#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/11/2011114.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2011114_Fobs loop_ _publ_author_name 'Bats, Jan W.' 'Rivas Nass, Andreas' 'Hashmi, A. Stephen K.' _publ_section_title ; Tetraallyl (2,2'-bipyridyl)-rac-3,3,7,7-tetramethyl-trans-5-palladatricyclo[4.1.0.0^2,^^4^]heptane-1,2,4,6-tetracarboxylate above and below the phase-transition temperature of 194K ; _journal_issue 7 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 814 _journal_page_last 817 _journal_volume 56 _journal_year 2000 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 95.641 _cell_angle_beta 97.375 _cell_angle_gamma 93.083 _cell_length_a 9.0197 _cell_length_b 17.9183 _cell_length_c 21.3749 _exptl_crystal_F_000 1520.00 _reflns_d_resolution_high 0.6456 _[local]_cod_data_source_file fg1601I143Ksup2.hkl _[local]_cod_data_source_block I143K #BEGIN Tags that were not found in dictionaries: _shelx_title ' am in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 378.66 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 35.57 45.64 10.13 o 2 0 0 18330.04 18311.27 268.96 o 3 0 0 1160.24 1094.58 122.66 o 4 0 0 2401.43 2435.79 56.83 o 5 0 0 2440.77 2455.32 103.27 o 6 0 0 23.39 15.16 15.98 o 7 0 0 2143.43 2041.43 88.14 o 8 0 0 549.23 534.37 30.77 o 9 0 0 6333.77 6465.29 161.08 o 10 0 0 23.66 42.94 35.41 o 11 0 0 373.16 381.58 60.96 o 12 0 0 148.32 226.17 66.42 o 13 0 0 9.69 193.12 111.16 o -13 1 0 6.86 -92.79 92.79 o -12 1 0 1207.89 1464.11 94.24 o -11 1 0 97.70 339.27 155.44 o -10 1 0 1065.20 1107.74 54.77 o -9 1 0 134.88 92.88 46.21 o -8 1 0 11.10 4.10 25.29 o -7 1 0 1015.19 1059.12 34.50 o -6 1 0 48.39 75.44 17.33 o -5 1 0 319.36 324.65 15.07 o -4 1 0 430.64 393.86 21.96 o -3 1 0 2807.24 2966.65 67.38 o -2 1 0 21017.01 19662.26 1163.82 o -1 1 0 1801.99 1963.37 42.00 o 1 1 0 3475.19 3650.47 67.35 o 2 1 0 72.04 80.67 9.13 o 3 1 0 6199.94 5922.60 217.18 o 4 1 0 200.89 170.93 11.43 o 5 1 0 2692.38 2576.46 87.06 o 6 1 0 97.45 75.65 17.24 o 7 1 0 3008.25 3012.11 84.69 o 8 1 0 15.23 10.47 31.44 o 9 1 0 518.05 488.08 114.49 o 10 1 0 869.28 703.90 49.59 o 11 1 0 1425.75 1280.89 125.79 o 12 1 0 333.69 287.78 66.61 o 13 1 0 21.97 -89.02 89.02 o -13 2 0 30.26 -85.73 85.73 o -12 2 0 874.72 863.95 111.17 o -11 2 0 337.82 337.17 66.42 o -10 2 0 808.89 795.32 128.50 o -9 2 0 1589.20 1592.54 48.70 o -8 2 0 15.00 -9.87 25.56 o -7 2 0 6911.55 7308.56 109.61 o -6 2 0 517.79 559.83 26.20 o -5 2 0 17387.69 16352.77 508.67 o -4 2 0 14245.71 14790.06 233.36 o -3 2 0 18154.77 16972.90 1139.71 o -2 2 0 12405.08 12280.42 449.17 o -1 2 0 27.38 62.34 6.32 o 0 2 0 8730.29 8828.89 158.64 o 1 2 0 848.52 887.53 53.73 o 2 2 0 9479.26 9894.25 344.55 o 3 2 0 6263.42 6325.09 85.34 o 4 2 0 6414.05 6542.42 125.34 o 5 2 0 13.64 -9.72 26.49 o 6 2 0 1869.27 1886.41 58.51 o 7 2 0 697.60 742.87 30.27 o 8 2 0 337.22 366.88 36.24 o 9 2 0 164.89 114.24 40.14 o 10 2 0 1395.88 1389.55 82.67 o 11 2 0 5.47 74.42 81.02 o 12 2 0 1220.83 1100.20 89.79 o -13 3 0 136.27 261.90 110.69 o -12 3 0 3.22 138.95 88.08 o -11 3 0 3369.74 3337.62 113.56 o -10 3 0 31.73 141.79 33.95 o -9 3 0 2216.92 2203.36 55.40 o -8 3 0 232.88 277.69 29.98 o -7 3 0 3909.71 3950.17 68.48 o -6 3 0 48.37 35.94 16.77 o -5 3 0 2155.04 2129.68 82.03 o -4 3 0 524.54 604.77 28.97 o -3 3 0 6964.65 6789.10 156.78 o -2 3 0 734.76 750.95 32.00 o -1 3 0 796.51 726.68 13.72 o 0 3 0 656.52 655.26 16.83 o 1 3 0 167.85 176.60 15.16 o 2 3 0 4451.11 4197.85 57.70 o 3 3 0 93.61 134.64 23.74 o 4 3 0 2052.56 1788.03 69.71 o 5 3 0 473.25 526.25 18.74 o 6 3 0 1530.52 1512.95 67.85 o 7 3 0 3030.39 3273.48 138.85 o 8 3 0 223.05 290.30 44.44 o 9 3 0 1977.22 1743.62 89.98 o 10 3 0 400.70 333.14 72.08 o 11 3 0 753.31 653.38 89.50 o 12 3 0 796.99 496.51 117.30 o -13 4 0 12.17 163.92 125.29 o -12 4 0 934.95 916.72 123.42 o -11 4 0 967.35 880.74 131.90 o -10 4 0 504.54 658.37 61.41 o -9 4 0 139.93 165.62 27.81 o -8 4 0 1129.53 1169.29 40.45 o -7 4 0 17.96 61.84 21.24 o -6 4 0 99.97 116.21 19.61 o -5 4 0 3800.22 4221.60 109.17 o -4 4 0 4.45 -5.33 11.67 o -3 4 0 2144.24 2110.76 31.30 o -2 4 0 14672.39 13602.45 225.68 o -1 4 0 4.00 19.52 6.21 o 0 4 0 10286.69 10017.07 337.84 o 1 4 0 636.60 644.75 17.21 o 2 4 0 4731.04 5183.26 73.50 o 3 4 0 5108.20 5018.97 138.68 o 4 4 0 1319.99 1608.47 30.53 o 5 4 0 10763.26 10779.79 164.46 o 6 4 0 4.77 34.20 18.47 o 7 4 0 2756.26 2642.45 60.68 o 8 4 0 763.50 826.14 43.70 o 9 4 0 4563.70 4462.71 227.58 o 10 4 0 50.50 122.95 51.44 o 11 4 0 1182.15 1007.20 103.64 o 12 4 0 68.21 13.19 89.03 o -13 5 0 22.28 -79.13 79.13 o -12 5 0 480.12 517.69 114.00 o -11 5 0 494.78 568.73 75.10 o -10 5 0 493.32 524.63 38.69 o -9 5 0 4464.11 4324.46 67.43 o -8 5 0 14.88 24.46 19.64 o -7 5 0 3934.06 3921.31 73.26 o -6 5 0 421.85 499.00 18.69 o -5 5 0 19638.58 19736.31 183.19 o -4 5 0 2310.95 2366.63 31.77 o -3 5 0 2288.26 2071.81 29.10 o -2 5 0 7395.45 7801.39 93.18 o -1 5 0 4124.86 3869.82 90.25 o 0 5 0 10795.52 10566.56 312.30 o 1 5 0 190.49 163.90 17.61 o 2 5 0 5032.06 5300.38 72.72 o 3 5 0 8269.39 8684.62 197.17 o 4 5 0 6901.12 7387.40 208.48 o 5 5 0 7099.02 7440.22 232.34 o 6 5 0 254.23 239.04 49.23 o 7 5 0 2768.21 2658.53 53.93 o 8 5 0 1213.73 1157.24 46.41 o 9 5 0 527.58 483.88 53.22 o 10 5 0 504.18 618.68 146.97 o 11 5 0 232.90 275.56 95.15 o -13 6 0 13.78 195.95 120.11 o -12 6 0 1.65 335.37 106.45 o -11 6 0 258.27 169.58 79.61 o -10 6 0 63.44 99.93 31.14 o -9 6 0 216.19 238.14 30.02 o -8 6 0 38.89 43.33 20.87 o -7 6 0 11496.59 11266.75 320.45 o -6 6 0 1410.06 1469.19 28.60 o -5 6 0 6327.79 6435.68 106.19 o -4 6 0 2572.01 2528.50 41.90 o -3 6 0 4999.17 5070.94 55.10 o -2 6 0 1884.61 1753.27 54.29 o -1 6 0 2846.65 2852.24 42.72 o 0 6 0 2739.08 2645.74 40.13 o 1 6 0 146.46 125.91 11.11 o 2 6 0 31386.67 31697.17 403.25 o 3 6 0 48.03 82.41 12.06 o 4 6 0 6614.50 6602.67 243.61 o 5 6 0 1026.80 1035.68 35.54 o 6 6 0 1237.40 1171.64 40.22 o 7 6 0 91.63 49.28 24.05 o 8 6 0 506.55 541.59 114.23 o 9 6 0 573.52 517.67 56.15 o 10 6 0 739.21 717.78 68.26 o 11 6 0 463.63 425.36 99.39 o -13 7 0 25.86 184.64 111.16 o -12 7 0 649.00 763.59 114.00 o -10 7 0 1229.72 1331.21 57.57 o -9 7 0 310.36 285.33 31.20 o -8 7 0 14.52 9.07 19.54 o -7 7 0 81.44 57.09 41.48 o -6 7 0 85.89 104.92 27.09 o -5 7 0 281.07 305.74 16.50 o -4 7 0 2760.31 2461.45 49.21 o -3 7 0 4167.30 4287.67 95.58 o -2 7 0 33590.66 34905.65 560.28 o -1 7 0 1542.58 1487.60 49.56 o 0 7 0 54414.84 51260.82 2117.96 o 1 7 0 816.12 945.86 20.47 o 2 7 0 10596.56 10833.24 142.71 o 3 7 0 1026.44 1068.02 29.58 o 4 7 0 4080.80 4210.70 57.40 o 5 7 0 12810.06 12468.58 169.19 o 6 7 0 136.02 245.95 29.70 o 7 7 0 9448.18 8833.84 298.90 o 8 7 0 8.88 -0.50 35.56 o 9 7 0 2832.85 2744.48 92.29 o 10 7 0 20.12 -0.94 67.83 o 11 7 0 1365.55 1456.18 140.39 o -12 8 0 1589.28 1659.73 137.09 o -11 8 0 292.51 316.07 87.14 o -10 8 0 949.42 958.94 40.54 o -9 8 0 180.06 228.68 27.11 o -8 8 0 512.20 452.57 27.62 o -7 8 0 2651.85 2705.50 47.27 o -6 8 0 1153.97 1219.58 47.91 o -5 8 0 1451.31 1565.85 27.97 o -4 8 0 1719.33 1812.46 29.94 o -3 8 0 2931.61 2912.73 33.40 o -2 8 0 1706.07 1953.83 31.22 o -1 8 0 6059.83 5883.44 111.09 o 0 8 0 286.09 327.18 18.54 o 1 8 0 217.71 223.63 23.99 o 2 8 0 12.09 25.95 15.88 o 3 8 0 1624.93 1695.27 36.69 o 4 8 0 2670.24 2669.67 47.84 o 5 8 0 6980.29 7127.77 117.09 o 6 8 0 102.87 64.00 23.79 o 7 8 0 1802.64 1915.50 130.32 o 8 8 0 295.44 182.16 98.68 o 9 8 0 216.17 173.20 97.03 o 10 8 0 56.00 -41.47 52.91 o 11 8 0 161.94 84.32 89.50 o -12 9 0 211.27 258.60 102.22 o -11 9 0 473.22 435.25 99.86 o -10 9 0 4.85 -17.86 28.19 o -9 9 0 2123.36 2175.99 49.20 o -8 9 0 6.44 -24.26 24.26 o -7 9 0 5159.10 4858.72 178.36 o -6 9 0 0.94 -15.38 15.38 o -5 9 0 5659.58 5680.45 81.86 o -4 9 0 412.33 452.60 18.43 o -3 9 0 1777.53 1801.23 39.83 o -2 9 0 5822.34 5628.51 125.53 o -1 9 0 1906.86 1896.99 31.87 o 0 9 0 24722.74 24902.98 593.15 o 1 9 0 216.70 230.76 21.00 o 2 9 0 28611.18 29815.62 343.13 o 3 9 0 1303.39 1322.04 27.22 o 4 9 0 11353.36 11194.56 170.08 o 5 9 0 92.03 134.04 20.26 o 6 9 0 303.05 354.14 55.53 o 7 9 0 768.54 743.27 41.69 o 8 9 0 58.44 104.65 44.13 o 9 9 0 994.29 910.61 98.46 o 10 9 0 569.30 438.56 98.92 o -12 10 0 527.98 572.80 108.81 o -11 10 0 575.07 675.50 112.11 o -10 10 0 609.97 624.69 94.36 o -9 10 0 1014.23 931.13 48.49 o -8 10 0 105.94 92.10 31.35 o -7 10 0 2116.34 1998.87 51.27 o -6 10 0 50.95 56.52 17.47 o -5 10 0 4.65 9.63 14.52 o -4 10 0 1829.63 1685.48 29.10 o -3 10 0 171.01 182.98 22.26 o -2 10 0 3825.30 3574.81 51.59 o -1 10 0 12.33 21.42 24.51 o 0 10 0 1005.90 846.29 35.39 o 1 10 0 100.74 82.42 21.76 o 2 10 0 22063.85 21469.27 250.09 o 3 10 0 1175.18 1269.06 32.68 o 4 10 0 3002.66 3081.95 107.89 o 5 10 0 247.29 231.76 28.96 o 6 10 0 159.91 182.28 30.72 o 7 10 0 3547.60 3693.29 101.96 o 8 10 0 47.28 2.28 110.22 o 9 10 0 2037.02 2115.18 87.11 o 10 10 0 75.95 -58.88 66.42 o -12 11 0 1726.03 1822.75 147.93 o 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989.85 1003.73 61.93 o 0 12 0 1489.14 1298.06 44.25 o 1 12 0 1.30 14.59 17.90 o 2 12 0 11660.22 11460.62 184.85 o 3 12 0 434.57 470.34 43.24 o 4 12 0 1322.55 1315.94 45.47 o 5 12 0 2.10 -23.13 23.13 o 6 12 0 1202.75 1406.74 96.58 o 7 12 0 19.05 47.28 37.57 o 8 12 0 44.38 -36.10 36.10 o 9 12 0 19.31 72.07 71.60 o 10 12 0 700.22 930.83 133.31 o -12 13 0 439.87 389.09 132.84 o -11 13 0 5.27 -63.59 72.07 o -10 13 0 285.43 343.86 101.27 o -9 13 0 1081.37 1009.17 53.10 o -8 13 0 48.43 24.99 24.28 o -7 13 0 1535.39 1524.62 39.47 o -6 13 0 1.43 -15.41 19.50 o -5 13 0 281.97 286.58 34.09 o -4 13 0 291.03 346.68 24.24 o -3 13 0 954.00 865.01 69.10 o -2 13 0 1399.93 1445.04 33.15 o -1 13 0 83.05 45.99 21.30 o 0 13 0 12916.16 13324.11 182.38 o 1 13 0 102.92 125.75 21.05 o 2 13 0 2869.52 2959.71 85.28 o 3 13 0 11.35 1.12 27.38 o 4 13 0 3308.50 3597.94 117.82 o 5 13 0 2773.67 2691.30 75.16 o 6 13 0 1324.45 1174.45 60.63 o 7 13 0 723.26 713.15 59.29 o 8 13 0 129.75 118.88 53.95 o 9 13 0 2697.12 2758.27 149.83 o -12 14 0 1824.80 1768.11 163.95 o -11 14 0 108.43 235.99 94.21 o -10 14 0 1281.73 1352.05 119.66 o -9 14 0 789.44 752.28 57.45 o -8 14 0 65.18 38.86 25.51 o -7 14 0 461.41 529.19 31.30 o -6 14 0 2.82 -1.66 41.88 o -5 14 0 2777.49 2757.62 90.10 o -4 14 0 419.53 518.88 45.35 o -3 14 0 4366.03 4379.68 268.50 o -2 14 0 3595.10 3661.07 65.17 o -1 14 0 1668.31 1745.83 80.02 o 0 14 0 560.99 648.59 30.05 o 1 14 0 0.72 -12.14 29.89 o 2 14 0 274.55 346.16 30.87 o 3 14 0 196.41 198.83 47.62 o 4 14 0 148.55 103.25 30.44 o 5 14 0 4406.74 4187.34 89.78 o 6 14 0 1069.18 1086.02 270.17 o 7 14 0 5595.57 5907.41 149.31 o 8 14 0 119.11 106.62 51.70 o 9 14 0 1723.48 1600.87 126.26 o -11 15 0 2.06 -82.43 82.43 o -10 15 0 241.67 137.54 81.02 o -9 15 0 885.89 791.88 96.10 o -8 15 0 28.57 27.23 39.72 o -7 15 0 1610.97 1502.83 52.30 o -6 15 0 378.18 379.94 54.80 o -5 15 0 8150.90 8229.19 246.43 o -4 15 0 257.91 351.54 45.82 o -3 15 0 4283.52 4720.12 185.43 o -2 15 0 1307.16 1391.63 49.35 o -1 15 0 1098.83 1057.85 52.22 o 0 15 0 388.58 562.65 42.97 o 1 15 0 20.07 9.54 38.55 o 2 15 0 696.90 756.22 41.51 o 3 15 0 480.14 539.41 39.42 o 4 15 0 6254.58 5864.61 154.17 o 5 15 0 1165.69 971.76 110.95 o 6 15 0 1453.06 1327.61 97.52 o 7 15 0 404.99 557.18 67.35 o 8 15 0 29.68 39.54 83.37 o -11 16 0 104.21 -89.03 89.03 o -10 16 0 253.45 242.59 88.56 o -9 16 0 383.27 317.02 96.09 o -8 16 0 464.10 560.08 82.91 o -7 16 0 363.36 470.81 51.58 o -6 16 0 320.75 349.85 42.87 o -5 16 0 3488.21 3403.31 82.26 o -4 16 0 981.12 935.01 70.76 o -3 16 0 25.10 33.00 26.69 o -2 16 0 576.66 643.31 33.90 o -1 16 0 1.27 -4.89 23.18 o 0 16 0 4015.39 3912.42 149.43 o 1 16 0 61.77 -6.35 29.70 o 2 16 0 1986.69 1938.67 58.37 o 3 16 0 64.10 56.20 35.78 o 4 16 0 1812.32 2013.92 123.99 o 5 16 0 1134.21 1111.60 94.46 o 6 16 0 163.17 189.39 114.23 o 7 16 0 1824.37 1852.43 215.54 o 8 16 0 1.82 -65.47 65.47 o 9 16 0 1375.28 1396.81 130.49 o -11 17 0 2.73 -90.91 90.91 o -10 17 0 660.59 602.02 126.72 o -7 17 0 395.26 344.49 49.64 o -6 17 0 83.94 5.40 35.85 o -5 17 0 485.22 456.26 45.18 o -4 17 0 551.71 599.94 48.48 o -3 17 0 1860.99 1879.82 61.87 o -2 17 0 1512.74 1431.23 78.07 o -1 17 0 312.26 336.08 45.89 o 0 17 0 736.48 854.10 43.40 o 1 17 0 193.55 128.89 60.88 o 2 17 0 1336.49 1318.12 58.20 o 3 17 0 871.13 887.51 54.85 o 4 17 0 18.29 47.29 33.97 o 5 17 0 1862.95 1973.34 85.11 o 6 17 0 93.15 129.64 52.51 o 7 17 0 1325.86 1013.34 106.00 o 8 17 0 0.43 165.80 89.97 o -7 18 0 768.71 799.41 105.52 o -6 18 0 913.80 968.91 62.50 o -5 18 0 4695.09 4823.41 173.85 o -4 18 0 71.65 111.74 45.72 o -3 18 0 4097.89 4066.58 238.33 o -2 18 0 642.88 654.92 73.98 o -1 18 0 1204.75 1154.42 60.46 o 0 18 0 1587.79 1531.49 70.33 o 1 18 0 394.82 368.29 60.75 o 2 18 0 587.94 684.26 52.03 o 3 18 0 80.09 84.55 34.07 o 4 18 0 1383.65 1366.15 109.69 o 5 18 0 6.39 -46.54 73.01 o 6 18 0 1016.35 858.59 71.14 o 7 18 0 10.36 9.89 70.18 o -7 19 0 3041.29 3055.71 168.22 o -6 19 0 539.14 592.99 56.55 o -5 19 0 1036.19 996.68 59.22 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