#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2010919.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2010919_Fobs loop_ _publ_author_name 'Hensen, Karl' 'Mayr-Stein, Ralf' 'Spangenberg, Bj\"orn' 'Bolte, Michael' _publ_section_title ; Complexes of mixed silicon halides with 4-picoline ; _journal_issue 5 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 610 _journal_page_last 613 _journal_volume 56 _journal_year 2000 _space_group_IT_number 53 _symmetry_space_group_name_Hall '-P 2ac 2' _symmetry_space_group_name_H-M 'P m n a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 7.1766 _cell_length_b 7.8911 _cell_length_c 13.7036 _exptl_crystal_F_000 364.00 _reflns_d_resolution_high 0.8030 _[local]_cod_data_source_file ln1098Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' he43 in Pmna' _shelx_refln_list_code 4 _shelx_f_calc_maximum 131.15 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x+1/2, y, -z+1/2' 'x, -y, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x-1/2, -y, z-1/2' '-x, y, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 3867.44 4019.11 45.83 o 4 0 0 17199.83 16376.00 134.13 o 6 0 0 1117.95 1109.85 12.44 o 8 0 0 914.66 867.71 10.19 o 0 1 0 5124.02 5140.41 74.44 o 2 1 0 1724.71 1791.22 12.69 o 4 1 0 1324.90 1312.41 8.32 o 6 1 0 3.15 19.39 7.28 o 8 1 0 32.80 36.45 1.39 o 0 2 0 226.03 254.48 3.54 o 2 2 0 3844.43 3640.34 20.88 o 4 2 0 3.75 5.72 0.75 o 6 2 0 199.49 203.56 3.72 o 8 2 0 73.94 75.38 2.53 o 0 3 0 6758.81 6872.98 123.90 o 2 3 0 6839.02 6572.45 35.68 o 4 3 0 794.12 767.33 5.75 o 6 3 0 447.98 462.96 4.46 o 8 3 0 29.55 25.67 1.96 o 0 4 0 3511.68 3841.20 32.29 o 2 4 0 690.13 577.56 3.94 o 4 4 0 925.80 966.57 6.30 o 6 4 0 70.59 74.88 1.67 o 8 4 0 37.10 28.04 2.35 o 0 5 0 899.28 832.79 8.54 o 2 5 0 87.72 83.38 1.27 o 4 5 0 189.15 190.27 2.37 o 6 5 0 38.24 38.07 1.39 o 0 6 0 4712.81 4555.47 41.19 o 2 6 0 567.45 591.52 4.59 o 4 6 0 1601.21 1589.51 12.79 o 6 6 0 5.25 5.31 1.17 o 0 7 0 2197.50 2122.47 22.25 o 2 7 0 61.26 64.86 1.39 o 4 7 0 1047.10 1055.22 8.92 o 6 7 0 0.10 -0.25 1.73 o 0 8 0 141.78 125.61 3.25 o 2 8 0 21.05 23.93 1.64 o 4 8 0 8.81 8.85 1.61 o 0 9 0 362.57 358.73 5.28 o 2 9 0 912.26 974.75 10.39 o 1 0 1 4147.00 4286.51 66.28 o 3 0 1 111.65 114.72 1.48 o 5 0 1 3550.93 3444.45 23.73 o 7 0 1 270.75 275.50 4.47 o 0 1 1 2041.31 1983.89 21.52 o 1 1 1 2925.00 2901.95 17.21 o 2 1 1 9062.62 9063.98 40.49 o 3 1 1 26.29 30.57 0.68 o 4 1 1 435.69 520.44 3.08 o 5 1 1 1327.17 1318.22 7.37 o 6 1 1 605.05 624.50 3.83 o 7 1 1 9.89 9.46 0.75 o 8 1 1 184.26 164.21 1.70 o 0 2 1 1634.11 1650.38 11.23 o 1 2 1 9.79 18.97 0.60 o 2 2 1 785.46 787.58 3.64 o 3 2 1 805.98 797.34 3.86 o 4 2 1 230.06 239.03 1.75 o 5 2 1 95.09 95.34 1.11 o 6 2 1 18.70 18.70 0.81 o 7 2 1 327.71 335.27 2.51 o 8 2 1 0.68 1.17 0.90 o 0 3 1 1140.81 1197.56 7.62 o 1 3 1 105.19 107.47 0.94 o 2 3 1 1023.50 1111.27 4.69 o 3 3 1 2728.20 2665.74 10.50 o 4 3 1 259.88 294.16 1.84 o 5 3 1 445.72 437.50 2.88 o 6 3 1 190.19 197.52 1.77 o 7 3 1 1203.40 1184.07 7.59 o 8 3 1 37.56 31.07 1.44 o 0 4 1 430.23 435.17 3.27 o 1 4 1 0.20 3.38 0.54 o 2 4 1 426.67 420.51 2.26 o 3 4 1 441.73 429.44 2.22 o 4 4 1 69.81 70.78 0.93 o 5 4 1 117.66 109.61 1.16 o 6 4 1 9.13 10.50 0.84 o 7 4 1 309.89 312.55 2.92 o 8 4 1 2.65 2.24 1.53 o 0 5 1 126.73 103.65 1.76 o 1 5 1 170.00 146.69 1.20 o 2 5 1 753.06 787.96 4.10 o 3 5 1 32.08 39.42 0.75 o 4 5 1 20.74 21.80 0.73 o 5 5 1 345.39 336.37 2.48 o 6 5 1 85.89 78.61 1.30 o 7 5 1 24.63 22.33 1.07 o 0 6 1 7.74 6.86 0.96 o 1 6 1 533.31 539.24 3.09 o 2 6 1 71.65 69.94 0.99 o 3 6 1 95.34 89.45 1.06 o 4 6 1 0.70 1.84 0.79 o 5 6 1 1115.92 1126.81 6.09 o 6 6 1 31.86 31.40 1.03 o 7 6 1 171.36 165.31 3.39 o 0 7 1 15.93 21.93 1.34 o 1 7 1 344.12 337.55 2.44 o 2 7 1 327.01 310.99 2.31 o 3 7 1 15.90 14.94 0.76 o 4 7 1 2.34 1.85 0.85 o 5 7 1 483.71 480.85 3.50 o 6 7 1 36.03 36.74 1.87 o 0 8 1 102.21 109.77 2.00 o 1 8 1 33.50 30.71 1.03 o 2 8 1 175.63 173.98 2.29 o 3 8 1 242.67 239.49 2.23 o 4 8 1 31.04 29.38 1.21 o 5 8 1 2.88 4.71 1.30 o 0 9 1 34.99 27.89 1.36 o 1 9 1 0.39 2.60 0.84 o 2 9 1 0.22 0.21 1.09 o 3 9 1 319.37 341.26 4.61 o 0 0 2 2178.11 2254.77 31.19 o 2 0 2 9268.51 9165.43 58.24 o 4 0 2 342.96 287.50 2.67 o 6 0 2 316.13 333.46 3.37 o 8 0 2 8.11 4.05 1.15 o 0 1 2 3770.84 3859.27 36.87 o 1 1 2 44.90 47.73 0.81 o 2 1 2 339.59 345.59 2.17 o 3 1 2 1739.96 1811.21 8.43 o 4 1 2 927.02 934.73 4.65 o 5 1 2 339.05 331.44 2.20 o 6 1 2 6.26 11.27 1.03 o 7 1 2 537.23 541.40 3.68 o 8 1 2 56.49 57.25 1.15 o 0 2 2 348.37 377.21 4.01 o 1 2 2 3.23 10.24 1.57 o 2 2 2 1321.63 1279.11 6.43 o 3 2 2 1070.59 1108.66 5.42 o 4 2 2 1.91 2.64 0.56 o 5 2 2 422.26 395.01 2.46 o 6 2 2 128.21 134.83 1.40 o 7 2 2 482.74 496.99 3.58 o 8 2 2 48.04 44.91 1.12 o 0 3 2 1920.13 1866.51 11.39 o 1 3 2 14.44 17.97 0.61 o 2 3 2 4112.75 3969.70 15.73 o 3 3 2 9.27 10.92 0.55 o 4 3 2 220.81 219.62 1.48 o 5 3 2 3.76 5.43 0.70 o 6 3 2 330.09 329.99 2.57 o 7 3 2 7.16 6.80 0.87 o 8 3 2 18.16 16.49 1.34 o 0 4 2 3.82 2.88 0.72 o 1 4 2 483.62 514.79 2.69 o 2 4 2 2739.41 2803.91 11.92 o 3 4 2 113.60 100.89 0.97 o 4 4 2 11.50 16.85 0.66 o 5 4 2 743.95 766.31 4.60 o 6 4 2 542.32 564.41 3.55 o 7 4 2 126.49 122.84 1.95 o 8 4 2 46.74 43.33 1.90 o 0 5 2 635.79 593.42 7.09 o 1 5 2 0.70 5.62 0.66 o 2 5 2 0.83 2.26 0.61 o 3 5 2 544.96 547.39 2.85 o 4 5 2 166.19 163.72 1.40 o 5 5 2 231.61 234.27 1.90 o 6 5 2 44.06 41.53 1.04 o 7 5 2 316.15 310.90 4.23 o 0 6 2 2187.82 2174.23 16.30 o 1 6 2 24.63 23.22 0.81 o 2 6 2 265.75 253.93 1.99 o 3 6 2 12.32 14.27 0.77 o 4 6 2 751.48 750.65 4.65 o 5 6 2 5.77 6.24 0.83 o 6 6 2 0.05 1.35 0.91 o 7 6 2 16.78 11.88 3.33 o 0 7 2 1165.88 1155.13 8.66 o 1 7 2 95.25 97.26 1.23 o 2 7 2 20.15 20.55 0.87 o 3 7 2 75.54 82.69 1.24 o 4 7 2 581.34 594.35 4.30 o 5 7 2 298.13 294.57 2.84 o 6 7 2 0.61 1.74 1.42 o 0 8 2 89.40 78.33 1.73 o 1 8 2 11.37 7.23 0.80 o 2 8 2 336.39 321.02 2.46 o 3 8 2 299.96 287.80 2.45 o 4 8 2 126.67 117.47 1.72 o 5 8 2 49.12 53.17 1.96 o 0 9 2 57.15 50.83 1.69 o 1 9 2 20.17 21.36 1.05 o 2 9 2 654.62 677.39 5.39 o 3 9 2 20.22 16.81 1.41 o 1 0 3 271.89 272.18 4.89 o 3 0 3 43.48 51.49 1.16 o 5 0 3 426.17 416.70 3.90 o 7 0 3 25.36 23.26 1.27 o 0 1 3 7035.05 7014.28 45.29 o 1 1 3 130.77 115.82 1.13 o 2 1 3 4907.15 4742.56 21.59 o 3 1 3 3.64 2.16 0.57 o 4 1 3 997.56 991.49 5.14 o 5 1 3 207.22 196.06 1.50 o 6 1 3 108.17 109.32 1.28 o 7 1 3 0.27 1.43 1.01 o 8 1 3 0.57 1.97 0.83 o 0 2 3 7348.33 7240.04 44.75 o 1 2 3 80.41 73.91 0.88 o 2 2 3 3925.69 3839.17 16.44 o 3 2 3 245.33 235.66 1.58 o 4 2 3 1134.34 1090.91 5.34 o 5 2 3 3.60 3.91 0.63 o 6 2 3 160.47 165.38 1.62 o 7 2 3 104.44 107.02 1.43 o 8 2 3 0.02 -0.52 1.04 o 0 3 3 102.98 119.21 1.58 o 1 3 3 44.84 43.34 0.74 o 2 3 3 6.49 8.15 0.54 o 3 3 3 518.35 510.28 2.74 o 4 3 3 84.51 89.01 1.01 o 5 3 3 8.22 8.33 0.70 o 6 3 3 5.02 5.60 0.78 o 7 3 3 251.40 255.01 2.43 o 8 3 3 25.33 21.60 1.28 o 0 4 3 2295.66 2249.52 14.21 o 1 4 3 331.52 346.97 2.04 o 2 4 3 2016.75 1896.49 8.24 o 3 4 3 486.79 484.65 2.71 o 4 4 3 406.24 418.15 2.44 o 5 4 3 40.02 41.71 0.88 o 6 4 3 59.17 59.83 1.02 o 7 4 3 189.89 187.56 1.82 o 8 4 3 17.59 14.78 1.90 o 0 5 3 2319.47 2293.89 17.69 o 1 5 3 352.81 350.75 2.20 o 2 5 3 1893.03 1841.96 9.09 o 3 5 3 122.35 127.69 1.27 o 4 5 3 646.71 654.60 3.79 o 5 5 3 239.65 244.52 2.03 o 6 5 3 127.22 126.48 1.68 o 7 5 3 21.56 18.20 1.28 o 0 6 3 73.51 72.11 2.98 o 1 6 3 662.40 661.58 4.92 o 2 6 3 511.44 511.02 3.27 o 3 6 3 146.66 150.15 1.49 o 4 6 3 16.80 15.70 0.81 o 5 6 3 568.23 577.08 4.79 o 6 6 3 242.56 239.29 2.50 o 0 7 3 620.44 605.14 5.47 o 1 7 3 46.15 47.94 0.97 o 2 7 3 678.82 700.77 4.38 o 3 7 3 1.28 2.05 0.84 o 4 7 3 98.70 98.19 1.44 o 5 7 3 66.06 63.38 1.78 o 6 7 3 12.41 10.61 1.48 o 0 8 3 803.52 854.18 7.63 o 1 8 3 89.36 90.79 1.30 o 2 8 3 711.01 706.96 4.60 o 3 8 3 127.70 131.01 1.53 o 4 8 3 262.59 266.63 2.81 o 0 9 3 6.92 7.90 1.34 o 1 9 3 59.28 52.18 1.19 o 2 9 3 101.72 93.50 1.86 o 3 9 3 164.42 155.11 2.22 o 0 0 4 129.90 144.10 2.21 o 2 0 4 2.00 5.04 0.79 o 4 0 4 16.30 16.46 0.94 o 6 0 4 1.39 2.18 0.94 o 8 0 4 22.73 22.91 1.40 o 0 1 4 1243.77 1203.37 7.71 o 1 1 4 0.06 0.96 0.56 o 2 1 4 745.99 729.99 3.73 o 3 1 4 2046.42 2105.42 9.66 o 4 1 4 327.18 323.28 2.05 o 5 1 4 697.61 673.26 3.82 o 6 1 4 120.94 121.71 1.34 o 7 1 4 849.15 846.41 5.33 o 8 1 4 79.28 73.02 1.30 o 0 2 4 441.43 410.59 4.51 o 1 2 4 98.42 89.59 0.93 o 2 2 4 283.45 287.27 2.13 o 3 2 4 1128.23 1123.54 5.34 o 4 2 4 225.99 227.32 1.67 o 5 2 4 990.68 998.52 6.45 o 6 2 4 120.80 119.01 1.37 o 7 2 4 636.02 630.77 4.81 o 8 2 4 27.43 25.38 1.22 o 0 3 4 1205.64 1248.49 8.38 o 1 3 4 311.00 336.56 1.97 o 2 3 4 691.69 705.45 3.41 o 3 3 4 150.22 158.89 1.28 o 4 3 4 357.56 358.56 2.22 o 5 3 4 80.76 81.35 1.09 o 6 3 4 240.59 235.66 2.05 o 7 3 4 15.44 13.72 0.85 o 8 3 4 47.49 45.08 1.71 o 0 4 4 224.83 212.48 2.34 o 1 4 4 174.84 184.03 1.48 o 2 4 4 242.42 232.96 1.67 o 3 4 4 583.48 561.90 3.07 o 4 4 4 119.07 119.13 1.27 o 5 4 4 765.24 782.76 4.21 o 6 4 4 84.49 84.20 1.24 o 7 4 4 376.06 377.84 2.86 o 0 5 4 443.55 450.60 5.14 o 1 5 4 144.13 143.00 1.34 o 2 5 4 544.79 544.05 3.16 o 3 5 4 1544.62 1519.38 7.82 o 4 5 4 262.80 263.32 2.06 o 5 5 4 149.07 141.97 1.51 o 6 5 4 134.61 133.35 1.66 o 7 5 4 874.57 877.80 10.14 o 0 6 4 17.51 15.50 1.10 o 1 6 4 6.19 6.14 0.72 o 2 6 4 43.98 47.33 0.92 o 3 6 4 3.93 3.80 0.77 o 4 6 4 25.88 25.90 0.90 o 5 6 4 0.05 1.00 0.93 o 6 6 4 6.10 5.76 1.19 o 0 7 4 6.26 7.50 1.06 o 1 7 4 7.52 9.66 0.76 o 2 7 4 15.80 14.40 0.78 o 3 7 4 601.18 614.67 4.43 o 4 7 4 2.72 2.84 0.84 o 5 7 4 134.54 142.62 2.10 o 0 8 4 115.54 119.30 1.93 o 1 8 4 62.38 65.88 1.12 o 2 8 4 39.16 39.75 1.01 o 3 8 4 135.42 140.40 1.71 o 4 8 4 53.94 56.47 1.33 o 0 9 4 10.59 10.00 1.67 o 1 9 4 50.12 54.11 1.58 o 2 9 4 1.30 0.33 1.09 o 1 0 5 3.24 4.21 0.78 o 3 0 5 549.16 504.75 4.02 o 5 0 5 169.60 191.67 2.23 o 7 0 5 225.28 225.54 2.89 o 0 1 5 5956.28 5728.87 33.99 o 1 1 5 3.48 7.27 0.57 o 2 1 5 2390.02 2367.95 10.34 o 3 1 5 219.37 223.25 1.68 o 4 1 5 1181.32 1167.55 6.11 o 5 1 5 4.73 4.65 0.66 o 6 1 5 72.26 72.29 1.06 o 7 1 5 110.29 115.99 1.39 o 8 1 5 3.56 3.34 1.24 o 0 2 5 5462.20 5358.03 30.62 o 1 2 5 4160.48 4357.94 19.72 o 2 2 5 2511.12 2478.72 11.95 o 3 2 5 1211.43 1267.65 5.95 o 4 2 5 1120.59 1048.32 5.53 o 5 2 5 1391.62 1414.16 7.33 o 6 2 5 145.57 163.64 1.61 o 7 2 5 186.05 181.30 1.85 o 8 2 5 6.30 6.80 1.56 o 0 3 5 83.56 88.12 1.33 o 1 3 5 432.27 450.82 3.31 o 2 3 5 15.13 19.28 0.68 o 3 3 5 3.02 3.33 0.61 o 4 3 5 65.36 63.57 0.96 o 5 3 5 626.27 631.38 3.64 o 6 3 5 10.67 10.60 0.84 o 7 3 5 23.38 21.66 0.97 o 8 3 5 14.80 14.78 1.96 o 0 4 5 2384.32 2285.79 16.19 o 1 4 5 898.62 897.36 4.77 o 2 4 5 997.61 953.52 4.92 o 3 4 5 273.17 271.96 1.96 o 4 4 5 611.91 630.62 3.79 o 5 4 5 552.67 560.95 3.55 o 6 4 5 14.35 11.91 0.87 o 7 4 5 37.12 35.23 1.11 o 0 5 5 2032.30 1976.40 14.17 o 1 5 5 286.90 281.32 2.01 o 2 5 5 1491.59 1455.74 7.77 o 3 5 5 548.76 564.25 3.69 o 4 5 5 605.88 617.47 3.96 o 5 5 5 40.88 42.88 1.01 o 6 5 5 133.33 131.64 1.65 o 7 5 5 170.54 163.31 2.60 o 0 6 5 349.55 350.74 3.77 o 1 6 5 446.09 458.51 4.32 o 2 6 5 1.35 2.50 0.73 o 3 6 5 18.00 19.83 0.87 o 4 6 5 245.27 249.40 2.34 o 5 6 5 487.25 506.60 3.82 o 6 6 5 1.19 0.10 1.21 o 0 7 5 717.67 709.75 6.09 o 1 7 5 19.87 20.16 0.82 o 2 7 5 324.10 330.98 2.59 o 3 7 5 77.22 84.46 1.30 o 4 7 5 174.07 171.50 1.89 o 5 7 5 0.19 -0.25 1.50 o 0 8 5 875.35 889.61 7.40 o 1 8 5 28.67 23.67 0.89 o 2 8 5 479.91 490.80 3.61 o 3 8 5 1.13 2.29 0.90 o 4 8 5 326.58 335.51 3.32 o 0 9 5 75.78 73.43 2.87 o 1 9 5 71.93 69.29 1.50 o 2 9 5 32.25 27.21 1.23 o 0 0 6 2463.92 2368.16 22.61 o 2 0 6 3602.72 3499.28 22.72 o 4 0 6 203.47 202.04 2.28 o 6 0 6 216.65 224.35 2.64 o 8 0 6 44.77 43.32 2.21 o 0 1 6 192.06 221.88 2.04 o 1 1 6 1162.22 1274.56 5.64 o 2 1 6 1477.60 1415.02 6.41 o 3 1 6 1.45 5.64 0.64 o 4 1 6 7.70 10.55 0.70 o 5 1 6 1000.24 1011.02 5.57 o 6 1 6 157.51 161.34 1.50 o 7 1 6 40.28 42.45 0.99 o 8 1 6 32.31 31.30 1.75 o 0 2 6 2032.37 2002.08 12.38 o 1 2 6 315.95 339.59 2.02 o 2 2 6 1.95 1.29 0.55 o 3 2 6 84.29 82.88 1.04 o 4 2 6 595.56 611.26 3.44 o 5 2 6 562.56 559.38 3.41 o 6 2 6 73.21 72.18 1.09 o 7 2 6 152.73 147.90 1.67 o 8 2 6 16.31 14.09 1.61 o 0 3 6 3477.32 3380.33 22.44 o 1 3 6 282.93 319.39 2.04 o 2 3 6 860.02 832.64 4.46 o 3 3 6 199.57 228.24 1.75 o 4 3 6 905.44 903.55 5.44 o 5 3 6 72.18 85.20 1.19 o 6 3 6 0.00 1.36 0.80 o 7 3 6 55.79 54.62 1.19 o 0 4 6 1470.61 1452.95 10.64 o 1 4 6 0.01 1.52 0.63 o 2 4 6 48.82 48.65 0.94 o 3 4 6 357.10 347.88 2.33 o 4 4 6 577.35 589.61 3.97 o 5 4 6 127.06 125.72 1.43 o 6 4 6 3.05 3.39 0.80 o 7 4 6 219.76 216.99 2.81 o 0 5 6 0.97 1.98 0.92 o 1 5 6 1299.26 1293.47 8.17 o 2 5 6 713.66 721.94 4.65 o 3 5 6 189.20 202.14 1.82 o 4 5 6 57.21 57.01 1.09 o 5 5 6 1247.32 1294.17 8.00 o 6 5 6 63.72 64.41 1.30 o 7 5 6 3.57 2.12 1.80 o 0 6 6 533.95 553.96 4.71 o 1 6 6 27.00 24.80 0.86 o 2 6 6 1079.70 1104.74 6.70 o 3 6 6 10.41 12.15 0.83 o 4 6 6 87.12 87.22 1.45 o 5 6 6 20.46 20.20 0.97 o 6 6 6 72.81 70.39 2.54 o 0 7 6 39.52 40.71 1.32 o 1 7 6 160.92 153.56 1.63 o 2 7 6 558.65 574.93 4.04 o 3 7 6 1.17 2.48 0.83 o 4 7 6 6.86 7.75 0.95 o 5 7 6 268.43 260.07 3.17 o 0 8 6 263.52 271.46 3.04 o 1 8 6 44.67 43.00 1.03 o 2 8 6 4.14 5.18 0.87 o 3 8 6 27.33 27.88 1.14 o 4 8 6 62.94 68.22 1.69 o 0 9 6 539.57 558.26 6.45 o 1 9 6 53.41 56.73 1.34 o 1 0 7 32.54 36.74 1.00 o 3 0 7 2207.67 2231.44 15.65 o 5 0 7 361.55 362.60 3.59 o 7 0 7 1157.48 1177.26 10.05 o 0 1 7 918.42 968.14 6.68 o 1 1 7 135.76 125.89 1.07 o 2 1 7 73.60 69.38 0.88 o 3 1 7 926.39 902.88 4.74 o 4 1 7 311.97 317.86 2.23 o 5 1 7 20.30 21.88 0.80 o 6 1 7 6.23 5.65 0.72 o 7 1 7 399.25 422.39 3.12 o 8 1 7 26.05 22.67 1.79 o 0 2 7 550.75 616.80 4.35 o 1 2 7 7.73 21.03 0.66 o 2 2 7 257.96 231.05 1.75 o 3 2 7 398.67 445.70 2.96 o 4 2 7 199.03 197.60 1.72 o 5 2 7 148.66 143.46 1.51 o 6 2 7 39.77 42.19 1.01 o 7 2 7 157.87 152.10 1.87 o 0 3 7 14.74 17.18 0.87 o 1 3 7 558.69 547.91 3.35 o 2 3 7 17.34 20.07 0.73 o 3 3 7 241.70 239.40 1.99 o 4 3 7 6.89 5.66 0.74 o 5 3 7 1391.84 1400.53 8.21 o 6 3 7 5.21 6.13 0.78 o 7 3 7 251.95 253.13 2.48 o 0 4 7 104.74 103.29 1.63 o 1 4 7 62.11 64.65 0.99 o 2 4 7 178.02 174.85 1.65 o 3 4 7 69.50 67.74 1.14 o 4 4 7 34.75 33.05 0.92 o 5 4 7 265.75 267.81 2.19 o 6 4 7 30.50 26.67 0.91 o 7 4 7 102.82 100.45 2.89 o 0 5 7 352.80 330.16 3.19 o 1 5 7 47.82 49.43 0.93 o 2 5 7 125.88 125.28 1.41 o 3 5 7 421.78 431.50 3.12 o 4 5 7 155.67 154.63 1.71 o 5 5 7 15.84 15.43 0.90 o 6 5 7 18.14 19.67 1.17 o 0 6 7 284.20 292.50 2.96 o 1 6 7 447.21 451.92 2.94 o 2 6 7 29.58 29.65 0.93 o 3 6 7 1929.92 1959.61 11.67 o 4 6 7 159.74 158.78 1.89 o 5 6 7 1.45 2.11 0.91 o 6 6 7 10.81 8.69 1.46 o 0 7 7 148.79 150.95 2.30 o 1 7 7 80.30 78.60 1.22 o 2 7 7 0.02 0.12 0.81 o 3 7 7 324.20 336.11 2.85 o 4 7 7 68.82 59.31 1.41 o 5 7 7 3.35 3.58 1.21 o 0 8 7 79.33 67.41 2.33 o 1 8 7 207.51 223.64 2.05 o 2 8 7 99.07 92.11 1.97 o 3 8 7 10.74 11.75 1.13 o 0 0 8 2005.53 1996.03 26.46 o 2 0 8 5123.66 4921.10 31.63 o 4 0 8 311.85 320.24 3.27 o 6 0 8 473.32 493.64 4.57 o 0 1 8 343.55 347.33 2.92 o 1 1 8 15.78 19.39 0.64 o 2 1 8 1760.55 1688.63 8.40 o 3 1 8 7.26 6.39 0.71 o 4 1 8 34.55 36.62 0.86 o 5 1 8 25.43 24.82 0.86 o 6 1 8 224.63 225.22 2.05 o 7 1 8 0.44 1.34 0.92 o 0 2 8 1460.07 1367.27 10.75 o 1 2 8 23.91 27.26 0.70 o 2 2 8 121.23 128.45 1.27 o 3 2 8 69.74 67.50 1.11 o 4 2 8 425.19 411.86 3.44 o 5 2 8 0.06 1.74 0.76 o 6 2 8 11.68 10.71 0.78 o 7 2 8 17.75 17.02 1.12 o 0 3 8 3712.98 3523.55 24.56 o 1 3 8 24.92 33.90 0.85 o 2 3 8 1498.70 1475.30 9.00 o 3 3 8 11.35 15.53 0.80 o 4 3 8 1152.99 1152.58 6.74 o 5 3 8 14.78 16.15 0.80 o 6 3 8 33.79 31.61 0.93 o 7 3 8 2.86 2.59 1.28 o 0 4 8 1879.32 1857.18 20.33 o 1 4 8 89.97 89.34 1.13 o 2 4 8 169.30 166.35 1.77 o 3 4 8 6.62 5.36 0.80 o 4 4 8 777.72 793.71 5.25 o 5 4 8 64.97 62.93 1.10 o 6 4 8 1.90 1.65 0.79 o 7 4 8 1.75 2.36 3.03 o 0 5 8 232.91 228.30 2.52 o 1 5 8 86.78 89.51 1.18 o 2 5 8 159.05 164.11 2.22 o 3 5 8 27.24 28.43 0.93 o 4 5 8 21.45 17.99 0.91 o 5 5 8 68.82 70.42 1.24 o 6 5 8 0.02 0.31 1.25 o 0 6 8 404.29 408.01 3.98 o 1 6 8 4.84 2.91 0.73 o 2 6 8 2112.79 2117.91 12.16 o 3 6 8 0.08 0.83 0.98 o 4 6 8 50.04 51.42 1.28 o 5 6 8 5.05 2.70 1.09 o 0 7 8 49.80 49.67 1.62 o 1 7 8 20.08 18.81 0.92 o 2 7 8 1062.10 1099.25 7.33 o 3 7 8 0.08 1.09 0.92 o 4 7 8 7.87 7.64 1.15 o 0 8 8 268.89 273.20 3.52 o 1 8 8 2.20 1.82 0.87 o 2 8 8 13.33 12.33 1.05 o 3 8 8 9.50 9.78 1.26 o 1 0 9 90.95 87.54 1.43 o 3 0 9 1456.99 1430.11 14.03 o 5 0 9 165.09 173.88 2.61 o 7 0 9 758.74 800.15 15.22 o 0 1 9 155.95 149.41 1.92 o 1 1 9 599.56 606.06 3.27 o 2 1 9 625.42 613.04 3.68 o 3 1 9 1194.69 1196.55 6.75 o 4 1 9 4.42 4.05 0.69 o 5 1 9 23.24 23.47 0.84 o 6 1 9 26.48 26.74 0.93 o 7 1 9 488.55 479.45 4.77 o 0 2 9 591.19 575.37 5.10 o 1 2 9 177.02 180.23 1.52 o 2 2 9 171.77 165.00 1.45 o 3 2 9 2.34 3.24 0.73 o 4 2 9 107.06 109.23 1.40 o 5 2 9 323.66 331.41 2.52 o 6 2 9 0.34 1.48 0.77 o 7 2 9 15.83 16.48 1.50 o 0 3 9 51.92 51.34 1.27 o 1 3 9 517.05 523.68 3.57 o 2 3 9 33.46 33.73 0.90 o 3 3 9 50.09 51.98 1.05 o 4 3 9 14.25 15.12 0.84 o 5 3 9 994.19 1024.56 6.34 o 6 3 9 19.36 17.09 0.86 o 7 3 9 139.18 141.66 2.64 o 0 4 9 275.54 277.03 3.00 o 1 4 9 127.10 122.73 1.39 o 2 4 9 200.56 204.59 1.89 o 3 4 9 5.37 5.39 0.81 o 4 4 9 44.94 46.87 1.12 o 5 4 9 289.00 294.60 2.52 o 6 4 9 0.01 0.82 1.15 o 0 5 9 222.79 244.34 2.98 o 1 5 9 3.90 2.14 0.79 o 2 5 9 159.74 154.96 1.64 o 3 5 9 69.78 75.92 1.26 o 4 5 9 40.26 39.36 1.01 o 5 5 9 54.28 50.28 1.13 o 6 5 9 2.94 2.41 1.18 o 0 6 9 42.12 38.67 1.30 o 1 6 9 2.11 3.53 0.83 o 2 6 9 44.25 41.52 1.06 o 3 6 9 414.11 423.46 3.67 o 4 6 9 42.29 37.27 1.14 o 5 6 9 136.00 138.98 2.51 o 0 7 9 122.29 120.29 2.67 o 1 7 9 54.90 57.62 1.26 o 2 7 9 100.85 113.82 1.56 o 3 7 9 242.86 247.99 3.30 o 4 7 9 14.47 13.26 1.49 o 0 8 9 39.98 41.56 1.66 o 1 8 9 57.31 54.61 1.49 o 2 8 9 118.02 115.18 1.93 o 0 0 10 94.61 87.30 2.71 o 2 0 10 4756.86 4665.49 37.30 o 4 0 10 128.53 141.68 2.09 o 6 0 10 1081.34 1140.69 11.00 o 0 1 10 58.74 58.14 1.40 o 1 1 10 145.39 145.43 1.39 o 2 1 10 675.58 687.31 4.05 o 3 1 10 183.03 179.50 1.58 o 4 1 10 6.85 6.28 0.74 o 5 1 10 445.88 457.66 3.19 o 6 1 10 138.20 138.15 1.65 o 7 1 10 147.55 149.17 2.73 o 0 2 10 579.63 584.35 5.19 o 1 2 10 323.90 300.20 2.37 o 2 2 10 0.74 1.19 0.74 o 3 2 10 38.78 41.02 0.95 o 4 2 10 230.83 227.95 2.03 o 5 2 10 660.39 683.05 5.21 o 6 2 10 7.11 5.92 0.83 o 7 2 10 66.90 69.60 4.21 o 0 3 10 1641.25 1563.76 12.15 o 1 3 10 2.62 2.85 0.78 o 2 3 10 219.23 218.61 2.21 o 3 3 10 1.28 1.73 0.79 o 4 3 10 708.62 725.66 4.73 o 5 3 10 1.71 1.41 0.79 o 6 3 10 3.78 3.19 0.98 o 0 4 10 370.06 423.68 4.67 o 1 4 10 4.90 2.91 0.76 o 2 4 10 230.92 203.85 2.05 o 3 4 10 478.64 472.51 3.79 o 4 4 10 155.27 160.80 1.75 o 5 4 10 99.35 101.55 1.48 o 6 4 10 44.65 45.07 1.60 o 0 5 10 12.95 12.31 1.27 o 1 5 10 100.89 99.83 1.39 o 2 5 10 198.92 199.27 2.04 o 3 5 10 61.39 64.11 1.20 o 4 5 10 23.75 25.77 1.01 o 5 5 10 308.08 322.40 3.42 o 0 6 10 96.29 91.52 1.98 o 1 6 10 8.78 7.30 0.86 o 2 6 10 737.45 751.14 7.30 o 3 6 10 12.82 10.42 0.98 o 4 6 10 14.81 13.41 1.26 o 0 7 10 14.73 10.25 1.45 o 1 7 10 4.97 3.84 0.91 o 2 7 10 499.86 518.04 4.31 o 3 7 10 137.52 146.83 3.16 o 1 0 11 156.41 154.15 2.48 o 3 0 11 248.59 259.20 3.15 o 5 0 11 19.54 17.41 1.17 o 0 1 11 3778.69 3643.29 29.51 o 1 1 11 0.03 1.39 0.88 o 2 1 11 60.52 58.11 1.13 o 3 1 11 9.42 9.02 0.80 o 4 1 11 1355.94 1373.28 8.08 o 5 1 11 3.41 4.65 0.89 o 6 1 11 65.13 64.82 1.48 o 0 2 11 1344.75 1273.19 10.12 o 1 2 11 179.26 178.60 1.81 o 2 2 11 970.91 959.18 6.41 o 3 2 11 101.91 104.81 1.36 o 4 2 11 347.41 348.35 2.61 o 5 2 11 107.88 109.52 1.41 o 6 2 11 53.10 51.60 1.44 o 0 3 11 219.78 183.42 2.69 o 1 3 11 142.95 144.78 1.69 o 2 3 11 75.11 62.65 1.31 o 3 3 11 41.20 39.98 1.08 o 4 3 11 156.86 151.71 1.64 o 5 3 11 150.03 152.94 1.60 o 6 3 11 19.03 18.50 1.30 o 0 4 11 885.49 904.20 8.58 o 1 4 11 129.76 129.63 1.56 o 2 4 11 518.16 509.22 4.00 o 3 4 11 43.21 46.32 1.18 o 4 4 11 212.64 217.02 2.09 o 5 4 11 101.24 97.73 1.60 o 0 5 11 1203.68 1167.04 10.75 o 1 5 11 125.43 115.69 1.55 o 2 5 11 375.94 401.75 3.38 o 3 5 11 108.06 105.75 1.87 o 4 5 11 421.57 418.11 3.85 o 5 5 11 52.38 48.90 1.64 o 0 6 11 99.86 103.50 2.10 o 1 6 11 41.21 40.56 1.16 o 2 6 11 3.16 5.09 0.92 o 3 6 11 78.39 78.72 1.66 o 4 6 11 84.76 79.97 1.93 o 0 7 11 658.81 716.40 11.43 o 1 7 11 32.77 28.75 1.28 o 2 7 11 64.10 56.75 1.60 o 0 0 12 359.94 360.37 7.14 o 2 0 12 488.37 501.63 5.47 o 4 0 12 322.84 330.58 3.77 o 6 0 12 70.99 60.40 2.52 o 0 1 12 114.68 106.51 1.93 o 1 1 12 147.48 147.41 1.91 o 2 1 12 81.66 81.72 1.48 o 3 1 12 129.94 132.96 1.91 o 4 1 12 43.34 40.44 1.06 o 5 1 12 491.12 497.97 3.59 o 6 1 12 59.25 63.62 2.21 o 0 2 12 42.06 44.21 1.69 o 1 2 12 4.83 4.98 0.93 o 2 2 12 123.35 127.66 1.90 o 3 2 12 376.88 394.12 4.08 o 4 2 12 58.14 56.72 1.34 o 5 2 12 231.40 228.00 2.40 o 6 2 12 18.54 19.50 1.75 o 0 3 12 87.51 87.82 1.91 o 1 3 12 1.53 1.12 0.90 o 2 3 12 175.31 173.80 2.06 o 3 3 12 0.60 1.58 1.04 o 4 3 12 109.10 107.49 1.51 o 5 3 12 2.20 1.19 1.02 o 0 4 12 380.22 351.51 4.12 o 1 4 12 16.64 15.80 0.89 o 2 4 12 267.24 247.41 2.57 o 3 4 12 216.23 224.57 2.31 o 4 4 12 269.66 258.81 2.43 o 5 4 12 208.04 210.26 3.17 o 0 5 12 241.37 239.55 3.55 o 1 5 12 68.75 65.49 1.31 o 2 5 12 54.44 49.64 1.27 o 3 5 12 89.99 96.23 1.53 o 4 5 12 95.06 95.60 2.04 o 0 6 12 22.55 24.87 1.78 o 1 6 12 3.95 4.17 1.05 o 2 6 12 0.03 0.39 1.15 o 3 6 12 1.77 2.50 1.29 o 1 0 13 31.96 30.01 1.77 o 3 0 13 91.60 88.45 1.99 o 5 0 13 155.36 156.79 3.46 o 0 1 13 240.27 243.50 3.28 o 1 1 13 108.37 106.84 1.75 o 2 1 13 1162.97 1168.64 9.20 o 3 1 13 4.91 5.34 1.03 o 4 1 13 43.74 42.96 1.36 o 5 1 13 125.43 124.82 2.08 o 0 2 13 586.86 596.02 7.34 o 1 2 13 93.79 92.54 1.74 o 2 2 13 770.07 773.35 6.40 o 3 2 13 255.97 270.33 5.85 o 4 2 13 197.12 194.51 2.43 o 5 2 13 5.51 6.10 1.34 o 0 3 13 16.48 13.56 1.43 o 1 3 13 0.71 1.22 1.20 o 2 3 13 122.71 118.49 1.96 o 3 3 13 196.97 204.60 2.81 o 4 3 13 9.08 6.86 1.42 o 5 3 13 48.42 46.55 2.03 o 0 4 13 459.20 473.58 5.64 o 1 4 13 148.96 137.89 1.85 o 2 4 13 274.33 267.02 2.70 o 3 4 13 247.13 237.23 2.52 o 4 4 13 147.88 151.31 2.65 o 0 5 13 386.42 408.53 5.09 o 1 5 13 124.83 125.23 1.70 o 2 5 13 536.80 530.40 5.19 o 3 5 13 11.22 11.81 1.26 o 0 6 13 45.41 45.97 2.29 o 1 6 13 81.97 84.20 1.79 o 0 0 14 1332.87 1302.26 21.29 o 2 0 14 93.79 92.97 2.53 o 4 0 14 431.25 423.48 4.91 o 0 1 14 648.04 654.30 13.26 o 1 1 14 1.10 0.77 1.05 o 2 1 14 3.01 6.06 1.10 o 3 1 14 85.12 85.16 1.63 o 4 1 14 255.66 254.05 3.23 o 0 2 14 5.54 3.30 1.53 o 1 2 14 3.63 3.41 1.24 o 2 2 14 324.93 333.50 3.83 o 3 2 14 50.93 56.01 1.80 o 4 2 14 4.87 6.59 1.50 o 0 3 14 181.11 164.35 2.90 o 1 3 14 13.40 12.82 1.38 o 2 3 14 728.11 766.10 6.74 o 3 3 14 17.10 16.20 1.51 o 4 3 14 11.70 11.87 1.70 o 0 4 14 42.41 38.83 2.93 o 1 4 14 25.29 20.38 1.23 o 2 4 14 180.58 182.35 3.08 o 3 4 14 4.91 6.14 1.63 o 0 5 14 258.75 274.25 5.37 o 1 5 14 0.79 1.54 1.39 o 2 5 14 0.01 0.69 1.39 o 1 0 15 138.23 138.84 3.03 o 3 0 15 70.77 72.24 2.34 o 0 1 15 11.76 14.21 2.38 o 1 1 15 112.94 109.38 2.21 o 2 1 15 84.97 88.40 1.89 o 3 1 15 0.02 -0.54 1.39 o 4 1 15 12.33 10.66 1.66 o 0 2 15 98.01 96.79 3.63 o 1 2 15 78.37 84.56 1.98 o 2 2 15 28.77 27.92 1.37 o 3 2 15 286.42 299.46 4.63 o 0 3 15 3.95 2.23 2.18 o 1 3 15 8.06 5.78 1.43 o 2 3 15 11.94 14.49 1.68 o 3 3 15 376.87 381.13 5.54 o 0 4 15 0.32 2.54 3.15 o 1 4 15 6.06 6.46 1.59 o 2 4 15 65.27 70.44 2.63 o 0 0 16 1287.13 1273.98 31.32 o 2 0 16 121.79 122.29 3.45 o 0 1 16 241.57 226.03 8.35 o 1 1 16 66.63 67.60 2.54 o 2 1 16 76.79 75.26 2.09 o 1 2 16 10.37 8.94 2.52 o 2 2 16 252.01 251.30 6.96 o 1 3 16 30.00 34.72 2.67 o