 1509.83 1539.47 12.31 o 4 0 2 23.09 -42.96 42.96 o -4 1 2 235.51 226.73 11.94 o -3 1 2 505.45 506.39 9.87 o -2 1 2 42.35 19.92 8.59 o -1 1 2 5164.04 5292.60 37.70 o 0 1 2 123.14 117.03 2.75 o 1 1 2 5794.95 6073.19 42.01 o 2 1 2 34.72 2.61 25.06 o 3 1 2 471.94 469.06 9.89 o 4 1 2 243.04 232.79 19.23 o -4 2 2 39.46 36.65 30.03 o -3 2 2 23.13 17.94 34.90 o -2 2 2 4206.49 4179.60 120.70 o -1 2 2 108.59 102.58 5.27 o 0 2 2 116.36 103.15 3.79 o 1 2 2 70.03 68.98 5.34 o 2 2 2 4366.08 4388.00 87.68 o 3 2 2 21.79 41.48 18.03 o 4 2 2 39.38 -6.09 55.54 o -4 3 2 251.88 239.40 18.71 o -3 3 2 415.06 428.48 10.71 o -2 3 2 372.78 377.43 14.11 o -1 3 2 1892.45 1864.20 36.12 o 0 3 2 6462.78 6391.58 49.41 o 1 3 2 1713.29 1736.01 58.49 o 2 3 2 384.14 388.41 14.46 o 3 3 2 414.36 406.53 10.72 o 4 3 2 231.49 219.85 12.30 o -4 4 2 32.97 -24.44 71.80 o -3 4 2 325.30 308.08 10.61 o -2 4 2 209.84 217.99 7.89 o -1 4 2 3562.09 3540.62 63.71 o 0 4 2 80.67 79.16 3.56 o 1 4 2 3734.31 3755.96 138.54 o 2 4 2 189.44 211.05 7.91 o 3 4 2 330.63 326.19 10.58 o 4 4 2 35.25 47.80 12.39 o -4 5 2 19.36 10.44 18.77 o -3 5 2 391.28 418.94 11.19 o -2 5 2 143.92 165.45 22.15 o -1 5 2 2183.80 2137.34 72.41 o 0 5 2 98.20 79.27 4.03 o 1 5 2 2206.58 2190.85 66.80 o 2 5 2 124.18 108.69 34.94 o 3 5 2 320.15 327.65 16.99 o 4 5 2 18.73 -29.23 54.18 o -3 6 2 53.49 -42.43 42.43 o -2 6 2 1258.73 1175.41 12.51 o -1 6 2 727.83 723.25 16.28 o 0 6 2 62.30 66.43 4.59 o 1 6 2 660.67 662.69 11.43 o 2 6 2 1257.19 1262.21 44.07 o 3 6 2 49.74 -23.12 42.72 o -3 7 2 22.36 37.91 44.99 o -2 7 2 29.11 31.25 28.80 o -1 7 2 176.57 164.91 8.65 o 0 7 2 1822.95 1771.50 21.12 o 1 7 2 200.10 186.75 8.98 o 2 7 2 42.93 -8.13 60.23 o 3 7 2 24.49 -1.27 27.25 o -3 8 2 80.35 60.27 20.52 o -2 8 2 200.78 198.89 10.73 o -1 8 2 335.88 354.65 10.07 o 0 8 2 0.08 3.32 9.35 o 1 8 2 341.51 350.75 10.14 o 2 8 2 142.47 140.72 10.77 o 3 8 2 75.08 16.49 48.66 o -2 9 2 31.83 20.25 15.37 o -1 9 2 251.32 257.28 14.21 o 0 9 2 169.07 174.21 7.03 o 1 9 2 236.64 236.67 21.25 o 2 9 2 25.27 23.32 16.77 o -1 10 2 120.09 123.99 11.75 o 0 10 2 7.58 -29.75 29.75 o 1 10 2 112.34 104.38 16.74 o 1 0 3 16692.07 16877.36 298.70 o 2 0 3 533.78 497.94 12.98 o 3 0 3 709.52 724.04 10.59 o 4 0 3 2.89 13.78 20.88 o -4 1 3 111.52 98.39 20.56 o -3 1 3 241.33 254.02 18.91 o -2 1 3 1309.31 1287.89 9.94 o -1 1 3 10210.78 10241.38 134.06 o 0 1 3 2428.63 2455.03 12.19 o 1 1 3 10811.86 11412.27 124.05 o 2 1 3 1395.86 1375.91 12.94 o 3 1 3 226.81 232.29 9.29 o 4 1 3 94.46 82.30 11.46 o -4 2 3 252.87 231.48 18.31 o -3 2 3 222.45 238.70 12.89 o -2 2 3 111.73 126.87 9.22 o -1 2 3 2342.08 2269.74 15.60 o 0 2 3 12939.12 12253.35 78.88 o 1 2 3 2397.98 2429.69 104.20 o 2 2 3 125.69 137.34 6.70 o 3 2 3 239.55 254.06 9.92 o 4 2 3 248.95 224.66 20.95 o -4 3 3 109.82 134.36 12.00 o -3 3 3 765.83 808.28 37.24 o -2 3 3 2418.69 2472.22 42.86 o -1 3 3 607.90 589.81 15.76 o 0 3 3 976.53 967.03 7.78 o 1 3 3 516.25 497.05 6.66 o 2 3 3 2388.48 2480.77 17.83 o 3 3 3 817.29 829.63 23.16 o 4 3 3 111.10 107.28 46.93 o -4 4 3 54.50 -10.42 49.30 o -3 4 3 443.77 443.54 25.30 o -2 4 3 705.08 693.03 20.81 o -1 4 3 4154.19 4184.95 62.01 o 0 4 3 150.67 138.69 3.92 o 1 4 3 4122.33 4263.46 29.55 o 2 4 3 848.27 876.68 34.72 o 3 4 3 378.39 376.56 10.82 o 4 4 3 46.68 55.38 12.63 o -4 5 3 32.84 22.99 56.06 o -3 5 3 209.84 209.55 10.59 o -2 5 3 460.08 453.90 16.24 o -1 5 3 1452.39 1462.80 13.98 o 0 5 3 2211.86 2256.63 20.45 o 1 5 3 1499.09 1523.06 39.28 o 2 5 3 408.36 414.00 15.33 o 3 5 3 170.61 159.28 10.40 o 4 5 3 35.08 25.87 17.01 o -3 6 3 117.19 128.06 27.05 o -2 6 3 219.22 226.24 10.06 o -1 6 3 647.41 652.90 9.01 o 0 6 3 3210.75 3124.15 18.40 o 1 6 3 662.23 674.46 25.04 o 2 6 3 215.08 204.09 16.67 o 3 6 3 126.40 136.74 16.13 o -3 7 3 254.73 246.15 12.64 o -2 7 3 980.54 974.91 12.42 o -1 7 3 158.96 151.23 19.11 o 0 7 3 76.47 82.23 7.88 o 1 7 3 121.22 137.18 8.70 o 2 7 3 1065.25 1057.99 29.85 o 3 7 3 266.44 287.38 12.48 o -3 8 3 90.51 79.02 49.54 o -2 8 3 240.24 242.00 10.96 o -1 8 3 259.27 273.36 9.74 o 0 8 3 538.16 513.04 7.33 o 1 8 3 325.90 307.67 10.15 o 2 8 3 286.94 275.08 11.39 o 3 8 3 91.25 95.84 40.80 o -2 9 3 10.42 0.37 16.24 o -1 9 3 257.96 237.85 10.95 o 0 9 3 149.04 178.16 7.09 o 1 9 3 270.99 279.05 10.89 o 2 9 3 14.63 5.46 42.87 o -1 10 3 94.79 28.97 45.78 o 0 10 3 181.29 172.90 8.34 o 1 10 3 82.39 45.01 16.76 o 0 0 4 20989.82 20152.67 125.74 o 1 0 4 1555.55 1612.18 40.56 o 2 0 4 396.99 395.11 7.24 o 3 0 4 19.56 34.05 16.07 o 4 0 4 456.45 464.67 19.10 o -4 1 4 28.67 32.98 15.33 o -3 1 4 246.35 240.48 9.69 o -2 1 4 3731.53 3947.95 35.92 o -1 1 4 3273.11 3328.40 23.70 o 0 1 4 33.02 24.94 5.00 o 1 1 4 3529.39 3610.93 110.95 o 2 1 4 3228.35 3453.37 37.30 o 3 1 4 235.45 230.47 9.38 o 4 1 4 25.07 -16.44 42.38 o -4 2 4 2.87 17.58 44.22 o -3 2 4 1583.98 1599.62 13.63 o -2 2 4 58.28 61.89 6.72 o -1 2 4 1924.52 1913.74 23.42 o 0 2 4 701.97 708.42 8.05 o 1 2 4 1446.24 1443.39 52.24 o 2 2 4 44.82 39.43 23.05 o 3 2 4 1579.29 1592.20 13.55 o 4 2 4 3.19 18.23 15.94 o -4 3 4 10.99 -11.00 74.33 o -3 3 4 339.86 351.97 21.83 o -2 3 4 926.42 899.08 12.61 o -1 3 4 1768.42 1870.75 19.36 o 0 3 4 50.30 40.48 8.37 o 1 3 4 1527.59 1584.63 31.65 o 2 3 4 979.49 963.86 16.88 o 3 3 4 332.86 354.34 10.63 o 4 3 4 11.18 30.99 45.70 o -4 4 4 373.49 364.34 13.99 o -3 4 4 143.74 157.38 15.15 o -2 4 4 111.07 121.95 7.87 o -1 4 4 274.57 265.99 9.73 o 0 4 4 4366.68 4260.16 21.35 o 1 4 4 220.99 219.74 6.39 o 2 4 4 93.70 103.01 10.25 o 3 4 4 137.96 155.95 61.65 o 4 4 4 394.36 373.03 13.99 o -4 5 4 27.68 -47.08 50.53 o -3 5 4 86.50 -2.82 39.65 o -2 5 4 1642.76 1647.42 15.80 o -1 5 4 1106.93 1101.15 9.34 o 0 5 4 126.01 116.59 4.61 o 1 5 4 1152.32 1157.71 19.17 o 2 5 4 1593.81 1634.62 43.77 o 3 5 4 71.86 89.28 27.84 o 4 5 4 31.80 22.01 41.64 o -3 6 4 457.27 466.40 12.95 o -2 6 4 17.03 -35.31 35.31 o -1 6 4 886.01 885.92 23.57 o 0 6 4 307.84 298.54 5.36 o 1 6 4 836.81 833.93 25.45 o 2 6 4 13.64 38.36 35.21 o 3 6 4 497.20 497.82 21.10 o -3 7 4 64.60 70.81 12.51 o -2 7 4 158.87 167.18 11.09 o -1 7 4 1235.95 1242.46 44.89 o 0 7 4 3.79 9.62 8.50 o 1 7 4 1181.23 1213.35 19.28 o 2 7 4 131.00 119.00 11.42 o 3 7 4 82.98 78.83 61.53 o -3 8 4 187.16 208.47 13.88 o -2 8 4 65.37 63.81 10.35 o -1 8 4 52.57 50.13 9.07 o 0 8 4 1087.22 1079.44 8.62 o 1 8 4 81.77 84.64 9.30 o 2 8 4 73.85 41.82 13.77 o 3 8 4 183.70 197.89 13.62 o -2 9 4 466.18 471.68 13.63 o -1 9 4 1.02 -2.14 39.19 o 0 9 4 1.98 -4.85 20.96 o 1 9 4 1.42 -11.68 38.24 o 2 9 4 484.88 506.81 15.96 o -1 10 4 153.43 136.85 12.32 o 0 10 4 237.73 232.60 11.20 o 1 10 4 145.81 158.54 12.25 o 1 0 5 1632.87 1725.75 32.54 o 2 0 5 3004.54 2986.09 42.51 o 3 0 5 556.88 548.50 11.59 o 4 0 5 0.64 -36.19 44.31 o -4 1 5 104.93 124.02 11.54 o -3 1 5 350.89 357.41 17.13 o -2 1 5 2417.29 2449.55 17.47 o -1 1 5 3047.20 3108.25 22.01 o 0 1 5 2314.60 2321.66 14.85 o 1 1 5 2869.14 2873.49 125.91 o 2 1 5 2112.28 2183.67 27.61 o 3 1 5 316.78 352.05 26.33 o 4 1 5 109.19 92.86 52.48 o -4 2 5 122.56 122.34 12.01 o -3 2 5 261.35 246.07 10.27 o -2 2 5 103.06 112.94 14.09 o -1 2 5 2341.83 2284.81 28.61 o 0 2 5 5433.85 5378.46 52.75 o 1 2 5 2632.32 2638.29 99.21 o 2 2 5 130.69 135.96 7.02 o 3 2 5 286.97 312.01 10.21 o 4 2 5 109.71 98.01 33.16 o -4 3 5 62.09 -35.40 78.13 o -3 3 5 494.19 495.70 11.21 o -2 3 5 995.25 979.16 9.80 o -1 3 5 1203.22 1222.27 24.73 o 0 3 5 3967.63 3849.27 35.28 o 1 3 5 1142.67 1169.10 29.68 o 2 3 5 956.61 990.51 10.50 o 3 3 5 525.60 542.91 11.20 o 4 3 5 46.04 31.67 44.89 o -4 4 5 2.25 -55.12 62.68 o -3 4 5 221.36 219.76 10.27 o -2 4 5 1834.89 1763.45 12.45 o -1 4 5 1578.17 1620.77 34.08 o 0 4 5 121.78 122.53 4.08 o 1 4 5 1530.01 1592.82 45.53 o 2 4 5 1870.30 1830.60 58.24 o 3 4 5 211.96 216.16 10.24 o 4 4 5 2.74 -13.35 46.70 o -4 5 5 71.66 23.72 51.53 o -3 5 5 85.45 12.63 43.21 o -2 5 5 436.02 434.99 10.06 o -1 5 5 908.84 897.49 9.14 o 0 5 5 3536.65 3491.47 21.16 o 1 5 5 949.34 945.87 41.69 o 2 5 5 369.28 381.37 9.49 o 3 5 5 101.04 105.84 19.98 o 4 5 5 68.52 31.15 49.86 o -3 6 5 193.72 197.90 11.51 o -2 6 5 208.00 188.20 17.47 o -1 6 5 349.60 340.11 17.79 o 0 6 5 919.01 984.33 9.95 o 1 6 5 478.51 465.95 8.97 o 2 6 5 150.86 150.62 9.51 o 3 6 5 220.83 225.30 11.64 o -3 7 5 200.38 181.72 15.81 o -2 7 5 217.02 224.33 10.36 o -1 7 5 446.64 454.89 18.61 o 0 7 5 6.32 -22.40 22.40 o 1 7 5 348.08 323.37 12.56 o 2 7 5 243.22 248.93 16.93 o 3 7 5 178.04 174.38 18.38 o -3 8 5 29.12 21.55 50.42 o -2 8 5 371.34 376.15 21.35 o -1 8 5 424.17 441.87 10.69 o 0 8 5 161.89 166.41 6.61 o 1 8 5 373.11 384.06 11.06 o 2 8 5 317.40 314.51 11.72 o 3 8 5 25.61 6.83 50.67 o -2 9 5 16.14 -25.98 43.31 o -1 9 5 221.28 253.38 10.94 o 0 9 5 541.99 541.52 8.39 o 1 9 5 240.69 231.11 38.13 o 2 9 5 14.07 -24.04 46.16 o -1 10 5 120.72 132.55 12.22 o 0 10 5 97.66 113.13 28.35 o 1 10 5 114.35 134.50 12.21 o 0 0 6 4015.98 3959.41 43.96 o 1 0 6 1772.29 1750.05 12.08 o 2 0 6 75.69 66.10 14.79 o 3 0 6 161.32 180.97 9.83 o 4 0 6 9.05 1.93 11.47 o -4 1 6 171.31 191.79 12.01 o -3 1 6 285.24 286.97 14.50 o -2 1 6 735.44 751.61 8.61 o -1 1 6 1190.04 1181.30 8.72 o 0 1 6 5066.70 4886.69 27.49 o 1 1 6 1415.19 1446.38 48.59 o 2 1 6 729.56 743.67 8.56 o 3 1 6 313.36 326.61 10.24 o 4 1 6 186.25 187.59 12.06 o -4 2 6 35.04 37.69 22.00 o -3 2 6 128.70 132.38 9.90 o -2 2 6 2581.17 2567.07 18.08 o -1 2 6 713.25 704.84 10.48 o 0 2 6 1352.63 1426.18 19.70 o 1 2 6 776.64 799.20 21.62 o 2 2 6 2994.78 2953.02 110.16 o 3 2 6 138.60 142.16 11.32 o 4 2 6 44.60 39.13 15.66 o -4 3 6 216.85 249.44 14.06 o -3 3 6 72.94 57.85 9.80 o -2 3 6 886.91 922.82 9.94 o -1 3 6 835.77 841.87 14.93 o 0 3 6 2652.05 2420.64 26.68 o 1 3 6 989.73 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