#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/11/2011109.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2011109_Fobs loop_ _publ_author_name 'Bernhardt, Paul V.' _publ_section_title ; Ni^II^ and Zn^II^ complexes of the hexadentate macrocyclic ligand cis-6,13-dimethyl-1,4,8,11-tetraazacyclotetradecane-6,13-diamine ; _journal_issue 7 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 744 _journal_page_last 746 _journal_volume 56 _journal_year 2000 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _cell_angle_alpha 90.000 _cell_angle_beta 113.090 _cell_angle_gamma 90.000 _cell_length_a 9.1980 _cell_length_b 12.7710 _cell_length_c 9.8800 _exptl_crystal_F_000 540.00 _reflns_d_resolution_high 0.8416 _[local]_cod_data_source_file fg1588Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' FG1585 Ni complex redone' _shelx_refln_list_code 4 _shelx_f_calc_maximum 139.32 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 4886.02 3901.06 33.94 o 2 0 0 15471.15 12122.29 97.97 o 3 0 0 23.40 26.06 1.22 o 4 0 0 2349.64 2347.88 17.21 o 5 0 0 1810.47 1489.57 13.58 o 6 0 0 22.31 18.07 1.66 o 7 0 0 468.78 428.72 6.56 o 8 0 0 681.68 725.36 9.22 o 9 0 0 97.67 100.85 4.40 o 10 0 0 0.15 1.47 3.20 o 1 1 0 2249.65 1764.66 7.71 o 2 1 0 495.16 516.43 5.01 o 3 1 0 1869.77 1553.57 12.01 o 4 1 0 44.51 42.56 1.64 o 5 1 0 650.91 577.41 6.07 o 6 1 0 638.79 620.34 7.08 o 7 1 0 489.43 511.98 7.12 o 8 1 0 47.84 46.78 2.96 o 9 1 0 65.19 67.49 3.63 o 10 1 0 11.49 13.75 2.46 o 0 2 0 7177.82 8325.41 73.31 o 1 2 0 5814.74 6913.63 65.13 o 2 2 0 1127.54 882.94 7.85 o 3 2 0 1793.63 1539.13 12.38 o 4 2 0 1247.47 976.98 9.95 o 5 2 0 334.09 343.77 4.83 o 6 2 0 399.24 372.93 5.56 o 7 2 0 13.81 12.60 1.81 o 8 2 0 772.93 754.69 9.51 o 9 2 0 166.30 159.62 5.36 o 1 3 0 19409.92 21889.46 155.34 o 2 3 0 1264.74 1589.69 12.98 o 3 3 0 827.12 649.21 6.48 o 4 3 0 543.20 464.00 5.06 o 5 3 0 320.26 288.64 4.54 o 6 3 0 338.99 315.60 5.28 o 7 3 0 260.52 270.33 5.40 o 8 3 0 16.92 13.04 2.42 o 9 3 0 33.26 35.71 3.24 o 0 4 0 934.19 839.37 7.95 o 1 4 0 1041.70 1427.74 12.36 o 2 4 0 775.33 964.50 9.55 o 3 4 0 615.53 675.12 6.79 o 4 4 0 648.57 417.98 4.90 o 5 4 0 722.81 626.89 6.76 o 6 4 0 77.49 75.19 2.82 o 7 4 0 243.80 243.85 5.22 o 8 4 0 29.52 20.90 2.28 o 9 4 0 122.75 136.83 5.12 o 1 5 0 86.43 95.27 2.41 o 2 5 0 429.61 445.34 5.08 o 3 5 0 9.16 15.59 1.47 o 4 5 0 18.95 18.03 1.74 o 5 5 0 67.90 57.61 2.34 o 6 5 0 273.64 233.69 4.78 o 7 5 0 339.91 322.88 6.08 o 8 5 0 46.01 41.28 3.07 o 9 5 0 74.36 88.81 4.35 o 0 6 0 185.94 163.04 3.24 o 1 6 0 1734.04 1833.51 17.06 o 2 6 0 1068.12 1126.62 10.88 o 3 6 0 572.98 664.33 7.10 o 4 6 0 944.49 1116.78 11.39 o 5 6 0 217.93 215.46 4.45 o 6 6 0 308.19 274.52 5.31 o 7 6 0 161.12 144.53 4.37 o 8 6 0 164.05 157.84 5.17 o 9 6 0 61.51 62.77 4.03 o 1 7 0 1175.74 1091.39 11.17 o 2 7 0 520.35 582.84 6.75 o 3 7 0 143.02 180.21 4.11 o 4 7 0 2.82 4.34 2.57 o 5 7 0 157.66 169.56 4.68 o 6 7 0 242.26 237.50 5.13 o 7 7 0 340.02 270.38 6.33 o 8 7 0 9.49 6.87 2.41 o 0 8 0 2122.67 2052.61 18.13 o 1 8 0 536.06 602.90 7.08 o 2 8 0 71.84 86.29 3.04 o 3 8 0 316.47 402.65 6.37 o 4 8 0 1562.68 1759.74 17.39 o 5 8 0 441.02 529.94 8.27 o 6 8 0 159.18 181.31 5.61 o 7 8 0 225.99 207.90 5.53 o 8 8 0 45.23 35.40 3.04 o 1 9 0 1678.43 1927.99 19.13 o 2 9 0 1257.35 1359.54 13.50 o 3 9 0 199.05 243.03 5.25 o 4 9 0 48.54 44.94 3.11 o 5 9 0 92.08 114.89 4.32 o 6 9 0 242.01 321.44 7.88 o 7 9 0 161.29 200.96 6.74 o 8 9 0 2.31 2.40 1.94 o 0 10 0 78.96 94.43 3.53 o 1 10 0 317.32 297.94 5.91 o 2 10 0 57.37 46.41 2.99 o 3 10 0 381.91 390.17 7.10 o 4 10 0 454.81 533.10 8.58 o 5 10 0 159.86 160.69 5.53 o 6 10 0 57.66 60.42 4.15 o 7 10 0 30.69 30.65 3.63 o 1 11 0 136.67 139.34 4.37 o 2 11 0 884.73 929.21 11.00 o 3 11 0 344.22 397.73 7.46 o 4 11 0 22.58 25.29 3.01 o 5 11 0 73.17 80.66 4.43 o 6 11 0 165.77 187.25 6.73 o 0 12 0 940.85 854.94 11.00 o 1 12 0 242.22 229.48 5.84 o 2 12 0 43.31 50.06 3.31 o 3 12 0 81.65 84.50 4.14 o 4 12 0 114.96 115.25 5.25 o 5 12 0 187.09 188.70 6.59 o 6 12 0 5.13 1.83 4.69 o 1 13 0 147.81 149.39 5.72 o 2 13 0 226.36 211.49 6.67 o 3 13 0 183.83 176.07 6.20 o 4 13 0 16.49 11.42 3.12 o 5 13 0 115.70 111.26 5.58 o 0 14 0 190.92 167.84 6.02 o 1 14 0 114.53 106.23 5.01 o 2 14 0 0.30 4.63 3.54 o 3 14 0 118.35 109.16 5.24 o 1 15 0 18.19 10.51 2.69 o -10 0 1 172.96 178.30 5.91 o -9 0 1 72.61 77.23 3.96 o -8 0 1 733.94 773.48 9.25 o -7 0 1 60.36 60.33 2.60 o -6 0 1 5.00 5.06 1.23 o -5 0 1 1878.33 1659.39 15.85 o -4 0 1 1092.71 969.92 9.09 o -3 0 1 9763.70 8549.03 82.55 o -2 0 1 9848.09 8803.79 79.09 o -1 0 1 517.03 404.82 3.52 o 0 0 1 2668.79 1189.02 794.24 o 1 0 1 982.02 904.84 6.73 o 2 0 1 98.67 99.38 1.73 o 3 0 1 223.47 247.18 3.24 o 4 0 1 503.47 459.10 5.04 o 5 0 1 120.83 109.00 2.91 o 6 0 1 419.27 441.29 6.26 o 7 0 1 291.73 283.14 5.56 o 8 0 1 91.70 102.17 4.21 o 9 0 1 73.80 64.80 3.80 o -10 1 1 24.42 32.06 2.78 o -9 1 1 169.05 170.79 5.31 o -8 1 1 341.24 325.53 6.11 o -7 1 1 26.27 23.88 1.86 o -6 1 1 272.27 230.36 4.19 o -5 1 1 2100.72 1773.10 16.30 o -4 1 1 2728.56 2294.02 16.07 o -3 1 1 451.25 450.92 4.40 o -2 1 1 4182.87 3718.16 36.50 o -1 1 1 6276.99 6350.38 57.01 o 0 1 1 4851.97 5077.11 77.27 o 1 1 1 7273.95 6795.54 61.14 o 2 1 1 1341.20 1077.32 9.34 o 3 1 1 4280.95 3515.62 19.60 o 4 1 1 2789.79 2607.22 19.48 o 5 1 1 91.51 95.50 2.75 o 6 1 1 165.17 160.77 3.89 o 7 1 1 217.59 184.35 4.70 o 8 1 1 131.71 120.86 4.46 o 9 1 1 51.25 51.77 3.40 o -10 2 1 72.13 86.88 4.34 o -9 2 1 3.08 0.61 2.70 o -8 2 1 73.95 57.18 2.92 o -7 2 1 308.62 281.56 5.15 o -6 2 1 657.42 561.55 6.49 o -5 2 1 54.45 61.91 2.03 o -4 2 1 726.70 632.45 6.22 o -3 2 1 703.82 558.14 5.37 o -2 2 1 6788.75 6660.54 67.92 o -1 2 1 3200.03 3963.92 40.24 o 0 2 1 9873.48 10764.96 377.52 o 1 2 1 134.04 171.16 2.12 o 2 2 1 786.21 781.67 7.30 o 3 2 1 1813.35 1603.28 13.70 o 4 2 1 55.11 52.79 1.94 o 5 2 1 788.56 685.01 7.05 o 6 2 1 353.33 306.19 5.31 o 7 2 1 14.95 17.88 2.03 o 8 2 1 15.44 14.91 2.40 o 9 2 1 63.58 73.79 3.90 o -10 3 1 64.54 66.33 4.08 o -9 3 1 310.15 325.03 7.21 o -8 3 1 127.41 127.50 4.06 o -7 3 1 548.96 535.47 7.15 o -6 3 1 492.20 458.30 5.95 o -5 3 1 2217.32 1901.33 17.61 o -4 3 1 745.52 736.58 7.32 o -3 3 1 235.62 223.27 3.07 o -2 3 1 700.80 930.05 8.13 o -1 3 1 570.91 803.62 7.20 o 0 3 1 972.05 1186.00 30.55 o 1 3 1 123.02 222.51 2.67 o 2 3 1 490.72 599.60 6.23 o 3 3 1 913.29 990.15 9.91 o 4 3 1 1178.96 981.04 9.81 o 5 3 1 148.02 124.18 3.26 o 6 3 1 262.79 267.61 5.10 o 7 3 1 161.08 160.50 4.35 o 8 3 1 138.01 120.48 4.57 o 9 3 1 60.81 56.26 3.77 o -10 4 1 60.91 65.28 3.83 o -9 4 1 10.30 8.75 2.33 o -8 4 1 99.82 88.86 3.47 o -7 4 1 158.33 123.35 3.68 o -6 4 1 57.98 53.14 2.41 o -5 4 1 27.30 30.75 1.67 o -4 4 1 303.65 296.97 4.11 o -3 4 1 1368.10 1355.89 13.48 o -2 4 1 1332.42 1499.04 13.66 o -1 4 1 1541.43 1752.51 13.74 o 0 4 1 626.21 630.49 11.58 o 1 4 1 468.97 512.98 5.04 o 2 4 1 1128.29 1076.32 10.10 o 3 4 1 20.33 27.10 1.55 o 4 4 1 330.94 268.45 4.39 o 5 4 1 366.15 347.05 5.37 o 6 4 1 324.04 269.51 5.19 o 7 4 1 56.07 52.00 3.13 o 8 4 1 37.08 31.30 2.97 o 9 4 1 49.06 47.78 3.52 o -9 5 1 181.36 191.35 5.72 o -8 5 1 72.04 68.81 3.37 o -7 5 1 71.88 64.70 2.93 o -6 5 1 94.32 89.11 2.95 o -5 5 1 241.84 237.32 4.24 o -4 5 1 568.92 577.90 6.19 o -3 5 1 655.18 804.29 8.30 o -2 5 1 1863.98 2255.79 18.16 o -1 5 1 2217.30 2481.14 18.13 o 0 5 1 2238.13 2515.39 12.74 o 1 5 1 130.20 115.20 2.67 o 2 5 1 249.73 317.96 4.41 o 3 5 1 686.84 811.77 8.36 o 4 5 1 752.40 744.40 7.52 o 5 5 1 229.69 207.63 4.44 o 6 5 1 55.96 48.21 2.60 o 7 5 1 269.44 268.79 5.87 o 8 5 1 140.30 130.59 4.76 o 9 5 1 4.76 5.21 2.10 o -9 6 1 8.55 6.96 3.68 o -8 6 1 23.19 23.79 2.64 o -7 6 1 382.40 343.25 6.16 o -6 6 1 623.10 563.66 7.25 o -5 6 1 85.82 93.75 3.05 o -4 6 1 786.30 862.05 8.50 o -3 6 1 1370.84 1785.13 16.15 o -2 6 1 947.02 1056.79 10.49 o -1 6 1 490.56 474.23 5.41 o 0 6 1 441.73 292.14 3.01 o 1 6 1 1106.92 1472.69 13.41 o 2 6 1 674.97 732.33 7.09 o 3 6 1 142.76 112.42 3.27 o 4 6 1 440.87 436.42 6.12 o 5 6 1 1470.22 1394.82 14.64 o 6 6 1 273.80 244.67 5.35 o 7 6 1 7.37 6.60 1.97 o 8 6 1 12.13 9.99 2.17 o -9 7 1 108.04 100.22 4.58 o -8 7 1 82.61 72.58 3.71 o -7 7 1 0.34 2.13 2.39 o -6 7 1 129.43 120.15 3.95 o -5 7 1 181.33 187.65 4.62 o -4 7 1 389.93 418.82 6.34 o -3 7 1 179.87 177.82 4.04 o -2 7 1 361.55 279.08 4.71 o -1 7 1 879.61 997.95 9.78 o 0 7 1 1371.14 1520.66 15.19 o 1 7 1 445.63 517.18 6.21 o 2 7 1 287.54 258.54 4.61 o 3 7 1 233.23 291.61 5.18 o 4 7 1 653.97 767.51 8.78 o 5 7 1 272.46 256.76 5.38 o 6 7 1 99.25 82.14 3.63 o 7 7 1 289.64 245.38 6.45 o 8 7 1 169.78 145.25 5.50 o -8 8 1 31.67 30.51 2.90 o -7 8 1 218.47 213.43 5.80 o -6 8 1 215.47 228.98 5.66 o -5 8 1 80.17 111.97 4.11 o -4 8 1 638.89 722.05 8.87 o -3 8 1 1727.55 2053.00 19.49 o -2 8 1 49.62 66.80 2.72 o -1 8 1 87.12 104.56 3.21 o 0 8 1 76.94 94.08 14.10 o 1 8 1 1399.04 1446.92 13.97 o 2 8 1 2728.11 2937.40 26.34 o 3 8 1 18.27 22.77 2.25 o 4 8 1 898.42 1035.80 10.78 o 5 8 1 274.22 309.65 6.33 o 6 8 1 107.58 121.33 4.61 o 7 8 1 41.34 38.30 3.22 o 8 8 1 7.49 6.24 3.34 o -8 9 1 59.94 53.86 3.82 o -7 9 1 27.74 31.03 3.13 o -6 9 1 85.60 119.24 4.80 o -5 9 1 186.87 244.61 5.87 o -4 9 1 848.65 944.26 10.54 o -3 9 1 245.72 304.40 5.94 o -2 9 1 433.27 466.65 6.92 o -1 9 1 858.38 911.54 9.38 o 0 9 1 493.87 551.80 5.38 o 1 9 1 398.58 351.39 5.96 o 2 9 1 658.93 693.33 8.53 o 3 9 1 608.71 715.54 9.01 o 4 9 1 4.15 15.88 2.14 o 5 9 1 90.35 84.68 3.89 o 6 9 1 22.15 34.32 3.38 o 7 9 1 179.98 186.14 6.24 o -7 10 1 310.58 377.53 8.97 o -6 10 1 348.33 412.17 8.93 o -5 10 1 97.86 102.45 4.20 o -4 10 1 343.03 352.49 6.98 o -3 10 1 127.07 124.23 4.33 o -2 10 1 378.44 421.28 7.03 o -1 10 1 124.04 133.88 4.15 o 0 10 1 690.93 719.07 6.33 o 1 10 1 745.89 766.39 9.30 o 2 10 1 634.40 702.27 9.12 o 3 10 1 79.35 79.46 3.65 o 4 10 1 52.13 55.07 3.46 o 5 10 1 213.69 227.42 6.60 o 6 10 1 150.59 174.47 6.28 o 7 10 1 1.20 7.85 4.28 o -7 11 1 11.51 8.43 3.44 o -6 11 1 181.78 211.60 6.82 o -5 11 1 303.33 326.86 7.99 o -4 11 1 80.42 83.50 4.11 o -3 11 1 219.12 238.50 6.00 o -2 11 1 78.86 85.20 3.83 o -1 11 1 904.70 896.22 10.63 o 0 11 1 193.93 194.54 7.70 o 1 11 1 247.93 274.87 6.21 o 2 11 1 57.09 72.96 3.62 o 3 11 1 245.04 237.64 5.99 o 4 11 1 84.50 96.54 4.52 o 5 11 1 121.30 146.72 5.50 o 6 11 1 10.72 16.09 2.92 o -6 12 1 89.44 100.88 5.29 o -5 12 1 28.89 25.79 3.65 o -4 12 1 60.74 69.32 4.17 o -3 12 1 526.04 482.26 9.31 o -2 12 1 413.23 425.84 8.09 o -1 12 1 9.41 13.70 2.26 o 0 12 1 34.26 26.06 1.89 o 1 12 1 300.25 292.25 6.63 o 2 12 1 440.12 433.73 8.81 o 3 12 1 126.36 125.12 5.02 o 4 12 1 45.11 44.73 3.97 o 5 12 1 59.22 56.18 4.40 o -5 13 1 109.88 112.94 5.76 o -4 13 1 278.27 290.69 7.97 o -3 13 1 25.55 25.27 3.28 o -2 13 1 75.01 81.25 4.34 o -1 13 1 82.51 85.60 4.41 o 0 13 1 267.96 241.51 5.50 o 1 13 1 280.19 261.83 7.32 o 2 13 1 14.12 12.53 2.76 o 3 13 1 277.24 277.25 7.67 o 4 13 1 96.43 89.83 4.85 o -4 14 1 18.11 18.12 3.22 o -3 14 1 137.77 126.72 5.62 o -2 14 1 284.12 279.00 7.80 o -1 14 1 86.48 77.39 4.35 o 0 14 1 79.92 67.46 3.47 o 1 14 1 231.29 188.67 6.62 o 2 14 1 65.84 64.39 4.33 o 3 14 1 58.26 59.36 4.30 o -1 15 1 49.94 44.67 4.29 o 0 15 1 126.37 109.86 3.91 o -10 0 2 138.70 147.59 5.15 o -9 0 2 80.95 68.33 3.61 o -8 0 2 0.52 1.44 1.95 o -7 0 2 3.73 4.39 1.38 o -6 0 2 348.02 316.96 4.71 o -5 0 2 2672.48 2688.46 19.69 o -4 0 2 2548.25 2226.09 15.80 o -3 0 2 124.73 146.30 2.20 o -2 0 2 7702.10 6480.95 62.31 o -1 0 2 4120.53 4056.06 41.07 o 0 0 2 7172.18 6549.30 200.05 o 1 0 2 362.28 329.56 3.16 o 2 0 2 57.56 63.45 1.74 o 3 0 2 7108.96 6363.27 29.06 o 4 0 2 887.91 727.51 7.34 o 5 0 2 353.79 306.19 4.99 o 6 0 2 350.62 326.64 5.74 o 7 0 2 57.05 69.97 3.14 o 8 0 2 62.23 63.63 3.49 o 9 0 2 0.13 1.84 3.46 o -10 1 2 48.92 57.83 3.61 o -9 1 2 126.28 132.54 4.52 o -8 1 2 143.53 137.69 4.00 o -7 1 2 850.21 800.01 8.24 o -6 1 2 550.10 544.69 6.16 o -5 1 2 388.55 303.16 4.21 o -4 1 2 2728.25 2436.01 16.33 o -3 1 2 1327.41 1042.80 9.26 o -2 1 2 6328.29 5925.40 62.91 o -1 1 2 3823.01 3964.53 39.26 o 0 1 2 1234.37 1316.52 6.61 o 1 1 2 2084.89 2227.20 13.44 o 2 1 2 871.85 789.30 7.97 o 3 1 2 158.12 151.33 2.94 o 4 1 2 677.52 668.63 6.64 o 5 1 2 134.30 108.24 3.12 o 6 1 2 9.15 8.18 1.54 o 7 1 2 15.99 15.58 1.91 o 8 1 2 37.12 38.94 3.16 o 9 1 2 103.06 110.55 5.03 o -10 2 2 207.66 216.84 6.18 o -9 2 2 242.56 252.42 6.27 o -8 2 2 47.02 53.76 2.73 o -7 2 2 22.47 25.88 2.01 o -6 2 2 101.88 96.05 2.82 o -5 2 2 4122.88 3613.68 22.84 o -4 2 2 777.15 643.76 6.63 o -3 2 2 2627.12 2499.91 15.33 o -2 2 2 5809.89 6038.66 61.49 o -1 2 2 818.79 962.00 8.56 o 0 2 2 2843.58 2932.16 47.11 o 1 2 2 66.22 59.44 1.66 o 2 2 2 2632.04 2432.98 16.55 o 3 2 2 1436.60 1233.27 11.61 o 4 2 2 883.98 790.23 7.87 o 5 2 2 41.91 52.55 2.35 o 6 2 2 148.93 134.91 3.88 o 7 2 2 403.38 392.06 6.99 o 8 2 2 55.38 61.26 3.58 o 9 2 2 10.81 8.17 4.23 o -10 3 2 33.17 31.94 2.77 o -9 3 2 57.63 62.85 3.29 o -8 3 2 269.33 269.08 5.66 o -7 3 2 614.27 593.44 7.49 o -6 3 2 135.20 120.29 3.10 o -5 3 2 486.15 420.72 4.94 o -4 3 2 924.19 878.71 8.32 o -3 3 2 439.16 433.91 4.28 o -2 3 2 867.10 905.25 8.27 o -1 3 2 1418.00 1613.13 12.55 o 0 3 2 1867.26 1973.00 42.67 o 1 3 2 2844.18 3018.00 17.81 o 2 3 2 1198.15 1196.27 10.64 o 3 3 2 103.94 89.33 2.49 o 4 3 2 831.81 734.54 7.27 o 5 3 2 92.60 102.44 3.16 o 6 3 2 170.75 137.66 4.01 o 7 3 2 51.18 53.71 3.01 o 8 3 2 54.67 51.74 3.56 o -10 4 2 70.49 78.53 3.94 o -9 4 2 70.27 65.40 3.54 o -8 4 2 284.73 300.57 6.03 o -7 4 2 76.32 55.68 2.69 o -6 4 2 1233.63 1080.26 11.33 o -5 4 2 457.45 364.61 4.94 o -4 4 2 1768.65 1699.58 15.80 o -3 4 2 757.29 778.68 7.87 o -2 4 2 4325.91 4832.08 24.55 o -1 4 2 8862.27 9564.23 96.01 o 0 4 2 1488.65 1674.41 9.97 o 1 4 2 560.21 635.20 6.25 o 2 4 2 2101.71 2105.54 17.38 o 3 4 2 2435.40 2514.21 20.76 o 4 4 2 521.70 528.21 6.42 o 5 4 2 62.26 68.78 2.90 o 6 4 2 339.60 315.98 6.06 o 7 4 2 195.54 188.96 5.31 o 8 4 2 45.78 46.88 3.53 o -10 5 2 24.13 32.25 3.05 o -9 5 2 80.70 88.73 4.01 o -8 5 2 114.49 108.63 3.77 o -7 5 2 408.35 390.30 6.32 o -6 5 2 56.55 53.07 2.53 o -5 5 2 316.04 269.97 4.57 o -4 5 2 344.32 343.43 4.85 o -3 5 2 1753.38 1921.93 17.68 o -2 5 2 1632.86 2163.24 18.08 o -1 5 2 276.10 301.33 4.21 o 0 5 2 2869.29 3145.65 14.93 o 1 5 2 603.58 782.15 7.64 o 2 5 2 366.26 480.39 5.42 o 3 5 2 265.69 244.78 4.33 o 4 5 2 541.00 521.32 6.67 o 5 5 2 899.29 812.15 8.95 o 6 5 2 191.15 192.31 4.85 o 7 5 2 17.98 19.78 2.76 o 8 5 2 96.80 97.57 4.48 o -9 6 2 227.73 206.28 5.77 o -8 6 2 81.41 78.68 3.70 o -7 6 2 283.28 249.02 5.27 o -6 6 2 578.71 589.68 7.43 o -5 6 2 550.96 590.20 7.03 o -4 6 2 282.70 303.50 4.98 o -3 6 2 310.29 354.47 5.19 o -2 6 2 822.78 880.52 8.93 o -1 6 2 497.03 584.24 6.15 o 0 6 2 2487.66 2601.25 53.26 o 1 6 2 34.82 47.45 2.07 o 2 6 2 2783.70 2909.43 23.49 o 3 6 2 754.81 772.83 7.81 o 4 6 2 174.95 176.40 4.24 o 5 6 2 78.76 75.33 3.19 o 6 6 2 162.91 139.35 4.45 o 7 6 2 287.51 274.77 6.73 o 8 6 2 49.13 47.39 3.41 o -9 7 2 25.27 24.18 2.91 o -8 7 2 46.11 45.66 2.93 o -7 7 2 167.44 166.56 4.51 o -6 7 2 27.15 34.45 2.46 o -5 7 2 116.81 123.78 3.81 o -4 7 2 338.41 374.55 5.94 o -3 7 2 1795.82 1944.47 18.05 o -2 7 2 620.08 731.00 7.60 o -1 7 2 74.40 50.39 2.23 o 0 7 2 1874.25 2143.31 14.51 o 1 7 2 682.26 820.51 7.98 o 2 7 2 295.12 322.42 5.30 o 3 7 2 105.34 138.03 3.74 o 4 7 2 279.60 283.84 5.55 o 5 7 2 769.14 799.59 9.62 o 6 7 2 225.83 209.10 5.84 o 7 7 2 25.86 22.68 2.78 o 8 7 2 97.65 82.04 4.61 o -9 8 2 48.08 46.30 3.18 o -8 8 2 239.44 234.20 6.35 o -7 8 2 31.07 32.55 2.83 o -6 8 2 1028.97 1089.86 11.48 o -5 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