#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2010925.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2010925_Fobs loop_ _publ_author_name 'Freire, Eleonora' 'Baggio, Sergio' 'Mombru, Alvaro' 'Baggio, Ricardo' _publ_section_title ; Tris(2,2'-bipyridyl-N,N')nickel(II) thiosulfate heptahydrate ; _journal_issue 5 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 541 _journal_page_last 543 _journal_volume 56 _journal_year 2000 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 115.649 _cell_angle_gamma 90.000 _cell_length_a 22.9340 _cell_length_b 13.4810 _cell_length_c 24.9042 _exptl_crystal_F_000 3200.00 _reflns_d_resolution_high 0.7697 _[local]_cod_data_source_file na1452Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ro in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 472.80 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 64628.06 57337.93 724.08 o 6 0 0 9334.34 6773.70 201.35 o 8 0 0 13211.20 11592.49 311.25 o 10 0 0 6793.47 4466.10 211.71 o 12 0 0 9848.54 8850.90 326.34 o 14 0 0 208.45 99.77 86.93 o 16 0 0 4889.51 5048.52 303.82 o 18 0 0 46.53 45.72 113.51 o 20 0 0 1864.47 2219.09 141.44 o 22 0 0 4672.83 5463.82 279.50 o 24 0 0 146.79 105.85 106.75 o 26 0 0 157.15 80.40 136.93 o 3 1 0 61263.27 65284.79 734.21 o 5 1 0 44113.48 40287.96 731.40 o 7 1 0 3388.67 3112.10 104.74 o 9 1 0 5777.85 6434.21 213.85 o 11 1 0 3649.91 3652.78 145.04 o 13 1 0 6317.05 5604.36 193.89 o 15 1 0 5045.42 4860.27 197.20 o 17 1 0 1018.65 875.28 76.69 o 19 1 0 5922.18 5304.49 204.05 o 21 1 0 121.52 77.48 73.53 o 23 1 0 243.86 148.74 62.84 o 25 1 0 611.57 719.46 64.48 o 0 2 0 96772.80 88906.02 1015.51 o 2 2 0 8369.99 10770.22 215.08 o 4 2 0 29031.74 29798.10 469.81 o 6 2 0 27292.33 25834.46 471.16 o 8 2 0 23433.58 26356.07 522.73 o 10 2 0 15661.52 14416.29 401.12 o 12 2 0 16.64 -16.89 54.28 o 14 2 0 2143.74 1806.03 101.35 o 16 2 0 918.40 731.51 65.76 o 18 2 0 197.62 21.85 130.85 o 20 2 0 1405.33 1218.44 89.86 o 22 2 0 577.34 544.81 93.47 o 24 2 0 90.98 148.42 130.85 o 26 2 0 3.76 36.04 110.58 o 1 3 0 9956.57 8406.70 144.60 o 3 3 0 8626.31 7069.19 198.42 o 5 3 0 335.84 341.88 29.05 o 7 3 0 10124.24 11116.15 310.58 o 9 3 0 1695.63 1779.46 98.65 o 11 3 0 308.71 201.80 38.96 o 13 3 0 587.84 638.72 58.11 o 15 3 0 2171.46 2575.38 149.55 o 17 3 0 361.56 116.44 137.61 o 19 3 0 2697.88 2565.70 160.13 o 21 3 0 10.30 113.96 93.92 o 23 3 0 2.89 -87.39 150.22 o 25 3 0 10.52 35.81 163.73 o 0 4 0 313.42 254.72 30.63 o 2 4 0 2642.02 2584.17 128.38 o 4 4 0 122.50 52.25 45.27 o 6 4 0 9976.35 10870.89 311.48 o 8 4 0 11657.03 13419.70 374.09 o 10 4 0 603.82 594.80 47.30 o 12 4 0 459.40 502.24 57.66 o 14 4 0 5.90 101.57 54.50 o 16 4 0 2466.88 2684.84 165.99 o 18 4 0 27.90 -135.13 135.13 o 20 4 0 32.14 -75.90 138.51 o 22 4 0 70.62 29.05 152.70 o 24 4 0 27.33 9.46 98.87 o 26 4 0 7.03 -28.15 131.30 o 1 5 0 1554.31 1056.22 48.97 o 3 5 0 3976.60 2698.58 148.87 o 5 5 0 420.14 600.43 42.34 o 7 5 0 21691.67 20949.00 496.83 o 9 5 0 1535.70 1509.65 98.87 o 11 5 0 3646.38 3687.07 225.22 o 13 5 0 1888.95 1811.66 106.53 o 15 5 0 29.19 52.48 76.35 o 17 5 0 2416.90 2112.11 135.81 o 19 5 0 1485.77 1507.39 104.50 o 21 5 0 30.77 150.67 132.20 o 23 5 0 64.87 36.26 153.37 o 25 5 0 83.89 -53.38 123.87 o 0 6 0 8625.09 6016.96 238.28 o 2 6 0 16419.09 14498.95 381.97 o 4 6 0 941.39 1483.75 89.41 o 6 6 0 12276.93 13496.05 401.57 o 8 6 0 6306.67 6497.80 287.38 o 10 6 0 24460.29 24185.63 602.24 o 12 6 0 2122.50 1986.43 132.88 o 14 6 0 2952.86 2830.11 164.18 o 16 6 0 6342.85 7084.50 390.76 o 18 6 0 1416.38 1453.34 104.28 o 20 6 0 128.09 240.53 124.32 o 22 6 0 262.95 460.57 84.01 o 24 6 0 36.43 148.87 96.17 o 1 7 0 752.57 535.71 37.50 o 3 7 0 69805.07 70504.25 1110.11 o 5 7 0 287.87 294.36 43.02 o 7 7 0 23415.89 23458.40 586.70 o 9 7 0 9801.67 10044.33 385.58 o 11 7 0 804.50 836.69 66.21 o 13 7 0 6606.41 6844.19 356.30 o 15 7 0 1039.09 1062.36 85.58 o 17 7 0 245.75 243.46 133.78 o 19 7 0 2641.01 2258.73 140.09 o 21 7 0 70.00 136.71 70.27 o 23 7 0 2.15 146.39 94.37 o 0 8 0 19304.43 15521.22 455.39 o 2 8 0 422.21 980.38 60.81 o 4 8 0 121.91 15.99 60.81 o 6 8 0 24937.23 25417.58 629.49 o 8 8 0 1111.17 1051.55 73.42 o 10 8 0 8543.49 9494.12 402.92 o 12 8 0 4151.00 4235.48 277.92 o 14 8 0 999.95 1129.93 91.21 o 16 8 0 2899.04 2917.49 158.55 o 18 8 0 454.38 522.96 83.56 o 20 8 0 15.20 -174.77 174.77 o 22 8 0 579.77 657.19 94.37 o 1 9 0 241.30 145.98 64.41 o 3 9 0 7999.34 7648.67 330.62 o 5 9 0 1045.84 942.54 68.47 o 7 9 0 15717.93 16641.01 529.04 o 9 9 0 5294.25 5545.35 324.99 o 11 9 0 159.81 97.29 104.73 o 13 9 0 834.28 885.79 77.48 o 15 9 0 108.14 276.57 52.03 o 17 9 0 26.60 25.90 103.15 o 19 9 0 105.18 165.99 127.02 o 21 9 0 22.26 194.81 99.77 o 23 9 0 39.33 101.80 94.14 o 0 10 0 8277.06 8270.73 374.54 o 2 10 0 4204.02 3843.82 255.40 o 4 10 0 2574.45 2700.16 159.23 o 6 10 0 5.90 -102.02 102.02 o 8 10 0 3520.89 3613.42 194.36 o 10 10 0 210.53 413.73 55.63 o 12 10 0 94.53 107.43 119.37 o 14 10 0 504.60 649.76 75.00 o 16 10 0 10.65 -11.94 82.21 o 18 10 0 38.29 26.35 114.64 o 20 10 0 13.89 26.35 125.22 o 22 10 0 357.38 110.13 198.42 o 1 11 0 5.62 49.69 42.31 o 3 11 0 424.06 484.67 60.13 o 5 11 0 370.82 215.08 143.69 o 7 11 0 3598.61 3395.63 200.22 o 9 11 0 194.79 -163.96 163.96 o 11 11 0 26.41 62.39 95.94 o 13 11 0 1504.85 1587.12 111.03 o 15 11 0 54.97 -52.25 130.18 o 17 11 0 210.00 83.56 154.28 o 19 11 0 0.02 -102.02 112.83 o 0 12 0 3728.71 3527.16 201.80 o 2 12 0 20.89 62.61 74.10 o 4 12 0 2462.34 2578.09 144.37 o 6 12 0 33.74 52.03 115.09 o 8 12 0 0.13 52.70 60.58 o 10 12 0 557.96 446.84 83.33 o 12 12 0 114.69 181.30 103.60 o 14 12 0 87.84 98.87 61.48 o 16 12 0 22.87 58.78 102.93 o 18 12 0 29.89 9.01 104.28 o 1 13 0 60.41 -13.40 72.46 o 3 13 0 3386.21 3460.95 223.19 o 5 13 0 139.98 175.00 53.38 o 7 13 0 530.71 587.60 84.23 o 9 13 0 1536.18 1624.28 114.64 o 11 13 0 73.98 47.97 110.81 o 13 13 0 1651.07 1438.70 120.72 o 15 13 0 4.51 -180.63 180.63 o 17 13 0 12.85 -80.63 121.17 o 0 14 0 5539.44 6213.80 304.95 o 2 14 0 18.49 -70.49 123.19 o 4 14 0 2315.83 2038.69 131.75 o 6 14 0 2308.83 2370.88 148.87 o 8 14 0 3.26 -25.90 121.62 o 10 14 0 2696.05 2726.73 170.72 o 12 14 0 1361.07 1248.84 103.60 o 14 14 0 142.05 -42.12 158.55 o 16 14 0 229.15 175.45 129.95 o 1 15 0 19.37 -62.66 95.40 o 3 15 0 5016.29 5065.41 280.40 o 5 15 0 264.42 156.08 90.09 o 7 15 0 1983.50 2157.38 142.11 o 9 15 0 209.82 150.45 134.01 o 11 15 0 69.06 112.83 115.31 o 13 15 0 229.81 244.59 155.18 o 0 16 0 2716.26 3122.67 190.76 o 2 16 0 2.49 42.34 76.35 o 4 16 0 419.16 426.12 71.84 o 6 16 0 1223.21 959.66 109.46 o 8 16 0 7.87 -157.88 168.24 o 10 16 0 1450.32 1025.42 126.12 o 1 17 0 29.27 -93.49 162.95 o 3 17 0 318.43 218.91 201.57 o 5 17 0 166.56 202.25 132.43 o -27 1 1 14.92 126.96 41.54 o -25 1 1 346.48 313.80 69.37 o -23 1 1 87.59 17.62 167.11 o -21 1 1 1722.92 1974.47 85.76 o -19 1 1 435.00 411.04 45.79 o -17 1 1 0.32 -55.88 55.88 o -15 1 1 3249.63 3187.88 113.56 o -13 1 1 3740.42 3767.11 157.25 o -11 1 1 36.81 23.11 26.69 o -9 1 1 142.54 187.95 32.88 o -7 1 1 24449.87 23159.48 557.42 o -5 1 1 3545.53 3816.50 95.94 o -3 1 1 33722.89 28369.03 779.93 o 1 1 1 2911.28 3452.90 44.71 o 3 1 1 4979.78 6002.79 185.36 o 5 1 1 169151.83 164541.30 1420.69 o 7 1 1 4600.54 4496.11 129.19 o 9 1 1 7434.21 8916.00 207.65 o 11 1 1 11923.76 10999.35 256.20 o 13 1 1 96.98 50.19 55.29 o 15 1 1 341.06 384.94 36.75 o 17 1 1 1164.16 1046.40 93.13 o 19 1 1 656.80 651.17 56.13 o 21 1 1 817.78 745.34 61.63 o 23 1 1 241.21 171.56 60.70 o 25 1 1 103.29 209.74 50.15 o -26 2 1 202.60 -195.04 195.04 o -24 2 1 136.72 115.09 141.21 o -22 2 1 1630.47 1861.89 118.47 o -20 2 1 6.84 39.19 106.30 o -18 2 1 2194.55 2554.21 143.69 o -16 2 1 3986.50 3928.28 185.58 o -14 2 1 396.31 524.09 52.03 o -12 2 1 4938.40 4479.39 229.95 o -10 2 1 5068.99 4403.49 209.45 o -8 2 1 35964.89 35576.33 623.63 o -6 2 1 20609.40 19715.25 389.63 o -4 2 1 45190.43 38132.57 553.59 o -2 2 1 4005.03 5508.64 144.82 o 0 2 1 64929.79 63588.35 536.52 o 2 2 1 40259.81 47199.67 621.16 o 4 2 1 50585.60 60325.23 808.09 o 6 2 1 71280.52 73293.37 999.75 o 8 2 1 15406.86 17120.50 410.35 o 10 2 1 15725.57 13527.13 389.85 o 12 2 1 165.68 193.46 33.33 o 14 2 1 384.16 443.46 48.65 o 16 2 1 6818.55 6229.12 356.30 o 18 2 1 10.29 -11.94 80.18 o 20 2 1 34.37 122.97 104.73 o 22 2 1 2079.29 2480.79 154.73 o 24 2 1 11.49 -6.31 136.03 o 26 2 1 288.61 272.29 74.77 o -25 3 1 2226.58 2327.19 151.57 o -23 3 1 2.10 19.82 126.80 o -21 3 1 16.67 76.12 129.73 o -19 3 1 3487.86 3449.01 197.97 o -17 3 1 199.53 143.01 106.30 o -15 3 1 8564.24 8067.13 364.63 o -13 3 1 5724.33 5184.78 266.88 o -11 3 1 1451.02 1084.43 70.49 o -9 3 1 23639.67 23710.20 517.55 o -7 3 1 7116.95 7388.32 246.62 o -5 3 1 26040.14 21428.95 413.73 o -3 3 1 72641.57 64899.67 853.36 o -1 3 1 74264.71 61906.00 902.57 o 1 3 1 3160.34 2830.37 142.34 o 3 3 1 9632.90 9018.01 233.10 o 5 3 1 20447.45 19858.49 406.52 o 7 3 1 17399.40 14196.03 368.46 o 9 3 1 20993.91 24433.15 540.75 o 11 3 1 543.96 486.70 50.45 o 13 3 1 16578.04 15350.73 490.08 o 15 3 1 1084.34 1239.38 79.05 o 17 3 1 79.23 91.44 57.21 o 19 3 1 4911.57 5845.34 370.26 o 21 3 1 931.04 639.62 87.61 o 23 3 1 569.50 445.93 99.77 o 25 3 1 1123.88 1150.42 111.48 o -26 4 1 287.56 71.84 158.55 o -24 4 1 13.22 -103.60 126.12 o -22 4 1 4855.31 5243.78 271.84 o -20 4 1 74.25 108.33 62.16 o -18 4 1 4732.70 4356.42 217.79 o -16 4 1 6323.15 5131.17 316.43 o -14 4 1 220.18 213.28 42.57 o -12 4 1 109.74 74.32 67.12 o -10 4 1 9269.44 7332.47 297.06 o -8 4 1 283.62 143.69 73.65 o -6 4 1 15312.10 13407.99 350.22 o -4 4 1 36.59 430.62 28.83 o -2 4 1 39153.68 32189.48 534.22 o 0 4 1 54436.94 51106.75 520.23 o 2 4 1 2184.82 2037.33 113.51 o 4 4 1 1285.32 1752.88 83.56 o 6 4 1 9343.44 9730.15 295.94 o 8 4 1 3269.17 2260.53 152.25 o 10 4 1 5771.57 4697.63 237.83 o 12 4 1 10597.38 9831.28 372.51 o 14 4 1 282.95 537.60 52.03 o 16 4 1 7752.91 7515.35 389.18 o 18 4 1 6.86 -31.53 82.43 o 20 4 1 227.44 -147.07 147.07 o 22 4 1 2126.88 2595.20 170.27 o 24 4 1 150.42 128.15 134.91 o -25 5 1 551.38 620.25 90.54 o -23 5 1 507.15 460.12 79.50 o -21 5 1 484.82 449.09 66.21 o -19 5 1 1288.10 1272.71 97.97 o -17 5 1 522.15 392.11 70.27 o -15 5 1 2251.96 2422.91 152.70 o -13 5 1 4778.00 4178.50 263.06 o -11 5 1 2463.41 2355.12 127.25 o -9 5 1 11744.36 12994.71 400.21 o -7 5 1 555.61 441.88 41.89 o -5 5 1 10396.37 8892.34 286.70 o -3 5 1 93540.66 85047.79 1158.30 o -1 5 1 6989.22 5127.63 140.19 o 1 5 1 1071.16 1362.75 80.40 o 3 5 1 3614.43 3660.04 180.85 o 5 5 1 884.41 390.08 38.29 o 7 5 1 36613.27 34573.20 679.49 o 9 5 1 1994.11 1896.35 109.68 o 11 5 1 48.93 75.00 77.03 o 13 5 1 4071.46 3913.19 252.70 o 15 5 1 7146.50 7601.15 386.03 o 17 5 1 458.82 417.11 67.12 o 19 5 1 6254.14 7160.40 449.09 o 21 5 1 92.76 98.87 98.42 o 23 5 1 167.87 265.31 158.78 o 25 5 1 390.57 337.60 86.26 o -24 6 1 7.35 197.74 101.12 o -22 6 1 2091.91 2160.53 135.13 o -20 6 1 1468.22 1636.89 110.36 o -18 6 1 2300.88 3007.80 196.39 o -16 6 1 578.33 677.91 74.77 o -14 6 1 30.74 -59.91 83.78 o -12 6 1 4323.69 4635.24 275.67 o -10 6 1 2163.13 2034.86 124.55 o -8 6 1 168.30 199.54 34.23 o -6 6 1 14034.78 12555.08 380.62 o -4 6 1 158.57 205.85 31.98 o -2 6 1 6568.33 4363.40 203.82 o 0 6 1 10621.69 9348.74 212.05 o 2 6 1 12475.99 11964.33 344.14 o 4 6 1 6561.74 6791.49 272.29 o 6 6 1 1053.04 1436.22 91.89 o 8 6 1 4660.29 4660.24 250.89 o 10 6 1 3183.90 3751.93 229.05 o 12 6 1 2643.01 2961.86 158.33 o 14 6 1 712.10 718.45 69.59 o 16 6 1 2134.26 2625.61 170.27 o 18 6 1 17.10 15.09 120.04 o 20 6 1 832.84 614.62 83.33 o 22 6 1 313.55 388.73 71.84 o 24 6 1 6.57 -61.94 143.24 o -23 7 1 6.90 77.48 129.05 o -21 7 1 448.00 411.03 84.23 o -19 7 1 84.68 197.29 102.47 o -17 7 1 380.47 422.96 65.31 o -15 7 1 2866.57 2897.22 187.16 o -13 7 1 290.73 212.61 53.15 o -11 7 1 566.31 513.50 55.85 o -9 7 1 149.28 100.67 79.95 o -7 7 1 376.54 346.61 47.52 o -5 7 1 1692.23 1647.48 107.43 o -3 7 1 10247.31 10265.27 342.78 o -1 7 1 947.02 1082.18 48.31 o 1 7 1 37.66 28.10 26.04 o 3 7 1 16.72 21.40 63.29 o 5 7 1 2157.25 1912.11 112.16 o 7 7 1 486.67 557.64 52.03 o 9 7 1 90.19 110.13 35.13 o 11 7 1 515.57 581.52 54.95 o 13 7 1 218.96 128.83 47.75 o 15 7 1 781.58 799.08 76.35 o 17 7 1 322.77 205.17 143.46 o 19 7 1 52.49 -45.49 114.19 o 21 7 1 50.94 66.89 138.06 o 23 7 1 0.10 -43.47 97.75 o -24 8 1 12.12 118.92 122.97 o -22 8 1 56.19 59.46 105.18 o -20 8 1 531.15 487.37 77.70 o -18 8 1 2016.50 1895.22 123.19 o -16 8 1 315.22 401.57 58.11 o -14 8 1 5.16 -99.10 99.10 o -12 8 1 44.49 -100.67 100.67 o -10 8 1 8776.09 8870.49 388.95 o -8 8 1 147.15 -30.63 94.14 o -6 8 1 715.62 557.87 67.79 o -4 8 1 57.82 59.68 70.94 o -2 8 1 533.09 543.00 47.75 o 0 8 1 901.78 747.44 40.43 o 2 8 1 2792.79 3667.70 211.93 o 4 8 1 422.21 449.54 46.85 o 6 8 1 473.90 506.74 58.56 o 8 8 1 22.01 6.08 61.26 o 10 8 1 52.01 -78.38 78.38 o 12 8 1 761.78 708.54 73.42 o 14 8 1 13.00 11.49 117.56 o 16 8 1 1339.33 1494.11 105.63 o 18 8 1 1419.74 1667.07 111.03 o 20 8 1 193.61 209.68 148.42 o 22 8 1 7.73 -128.60 128.60 o -23 9 1 116.05 58.78 90.09 o -21 9 1 8.49 -65.31 88.96 o -19 9 1 1703.38 1535.55 118.01 o -17 9 1 75.48 151.35 113.74 o -15 9 1 975.59 948.85 93.69 o -13 9 1 497.97 557.19 66.44 o -11 9 1 1836.08 1669.55 108.11 o -9 9 1 2965.57 3111.63 167.11 o -7 9 1 1521.89 1471.58 94.59 o -5 9 1 3161.78 3643.82 229.50 o -3 9 1 7086.42 6823.92 320.94 o -1 9 1 358.15 271.17 43.81 o 1 9 1 8.06 54.36 37.62 o 3 9 1 7765.43 8667.79 360.58 o 5 9 1 2911.47 2444.08 147.52 o 7 9 1 4370.11 4097.19 265.98 o 9 9 1 3401.54 3953.50 199.77 o 11 9 1 1601.20 1483.07 93.24 o 13 9 1 2794.44 2531.92 141.21 o 15 9 1 1440.32 1449.06 104.73 o 17 9 1 347.95 504.04 73.65 o 19 9 1 1190.82 1205.15 108.56 o 21 9 1 12.09 198.19 101.35 o -22 10 1 1044.99 1130.38 109.23 o -20 10 1 68.30 -178.60 178.60 o -18 10 1 966.81 971.60 100.00 o -16 10 1 1736.98 1881.26 124.10 o -14 10 1 371.02 485.35 67.12 o -12 10 1 4095.42 3994.04 212.83 o -10 10 1 2124.47 2027.88 132.43 o -8 10 1 13.32 -35.58 100.67 o -6 10 1 9497.55 10053.34 420.71 o -4 10 1 16.38 138.96 70.04 o -2 10 1 6973.68 7220.53 343.68 o 0 10 1 15650.26 16180.19 374.41 o 2 10 1 1183.95 1179.25 72.52 o 4 10 1 11012.64 10898.82 441.88 o 6 10 1 1139.08 1325.87 89.19 o 8 10 1 790.62 689.62 74.77 o 10 10 1 1519.12 1483.75 95.27 o 12 10 1 2880.99 2841.14 185.36 o 14 10 1 21.79 65.54 101.57 o 16 10 1 3535.89 3869.49 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563.42 258.33 o -11 1 32 675.80 626.27 149.88 o -14 2 32 411.39 271.16 179.95 o -12 2 32 35.28 139.41 149.55 o