#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/09/2010922.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2010922_Fobs loop_ _publ_author_name 'Hensen, Karl' 'Mayr-Stein, Ralf' 'Spangenberg, Bj\"orn' 'Bolte, Michael' _publ_section_title ; Complexes of mixed silicon halides with 4-picoline ; _journal_issue 5 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 610 _journal_page_last 613 _journal_volume 56 _journal_year 2000 _space_group_IT_number 53 _symmetry_space_group_name_Hall '-P 2ac 2' _symmetry_space_group_name_H-M 'P m n a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 7.2960 _cell_length_b 8.2110 _cell_length_c 13.4720 _exptl_crystal_F_000 472.00 _reflns_d_resolution_high 0.7702 _[local]_cod_data_source_file ln1098IVsup5.hkl _[local]_cod_data_source_block IV #BEGIN Tags that were not found in dictionaries: _shelx_title ' he71 in Pmna' _shelx_refln_list_code 4 _shelx_f_calc_maximum 210.58 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x+1/2, y, -z+1/2' 'x, -y, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x-1/2, -y, z-1/2' '-x, y, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1198.58 1240.04 48.09 o 4 0 0 44345.17 43188.11 513.55 o 6 0 0 321.09 299.15 20.86 o 8 0 0 4145.29 3745.74 94.71 o 0 1 0 15631.06 16459.97 235.19 o 2 1 0 8422.43 8489.48 92.51 o 4 1 0 5769.18 5476.06 52.11 o 6 1 0 829.60 861.28 20.86 o 8 1 0 537.46 529.95 35.67 o 0 2 0 4268.93 4401.05 56.40 o 2 2 0 9898.57 9735.71 81.49 o 4 2 0 1361.97 1391.09 19.55 o 6 2 0 1239.54 1249.76 38.02 o 8 2 0 20.35 0.62 25.59 o 0 3 0 30184.70 30689.03 323.38 o 2 3 0 27251.56 27235.46 252.76 o 4 3 0 9243.73 8593.38 74.79 o 6 3 0 4653.33 4607.38 57.70 o 8 3 0 513.29 583.05 34.17 o 0 4 0 11305.32 11615.19 153.75 o 2 4 0 4925.14 4516.06 41.16 o 4 4 0 4470.11 4461.80 56.23 o 6 4 0 1196.14 1226.13 32.01 o 8 4 0 571.31 549.53 33.72 o 0 5 0 3557.44 3323.22 71.88 o 2 5 0 1242.74 1314.18 20.95 o 4 5 0 1262.21 1263.13 23.63 o 6 5 0 47.60 35.36 18.19 o 8 5 0 33.57 59.67 25.81 o 0 6 0 16987.80 16346.39 239.51 o 2 6 0 6641.57 6276.47 92.21 o 4 6 0 7596.65 7164.88 74.20 o 6 6 0 987.13 990.01 34.60 o 0 7 0 6369.75 5955.04 100.69 o 2 7 0 1495.32 1573.46 62.55 o 4 7 0 3456.71 3461.47 100.73 o 6 7 0 421.47 420.66 35.40 o 0 8 0 668.34 629.74 51.61 o 2 8 0 386.57 431.21 24.11 o 4 8 0 165.74 129.12 51.34 o 6 8 0 5.79 20.50 31.64 o 0 9 0 2918.65 2883.81 66.03 o 2 9 0 3955.55 4003.62 63.23 o 4 9 0 1236.52 1214.86 44.74 o 0 10 0 855.72 868.34 46.91 o 2 10 0 1488.80 1483.47 47.33 o 1 0 1 4730.19 4882.81 39.25 o 3 0 1 471.33 476.84 11.97 o 5 0 1 6520.42 6227.50 90.47 o 7 0 1 1297.41 1347.82 32.82 o 9 0 1 1798.91 1785.24 54.49 o 0 1 1 57.29 65.23 4.51 o 1 1 1 3080.68 3206.51 33.61 o 2 1 1 18906.08 20201.21 118.98 o 3 1 1 3.61 10.59 4.27 o 4 1 1 59.68 43.78 5.75 o 5 1 1 2097.34 2106.95 23.56 o 6 1 1 2129.74 2118.16 22.75 o 7 1 1 147.02 148.47 16.91 o 8 1 1 19.00 8.91 18.59 o 9 1 1 607.78 637.64 30.92 o 0 2 1 6848.66 6968.95 74.51 o 1 2 1 46.67 69.39 4.11 o 2 2 1 4450.92 4510.58 27.87 o 3 2 1 1227.79 1242.81 12.12 o 4 2 1 2010.37 1962.35 17.55 o 5 2 1 445.62 457.66 10.56 o 6 2 1 609.26 624.55 14.56 o 7 2 1 893.63 934.28 21.02 o 8 2 1 155.98 158.96 23.39 o 9 2 1 162.23 127.28 24.69 o 0 3 1 924.77 1015.87 15.50 o 1 3 1 56.88 77.65 4.77 o 2 3 1 1151.01 1266.00 11.22 o 3 3 1 4279.24 4185.92 35.58 o 4 3 1 188.06 224.48 8.01 o 5 3 1 1512.14 1549.62 18.17 o 6 3 1 255.90 280.69 13.84 o 7 3 1 2923.73 2855.94 31.57 o 8 3 1 22.56 2.97 17.52 o 9 3 1 659.34 680.12 31.69 o 0 4 1 2623.84 2587.55 55.01 o 1 4 1 3.07 14.65 4.75 o 2 4 1 2696.39 2631.79 36.31 o 3 4 1 614.61 623.68 9.25 o 4 4 1 946.19 964.16 13.58 o 5 4 1 269.76 259.33 11.38 o 6 4 1 355.47 358.26 15.31 o 7 4 1 571.45 562.40 19.24 o 8 4 1 46.26 66.97 18.51 o 0 5 1 1711.33 1602.24 29.44 o 1 5 1 216.09 217.54 7.44 o 2 5 1 3324.42 3397.09 29.87 o 3 5 1 205.76 215.10 8.64 o 4 5 1 733.52 718.87 13.48 o 5 5 1 854.99 830.99 18.09 o 6 5 1 695.14 666.50 19.04 o 7 5 1 258.77 255.67 16.54 o 8 5 1 40.20 61.67 27.52 o 0 6 1 1.22 -12.79 12.79 o 1 6 1 724.84 779.31 15.02 o 2 6 1 124.33 127.68 10.42 o 3 6 1 382.23 383.71 12.22 o 4 6 1 7.95 11.64 10.46 o 5 6 1 2247.27 2264.82 28.73 o 6 6 1 66.12 55.52 14.78 o 7 6 1 752.30 755.64 24.43 o 0 7 1 707.82 758.49 23.82 o 1 7 1 480.29 453.81 14.29 o 2 7 1 1173.09 1186.48 20.14 o 3 7 1 22.58 21.03 11.62 o 4 7 1 225.86 254.16 19.24 o 5 7 1 725.28 766.32 25.67 o 6 7 1 207.52 245.48 22.09 o 7 7 1 22.61 49.02 22.26 o 0 8 1 960.33 1001.05 28.17 o 1 8 1 32.62 20.85 11.91 o 2 8 1 892.38 881.03 19.56 o 3 8 1 549.72 520.10 20.66 o 4 8 1 479.14 460.65 22.99 o 5 8 1 72.88 64.63 20.41 o 6 8 1 201.06 227.04 29.94 o 0 9 1 138.79 143.73 22.52 o 1 9 1 6.39 21.29 13.88 o 2 9 1 1.17 12.71 16.04 o 3 9 1 545.15 549.98 26.50 o 4 9 1 110.32 67.03 20.62 o 5 9 1 405.13 409.35 28.13 o 0 10 1 217.24 178.91 27.38 o 1 10 1 76.57 70.62 17.23 o 2 10 1 273.37 295.34 23.16 o 3 10 1 246.49 249.68 25.43 o 0 0 2 10121.79 10672.98 129.67 o 2 0 2 21290.70 22644.76 225.27 o 4 0 2 3702.14 3410.50 38.51 o 6 0 2 2424.33 2468.17 33.25 o 8 0 2 269.36 341.21 33.77 o 0 1 2 8092.50 8346.68 56.62 o 1 1 2 14.35 22.86 3.11 o 2 1 2 1917.27 1889.42 26.08 o 3 1 2 3225.92 3294.91 23.31 o 4 1 2 2816.52 2755.26 20.72 o 5 1 2 1379.15 1371.20 14.65 o 6 1 2 172.25 159.60 11.30 o 7 1 2 1871.44 1892.95 31.51 o 8 1 2 347.66 405.59 24.78 o 9 1 2 533.04 572.01 29.99 o 0 2 2 1529.20 1576.28 26.16 o 1 2 2 28.81 34.38 3.71 o 2 2 2 3491.49 3527.49 24.17 o 3 2 2 2112.84 2151.67 18.13 o 4 2 2 337.55 336.17 7.89 o 5 2 2 1437.95 1395.98 17.37 o 6 2 2 631.99 639.38 14.81 o 7 2 2 1601.74 1645.25 30.07 o 8 2 2 0.93 -15.68 15.86 o 9 2 2 515.65 511.50 29.06 o 0 3 2 7914.67 7766.65 70.33 o 1 3 2 22.54 31.16 4.64 o 2 3 2 12021.01 11651.91 79.81 o 3 3 2 2.61 8.08 5.75 o 4 3 2 2669.52 2600.79 24.97 o 5 3 2 22.31 19.85 7.61 o 6 3 2 2152.07 2166.53 29.30 o 7 3 2 1.09 -12.43 12.43 o 8 3 2 169.76 189.52 21.10 o 9 3 2 2.17 -21.41 21.41 o 0 4 2 661.15 662.78 16.61 o 1 4 2 811.58 882.34 9.62 o 2 4 2 6180.88 5925.10 41.57 o 3 4 2 523.16 512.27 9.15 o 4 4 2 243.53 240.07 9.42 o 5 4 2 2073.66 2082.08 22.79 o 6 4 2 1646.06 1662.37 23.29 o 7 4 2 814.59 827.85 23.78 o 8 4 2 7.90 -0.44 19.21 o 0 5 2 1483.96 1418.85 22.30 o 1 5 2 3.45 7.92 5.28 o 2 5 2 228.11 249.05 8.69 o 3 5 2 1165.26 1191.61 13.69 o 4 5 2 566.37 550.36 13.26 o 5 5 2 767.95 784.40 15.69 o 6 5 2 2.43 -11.54 11.54 o 7 5 2 997.30 989.00 20.80 o 8 5 2 30.49 72.60 20.29 o 0 6 2 6521.56 6047.72 82.41 o 1 6 2 67.63 65.85 8.56 o 2 6 2 2111.04 2136.20 20.12 o 3 6 2 8.54 15.28 9.72 o 4 6 2 3023.89 2988.93 30.22 o 5 6 2 52.20 67.93 19.73 o 6 6 2 336.35 335.00 19.49 o 7 6 2 5.33 6.57 18.64 o 0 7 2 3241.01 3244.03 43.16 o 1 7 2 286.81 265.64 13.00 o 2 7 2 320.49 343.90 14.38 o 3 7 2 234.15 235.69 15.21 o 4 7 2 1837.57 1860.08 29.76 o 5 7 2 1079.64 1043.27 27.25 o 6 7 2 67.99 89.80 19.64 o 7 7 2 377.21 473.46 30.53 o 0 8 2 10.34 -6.86 15.93 o 1 8 2 18.18 14.85 11.81 o 2 8 2 632.56 601.78 17.58 o 3 8 2 676.92 630.65 21.97 o 4 8 2 39.84 8.82 16.96 o 5 8 2 167.96 152.97 21.44 o 6 8 2 110.40 116.40 33.20 o 0 9 2 655.12 631.68 27.96 o 1 9 2 23.57 39.74 14.55 o 2 9 2 1888.53 1931.58 31.32 o 3 9 2 60.77 38.11 16.73 o 4 9 2 262.41 296.26 25.17 o 0 10 2 260.80 275.73 29.75 o 1 10 2 90.42 135.44 19.31 o 2 10 2 718.94 766.11 28.08 o 3 10 2 82.91 86.93 25.03 o 1 0 3 233.55 286.54 9.57 o 3 0 3 0.17 4.79 6.85 o 5 0 3 281.41 282.36 12.84 o 7 0 3 4.98 -16.20 16.20 o 9 0 3 97.66 101.13 34.79 o 0 1 3 28266.88 30653.40 210.35 o 1 1 3 86.48 87.61 3.78 o 2 1 3 21732.70 21970.60 141.89 o 3 1 3 19.61 17.53 5.14 o 4 1 3 8714.68 8197.26 52.91 o 5 1 3 146.95 166.06 9.01 o 6 1 3 2728.18 2760.91 32.14 o 7 1 3 1.29 14.32 12.23 o 8 1 3 586.86 597.31 23.32 o 9 1 3 35.93 -6.52 21.26 o 0 2 3 28477.61 28966.27 265.83 o 1 2 3 117.17 135.34 4.76 o 2 2 3 19598.95 19840.32 112.92 o 3 2 3 191.32 185.49 7.62 o 4 2 3 9029.61 8450.91 63.97 o 5 2 3 15.73 22.07 8.23 o 6 2 3 3127.05 3153.07 29.73 o 7 2 3 96.91 110.14 15.76 o 8 2 3 661.25 682.82 25.04 o 9 2 3 0.90 -10.19 21.45 o 0 3 3 304.41 344.53 8.83 o 1 3 3 82.40 94.08 4.96 o 2 3 3 50.11 50.94 5.00 o 3 3 3 368.73 375.92 6.76 o 4 3 3 229.37 262.64 9.00 o 5 3 3 2.87 7.07 8.06 o 6 3 3 36.77 63.01 11.06 o 7 3 3 210.57 237.20 19.94 o 8 3 3 89.45 94.39 20.19 o 0 4 3 12498.77 12122.82 118.60 o 1 4 3 530.47 586.66 9.27 o 2 4 3 11027.36 10581.50 66.66 o 3 4 3 536.45 542.37 8.88 o 4 4 3 4584.99 4466.38 35.39 o 5 4 3 119.87 120.08 10.45 o 6 4 3 1658.21 1635.64 23.85 o 7 4 3 200.50 171.82 16.34 o 8 4 3 208.19 206.25 21.27 o 0 5 3 12901.74 12539.05 142.29 o 1 5 3 403.41 407.45 8.90 o 2 5 3 10291.07 10044.71 91.01 o 3 5 3 195.19 210.97 8.65 o 4 5 3 5656.91 5445.73 39.13 o 5 5 3 262.66 268.23 12.78 o 6 5 3 2053.60 2063.77 27.29 o 7 5 3 36.56 49.36 13.93 o 8 5 3 563.53 570.70 27.15 o 0 6 3 19.81 23.98 11.51 o 1 6 3 761.15 723.84 13.36 o 2 6 3 1103.87 1096.51 15.04 o 3 6 3 291.70 288.26 12.98 o 4 6 3 2.14 -10.59 10.59 o 5 6 3 563.39 559.97 18.34 o 6 6 3 578.80 590.11 23.26 o 7 6 3 49.65 20.34 18.51 o 0 7 3 3975.66 3945.05 52.55 o 1 7 3 29.54 22.90 10.50 o 2 7 3 4213.18 4067.04 37.00 o 3 7 3 3.01 -4.53 12.47 o 4 7 3 1487.01 1481.70 27.31 o 5 7 3 37.43 76.07 18.77 o 6 7 3 635.23 631.52 26.61 o 0 8 3 4014.02 4232.94 61.62 o 1 8 3 52.75 60.72 12.99 o 2 8 3 4657.88 4608.85 52.28 o 3 8 3 75.29 40.02 19.35 o 4 8 3 1917.59 1968.37 35.45 o 5 8 3 11.96 -6.33 20.47 o 6 8 3 1196.79 1206.39 35.13 o 0 9 3 54.24 52.75 21.32 o 1 9 3 125.95 103.41 15.34 o 2 9 3 315.70 300.86 21.36 o 3 9 3 204.73 190.74 20.58 o 4 9 3 72.01 67.52 22.50 o 0 10 3 1661.91 1621.64 46.26 o 1 10 3 0.10 15.92 19.50 o 2 10 3 622.85 634.65 27.25 o 0 0 4 3068.95 3238.59 38.43 o 2 0 4 1326.67 1252.52 17.83 o 4 0 4 455.29 485.79 13.13 o 6 0 4 252.38 229.44 17.58 o 8 0 4 0.47 -5.76 24.37 o 0 1 4 218.68 248.34 5.81 o 1 1 4 7.68 5.38 3.51 o 2 1 4 2231.43 2250.77 18.22 o 3 1 4 3191.01 3244.87 23.28 o 4 1 4 38.87 34.28 6.20 o 5 1 4 1799.48 1781.33 19.26 o 6 1 4 358.52 355.44 14.18 o 7 1 4 2231.07 2207.00 28.36 o 8 1 4 38.89 52.83 18.07 o 9 1 4 675.81 654.16 31.33 o 0 2 4 1575.87 1471.53 21.56 o 1 2 4 179.72 179.00 5.17 o 2 2 4 3.45 5.57 4.21 o 3 2 4 1818.74 1850.99 21.56 o 4 2 4 698.34 715.95 11.92 o 5 2 4 2189.43 2206.58 21.22 o 6 2 4 28.62 29.06 10.27 o 7 2 4 1650.48 1695.72 25.78 o 8 2 4 60.43 52.94 17.62 o 9 2 4 832.10 818.44 31.69 o 0 3 4 5507.43 5583.81 48.47 o 1 3 4 435.70 517.46 7.33 o 2 3 4 18.55 21.15 5.08 o 3 3 4 286.48 328.66 8.09 o 4 3 4 1889.89 1853.18 18.41 o 5 3 4 70.33 83.92 10.00 o 6 3 4 22.55 13.56 10.45 o 7 3 4 59.48 43.59 14.70 o 8 3 4 184.38 186.57 20.34 o 0 4 4 908.54 952.82 14.69 o 1 4 4 264.49 294.59 6.98 o 2 4 4 2.49 -1.81 5.74 o 3 4 4 1270.99 1228.97 12.97 o 4 4 4 462.19 488.09 11.33 o 5 4 4 1809.18 1800.11 19.38 o 6 4 4 4.42 23.34 10.79 o 7 4 4 1304.33 1297.80 23.49 o 8 4 4 59.23 41.89 20.77 o 0 5 4 66.97 74.12 11.88 o 1 5 4 49.23 67.83 6.78 o 2 5 4 1281.14 1301.36 14.02 o 3 5 4 2034.03 2071.78 18.96 o 4 5 4 75.76 64.14 9.12 o 5 5 4 606.71 609.07 14.99 o 6 5 4 257.53 280.02 16.72 o 7 5 4 1665.10 1641.70 27.45 o 8 5 4 68.13 65.73 22.78 o 0 6 4 361.35 367.70 20.17 o 1 6 4 9.55 2.95 7.85 o 2 6 4 899.21 941.67 14.49 o 3 6 4 0.96 -9.92 9.92 o 4 6 4 97.52 69.70 12.46 o 5 6 4 11.80 12.76 14.47 o 6 6 4 163.29 170.12 19.06 o 7 6 4 0.21 -12.16 17.69 o 0 7 4 302.33 267.55 19.44 o 1 7 4 26.62 19.00 10.72 o 2 7 4 7.37 8.13 10.79 o 3 7 4 1394.09 1368.53 23.71 o 4 7 4 163.24 172.37 18.65 o 5 7 4 390.56 394.95 23.30 o 6 7 4 0.92 -18.28 18.96 o 0 8 4 407.46 423.12 23.61 o 1 8 4 97.16 88.27 13.96 o 2 8 4 1.42 -12.71 12.71 o 3 8 4 265.12 284.91 22.95 o 4 8 4 173.30 168.17 20.12 o 5 8 4 638.38 617.32 35.94 o 0 9 4 419.48 404.93 25.30 o 1 9 4 63.91 42.52 18.60 o 2 9 4 83.45 71.99 17.41 o 3 9 4 17.98 -12.59 16.53 o 4 9 4 194.00 186.91 24.97 o 0 10 4 210.13 228.74 29.22 o 1 10 4 22.09 10.11 23.31 o 2 10 4 11.78 25.36 19.97 o 1 0 5 59.00 72.45 4.97 o 3 0 5 1740.30 1684.80 21.88 o 5 0 5 1484.44 1580.18 38.92 o 7 0 5 1439.02 1423.48 32.22 o 9 0 5 549.88 484.87 39.92 o 0 1 5 14356.53 14049.56 136.23 o 1 1 5 18.11 28.26 3.82 o 2 1 5 8738.77 8783.69 61.71 o 3 1 5 606.71 641.35 9.17 o 4 1 5 5173.62 5110.58 35.01 o 5 1 5 173.06 165.63 9.87 o 6 1 5 1458.77 1418.57 23.59 o 7 1 5 502.65 505.04 18.38 o 8 1 5 438.96 419.69 22.45 o 9 1 5 72.81 80.83 23.09 o 0 2 5 14130.06 13549.32 100.43 o 1 2 5 4682.91 5006.20 33.81 o 2 2 5 9078.80 8996.38 77.11 o 3 2 5 666.28 761.45 10.67 o 4 2 5 5206.61 4765.95 35.17 o 5 2 5 2623.26 2652.06 27.00 o 6 2 5 1767.50 1840.83 24.50 o 7 2 5 14.99 14.78 13.34 o 8 2 5 514.24 502.94 24.11 o 0 3 5 251.56 268.48 9.12 o 1 3 5 814.79 849.03 9.30 o 2 3 5 60.50 77.80 6.13 o 3 3 5 336.36 329.53 8.60 o 4 3 5 170.86 180.11 9.85 o 5 3 5 2323.25 2319.92 31.03 o 6 3 5 36.36 56.72 11.95 o 7 3 5 633.17 622.75 21.81 o 8 3 5 45.99 49.78 18.80 o 0 4 5 7643.67 7256.84 87.27 o 1 4 5 783.89 841.38 9.85 o 2 4 5 3854.86 3691.56 25.71 o 3 4 5 45.90 38.71 7.22 o 4 4 5 3203.04 3274.52 28.07 o 5 4 5 897.80 893.71 14.59 o 6 4 5 607.38 613.75 15.46 o 7 4 5 13.65 22.72 14.42 o 8 4 5 276.60 290.79 23.18 o 0 5 5 6527.92 6353.77 67.79 o 1 5 5 167.08 171.26 8.00 o 2 5 5 5798.60 5588.55 36.70 o 3 5 5 1000.50 1005.33 14.24 o 4 5 5 2961.54 2990.47 25.69 o 5 5 5 28.71 19.61 10.47 o 6 5 5 1352.18 1343.49 21.95 o 7 5 5 552.39 572.62 21.23 o 0 6 5 682.92 735.29 19.98 o 1 6 5 686.61 682.43 13.16 o 2 6 5 29.52 32.59 8.97 o 3 6 5 69.43 73.59 10.89 o 4 6 5 470.86 466.68 16.14 o 5 6 5 1513.74 1513.54 27.44 o 6 6 5 30.36 36.41 17.02 o 7 6 5 238.25 237.08 23.25 o 0 7 5 2300.94 2312.63 38.35 o 1 7 5 8.90 19.55 11.37 o 2 7 5 1488.96 1518.02 23.90 o 3 7 5 157.93 160.40 16.03 o 4 7 5 968.93 976.74 23.47 o 5 7 5 29.65 10.78 23.34 o 6 7 5 232.35 241.34 24.03 o 0 8 5 3170.75 3182.42 48.93 o 1 8 5 145.21 140.07 15.23 o 2 8 5 1743.66 1834.29 29.43 o 3 8 5 12.85 6.68 14.51 o 4 8 5 1645.11 1628.40 31.66 o 5 8 5 317.29 271.98 25.66 o 0 9 5 240.48 266.25 26.52 o 1 9 5 181.05 184.78 18.36 o 2 9 5 107.74 122.71 18.36 o 3 9 5 42.32 33.65 18.43 o 4 9 5 189.80 145.89 24.20 o 0 10 5 330.55 342.44 31.96 o 1 10 5 142.41 176.79 21.89 o 0 0 6 18974.67 18287.16 177.78 o 2 0 6 19824.31 19226.98 200.47 o 4 0 6 6148.39 5777.51 105.93 o 6 0 6 3341.28 3355.09 46.95 o 8 0 6 317.42 316.87 28.04 o 0 1 6 3913.90 3845.67 33.77 o 1 1 6 885.17 1020.05 9.77 o 2 1 6 5962.81 5778.29 40.77 o 3 1 6 47.28 53.54 6.55 o 4 1 6 1381.21 1384.33 16.78 o 5 1 6 699.86 703.55 13.93 o 6 1 6 1174.40 1196.58 19.40 o 7 1 6 12.15 1.88 13.88 o 8 1 6 61.54 49.04 17.79 o 0 2 6 7476.76 7294.71 84.14 o 1 2 6 211.45 225.05 5.68 o 2 2 6 1189.96 1179.45 12.18 o 3 2 6 13.48 21.62 6.44 o 4 2 6 2909.02 2947.15 24.10 o 5 2 6 333.31 341.61 12.46 o 6 2 6 65.60 67.98 11.73 o 7 2 6 89.48 95.10 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