#------------------------------------------------------------------------------ #$Date: 2016-04-02 21:21:17 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180779 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/10/2011091.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2011091_Fobs loop_ _publ_author_name 'Ruggiero, Silvana Guilardi' 'do Gambardella, Maria Teresa' 'Branco, Marcelo Cardoso' 'Demuner, Antonio Jacinto' 'Barbosa, Luis Claudio A.' 'Pil\'o-Veloso, Dorila' _publ_section_title ; 21\a-Fluoro-7-norvouacapane-17\b,21\a-lactone ; _journal_issue 7 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 868 _journal_page_last 869 _journal_volume 56 _journal_year 2000 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _cell_angle_alpha 90.000 _cell_angle_beta 101.685 _cell_angle_gamma 90.000 _cell_length_a 9.4398 _cell_length_b 9.3662 _cell_length_c 9.7406 _exptl_crystal_F_000 356.00 _reflns_d_resolution_high 0.8024 _cod_data_source_file da1124IIIsup2.hkl _cod_data_source_block III #BEGIN Tags that were not found in dictionaries: _shelx_title ' ADVF CRISTAL DEMUNER 17/11/95' _shelx_refln_list_code 4 _shelx_f_calc_maximum 121.92 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 -11 0 1.86 3.15 1.08 o 2 -11 0 4.31 1.48 2.02 o 3 -11 0 8.66 8.17 1.42 o 0 -10 0 10.92 12.74 1.02 o 1 -10 0 5.17 0.30 1.27 o 2 -10 0 0.22 0.19 0.59 o 3 -10 0 11.92 13.45 1.19 o 4 -10 0 2.54 0.51 1.62 o 5 -10 0 1.53 1.27 2.00 o 1 -9 0 0.98 -1.05 1.56 o 2 -9 0 16.71 14.23 1.08 o 3 -9 0 6.54 6.31 1.00 o 4 -9 0 8.31 9.57 1.03 o 5 -9 0 60.09 68.13 2.10 o 6 -9 0 16.38 18.48 1.34 o 7 -9 0 2.61 4.15 1.13 o 0 -8 0 165.97 163.94 4.69 o 1 -8 0 127.52 120.51 3.07 o 2 -8 0 8.50 9.75 1.00 o 3 -8 0 29.27 32.88 1.19 o 4 -8 0 31.98 27.82 1.18 o 5 -8 0 27.36 24.45 1.18 o 6 -8 0 33.43 34.55 1.32 o 7 -8 0 3.46 3.94 0.92 o 8 -8 0 4.13 5.26 1.10 o 1 -7 0 148.88 150.35 4.40 o 2 -7 0 272.15 266.50 5.85 o 3 -7 0 300.47 280.35 6.01 o 4 -7 0 22.49 28.13 1.10 o 5 -7 0 36.22 34.50 1.18 o 6 -7 0 17.94 15.74 1.08 o 7 -7 0 1.83 3.23 0.84 o 8 -7 0 4.80 7.20 0.97 o 9 -7 0 5.35 4.87 1.10 o 0 -6 0 890.34 883.19 8.54 o 1 -6 0 50.13 51.58 1.54 o 2 -6 0 18.53 23.20 0.95 o 3 -6 0 26.27 25.12 0.95 o 4 -6 0 33.73 33.01 1.10 o 5 -6 0 51.95 52.61 1.38 o 6 -6 0 28.63 29.80 1.13 o 7 -6 0 7.59 7.81 0.91 o 8 -6 0 1.17 0.76 1.40 o 9 -6 0 22.93 24.72 1.38 o 1 -5 0 591.72 622.88 6.77 o 2 -5 0 932.93 994.57 8.55 o 3 -5 0 263.02 292.21 5.04 o 4 -5 0 33.26 33.80 1.21 o 5 -5 0 157.26 155.56 4.37 o 6 -5 0 187.77 188.59 5.04 o 7 -5 0 68.23 66.56 2.40 o 8 -5 0 54.96 55.95 1.56 o 9 -5 0 2.86 1.29 1.75 o 10 -5 0 24.81 24.80 1.43 o 0 -4 0 2128.59 2239.48 10.94 o 1 -4 0 171.59 191.12 3.53 o 2 -4 0 200.63 202.64 3.75 o 3 -4 0 619.18 692.18 6.92 o 4 -4 0 138.80 126.80 3.50 o 5 -4 0 148.05 148.68 3.90 o 6 -4 0 22.61 24.64 0.91 o 7 -4 0 27.36 25.33 1.00 o 8 -4 0 30.46 28.89 1.07 o 9 -4 0 16.17 15.12 0.95 o 10 -4 0 4.50 3.42 0.92 o 1 -3 0 60.15 69.05 1.46 o 2 -3 0 3076.17 3165.54 12.12 o 3 -3 0 344.40 359.35 4.69 o 4 -3 0 19.23 20.96 0.70 o 5 -3 0 42.47 38.40 1.08 o 6 -3 0 54.04 52.79 1.62 o 7 -3 0 135.26 136.87 2.99 o 8 -3 0 112.63 118.50 3.04 o 9 -3 0 18.71 17.30 1.00 o 10 -3 0 7.73 8.33 0.94 o 11 -3 0 30.63 32.79 1.56 o 0 -2 0 865.42 837.81 4.61 o 1 -2 0 715.33 722.30 4.72 o 2 -2 0 929.98 929.52 5.84 o 3 -2 0 586.86 588.72 5.42 o 4 -2 0 427.56 431.25 5.14 o 5 -2 0 17.30 17.09 0.62 o 6 -2 0 51.95 57.10 1.51 o 7 -2 0 27.90 26.09 0.89 o 8 -2 0 12.01 10.54 0.79 o 9 -2 0 0.72 0.16 0.45 o 10 -2 0 46.16 47.10 1.59 o 11 -2 0 3.38 0.54 1.40 o 1 -1 0 1652.15 1548.92 5.34 o 2 -1 0 1523.44 1415.09 6.30 o 3 -1 0 960.78 904.65 6.23 o 4 -1 0 698.47 699.96 6.33 o 5 -1 0 134.02 147.81 3.29 o 6 -1 0 22.12 22.43 0.76 o 7 -1 0 21.98 17.46 0.79 o 8 -1 0 82.78 83.38 2.48 o 9 -1 0 3.50 4.31 0.72 o 10 -1 0 0.82 -0.30 1.02 o 11 -1 0 2.71 3.97 0.91 o 2 0 0 372.30 339.67 3.08 o 3 0 0 236.10 230.93 3.15 o 4 0 0 599.32 568.58 5.52 o 5 0 0 707.98 685.27 6.88 o 6 0 0 350.68 380.04 5.76 o 7 0 0 0.62 2.05 0.54 o 8 0 0 71.61 67.15 2.29 o 9 0 0 44.76 40.45 1.48 o 10 0 0 1.15 1.08 1.46 o 11 0 0 1.79 3.08 0.86 o -3 -11 1 5.76 8.90 1.34 o -2 -11 1 6.57 7.46 1.24 o -1 -11 1 16.58 19.24 1.43 o 0 -11 1 18.00 17.68 2.04 o 1 -11 1 6.87 6.34 1.27 o 2 -11 1 15.83 17.70 1.51 o 3 -11 1 4.90 4.71 1.30 o -6 -10 1 0.37 0.95 0.99 o -5 -10 1 39.19 40.50 1.67 o -4 -10 1 12.55 12.40 1.32 o -3 -10 1 2.14 -2.13 2.13 o -2 -10 1 14.94 17.20 1.16 o -1 -10 1 10.07 11.54 1.08 o 0 -10 1 0.80 2.51 0.60 o 1 -10 1 4.73 7.84 1.05 o 2 -10 1 3.75 5.85 1.05 o 3 -10 1 8.93 9.38 1.18 o 4 -10 1 0.53 0.72 1.80 o 5 -10 1 37.81 40.96 1.73 o -7 -9 1 14.41 14.50 1.37 o -6 -9 1 0.21 -0.46 0.75 o -5 -9 1 4.46 5.52 0.99 o -4 -9 1 9.07 12.26 1.08 o -3 -9 1 23.71 23.12 1.14 o -2 -9 1 19.04 19.38 1.13 o -1 -9 1 61.21 54.01 2.05 o 0 -9 1 62.43 66.91 1.52 o 1 -9 1 5.29 6.93 0.92 o 2 -9 1 5.00 7.31 0.99 o 3 -9 1 20.69 22.63 1.21 o 4 -9 1 11.21 12.26 1.14 o 5 -9 1 8.44 10.43 1.03 o 6 -9 1 14.25 15.65 1.29 o 7 -9 1 2.39 3.26 1.13 o -8 -8 1 3.93 5.96 1.11 o -7 -8 1 16.22 19.38 1.13 o -6 -8 1 14.90 14.41 1.07 o -5 -8 1 6.58 7.31 0.97 o -4 -8 1 15.07 19.41 1.05 o -3 -8 1 17.06 15.42 0.97 o -2 -8 1 194.45 199.92 5.41 o -1 -8 1 341.74 334.69 6.71 o 0 -8 1 9.91 12.06 0.69 o 1 -8 1 45.07 37.17 1.27 o 2 -8 1 266.58 251.60 6.20 o 3 -8 1 78.46 80.99 2.29 o 4 -8 1 1.09 0.95 0.75 o 5 -8 1 0.92 0.87 0.76 o 6 -8 1 31.12 28.05 1.30 o 7 -8 1 13.66 11.27 1.26 o 8 -8 1 7.88 5.20 1.22 o -9 -7 1 0.38 0.92 1.62 o -8 -7 1 1.82 -0.49 1.35 o -7 -7 1 11.87 11.19 0.99 o -6 -7 1 103.42 93.97 3.02 o -5 -7 1 43.68 45.30 1.34 o -4 -7 1 9.26 7.55 0.87 o -3 -7 1 105.87 98.34 2.77 o -2 -7 1 8.29 7.95 0.94 o -1 -7 1 225.86 216.60 5.17 o 0 -7 1 194.08 182.72 3.31 o 1 -7 1 13.80 12.70 0.94 o 2 -7 1 14.92 12.74 1.00 o 3 -7 1 29.22 33.39 1.14 o 4 -7 1 42.61 39.29 1.19 o 5 -7 1 5.35 4.96 0.84 o 6 -7 1 54.87 50.83 1.76 o 7 -7 1 19.96 19.03 1.11 o 8 -7 1 13.75 13.44 1.22 o -10 -6 1 7.56 8.32 1.18 o -9 -6 1 2.31 2.51 0.94 o -8 -6 1 7.03 7.14 0.92 o -7 -6 1 7.05 10.10 0.89 o -6 -6 1 99.67 93.57 2.78 o -5 -6 1 230.19 222.76 5.36 o -4 -6 1 140.72 132.06 2.85 o -3 -6 1 1.25 1.13 0.64 o -2 -6 1 119.23 120.78 2.62 o -1 -6 1 223.64 225.03 4.79 o 0 -6 1 30.53 30.47 0.68 o 1 -6 1 65.93 68.26 2.11 o 2 -6 1 281.05 289.22 5.56 o 3 -6 1 0.23 -0.45 0.56 o 4 -6 1 7.07 6.96 0.83 o 5 -6 1 57.21 51.87 1.61 o 6 -6 1 11.48 9.38 0.86 o 7 -6 1 7.94 8.05 0.91 o 8 -6 1 6.16 7.57 0.91 o 9 -6 1 1.44 1.42 1.78 o -10 -5 1 16.49 19.30 1.26 o -9 -5 1 16.57 17.90 1.05 o -8 -5 1 66.98 69.58 2.13 o -7 -5 1 90.60 83.52 2.62 o -6 -5 1 31.44 31.66 1.08 o -5 -5 1 19.57 20.30 0.89 o -4 -5 1 50.60 46.98 1.48 o -3 -5 1 59.97 59.47 1.48 o -2 -5 1 113.88 103.14 2.19 o -1 -5 1 193.24 227.30 4.21 o 0 -5 1 330.15 369.71 3.69 o 1 -5 1 282.95 307.82 5.04 o 2 -5 1 85.10 78.15 2.11 o 3 -5 1 23.15 25.96 0.86 o 4 -5 1 4.32 4.77 0.70 o 5 -5 1 36.65 42.04 1.35 o 6 -5 1 51.26 47.32 1.32 o 7 -5 1 36.40 33.66 1.16 o 8 -5 1 36.13 37.60 1.27 o 9 -5 1 2.41 2.88 0.84 o 10 -5 1 4.75 6.57 1.07 o -10 -4 1 1.30 1.57 0.75 o -9 -4 1 0.38 0.14 0.84 o -8 -4 1 14.41 13.99 0.89 o -7 -4 1 9.19 7.66 0.79 o -6 -4 1 5.58 5.88 0.72 o -5 -4 1 16.39 16.97 0.79 o -4 -4 1 101.77 87.35 2.02 o -3 -4 1 22.78 22.02 0.72 o -2 -4 1 476.12 509.00 5.58 o -1 -4 1 834.88 929.28 7.54 o 0 -4 1 117.75 120.73 2.01 o 1 -4 1 747.12 798.81 6.98 o 2 -4 1 1317.98 1400.13 9.56 o 3 -4 1 99.70 108.98 3.08 o 4 -4 1 27.37 27.46 0.84 o 5 -4 1 100.84 101.54 2.42 o 6 -4 1 24.49 24.88 0.95 o 7 -4 1 48.36 42.61 1.30 o 8 -4 1 16.64 16.35 0.97 o 9 -4 1 4.84 6.17 0.86 o 10 -4 1 9.75 10.67 1.10 o -11 -3 1 19.29 18.17 1.32 o -10 -3 1 20.09 20.30 1.08 o -9 -3 1 76.72 76.89 2.24 o -8 -3 1 31.03 29.57 1.03 o -7 -3 1 0.82 0.97 0.60 o -6 -3 1 12.30 11.54 0.70 o -5 -3 1 52.76 52.15 1.38 o -4 -3 1 920.52 923.70 7.76 o -3 -3 1 999.30 1006.18 7.58 o -2 -3 1 281.56 283.69 3.77 o -1 -3 1 452.01 443.61 4.53 o 0 -3 1 1247.58 1246.03 5.18 o 1 -3 1 9.53 11.38 0.51 o 2 -3 1 141.37 147.61 2.91 o 3 -3 1 220.14 229.72 3.86 o 4 -3 1 394.58 420.39 5.56 o 5 -3 1 322.51 339.67 5.58 o 6 -3 1 84.66 82.58 2.32 o 7 -3 1 4.24 3.74 0.70 o 8 -3 1 34.51 34.92 1.13 o 9 -3 1 50.05 50.04 1.35 o 10 -3 1 40.24 44.77 1.61 o -11 -2 1 8.40 7.57 1.08 o -10 -2 1 10.34 12.04 1.00 o -9 -2 1 148.85 124.65 3.29 o -8 -2 1 22.43 18.00 0.87 o -7 -2 1 110.83 113.10 2.62 o -6 -2 1 131.95 135.85 3.63 o -5 -2 1 98.58 114.54 3.07 o -4 -2 1 613.19 604.12 6.07 o -3 -2 1 38.83 38.49 1.14 o -2 -2 1 755.52 750.86 5.25 o -1 -2 1 2385.70 2330.98 8.47 o 0 -2 1 260.83 261.58 2.10 o 1 -2 1 476.08 495.25 4.26 o 2 -2 1 364.13 334.25 3.78 o 3 -2 1 58.25 56.92 1.45 o 4 -2 1 304.11 301.41 4.56 o 5 -2 1 237.01 252.36 4.56 o 6 -2 1 2.38 3.74 0.56 o 7 -2 1 35.94 38.19 1.13 o 8 -2 1 29.31 27.46 1.00 o 9 -2 1 30.52 26.22 1.14 o 10 -2 1 2.16 4.13 0.83 o 11 -2 1 3.63 3.21 0.99 o -11 -1 1 8.02 5.29 0.99 o -10 -1 1 20.65 19.48 1.02 o -9 -1 1 6.01 5.09 0.76 o -8 -1 1 32.30 30.99 0.97 o -7 -1 1 0.98 0.51 0.51 o -6 -1 1 108.22 105.10 2.29 o -5 -1 1 176.57 180.15 3.64 o -4 -1 1 140.71 137.52 2.80 o -3 -1 1 4.58 5.14 0.40 o -2 -1 1 384.01 347.79 3.28 o -1 -1 1 648.31 626.66 3.59 o 0 -1 1 3773.51 3458.71 26.58 o 1 -1 1 979.25 982.29 4.99 o 2 -1 1 13.96 11.92 0.45 o 3 -1 1 238.63 249.47 3.53 o 4 -1 1 429.22 444.94 5.22 o 5 -1 1 9.25 11.78 0.57 o 6 -1 1 18.27 19.30 0.76 o 7 -1 1 8.81 10.83 0.73 o 8 -1 1 6.82 6.52 0.73 o 9 -1 1 48.24 49.42 1.35 o 10 -1 1 22.71 22.48 1.10 o 11 -1 1 0.09 -1.45 1.45 o -11 0 1 0.35 -1.69 1.69 o -10 0 1 18.30 19.24 0.99 o -9 0 1 1.32 0.97 0.59 o -8 0 1 158.86 161.40 4.56 o -7 0 1 1.96 2.05 0.54 o -6 0 1 75.09 76.54 1.96 o -5 0 1 0.00 -1.02 1.02 o -4 0 1 66.99 56.32 1.38 o -3 0 1 23.68 20.51 0.65 o -2 0 1 2156.76 1982.39 7.11 o -1 0 1 97.82 95.67 1.48 o 1 0 1 1435.62 1178.15 4.93 o 2 0 1 3943.11 3656.60 10.61 o 3 0 1 61.31 64.68 1.92 o 4 0 1 13.48 10.72 0.49 o 5 0 1 47.10 40.86 1.18 o 6 0 1 55.07 60.09 1.86 o 7 0 1 46.75 42.71 1.30 o 8 0 1 8.79 7.84 0.70 o 9 0 1 36.45 40.54 1.27 o 10 0 1 0.77 -0.32 1.02 o 11 0 1 0.84 -0.35 1.03 o -3 -11 2 10.81 13.10 1.48 o -2 -11 2 6.97 6.07 1.27 o -1 -11 2 3.67 3.31 1.19 o 0 -11 2 1.78 0.33 0.92 o 1 -11 2 7.03 10.56 1.35 o 2 -11 2 4.12 2.73 1.22 o -6 -10 2 0.84 -2.40 2.40 o -5 -10 2 0.96 1.42 2.00 o -4 -10 2 2.58 1.37 2.05 o -3 -10 2 21.22 21.58 1.34 o -2 -10 2 31.71 33.66 1.38 o -1 -10 2 6.00 6.68 1.02 o 0 -10 2 0.25 -1.29 1.29 o 1 -10 2 2.29 1.22 0.91 o 2 -10 2 6.02 6.15 1.08 o 3 -10 2 1.85 0.35 1.42 o 4 -10 2 0.08 -0.99 0.99 o 5 -10 2 8.53 9.95 1.38 o -7 -9 2 5.73 7.28 1.18 o -6 -9 2 1.50 -0.49 1.56 o -5 -9 2 41.35 43.66 1.42 o -4 -9 2 16.57 19.80 1.13 o -3 -9 2 18.96 17.46 1.16 o -2 -9 2 18.71 16.50 1.16 o -1 -9 2 13.11 11.51 1.00 o 0 -9 2 3.79 5.12 1.33 o 1 -9 2 19.23 19.48 1.16 o 2 -9 2 33.74 34.69 1.32 o 3 -9 2 4.37 3.20 0.95 o 4 -9 2 17.97 16.81 1.18 o 5 -9 2 2.09 5.04 0.99 o 6 -9 2 5.66 8.01 1.19 o -8 -8 2 1.89 1.11 0.92 o -7 -8 2 4.27 3.63 0.92 o -6 -8 2 37.97 35.01 1.32 o -5 -8 2 9.95 12.15 0.94 o -4 -8 2 17.41 15.93 1.08 o -3 -8 2 123.93 115.23 3.16 o -2 -8 2 30.40 32.32 1.22 o -1 -8 2 42.15 39.24 1.26 o 0 -8 2 215.77 207.44 3.82 o 1 -8 2 102.02 102.90 2.99 o 2 -8 2 46.35 39.64 1.35 o 3 -8 2 32.38 31.12 1.29 o 4 -8 2 25.66 27.62 1.21 o 5 -8 2 22.23 24.80 1.19 o 6 -8 2 18.32 21.04 1.21 o 7 -8 2 3.36 0.91 1.81 o -9 -7 2 6.44 7.95 1.13 o -8 -7 2 4.42 0.33 1.21 o -7 -7 2 0.53 -1.73 1.73 o -6 -7 2 39.50 37.67 1.27 o -5 -7 2 8.26 6.25 0.86 o -4 -7 2 18.05 15.80 0.99 o -3 -7 2 72.71 73.09 2.05 o -2 -7 2 469.40 442.76 7.55 o -1 -7 2 24.77 24.80 1.07 o 0 -7 2 34.46 36.71 0.80 o 1 -7 2 2.53 1.78 0.78 o 2 -7 2 10.27 11.40 0.94 o 3 -7 2 95.86 100.65 2.88 o 4 -7 2 22.17 23.90 1.10 o 5 -7 2 60.78 57.40 1.75 o 6 -7 2 35.28 35.87 1.24 o 7 -7 2 20.88 22.40 1.18 o 8 -7 2 0.74 -1.91 1.91 o -10 -6 2 4.02 -1.65 1.76 o -9 -6 2 13.09 14.44 1.07 o -8 -6 2 22.03 22.78 1.14 o -7 -6 2 23.47 27.24 1.08 o -6 -6 2 30.95 28.00 1.10 o -5 -6 2 114.30 101.46 2.81 o -4 -6 2 18.29 22.78 0.95 o -3 -6 2 50.01 47.81 1.38 o -2 -6 2 26.33 26.87 0.99 o -1 -6 2 63.68 56.32 1.62 o 0 -6 2 322.49 340.98 4.11 o 1 -6 2 275.74 268.71 5.36 o 2 -6 2 66.28 69.58 2.40 o 3 -6 2 208.01 208.59 5.07 o 4 -6 2 2.01 0.11 0.73 o 5 -6 2 12.71 13.28 0.91 o 6 -6 2 10.36 10.61 0.94 o 7 -6 2 21.74 23.55 1.13 o 8 -6 2 7.97 7.20 0.99 o 9 -6 2 12.35 18.71 1.27 o -10 -5 2 7.81 7.73 1.08 o -9 -5 2 0.23 -1.54 1.70 o -8 -5 2 15.39 15.84 0.99 o -7 -5 2 29.82 32.02 1.13 o -6 -5 2 74.65 65.71 1.94 o -5 -5 2 441.29 431.09 6.79 o -4 -5 2 66.40 64.81 2.05 o -3 -5 2 76.92 71.99 2.04 o -2 -5 2 314.36 341.88 5.45 o -1 -5 2 459.68 502.01 6.44 o 0 -5 2 63.61 65.11 2.25 o 1 -5 2 19.08 16.19 0.73 o 2 -5 2 307.67 316.42 5.39 o 3 -5 2 299.20 315.56 5.66 o 4 -5 2 117.39 107.74 2.66 o 5 -5 2 69.77 68.07 1.91 o 6 -5 2 48.34 47.21 1.53 o 7 -5 2 29.80 31.39 1.11 o 8 -5 2 12.80 13.61 1.00 o 9 -5 2 8.53 11.15 1.10 o -11 -4 2 2.95 4.50 1.00 o -10 -4 2 38.57 42.82 1.42 o -9 -4 2 29.14 29.37 1.16 o -8 -4 2 25.30 24.09 1.02 o -7 -4 2 38.08 35.39 1.10 o -6 -4 2 40.74 41.26 1.13 o -5 -4 2 0.04 -0.08 0.56 o -4 -4 2 48.55 45.73 1.29 o -3 -4 2 339.93 366.03 5.18 o -2 -4 2 472.65 486.41 5.80 o -1 -4 2 94.88 85.88 1.92 o 0 -4 2 180.07 206.73 2.63 o 1 -4 2 93.87 104.03 2.85 o 2 -4 2 15.56 13.93 0.68 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